CN116919850A - Lip composition, preparation method thereof and lip cosmetic - Google Patents
Lip composition, preparation method thereof and lip cosmetic Download PDFInfo
- Publication number
- CN116919850A CN116919850A CN202210322700.7A CN202210322700A CN116919850A CN 116919850 A CN116919850 A CN 116919850A CN 202210322700 A CN202210322700 A CN 202210322700A CN 116919850 A CN116919850 A CN 116919850A
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- lip
- composition
- lips
- cosmetic
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- 239000000203 mixture Substances 0.000 title claims abstract description 70
- 239000002537 cosmetic Substances 0.000 title claims description 33
- 238000002360 preparation method Methods 0.000 title claims description 15
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 claims abstract description 40
- -1 polydimethylsiloxane Polymers 0.000 claims abstract description 40
- 239000000839 emulsion Substances 0.000 claims abstract description 38
- 239000001856 Ethyl cellulose Substances 0.000 claims abstract description 35
- 229920001249 ethyl cellulose Polymers 0.000 claims abstract description 35
- 235000019325 ethyl cellulose Nutrition 0.000 claims abstract description 35
- 239000004205 dimethyl polysiloxane Substances 0.000 claims abstract description 31
- 239000000945 filler Substances 0.000 claims abstract description 31
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 31
- 239000003381 stabilizer Substances 0.000 claims abstract description 29
- 239000002994 raw material Substances 0.000 claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229940065115 grapefruit extract Drugs 0.000 claims abstract description 15
- 229920001577 copolymer Polymers 0.000 claims description 17
- 238000002156 mixing Methods 0.000 claims description 17
- 238000004945 emulsification Methods 0.000 claims description 16
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 12
- NOPFSRXAKWQILS-UHFFFAOYSA-N docosan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCCCO NOPFSRXAKWQILS-UHFFFAOYSA-N 0.000 claims description 12
- 239000003974 emollient agent Substances 0.000 claims description 12
- 239000003086 colorant Substances 0.000 claims description 11
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 10
- 239000003795 chemical substances by application Substances 0.000 claims description 10
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 9
- 240000000560 Citrus x paradisi Species 0.000 claims description 9
- 239000003995 emulsifying agent Substances 0.000 claims description 9
- 150000002148 esters Chemical class 0.000 claims description 9
- 125000005645 linoleyl group Chemical group 0.000 claims description 9
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims description 9
- 230000001804 emulsifying effect Effects 0.000 claims description 8
- 239000002904 solvent Substances 0.000 claims description 8
- 239000002562 thickening agent Substances 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 7
- 239000003755 preservative agent Substances 0.000 claims description 7
- 230000002335 preservative effect Effects 0.000 claims description 7
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000000539 dimer Substances 0.000 claims description 6
- 229960000735 docosanol Drugs 0.000 claims description 6
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 claims description 6
- 239000004816 latex Substances 0.000 claims description 6
- 229920000126 latex Polymers 0.000 claims description 6
- 239000008346 aqueous phase Substances 0.000 claims description 5
- 239000000377 silicon dioxide Substances 0.000 claims description 5
- BANXPJUEBPWEOT-UHFFFAOYSA-N 2-methyl-Pentadecane Chemical compound CCCCCCCCCCCCCC(C)C BANXPJUEBPWEOT-UHFFFAOYSA-N 0.000 claims description 4
- LEACJMVNYZDSKR-UHFFFAOYSA-N 2-octyldodecan-1-ol Chemical compound CCCCCCCCCCC(CO)CCCCCCCC LEACJMVNYZDSKR-UHFFFAOYSA-N 0.000 claims description 4
- BTFJIXJJCSYFAL-UHFFFAOYSA-N arachidyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCO BTFJIXJJCSYFAL-UHFFFAOYSA-N 0.000 claims description 4
- 229920006037 cross link polymer Polymers 0.000 claims description 4
- 229940075894 denatured ethanol Drugs 0.000 claims description 4
- VWPOBUVSGMLNCM-UHFFFAOYSA-L disodium prop-2-enoate Chemical compound [Na+].C(C=C)(=O)[O-].[Na+].C(C=C)(=O)[O-] VWPOBUVSGMLNCM-UHFFFAOYSA-L 0.000 claims description 4
- 229920001083 polybutene Polymers 0.000 claims description 4
- 229940104261 taurate Drugs 0.000 claims description 4
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 4
- 229920002554 vinyl polymer Polymers 0.000 claims description 4
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 3
- ANZUDYZHSVGBRF-UHFFFAOYSA-N 3-ethylnonane-1,2,3-triol Chemical compound CCCCCCC(O)(CC)C(O)CO ANZUDYZHSVGBRF-UHFFFAOYSA-N 0.000 claims description 3
- OYHQOLUKZRVURQ-HZJYTTRNSA-M 9-cis,12-cis-Octadecadienoate Chemical class CCCCC\C=C/C\C=C/CCCCCCCC([O-])=O OYHQOLUKZRVURQ-HZJYTTRNSA-M 0.000 claims description 3
- 239000004375 Dextrin Substances 0.000 claims description 3
- 229920001353 Dextrin Polymers 0.000 claims description 3
- 229920001214 Polysorbate 60 Polymers 0.000 claims description 3
- 229920002125 Sokalan® Polymers 0.000 claims description 3
- HVUMOYIDDBPOLL-XWVZOOPGSA-N Sorbitan monostearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O HVUMOYIDDBPOLL-XWVZOOPGSA-N 0.000 claims description 3
- HGKOWIQVWAQWDS-UHFFFAOYSA-N bis(16-methylheptadecyl) 2-hydroxybutanedioate Chemical compound CC(C)CCCCCCCCCCCCCCCOC(=O)CC(O)C(=O)OCCCCCCCCCCCCCCCC(C)C HGKOWIQVWAQWDS-UHFFFAOYSA-N 0.000 claims description 3
- 229960001631 carbomer Drugs 0.000 claims description 3
- 229940082500 cetostearyl alcohol Drugs 0.000 claims description 3
- 229960000541 cetyl alcohol Drugs 0.000 claims description 3
- 235000019425 dextrin Nutrition 0.000 claims description 3
- KWLMIXQRALPRBC-UHFFFAOYSA-L hectorite Chemical compound [Li+].[OH-].[OH-].[Na+].[Mg+2].O1[Si]2([O-])O[Si]1([O-])O[Si]([O-])(O1)O[Si]1([O-])O2 KWLMIXQRALPRBC-UHFFFAOYSA-L 0.000 claims description 3
- 229910000271 hectorite Inorganic materials 0.000 claims description 3
- IPCSVZSSVZVIGE-UHFFFAOYSA-M hexadecanoate Chemical compound CCCCCCCCCCCCCCCC([O-])=O IPCSVZSSVZVIGE-UHFFFAOYSA-M 0.000 claims description 3
- ACCCMOQWYVYDOT-UHFFFAOYSA-N hexane-1,1-diol Chemical compound CCCCCC(O)O ACCCMOQWYVYDOT-UHFFFAOYSA-N 0.000 claims description 3
- 229920006007 hydrogenated polyisobutylene Polymers 0.000 claims description 3
- 229940049918 linoleate Drugs 0.000 claims description 3
- 239000010445 mica Substances 0.000 claims description 3
- 229910052618 mica group Inorganic materials 0.000 claims description 3
- GOQYKNQRPGWPLP-UHFFFAOYSA-N n-heptadecyl alcohol Natural products CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 claims description 3
- OEIJHBUUFURJLI-UHFFFAOYSA-N octane-1,8-diol Chemical compound OCCCCCCCCO OEIJHBUUFURJLI-UHFFFAOYSA-N 0.000 claims description 3
- UWJJYHHHVWZFEP-UHFFFAOYSA-N pentane-1,1-diol Chemical compound CCCCC(O)O UWJJYHHHVWZFEP-UHFFFAOYSA-N 0.000 claims description 3
- 229960005323 phenoxyethanol Drugs 0.000 claims description 3
- 229920003229 poly(methyl methacrylate) Polymers 0.000 claims description 3
- 239000004926 polymethyl methacrylate Substances 0.000 claims description 3
- 239000001818 polyoxyethylene sorbitan monostearate Substances 0.000 claims description 3
- 235000010989 polyoxyethylene sorbitan monostearate Nutrition 0.000 claims description 3
- 229940113124 polysorbate 60 Drugs 0.000 claims description 3
- 229950011392 sorbitan stearate Drugs 0.000 claims description 3
- 229940012831 stearyl alcohol Drugs 0.000 claims description 3
- UJMBCXLDXJUMFB-GLCFPVLVSA-K tartrazine Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)C1=NN(C=2C=CC(=CC=2)S([O-])(=O)=O)C(=O)C1\N=N\C1=CC=C(S([O-])(=O)=O)C=C1 UJMBCXLDXJUMFB-GLCFPVLVSA-K 0.000 claims description 3
- OULAJFUGPPVRBK-UHFFFAOYSA-N tetratriacontyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCO OULAJFUGPPVRBK-UHFFFAOYSA-N 0.000 claims description 3
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 claims description 3
- VLPFTAMPNXLGLX-UHFFFAOYSA-N trioctanoin Chemical compound CCCCCCCC(=O)OCC(OC(=O)CCCCCCC)COC(=O)CCCCCCC VLPFTAMPNXLGLX-UHFFFAOYSA-N 0.000 claims description 3
- 229940043268 2,2,4,4,6,8,8-heptamethylnonane Drugs 0.000 claims description 2
- 239000004698 Polyethylene Substances 0.000 claims description 2
- 235000013871 bee wax Nutrition 0.000 claims description 2
- 239000012166 beeswax Substances 0.000 claims description 2
- 239000000440 bentonite Substances 0.000 claims description 2
- 229910000278 bentonite Inorganic materials 0.000 claims description 2
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 2
- KUVMKLCGXIYSNH-UHFFFAOYSA-N isopentadecane Natural products CCCCCCCCCCCCC(C)C KUVMKLCGXIYSNH-UHFFFAOYSA-N 0.000 claims description 2
- 229920000573 polyethylene Polymers 0.000 claims description 2
- JHWNWJKBPDFINM-UHFFFAOYSA-N Laurolactam Chemical compound O=C1CCCCCCCCCCCN1 JHWNWJKBPDFINM-UHFFFAOYSA-N 0.000 claims 1
- 229920000299 Nylon 12 Polymers 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- UGFMBZYKVQSQFX-UHFFFAOYSA-N para-methoxy-n-methylamphetamine Chemical compound CNC(C)CC1=CC=C(OC)C=C1 UGFMBZYKVQSQFX-UHFFFAOYSA-N 0.000 claims 1
- 239000000454 talc Substances 0.000 claims 1
- 229910052623 talc Inorganic materials 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 23
- 239000004519 grease Substances 0.000 abstract description 8
- 239000002932 luster Substances 0.000 abstract description 8
- 230000005923 long-lasting effect Effects 0.000 abstract description 5
- 230000009286 beneficial effect Effects 0.000 abstract description 4
- 239000011248 coating agent Substances 0.000 abstract description 4
- 238000000576 coating method Methods 0.000 abstract description 4
- 230000014759 maintenance of location Effects 0.000 abstract description 4
- 230000035807 sensation Effects 0.000 abstract description 3
- 239000004480 active ingredient Substances 0.000 abstract description 2
- 230000003064 anti-oxidating effect Effects 0.000 abstract description 2
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 26
- 238000012360 testing method Methods 0.000 description 19
- 239000012071 phase Substances 0.000 description 12
- 239000003921 oil Substances 0.000 description 11
- 238000003756 stirring Methods 0.000 description 11
- 230000000052 comparative effect Effects 0.000 description 9
- 210000003491 skin Anatomy 0.000 description 8
- 230000008859 change Effects 0.000 description 6
- 235000013399 edible fruits Nutrition 0.000 description 6
- 238000010438 heat treatment Methods 0.000 description 4
- 230000001953 sensory effect Effects 0.000 description 4
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 230000002045 lasting effect Effects 0.000 description 3
- 239000002649 leather substitute Substances 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 238000006116 polymerization reaction Methods 0.000 description 3
- GTJOHISYCKPIMT-UHFFFAOYSA-N 2-methylundecane Chemical compound CCCCCCCCCC(C)C GTJOHISYCKPIMT-UHFFFAOYSA-N 0.000 description 2
- SGVYKUFIHHTIFL-UHFFFAOYSA-N Isobutylhexyl Natural products CCCCCCCC(C)C SGVYKUFIHHTIFL-UHFFFAOYSA-N 0.000 description 2
- 230000006978 adaptation Effects 0.000 description 2
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 description 2
- VKPSKYDESGTTFR-UHFFFAOYSA-N isododecane Natural products CC(C)(C)CC(C)CC(C)(C)C VKPSKYDESGTTFR-UHFFFAOYSA-N 0.000 description 2
- 239000010410 layer Substances 0.000 description 2
- 230000003020 moisturizing effect Effects 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- XOFYZVNMUHMLCC-ZPOLXVRWSA-N prednisone Chemical compound O=C1C=C[C@]2(C)[C@H]3C(=O)C[C@](C)([C@@](CC4)(O)C(=O)CO)[C@@H]4[C@@H]3CCC2=C1 XOFYZVNMUHMLCC-ZPOLXVRWSA-N 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- PQUXFUBNSYCQAL-UHFFFAOYSA-N 1-(2,3-difluorophenyl)ethanone Chemical compound CC(=O)C1=CC=CC(F)=C1F PQUXFUBNSYCQAL-UHFFFAOYSA-N 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- 206010040844 Skin exfoliation Diseases 0.000 description 1
- NWGKJDSIEKMTRX-AAZCQSIUSA-N Sorbitan monooleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O NWGKJDSIEKMTRX-AAZCQSIUSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 229940061720 alpha hydroxy acid Drugs 0.000 description 1
- 150000001280 alpha hydroxy acids Chemical class 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 210000003298 dental enamel Anatomy 0.000 description 1
- 229940008099 dimethicone Drugs 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 210000003780 hair follicle Anatomy 0.000 description 1
- NDJGGFVLWCNXSH-UHFFFAOYSA-N hydroxy(trimethoxy)silane Chemical compound CO[Si](O)(OC)OC NDJGGFVLWCNXSH-UHFFFAOYSA-N 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 230000001795 light effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000005012 migration Effects 0.000 description 1
- 238000013508 migration Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000000244 polyoxyethylene sorbitan monooleate Substances 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
- 229940068968 polysorbate 80 Drugs 0.000 description 1
- 229920000053 polysorbate 80 Polymers 0.000 description 1
- 239000011241 protective layer Substances 0.000 description 1
- 210000001732 sebaceous gland Anatomy 0.000 description 1
- 229920006268 silicone film Polymers 0.000 description 1
- 229940047670 sodium acrylate Drugs 0.000 description 1
- 229950004959 sorbitan oleate Drugs 0.000 description 1
- 239000012798 spherical particle Substances 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000002352 surface water Substances 0.000 description 1
- 210000000106 sweat gland Anatomy 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 210000001519 tissue Anatomy 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention provides a lip composition which comprises the following raw materials in parts by weight: 1-3 parts of ethyl cellulose; 3-8 parts of polydimethylsiloxane; 0.0001-5 parts of grapefruit extract; 2-4 parts of filler; 1-3 parts of emulsion stabilizer. The ethyl cellulose in the composition has the capability of slightly adsorbing water molecules, can moisten lips, can polymerize high-molecular non-volatile polydimethylsiloxane to provide a moist highlight coating on the lips, can form a card house structure to form a three-dimensional structure and lock active ingredients such as moisture retention and the like, can be attached to fine lines of the lips to fill gaps to keep a three-dimensional plump luster effect, has the effect of grease antioxidation, and can keep the color and luster and light sensation of lip glaze from being oxidized. Through the specific components or the specific proportions, the invention is more beneficial to improving the stable makeup holding performance of the product, improving the three-dimensional plump gloss of the product and enabling the long-lasting effect of the gloss of the product.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a lip composition, a preparation method thereof and a lip cosmetic.
Background
The lip glaze commonly used in the market is mainly provided with matt and soft fog makeup effect, and the makeup effect is slightly mature and exaggerated although the makeup effect looks higher, so that the age-reduced color makeup style has more one style of style, the appearance of naked makeup and 'pseudo-plain color' is brought up, and the lip is mainly provided with full-lip makeup effect and three-dimensional water-light mirror surface texture. A large number of mirror-surface water-based makeup lip products on the market have a plurality of defects, and are particularly characterized by phenomena of insufficient gloss, poor flatness, lasting makeup effect, insufficient three-dimensional fullness of the makeup effect, large application assistance, insufficient moistening, dry and chipped skin and poor appearance of lip color caused by easy oxidative discoloration.
The existing bright lip glaze contains a large amount of moist grease or grease with high refractive index, the gloss is improved, but the grease is easily oxidized on the skin to cause migration or absorption, and often the cosmetic effect is difficult to maintain for a long time. High gloss lip glazes have poorer permanence on the skin. Film forming agents are generally added to obtain long-lasting make-up effects, such as a large amount of silicone film forming agents and volatile oils, so that the make-up effects are improved permanently, but the gloss is reduced to some extent, and dry and skin peeling is caused after the oils volatilize. Although a large amount of film forming agent is covered on the lips to make the make-up effect durable, the lips lack a protective layer and are exposed to the air environment through wind and sun, and the lips are indispensable to form texture gaps due to the fact that the lips are fragile and thin in tissue structure layer and have no hair follicles, sweat glands and sebaceous glands attached. The lip portion is left in a film after the volatilization of the grease, and the lip portion is in a rugged state, and the film can not completely fill the rugged lip portion although being attached. Therefore, the cosmetic effect is uneven, and the cosmetic effect is durable but lacks a sense of three-dimensional fullness. Also, large amounts of film former can cause irritation of the consumer's lips, causing discomfort.
The CN 109512702A disclosed in the prior art mainly adopts volatile isododecane to be matched with and dissolve an oil phase film forming agent trimethyl silicic acid resin. The trimethyl silicate resin has very strong hard film forming effect and is matched with the high-volatility isododecane, so that a layer of tight film is left on the lip, and consumers feel very bad.
Therefore, it is necessary to provide a lip composition which can improve the stable makeup holding performance of the product, promote the three-dimensional fullness and glossiness of the high-gloss product, and make the long-lasting color and luster light effect of the product.
Disclosure of Invention
In view of the above, the technical problem to be solved by the invention is to provide a lip composition which is good in stability, good in stereoscopic fullness, high in glossiness and good in durability.
The invention provides a lip composition which comprises the following raw materials in parts by weight:
1-3 parts of ethyl cellulose; 3-8 parts of polydimethylsiloxane; 0.0001-5 parts of grapefruit extract; 2-4 parts of filler; 1-3 parts of emulsion stabilizer.
Preferably, the filler is selected from one or more of silica, mica, talcum powder, PMMA, chinlon-12, behenyl alcohol, cetyl alcohol, polyethylene, beeswax, bentonite, vinyl polydimethylsiloxane or polymethylsiloxane silsesquioxane cross-linked polymer.
Preferably, the emulsion stabilizer is selected from one or more of sodium acrylate-sodium acryloyldimethyl taurate copolymer emulsion and polyacrylate-13 emulsion.
The invention provides a preparation method of a lip composition, which is characterized by comprising the following steps:
mixing and emulsifying ethyl cellulose, polydimethylsiloxane and a filler to obtain a mixture;
mixing the emulsion stabilizer and the grapefruit extractive solution with the mixture.
Preferably, the temperature of the emulsification is 65-70 ℃; the emulsification time is 10-30 min; the rotational speed of the emulsification is 2000-3000 rpm.
The lip composition according to the technical scheme or the lip composition prepared by the preparation method according to the technical scheme is applied to preparation of lip cosmetics.
The invention provides a lip cosmetic, which comprises the lip composition according to any one of the technical schemes or the lip composition prepared by the preparation method according to any one of the technical schemes.
Preferably, the lip cosmetic further comprises one or more of an emollient, an emulsifier, a thickener, a solvent, a colorant, and a preservative;
the emollient is selected from one or more of octyl dodecanol, diisostearyl malate, polyglycerol-2 triisostearate, di-diglycerol polyacyl adipate-2, hydrogenated polyisobutene, caprylic triglyceride, capric triglyceride, di-behenyl dimer linoleyl dimer linoleate, isostearyl dimer linoleyl or phytosterol dimer linoleyl;
the emulsifier is one or more selected from polysorbate-60, sorbitan stearate, stearyl alcohol polyether-20, glycerol stearate and cetostearyl alcohol polyether-20;
the thickener is one or more selected from dextrin palmitate, polybutene, hectorite or carbomer;
the aqueous phase film forming agent is selected from one or more of acrylic acid (ester) copolymer latex, acrylic acid (ester)/methacrylic acid dimethyl amino ethyl ester copolymer latex, acrylic acid (ester)/methacrylic acid allyl ester copolymer AMP salt, VP/VA copolymer and PVP, and the solvent is selected from one or more of denatured ethanol or water;
the colorant is selected from one or more of CI 77491, CI 45410, CI 19140, CI 77492, CI 77499 or CI 15985;
the preservative is selected from one or more of phenoxyethanol, ethylhexyl glycerol, octanediol, pentanediol and hexanediol.
Preferably, the lip composition has a mass content of 7% to 21% in the cosmetic.
Preferably, the lip cosmetic includes a lip glaze.
Compared with the prior art, the invention provides a lip composition, which comprises the following raw materials in parts by weight:
1-3 parts of ethyl cellulose; 3-8 parts of polydimethylsiloxane; 0.0001-5 parts of grapefruit extract; 2-4 parts of filler; 1-3 parts of emulsion stabilizer. The ethyl cellulose in the composition has the capability of slightly adsorbing water molecules, can moisten lips, can polymerize high-molecular non-volatile polydimethylsiloxane to provide a plump moist highlight coating on the lips, can form a card house structure to form a three-dimensional structure and lock active ingredients such as moisture retention and the like, can be attached to fine lines of the lips to fill gaps to keep a three-dimensional plump luster effect, and the grapefruit extract has the effects of grease antioxidation and can keep the color and luster and light sensation of lip glaze oxidized. The emulsion stabilizer can emulsify and suspend the other four components, so that the combination of the composition is more uniform and fine, and the stable composition is obtained. Through the specific components or the specific proportions, the invention is more beneficial to improving the stable makeup holding performance of the product, improving the three-dimensional plump gloss of the product and enabling the long-lasting effect of the gloss of the product.
Detailed Description
The invention provides a composition for lips, a preparation method thereof and cosmetics for lips, and a person skilled in the art can use the content of the composition for lips to appropriately improve the technological parameters. It is expressly noted that all such similar substitutions and modifications will be apparent to those skilled in the art, and they are intended to be within the scope of the present invention. While the methods and applications of this invention have been described in terms of preferred embodiments, it will be apparent to those skilled in the relevant art that the invention can be practiced and practiced with modification and alteration and combination of the methods and applications herein without departing from the spirit and scope of the invention.
The invention provides a lip composition which comprises the following raw materials in parts by weight:
1-3 parts of ethyl cellulose; 3-8 parts of polydimethylsiloxane; 0.0001-5 parts of grapefruit extract; 2-4 parts of filler; 1-3 parts of emulsion stabilizer.
The lip composition provided by the invention comprises 1-3 parts by weight of ethyl cellulose; specifically, the amount may be 1 part by weight, 2 parts by weight, or 3 parts by weight, or a point value between any two of the above.
The ethyl cellulose of the invention has different types so as to meet the requirements of the adaptation formula on different physical properties, uses and viscosities. The ethyl cellulose is a film with 30-60 micron particle size, thickened oil phase and skin moisturizing effect. Ethylcellulose requires a pre-heat dissolution treatment to provide a uniform, high gloss, non-taut film.
Ethylcellulose is also available from different manufacturers, such as the Wanlu supplier, with ETHOCEL Std 4Premium and ETHOCEL Std 100Premium being used as examples. Two ethyl cellulose solutions of 5% were each tested for viscosity at 25 ℃ using a wushi viscosity meter with a solvent of 80% toluene and 20% ethanol. 5%ETHOCEL Std 4Premium the solution viscosity ranges from 3 to 5.5cps,5%ETHOCEL Std 100Premium and from 90 to 110cps. Meanwhile, the film forming speed, thickness and uniformity after film forming are observed. The obtained ETHOCEL Std 100Premium has better polymerization degree, higher film forming speed and better film forming uniformity. The viscosity of the polymer may vary from model to model. The film-forming effect varies depending on the degree of polymerization. The high degree of polymerization can form more films and thicken grease.
The lip composition provided by the invention comprises 3-8 parts by weight of polydimethylsiloxane; preferably 4 to 7 parts by weight; more preferably 4 to 6 parts by weight; specifically, the amount may be 4 parts by weight, 5 parts by weight, or 6 parts by weight, or a point value between any two of the above.
The polydimethylsiloxane disclosed by the invention is high in molecular weight, has excellent water retention capacity and waterproof capacity, and is high in refractive index, so that a high water-resistant film can be formed.
The lip composition provided by the invention comprises 0.0001-5 parts by weight of grapefruit extract; preferably comprises 0.001 to 5 parts by weight; more preferably 0.001 to 4 parts by weight; specifically, the amount may be 0.001 part by weight, 1 part by weight, 2 parts by weight, 3 parts by weight, 4 parts by weight, or a point value between any two of the above.
The lip composition provided by the invention comprises 2-4 parts by weight of filler; specifically, the amount may be 2 parts by weight, 3 parts by weight or 4 parts by weight, or a point value between any two of the above.
According to the invention, the filler is selected from one or more of silica, mica, talcum powder, PMMA, chinlon-12, behenyl alcohol, cetyl alcohol and vinyl polydimethylsiloxane-polymethylsiloxane silsesquioxane cross-linked polymer.
In a preferred embodiment of a part of the present invention, the filler is more preferably: one or two of silica, behenyl alcohol, vinyl dimethicone-polymethylsilicone silsesquioxane cross polymer.
The filler can fill the lip fine lines and can disperse and form the three-dimensional structure of the card house, and can weaken the effect of the lip fine lines and plump lips visually.
The lip composition provided by the invention comprises 1-3 parts by weight of emulsion stabilizer; specifically, the amount may be 1 part by weight, 2 parts by weight, or 3 parts by weight, or a point value between any two of the above.
According to the invention, the emulsion stabilizer is selected from one or more of sodium acrylate-sodium acryloyldimethyl taurate copolymer emulsion and polyacrylate-13 emulsion;
in a preferred embodiment of a part of the present invention, the filler is more preferably: silica, behenyl alcohol.
In a preferred embodiment of a part of the present invention, the emulsion stabilizer may include: sodium acrylate-sodium acryloyldimethyl taurate copolymer emulsion.
A preferred manufacturer may be Sibirch under the trade name SIMULGEL EG.
The weight percentages of the raw materials are as follows: 35-40% of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 20-25% of isohexadecane, 5-10% of polysorbate-80, 22.5-37.5% of water and 0-5% of sorbitan oleate.
In a preferred embodiment of a part of the present invention, the lip composition comprises the following raw materials in parts by weight:
1-3 parts of ethyl cellulose; 4-7 parts of polydimethylsiloxane; 0.001-4 parts of grapefruit extract; 2-4 parts of filler; 1-3 parts of emulsion stabilizer.
In a preferred embodiment of a part of the present invention, the lip composition comprises the following raw materials in parts by weight:
1-3 parts of ethyl cellulose; 4-6 parts of polydimethylsiloxane; 2-3 parts of filler; 1-3 parts of emulsion stabilizer.
In a preferred embodiment of a part of the present invention, the lip composition comprises the following raw materials in parts by weight:
2 parts of ethyl cellulose; 6 parts of polydimethylsiloxane; 2 parts of grapefruit fruit extract; 2.5 parts of filler; 2.5 parts of emulsion stabilizer.
In a preferred embodiment of a part of the present invention, the lip composition comprises the following raw materials in parts by weight:
1.5 parts of ethyl cellulose; 4 parts of polydimethylsiloxane; 3 parts of grapefruit fruit extract; 2 parts of filler; 2 parts of emulsion stabilizer.
In a preferred embodiment of a part of the present invention, the lip composition comprises the following raw materials in parts by weight:
2 parts of ethyl cellulose; 4 parts of polydimethylsiloxane; 2 parts of grapefruit fruit extract; 2 parts of filler; emulsion stabilizer 1.5 parts.
In a preferred embodiment of a part of the present invention, the lip composition comprises the following raw materials in parts by weight:
1.5 parts of ethyl cellulose; 5 parts of polydimethylsiloxane; 3 parts of grapefruit fruit extract; 2 parts of filler; 2.5 parts of emulsion stabilizer.
In a preferred embodiment of a part of the present invention, the lip composition comprises the following raw materials in parts by weight:
2 parts of ethyl cellulose; 4 parts of polydimethylsiloxane; 4 parts of grapefruit extract; 3 parts of filler; 2 parts of emulsion stabilizer.
The ethyl cellulose provided by the invention is thickened for an oil phase and has a film forming effect, and meanwhile, the ethyl cellulose has a slight capability of adsorbing water molecules, can form a flexible high-refraction film on lips and moisten skins, is matched with a filler with small particle size, and the filler with spherical particle size can be attached to gaps of lip textures and can cover the lip textures to form a smooth mirror light feel and make lips stereoscopic and plump. The grapefruit extract is rich in alpha-hydroxy acids, flavonoids, vitamins and carbohydrates. Has effects of keeping moisture, and resisting oxidation to oil and skin. The lip glaze is skillfully matched, so that the color, luster and luster of the lip glaze are not oxidized, the make-up effect is more durable and is not dull, meanwhile, the polydimethylsiloxane is matched, the raw material is high-glossiness emollients, and can form a water-resistant film on the skin, so that the moisture loss on the skin epidermis is prevented, the tightness brought by the solidified water-oil film forming agent is relieved, and the emulsion stabilizer can fully and perfectly refine and uniformly the raw materials for a plurality of functions, so that the light sense is longer. Long-acting light feel after being smeared and lasting mirror surface three-dimensional refraction make-up effect.
The invention provides a preparation method of a lip composition, which is characterized by comprising the following steps:
mixing and emulsifying ethyl cellulose, polydimethylsiloxane and a filler to obtain a mixture;
mixing the emulsion stabilizer and the grapefruit extractive solution with the mixture.
The preparation method of the lip composition provided by the invention comprises the steps of firstly mixing and emulsifying ethyl cellulose and polydimethylsiloxane to obtain a mixture.
The invention is not limited to the specific manner of mixing described, but may be practiced by those skilled in the art.
The temperature of the emulsification is preferably 65-70 ℃; the time of emulsification is preferably 10-30 min; the rotational speed of the emulsification is preferably 2000-3000 rpm.
The lip composition according to the technical scheme or the lip composition prepared by the preparation method according to the technical scheme is applied to preparation of lip cosmetics.
The invention provides a lip cosmetic, which comprises the lip composition according to any one of the technical schemes or the lip composition prepared by the preparation method according to any one of the technical schemes.
The lip cosmetic according to the present invention further comprises one or more of an emollient, an emulsifier, a thickener, an aqueous film former, a solvent, a colorant and a preservative;
wherein the emollient is 30 to 40 weight parts; preferably 32 to 38 parts by weight; 4-6 parts by weight of an emulsifier; specifically, the weight of the composition can be 4 weight parts, 5 weight parts or 6 weight parts;
8-15 parts by weight of water phase film forming agent; preferably 8 to 12 parts by weight; the solvent range is 35-45 parts by weight; the coloring agent comprises: 0.1 to 2 parts by weight, preferably 0.5 to 1.8 parts by weight, of a thickener of 0 to 5 parts by weight; more preferably 0.2 to 4.8 parts by weight.
The emollient is selected from one or more of octyl dodecanol, diisostearyl malate, polyglycerol-2 triisostearate, di-diglycerol polyacyl adipate-2, hydrogenated polyisobutene, caprylic triglyceride, capric triglyceride, di-behenyl dimer linoleyl dimer linoleate, isostearyl dimer linoleyl or phytosterol dimer linoleyl;
the emulsifier is one or more selected from polysorbate-60, sorbitan stearate, stearyl alcohol polyether-20, glycerol stearate and cetostearyl alcohol polyether-20;
the thickener is one or more selected from dextrin palmitate, hectorite, behenyl alcohol, polybutene or carbomer;
the aqueous phase film forming agent is one or more selected from acrylic acid (ester) copolymer latex, acrylic acid (ester)/methacrylic acid dimethyl amino ethyl ester copolymer latex, acrylic acid (ester)/methacrylic acid allyl ester copolymer AMP salt, VP/VA copolymer and PVP.
The solvent is one or more selected from denatured ethanol or water;
the colorant is selected from one or more of CI 77491, CI 45410, CI 19140, CI 77492, CI 77499 or CI 15985;
the preservative is selected from one or more of phenoxyethanol, ethylhexyl glycerol, octanediol, pentanediol and hexanediol.
The mass content of the lip composition in the cosmetic is preferably 7-23%; more preferably 10% to 20%.
The lip cosmetic of the present invention includes, but is not limited to, lip enamel.
The invention provides a preparation method of a lip cosmetic, which comprises the following steps:
step A: mixing a preservative, a water-soluble colorant and water as an aqueous phase;
and (B) step (B): heating and stirring ethyl cellulose and an emollient until the ethyl cellulose and the emollient are dissolved;
the heating temperature is 85-100 ℃, and the stirring speed is 30rpm.
Step C: polydimethyl siloxane, emulsifier, filler, thickener and oil-soluble colorant are mixed to be used as an oil phase;
step D: emulsifying the water phase obtained in the step A and the oil phase obtained in the step B;
step E: and C, adding the emulsion stabilizer grapefruit fruit extract into the mixture obtained in the step C to obtain the lip cosmetic.
The mixing in the step A, the step C and the step E comprises stirring and mixing; the mixing time is 20-60 min; the temperature of the mixing is 65-70 ℃; the rotation speed of the stirring and mixing is 1000-2500rpm
The temperature of the emulsification is preferably 65-70 ℃; the time of emulsification is preferably 10-30 min; the rotational speed of the emulsification is preferably 2000-3000 rpm.
The invention provides a lip composition which comprises the following raw materials in parts by weight: 1-3 parts of ethyl cellulose; 3-8 parts of polydimethylsiloxane; 0.0001-5 parts of grapefruit extract; 2-4 parts of filler; 1-3 parts of emulsion stabilizer. The ethyl cellulose in the composition has the capability of slightly adsorbing water molecules, can moisten lips, can polymerize high-molecular non-volatile polydimethylsiloxane to provide a plump and moist high-gloss coating on the lips, and the filler fills fine lines of the lips and can thicken the high-gloss coating, so that the light sensation is more stereoscopic and plump. The grapefruit extract can slow down the oxidation of grease and skin, and better protect the color and luster of lip glaze. The emulsion stabilizer can emulsify and suspend the other four components, so that the combination of the composition is more uniform and fine, and the stable composition is obtained. Through the specific components or the specific proportions, the invention is more beneficial to improving the stable makeup holding performance of the product, improving the three-dimensional plump gloss of the product and enabling the long-lasting effect of the gloss of the product.
In order to further illustrate the present invention, the present invention provides a lip composition, a method for preparing the same, and a cosmetic for lips, which are described in detail below with reference to examples.
Examples 1 to 5:
comparative examples 1 to 9:
the process comprises the following steps of the composition:
step 1: preparing an aqueous phase: mixing water-soluble colorant, antiseptic and water under stirring, heating to 65deg.C, and stirring at 30rpm/min.
Step 2: preparing an oil phase: (1) ethylcellulose and the emollient octyl dodecanol were heated with stirring until completely dissolved, clear and transparent, at a temperature of 95℃and at a stirring speed of 30rpm/min. (2) The oil phase colorant and the remaining portion of the emollient were mixed and milled using a mill to disperse uniformly. (3) And (3) uniformly stirring and mixing the product obtained in the step (1) and the step (2) with polydimethylsiloxane, an emulsifying agent, a filler, and heating to 65 ℃ at a stirring speed of 1000rpm/min.
Step 3: emulsification: mixing the water phase and the oil phase, and emulsifying at the speed of 2500rpm/min for the time of emulsification: 3-6min, emulsification temperature: 65 ℃.
Step 4: cooling to 35deg.C, adding water phase film forming agent, emulsion stabilizer, grapefruit fruit extractive solution, and denatured ethanol into emulsified material, stirring, emulsifying again, and emulsifying for a period of time: 3-5min, emulsification speed: 2500rpm/min.
Step 5: and (5) vacuumizing and discharging.
The polybutene and cyclopentadimethicone in the raw materials of comparative example 2/3/4 were substituted for ethylcellulose and dimethicone, respectively, and the process was similar and different.
Test examples
1. Centrifugal stability test
The test method comprises the following steps: the stable emulsion system of the prepared lip cosmetic was observed through a centrifugal test at 30mins,3000 rpm.
As shown by the centrifugal test results, the lip cosmetic prepared by the composition disclosed by the invention has the advantages of high centrifugal stability, good stability and no emulsion layering phenomenon.
2. Gloss test
Test sample: lip glazes obtained in examples 1 to 5 and comparative examples 1 to 9
Test instrument: multi-angle gloss meter (BYK, germany)
Test object: artificial leather
The testing method comprises the following steps: 1. sterilizing and cleaning the artificial leather, and defining a plurality of fixed areas of 2cm multiplied by 2cm on the artificial leather; 2. measuring the glossiness value of the fixed area by using a multi-angle gloss meter; 3. uniformly smearing 0.2g of test sample on the fixed area; 4. and measuring the glossiness value of the fixed area of the smeared product by using a multi-angle gloss meter.
As can be seen from the gloss test, the lip cosmetic prepared by using the composition of the invention has higher increment rate of gloss, and has better gloss.
3. Make-up holding test
Test sample: lip glazes obtained in examples 1 to 5 and comparative examples 1 to 9
Test instrument: 3nh grating spectrocolorimeter
Test object: healthy volunteers were selected with 120 women with daily cosmetic habits, aged 20-40 years.
The testing method comprises the following steps: the volunteers are randomly divided into 12 groups and grouped into 10 persons, the test samples are respectively coated on the lips of the volunteers in the group, the lips of the volunteers are tested after 2 hours, and a spectrocolorimeter is used for measuring the lip color change, namely, the lip dressing color difference delta E of the product for 2 hours, wherein the smaller delta E indicates the more complete dressing, namely, the smaller lip glaze color change and the better lasting degree are indicated.
As can be seen from the above table, the lip makeup color difference change data of examples 1 to 5 are smaller than those of comparative examples 1 to 9 and the lip makeup color difference change data of the market bid, and the lip makeup color difference change of examples 1 to 5 is smaller and the makeup durability is better. Meanwhile, the five compositions containing the ethylcellulose, the polydimethylsiloxane, the grapefruit extract, the filler and the emulsion stabilizer can reduce the color difference change in the formula of the lip glaze product and improve the durability under the specific proportioning content.
4. Crowd testing
The test method comprises the following steps: healthy volunteers were selected with 80 women with daily cosmetic habits, aged 20-40 years. The obtained lip glazes of examples 1 to 5 and comparative examples 1 to 9 were subjected to sensory test. Test dimension: gloss, makeup holding, moisturizing, smoothness of application, stereoscopic fullness of lips, and favorability. The evaluation was performed on 6 grades, of which 5 is very excellent, 4 is excellent, 3 is general, 2 is poor, and 1 is poor. The score was averaged over 80 volunteers.
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From the above sensory data, the sensory data for the population of examples 1-5 is superior to the sensory data for comparative examples 1-9. Meanwhile, the product prepared from five compositions of ethyl cellulose, polydimethylsiloxane, grapefruit extract, filler and emulsion stabilizer at a specific proportioning content has excellent glossiness, makeup retention, moistening feel, smoothness in application and three-dimensional fullness of lips. The difference from comparative examples 1-5 is remarkable, which shows that the five compositions of ethylcellulose, polydimethylsiloxane, grapefruit extract, filler and emulsion stabilizer have synergistic effect, and the experimental results of comparative examples 5-9 show that the compositions of the invention are more beneficial to improving glossiness, makeup retention and three-dimensional fullness in a certain ratio and dosage range.
The foregoing is merely a preferred embodiment of the present invention and it should be noted that modifications and adaptations to those skilled in the art may be made without departing from the principles of the present invention, which are intended to be comprehended within the scope of the present invention.
Claims (10)
1. The lip composition is characterized by comprising the following raw materials in parts by weight:
1-3 parts of ethyl cellulose; 3-8 parts of polydimethylsiloxane; 0.0001-5 parts of grapefruit extract; 2-4 parts of filler; 1-3 parts of emulsion stabilizer.
2. The composition according to claim 1, wherein the filler is selected from one or more of silica, mica, talc, PMMA, nylon-12, behenyl alcohol, polyethylene, beeswax, cetyl alcohol, bentonite, vinyl polydimethylsiloxane or polymethylsiloxane silsesquioxane cross-linked polymer.
3. The composition according to claim 1, wherein the emulsion stabilizer is one or more selected from the group consisting of sodium acrylate-sodium acryloyldimethyl taurate copolymer emulsion and polyacrylate-13 emulsion.
4. A method of preparing a lip composition comprising:
mixing and emulsifying ethyl cellulose, polydimethylsiloxane and a filler to obtain a mixture;
mixing emulsion stabilizer and grapefruit extractive solution with the mixture.
5. The method according to claim 4, wherein the temperature of the emulsification is 65 to 70 ℃; the emulsification time is 10-30 min; the rotational speed of the emulsification is 2000-3000 rpm.
6. Use of the lip composition according to any one of claims 1 to 3 or the lip composition prepared by the preparation method according to any one of claims 4 to 5 for preparing a cosmetic for lips.
7. A cosmetic for lips comprising the composition for lips according to any one of claims 1 to 3 or the composition for lips produced by the production method according to any one of claims 4 to 5.
8. The lip cosmetic according to claim 7, further comprising one or more of an emollient, an emulsifier, a thickener, an aqueous film former, a solvent, a colorant, and a preservative;
the emollient is selected from one or more of octyl dodecanol, diisostearyl malate, polyglycerol-2 triisostearate, di-diglycerol polyacyl adipate-2, hydrogenated polyisobutene, caprylic triglyceride, capric triglyceride, di-behenyl dimer linoleyl dimer linoleate, isostearyl dimer linoleyl or phytosterol dimer linoleyl;
the emulsifier is one or more selected from polysorbate-60, sorbitan stearate, stearyl alcohol polyether-20, glycerol stearate and cetostearyl alcohol polyether-20;
the thickener is one or more selected from dextrin palmitate, polybutene, hectorite or carbomer;
the aqueous phase film forming agent is one or more selected from acrylic acid (ester) copolymer latex, acrylic acid (ester)/methacrylic acid dimethyl amino ethyl ester copolymer latex, acrylic acid (ester)/methacrylic acid allyl ester copolymer AMP salt, VP/VA copolymer and PVP.
The solvent is one or more selected from denatured ethanol, isohexadecane or water;
the colorant is selected from one or more of CI 77491, CI 45410, CI 19140, CI 77492, CI 77499 or CI 15985;
the preservative is selected from one or more of phenoxyethanol, ethylhexyl glycerol, octanediol, pentanediol and hexanediol.
9. The lip cosmetic according to claim 7, wherein the mass content of the lip composition in the cosmetic is 7% to 23%.
10. The lip cosmetic according to claim 7, characterized in that the lip cosmetic comprises a lip glaze.
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