CN116548614A - Processing method of high metasilicate water concentrate - Google Patents
Processing method of high metasilicate water concentrate Download PDFInfo
- Publication number
- CN116548614A CN116548614A CN202310697939.7A CN202310697939A CN116548614A CN 116548614 A CN116548614 A CN 116548614A CN 202310697939 A CN202310697939 A CN 202310697939A CN 116548614 A CN116548614 A CN 116548614A
- Authority
- CN
- China
- Prior art keywords
- water
- fermentation
- metasilicate
- hydrolysis
- silicon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 66
- 239000012141 concentrate Substances 0.000 title claims abstract description 22
- 238000003672 processing method Methods 0.000 title claims abstract description 10
- 238000000855 fermentation Methods 0.000 claims abstract description 57
- 230000004151 fermentation Effects 0.000 claims abstract description 57
- 235000003130 Arctium lappa Nutrition 0.000 claims abstract description 48
- 235000008078 Arctium minus Nutrition 0.000 claims abstract description 48
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 25
- 230000007062 hydrolysis Effects 0.000 claims abstract description 24
- 239000000463 material Substances 0.000 claims abstract description 17
- 239000012535 impurity Substances 0.000 claims abstract description 14
- 238000001035 drying Methods 0.000 claims abstract description 13
- 238000004140 cleaning Methods 0.000 claims abstract description 10
- 238000010000 carbonizing Methods 0.000 claims abstract description 9
- 230000001954 sterilising effect Effects 0.000 claims abstract description 9
- 241000208843 Arctium Species 0.000 claims description 47
- 238000000034 method Methods 0.000 claims description 28
- 239000002245 particle Substances 0.000 claims description 21
- 244000025221 Humulus lupulus Species 0.000 claims description 12
- 235000008694 Humulus lupulus Nutrition 0.000 claims description 12
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 11
- 238000003763 carbonization Methods 0.000 claims description 11
- 239000000203 mixture Substances 0.000 claims description 11
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 8
- 239000000413 hydrolysate Substances 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 6
- 241000228245 Aspergillus niger Species 0.000 claims description 5
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims description 5
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 claims description 5
- 239000006004 Quartz sand Substances 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 5
- 229910052748 manganese Inorganic materials 0.000 claims description 5
- 239000011572 manganese Substances 0.000 claims description 5
- 239000012528 membrane Substances 0.000 claims description 5
- 238000012545 processing Methods 0.000 claims description 5
- 239000004576 sand Substances 0.000 claims description 5
- 238000000926 separation method Methods 0.000 claims description 5
- 238000000108 ultra-filtration Methods 0.000 claims description 5
- 241000186660 Lactobacillus Species 0.000 claims description 4
- 241000235342 Saccharomycetes Species 0.000 claims description 4
- 238000005520 cutting process Methods 0.000 claims description 4
- 239000008367 deionised water Substances 0.000 claims description 4
- 229910021641 deionized water Inorganic materials 0.000 claims description 4
- 239000011363 dried mixture Substances 0.000 claims description 4
- 230000003203 everyday effect Effects 0.000 claims description 4
- 230000003301 hydrolyzing effect Effects 0.000 claims description 4
- 229940039696 lactobacillus Drugs 0.000 claims description 4
- 239000011343 solid material Substances 0.000 claims description 4
- 238000004659 sterilization and disinfection Methods 0.000 claims description 4
- 238000005057 refrigeration Methods 0.000 claims description 3
- 108010009736 Protein Hydrolysates Proteins 0.000 claims description 2
- 238000001914 filtration Methods 0.000 claims description 2
- 229910052710 silicon Inorganic materials 0.000 abstract description 45
- 239000010703 silicon Substances 0.000 abstract description 45
- 239000000126 substance Substances 0.000 abstract description 11
- 239000000796 flavoring agent Substances 0.000 abstract description 9
- 235000019634 flavors Nutrition 0.000 abstract description 9
- 235000015097 nutrients Nutrition 0.000 abstract description 5
- 235000016709 nutrition Nutrition 0.000 abstract description 3
- 230000035764 nutrition Effects 0.000 abstract description 3
- 238000002360 preparation method Methods 0.000 abstract description 2
- 240000005528 Arctium lappa Species 0.000 abstract 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 44
- 239000000243 solution Substances 0.000 description 17
- 241000196324 Embryophyta Species 0.000 description 16
- 241000282414 Homo sapiens Species 0.000 description 14
- IJKVHSBPTUYDLN-UHFFFAOYSA-N dihydroxy(oxo)silane Chemical compound O[Si](O)=O IJKVHSBPTUYDLN-UHFFFAOYSA-N 0.000 description 10
- 238000000605 extraction Methods 0.000 description 10
- 230000000694 effects Effects 0.000 description 9
- 239000007864 aqueous solution Substances 0.000 description 7
- 239000000047 product Substances 0.000 description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 6
- 230000036541 health Effects 0.000 description 6
- 239000000843 powder Substances 0.000 description 6
- XJKVPKYVPCWHFO-UHFFFAOYSA-N silicon;hydrate Chemical compound O.[Si] XJKVPKYVPCWHFO-UHFFFAOYSA-N 0.000 description 6
- 239000007787 solid Substances 0.000 description 6
- 241000218228 Humulus Species 0.000 description 5
- 239000010419 fine particle Substances 0.000 description 5
- 239000002689 soil Substances 0.000 description 5
- 208000024827 Alzheimer disease Diseases 0.000 description 4
- 229920002472 Starch Polymers 0.000 description 4
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 4
- 229910052782 aluminium Inorganic materials 0.000 description 4
- 210000002808 connective tissue Anatomy 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 235000019698 starch Nutrition 0.000 description 4
- 239000008107 starch Substances 0.000 description 4
- 241000894006 Bacteria Species 0.000 description 3
- 229920002683 Glycosaminoglycan Polymers 0.000 description 3
- 206010039966 Senile dementia Diseases 0.000 description 3
- 229910052785 arsenic Inorganic materials 0.000 description 3
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 230000006378 damage Effects 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 230000018109 developmental process Effects 0.000 description 3
- 201000010099 disease Diseases 0.000 description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 3
- 229910052742 iron Inorganic materials 0.000 description 3
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- 108090000623 proteins and genes Proteins 0.000 description 3
- 102000004169 proteins and genes Human genes 0.000 description 3
- 210000002784 stomach Anatomy 0.000 description 3
- 208000024172 Cardiovascular disease Diseases 0.000 description 2
- 206010011224 Cough Diseases 0.000 description 2
- 206010061218 Inflammation Diseases 0.000 description 2
- 208000027418 Wounds and injury Diseases 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 230000003467 diminishing effect Effects 0.000 description 2
- 230000004054 inflammatory process Effects 0.000 description 2
- 208000014674 injury Diseases 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 244000005700 microbiome Species 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 230000000050 nutritive effect Effects 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 230000001737 promoting effect Effects 0.000 description 2
- 238000010298 pulverizing process Methods 0.000 description 2
- 238000002791 soaking Methods 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000013589 supplement Substances 0.000 description 2
- 239000002352 surface water Substances 0.000 description 2
- 231100000331 toxic Toxicity 0.000 description 2
- 230000002588 toxic effect Effects 0.000 description 2
- 238000003809 water extraction Methods 0.000 description 2
- 206010000060 Abdominal distension Diseases 0.000 description 1
- 206010063409 Acarodermatitis Diseases 0.000 description 1
- 206010003210 Arteriosclerosis Diseases 0.000 description 1
- 241000206761 Bacillariophyta Species 0.000 description 1
- 235000016068 Berberis vulgaris Nutrition 0.000 description 1
- 241000335053 Beta vulgaris Species 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 206010007247 Carbuncle Diseases 0.000 description 1
- 206010010774 Constipation Diseases 0.000 description 1
- 208000013558 Developmental Bone disease Diseases 0.000 description 1
- 244000085625 Equisetum Species 0.000 description 1
- 241000282412 Homo Species 0.000 description 1
- 206010024229 Leprosy Diseases 0.000 description 1
- 206010030113 Oedema Diseases 0.000 description 1
- 208000001132 Osteoporosis Diseases 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 241000209504 Poaceae Species 0.000 description 1
- 208000015634 Rectal Neoplasms Diseases 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 241000447727 Scabies Species 0.000 description 1
- 206010072610 Skeletal dysplasia Diseases 0.000 description 1
- 208000013738 Sleep Initiation and Maintenance disease Diseases 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 208000011775 arteriosclerosis disease Diseases 0.000 description 1
- 206010003246 arthritis Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000000740 bleeding effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 230000022159 cartilage development Effects 0.000 description 1
- 208000026106 cerebrovascular disease Diseases 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 238000005056 compaction Methods 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 208000029078 coronary artery disease Diseases 0.000 description 1
- 201000003146 cystitis Diseases 0.000 description 1
- 230000002354 daily effect Effects 0.000 description 1
- 230000007850 degeneration Effects 0.000 description 1
- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 208000002173 dizziness Diseases 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 201000006549 dyspepsia Diseases 0.000 description 1
- 230000002526 effect on cardiovascular system Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 239000003673 groundwater Substances 0.000 description 1
- 230000012010 growth Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 206010022437 insomnia Diseases 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 230000027939 micturition Effects 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- GALOTNBSUVEISR-UHFFFAOYSA-N molybdenum;silicon Chemical compound [Mo]#[Si] GALOTNBSUVEISR-UHFFFAOYSA-N 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 210000005036 nerve Anatomy 0.000 description 1
- 231100000956 nontoxicity Toxicity 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 208000008128 pulmonary tuberculosis Diseases 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 206010038038 rectal cancer Diseases 0.000 description 1
- 201000001275 rectum cancer Diseases 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 208000005687 scabies Diseases 0.000 description 1
- 238000004904 shortening Methods 0.000 description 1
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
- SBEQWOXEGHQIMW-UHFFFAOYSA-N silicon Chemical compound [Si].[Si] SBEQWOXEGHQIMW-UHFFFAOYSA-N 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 230000009645 skeletal growth Effects 0.000 description 1
- 230000012488 skeletal system development Effects 0.000 description 1
- 238000002798 spectrophotometry method Methods 0.000 description 1
- 230000001502 supplementing effect Effects 0.000 description 1
- 230000004083 survival effect Effects 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 210000001519 tissue Anatomy 0.000 description 1
- 208000004371 toothache Diseases 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 201000008827 tuberculosis Diseases 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/065—Microorganisms
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/30—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
- A23L5/32—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation using phonon wave energy, e.g. sound or ultrasonic waves
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a processing method of high metasilicate water concentrated solution, which comprises the following steps: s1, selecting materials, refrigerating, S2, cleaning, granulating, S3, inoculating tidal water, S4, pile fermentation, S5, drying, S6, crushing, S7, carbonizing, S8, ultrasonic-assisted hydrolysis, S9, removing impurities and sterilizing to obtain a high metasilicate water concentrate; the invention is characterized by safety, innocuity, rich nutrition and unique flavor by fermenting the burdock root and the hop and then extracting the soluble silicon with high efficiency and combining a plurality of fermentation nutrient substances and flavor substances, and the preparation method is quick, simple and convenient and has good economy.
Description
Technical Field
The invention relates to a processing method of a high metasilicate water concentrated solution, belonging to the technical field of burdock processing.
Background
Silicon (silicon) is about one fourth of the constituent materials of the soil, and is contained next to oxygen in the crust. In 1804 a research has been carried out to find that the plants contain silicon, which is present in almost all plants grown in the soil and affects the growth and development of the plants, especially essential elements of some plants such as gramineae, beet, equisetum and some diatoms. Silicon element is also an essential element for normal survival and development of human body, is one of components required by the integral formation of glycosaminoglycan and related protein complex in connective tissue, and participates in various physiological activities in human body, such as: silicon has physiological function in the process of skeletonization, and promotes skeletal development and growth; silicon participates in the metabolism of polysaccharide and is a main component of some glucosaminopolysaccharide carboxylic acid; silicon is associated with cardiovascular diseases, and people such as lack of silicon can cause arthritis, arteriosclerosis, coronary heart disease and the like; the reduction of silicon initiates the degeneration of connective tissue and elemental silicon helps the damaged tissue regenerate.
Conventionally, humans can ingest water containing metasilicic acid components and mineral nutrients required by the human body from groundwater, surface water and spring water, or supplement the water with absorbable silicon elements and various trace mineral elements from crops produced from soil. With the rapid development of industrialization, especially the rapid progress of chemical industry, serious pollution to different degrees is caused to natural surface water and soil, so that today we can not ingest enough silicon elements and other microelements through daily diet, thus causing the deficiency of silicon elements and microelements in modern people, and many people have the primary silicon element deficiency symptoms, such as cardiovascular diseases, cerebrovascular diseases, infant bone dysplasia, osteoporosis and the like.
The method for solving the problems is to treat the silicon in the nature into a water-soluble form, and to match other components needed by human body, thereby achieving the purpose of supplementing silicon and guaranteeing the health of human body. Currently, the methods for extracting silicon from plants on the market mainly include the following methods: (1) and (3) hydrolysis: crushing plants into fine particles, soaking the particles in water, and carrying out hydrolysis reaction under the condition of heating so as to extract silicon in the plants; (2) thermal oxidation process: crushing plants into fine particles, and carrying out oxidation reaction by using hot oxygen so as to extract silicon in the plants; (3) acid leaching: pulverizing plants into fine particles, soaking with acid, and extracting silicon from plants; (4) electrolytic method: crushing plants into fine particles, and carrying out electrolytic reaction by using current so as to extract silicon in the plants; (5) extracting method: pulverizing the plant into fine particles, and extracting silicon in the plant with solvent. The hydrolysis method and the thermal oxidation method are common methods, but the reaction rate is slower, the efficiency is lower, and the popularization and the use are not facilitated; the electrolytic method has higher efficiency, but expensive equipment is needed, which is not beneficial to reducing the production cost; the extraction method has higher efficiency, but the used solvent can be toxic, and strict control is needed to realize safety, no toxicity and no harm.
Therefore, the food-grade silicon water which has high extraction rate, short time and low cost, meets the production standards of food additives and nutrient element supplements, is safe, nontoxic and harmless, is easily absorbed and utilized by human bodies and has great significance for further improving the health condition of the human beings, preventing and assisting in treating various diseases.
Disclosure of Invention
Aiming at the existing technical problems, the invention provides a processing method of high metasilicate water concentrated solution, which improves the extraction rate and the extraction efficiency of soluble silicon and combines a plurality of fermentation nutrients to prepare the safe and nontoxic silicon water concentrated solution with rich nutrition and unique flavor.
In order to achieve the above purpose, the invention provides a processing method of a high metasilicate water concentrate, comprising the following steps:
s1, selecting materials and refrigerating: fresh burdock root is selected and stored in a refrigerating way for more than 3 months.
In a further step S1, the temperature of the refrigeration is 3-6 ℃.
The main purpose of the technical proposal is to naturally purify the burdock root, and the burdock root can generate more substance components which are favorable for subsequent fermentation, including sugar, organic matters and the like after long-term refrigeration at 3-6 ℃.
S2, cleaning and granulating: cleaning the refrigerated burdock root, draining until no water is present on the surface, and cutting into granules.
According to the technical scheme, after the burdock roots are cut into particles, the burdock roots can be fully contacted with the strains, so that the subsequent fermentation reaction is more sufficient, and the flavor of a fermentation product is stronger.
S3, inoculating tidal water: the burdock root particles, hops, saccharomycetes, aspergillus niger and lactobacillus are mixed according to the mass ratio of 1: 0.3:0.05:0.01:0.015, and performing tidal water treatment.
In a further step S3, the amount of the tidal water accounts for 30% of the mass of the whole fermentation pile.
In the technical scheme, the water addition amount directly affects the quality of strain fermentation: if the water content is too much, the fermentation process is anoxic, so that the fermentation product is sour; the less water, the insufficient water can be obtained by the strain, so that the fermentation process is slow, the fermentation time is too long, and the fermentation is insufficient. Therefore, it is necessary to uniformly mix the burdock root particles with hops, yeast, aspergillus niger and lactic acid bacteria, and then to perform the deliquescence treatment, and it is preferable to control the deliquescence amount to be 30% of the mass of the whole fermentation pile.
S4, pile fermentation: the mixture after tide is subjected to pile fermentation, and pile turning tide is carried out every day.
In a further step S4, the amount of the tidal water accounts for 30% of the mass of the whole fermentation pile.
In the step S4, the core temperature is controlled at 45 ℃ and the fermentation time is 20 days.
In the technical scheme, the burdock root has the effects of dispelling wind heat, reducing swelling and toxic materials, treating dizziness and pharyngalgia, odontalgia, cough, diabetes, carbuncle, scabies and the like, and also has the effects of reducing blood sugar, reducing blood pressure, eliminating constipation, preventing rectal cancer, diminishing inflammation, stopping bleeding and enhancing immunity; hops have the effects of invigorating stomach, promoting digestion, promoting urination, soothing nerves, resisting tuberculosis and diminishing inflammation, are commonly used for dyspepsia, abdominal distension, edema, cystitis, phthisis, cough, insomnia and leprosy, and can enable burdock roots to have unique flavor and aroma. The main purpose of fermentation by using burdock root and hops is to: on the one hand, both burdock roots and hops are used as sources of silicon, and silicon element is provided for the final product of the high metasilicate silicon water concentrate; on the other hand, the fermented burdock root and hop produce richer nutrient substances and unique flavor substances, so that the fermented product has higher nutritive value, has the health care effects of expelling toxin and nourishing face, preventing aging, clearing fat and nourishing stomach, and has the characteristics of no scorching and no bitter, sweet taste and fragrant smell.
S5, drying: and drying the fermented mixture until the water content is less than 8%.
In a further step S5, the temperature of the drying is 85 ℃.
In the technical scheme, the water content of the burdock root particles is controlled by drying mainly for stopping fermentation.
S6, crushing: and crushing the dried mixture to obtain a powdery material.
In the technical scheme, the crushing is mainly used for facilitating the full reaction of the subsequent carbonization.
S7, carbonizing: carbonizing the powdery material, and collecting the solid material after cooling.
In a further step S7, the carbonization conditions are as follows: the carbonization temperature is 300-600 ℃, and the carbonization time is 3-5h.
In the technical scheme, carbonization refers to a mode of preparing liquid or gas products by heating and decomposing solid or organic matters in the reaction process of isolating air or heating solid matters, and the carbonization temperature is controlled at 300-600 ℃, so that the main purpose is to thoroughly remove carbon elements and obtain plant silicon with better activity and water solubility.
S8, ultrasonic assisted hydrolysis: mixing the collected solid materials with deionized water according to a feed liquid ratio of 1:15-30, hydrolyzing under the conditions of heating and pressurizing and ultrasonic assistance, and collecting hydrolysate.
In a further step S8, the hydrolysis conditions are as follows: the ultrasonic power is 78-130w, the hydrolysis pressure is 0.5-0.7MPa, the hydrolysis temperature is 70-90 ℃, and the hydrolysis time is 20-60min.
In the technical scheme, the ultrasonic-assisted hydrolysis mode can enable the silicon to be dissolved in water in an acceleration way, and the condition of heating and pressurizing can improve the solubility of the silicon in the water, so that the extraction rate of the soluble silicon is improved.
S9, removing impurities and sterilizing: filtering and removing impurities from the collected hydrolysate, and performing ozone sterilization to obtain the high metasilicate water concentrate.
In the technical scheme, insoluble impurities, high polymer colloid or suspended particles with a certain size are separated from the solution, and bacteria in the solution are killed by utilizing the strong oxidizing property of ozone, so that the obtained high metasilicate water concentrate is ensured to meet the relevant national food safety standards.
In step S9, the hydrolysate is filtered and decontaminated by a quartz sand filter, a manganese sand filter, an activated carbon filter, an ultrafiltration and RO membrane combined separation device in sequence.
In the technical scheme, the quartz sand filter is mainly used for removing impurities and removing suspended particles insoluble in water; the manganese sand filter is mainly used for removing impurities and removing ionic impurity components such as iron, manganese, arsenic and the like in the aqueous solution; the activated carbon filter is mainly used for decoloring and adsorbing organic matters in the solution; the ultrafiltration and RO membrane combined separation device is mainly used for removing physical particles with the particle size of more than 0.001nm in the solution.
In conclusion, the method of the invention utilizes the burdock root and hop containing silicon to ferment, obtains more fermentation nutrient substances and fermentation flavor substances, and then utilizes the ultrasonic-assisted water extraction method to extract the silicon from the fermentation mixture, thereby not only improving the extraction rate of the soluble silicon, but also shortening the extraction time of the soluble silicon, and finally the produced silicon water concentrate has the characteristic of high metasilicic acid, and the silicon water concentrate containing metasilicic acid can reduce the incidence rate of senile dementia, has health care effect on cardiovascular and skeletal diseases of human bodies, and has a certain beautifying function.
Compared with the prior art, the invention has the technical advantages that:
1. the invention carries out pile fermentation on the burdock root and the hop, not only obtains fermentation substances with higher nutritive value than raw materials, such as vitamins, amino acid, calcium, phosphorus and protein which are contained by the fermentation substances, but also reduces tea polyphenol in the burdock root along with the higher fermentation degree, has no great irritation to intestines and stomach, is healthier and safer to drink, and also adds fragrant substances such as rich organic acid, so that the fermentation product is not scorched and bitter, is fragrant, sweet and moist and has fragrant.
2. The method for extracting food-grade water-soluble silicon from burdock roots and hops adopts the method for separating and extracting plant-source food-grade water-soluble silicon which can be absorbed by human bodies from carbonized burdock roots and hops fermentation products, has high safety, less impurity components and wider application prospect, and improves economic and social benefits.
3. The invention utilizes ultrasonic microwave auxiliary hydrolysis technology, can effectively extract the silicon in the burdock root and hop fermentation products, greatly shortens the extraction time of the silicon, improves the extraction rate of the silicon, and obtains the silicon water concentrate with high metasilicic acid.
Drawings
FIG. 1 is a schematic flow chart of the method of the present invention.
Detailed Description
The present invention will be described in further detail with reference to the following examples in order to make the objects, technical solutions and advantages of the present invention more apparent. It should be understood that the specific embodiments described herein are for purposes of illustration only and are not intended to limit the scope of the invention.
Example 1: as shown in fig. 1, this embodiment provides a processing method of a high metasilicate water concentrate, mainly using an ultrasonic-assisted water extraction method to extract a silicate, and adding hops containing silicon for fermentation, thereby preparing the silicate water, comprising the following steps:
s1, selecting materials and refrigerating: fresh burdock roots without decay and knife injury are selected, the fresh burdock roots are placed in a low-temperature warehouse for cooling, and stored for more than 3 months at the temperature of 3 ℃, so that starch in the burdock is aged, the starch is converted into reducing sugar, the preparation is fully made for the subsequent fermentation process, and meanwhile, the strong flavor is conveniently generated.
S2, cleaning and granulating: cleaning the refrigerated burdock root, and draining until the surface of the burdock root is free of water, so that soil and bacteria mixed in the burdock root are removed; and then cutting into particles with the length and width of about 1cm, so that microorganisms are easier to infiltrate into the burdock root in the subsequent fermentation and enzymolysis processes, the fermentation reaction process is more sufficient, and the effect is better.
S3, inoculating tidal water: mixing the granulated burdock root particles, hops, saccharomycetes, aspergillus niger and lactobacillus according to the mass ratio of 1:0.3:0.05:0.01:0.015, and carrying out tidal water treatment, wherein the tidal water accounts for 30% of the mass of the whole fermentation pile.
S4, pile fermentation: and (3) carrying out pile fermentation on the mixture after the tide water for 20 days, closely monitoring the core temperature in the pile fermentation process, controlling the core temperature to be 45 ℃, turning the tide water every day, and keeping the tide water to be 30% of the mass of the whole fermentation pile.
In the concrete implementation, in the industrial production, large-scale fermentation is generally adopted, the height of each pile is 1.0 meter after tide, and each pile is not less than 1000kg; after the tidal water is piled up, the four corners of the wet gunny bag are covered for compaction, so that the effects of humidification and heat preservation can be achieved, and fermentation is facilitated; and, pile up and need layer by layer (i.e. pile up and reason while opening) and need to guarantee soft, must not step on the pressure, in order to guarantee its air permeability. Especially, the fermentation temperature and the stacking temperature must be mastered in the fermentation process, the change of the environment is closely noted, the stacking is turned over timely, a thermometer and a hygrometer are required to be installed in the fermentation chamber, the thermometer is required to be inserted around the mixture stacking, a special person is responsible for recording the change of the temperature and the humidity, if the temperature is lower than 40 ℃, the ideal fermentation effect is difficult to achieve, and if the temperature is higher than 65 ℃, the conditions of burning and light taste can occur.
S5, drying: and (3) drying the fermented mixture at a temperature of 85 ℃ until the water content is less than 8%, thereby terminating the fermentation.
S6, crushing: and crushing the dried mixture by using a crusher to obtain powder materials, so that the powder materials are convenient for the subsequent carbonization to fully react.
S7, carbonizing: carbonizing the powder material at 300 ℃ for 5 hours, and collecting the solid after cooling to room temperature.
S8, ultrasonic assisted hydrolysis: mixing the collected solid and deionized water according to a feed-liquid ratio of 1:15, and hydrolyzing under the conditions of heating and pressurizing and ultrasonic assistance, wherein the ultrasonic power is 130w, the hydrolysis pressure is 0.7MPa, the hydrolysis temperature is 90 ℃, and the hydrolysis time is 20min; the hydrolysate was then collected.
S9, removing impurities and sterilizing: removing suspended matter particles insoluble in water from the collected hydrolysate sequentially through a quartz sand filter, removing ionic impurity components such as iron, manganese, arsenic and the like in the aqueous solution through a manganese sand filter, decoloring and removing organic matters in the solution through an activated carbon filter, removing physical particles with the particle size of more than 0.001nm in the solution through an ultrafiltration and RO membrane combined separation device, and performing ozone sterilization to obtain the high metasilicate aqueous concentrate.
Example 2: as shown in fig. 1, this embodiment provides another processing method of a high metasilicate water concentrate, which includes the following steps:
s1, selecting materials and refrigerating: selecting fresh burdock root without rot and knife injury, placing the fresh burdock root in a low-temperature warehouse, and storing for more than 4 months at 6 ℃, thereby aging starch in burdock and converting the starch into reducing sugar.
S2, cleaning and granulating: cleaning the refrigerated burdock root, draining until the surface is free of water, and cutting into particles with the length and width of about 1cm, so that microorganisms are easier to infiltrate into the burdock root in the subsequent fermentation and enzymolysis processes.
S3, inoculating tidal water: mixing the granulated burdock root particles, hops, saccharomycetes, aspergillus niger and lactobacillus according to the mass ratio of 1:0.3:0.05:0.01:0.015, and carrying out tidal water treatment, wherein the tidal water accounts for 30% of the mass of the whole fermentation pile.
S4, pile fermentation: pile fermentation is carried out on the mixture after the tide, the fermentation time is 20 days, the temperature of the pile core is controlled at 45 ℃, the pile turning tide is carried out every day, and the tide amount is kept to be 30% of the mass of the whole fermentation pile.
S5, drying: and (3) drying the fermented mixture at a temperature of 85 ℃ until the water content is less than 8%, thereby terminating the fermentation.
S6, crushing: and crushing the dried mixture by using a crusher to obtain powder materials, so that the powder materials are convenient for the subsequent carbonization to fully react.
S7, carbonizing: carbonizing the powder material at 600 ℃ for 3 hours, and collecting the solid after cooling to room temperature.
S8, ultrasonic assisted hydrolysis: mixing the collected solid and deionized water according to a feed-liquid ratio of 1:30, and hydrolyzing under the conditions of heating and pressurizing and ultrasonic assistance, wherein the ultrasonic power is 78w, the hydrolysis pressure is 0.5MPa, the hydrolysis temperature is 70 ℃, and the hydrolysis time is 60min; the hydrolysate was then collected.
S9, removing impurities and sterilizing: removing suspended matter particles insoluble in water from the collected hydrolysate sequentially through a quartz sand filter, removing ionic impurity components such as iron, manganese, arsenic and the like in the aqueous solution through a manganese sand filter, decoloring and removing organic matters in the solution through an activated carbon filter, removing physical particles with the particle size of more than 0.001nm in the solution through an ultrafiltration and RO membrane combined separation device, and performing ozone sterilization to obtain the high metasilicate aqueous concentrate.
After the processing is finished, the content of soluble silicon in the high metasilicate aqueous concentrated solution obtained by adopting a silicon molybdenum Huang Fen spectrophotometry test is 200mg/L. And, adopting steps of selecting fresh burdock root, cleaning, slicing, drying until the moisture is less than 8%, and the like to prepare raw burdock root, adopting the existing burdock root piling fermentation process, preparing fermented burdock root without adding hops, and comparing the high metasilicate aqueous concentrated solution with the raw burdock root aqueous solution and the soluble silicon content in the fermented burdock root aqueous solution, as shown in the table one.
From the above, the method for preparing the high metasilicate aqueous concentrate not only shortens the time used by the common hydrolysis method for extracting silicon, but also obviously improves the content of soluble silicon compared with the common raw burdock root aqueous solution and the fermented burdock root aqueous solution.
Furthermore, the long-term experience of the testers can be known: the silicon in the high metasilicic acid water concentrated solution has the function of resolving aluminum toxicity, and frequent drinking of the high metasilicic acid (namely silicon content) water concentrated solution is helpful for reducing the aluminum concentration in body fluid of a tester and the aluminum content in the human body of the tester, and the aluminum concentration of the human body is related to Alzheimer's disease, namely senile dementia which is commonly known by people, so that the incidence rate of senile dementia of the tester is reduced. In addition, silicon connects mucopolysaccharide with each other in connective tissue and cartilage formation, and combines the mucopolysaccharide with protein to form fibrous structure, which increases elasticity and strength of connective tissue, maintains structural integrity, and the high metasilicate aqueous concentrate has certain health care function for human skeleton of the testers. Therefore, the high metasilicate water concentrate has great significance for further improving, preventing and assisting in treating various diseases of human health, and is worthy of popularization and application for all human beings.
In conclusion, the processing method of the high metasilicic acid water concentrated solution realizes the efficient extraction of the soluble silicic acid in the burdock and the hop, is quick, simple and convenient, has good economy, has the characteristic of high metasilicic acid, and has rich nutrition and unique flavor.
It is apparent that the above examples are given by way of illustration only and are not limiting of the embodiments. Other variations or modifications of the above teachings will be apparent to those of ordinary skill in the art. It is not necessary here nor is it exhaustive of all embodiments. While still being apparent from variations or modifications that may be made by those skilled in the art are within the scope of the invention.
Claims (8)
1. The processing method of the high metasilicate water concentrate is characterized by comprising the following steps of:
s1, selecting materials and refrigerating: selecting fresh burdock root, refrigerating and storing for more than 3 months;
s2, cleaning and granulating: cleaning the refrigerated burdock root, draining until the surface is free of water, and cutting into particles;
s3, inoculating tidal water: the burdock root particles, hops, saccharomycetes, aspergillus niger and lactobacillus are mixed according to the mass ratio of 1: 0.3:0.05:0.01:0.015, and carrying out tidal water treatment;
s4, pile fermentation: piling up the mixture after tide water, fermenting, and turning up the tide water every day;
s5, drying: drying the fermented mixture until the water content is less than 8%;
s6, crushing: crushing the dried mixture to obtain a powdery material;
s7, carbonizing: carbonizing the powdery material, and collecting the solid material after cooling;
s8, ultrasonic assisted hydrolysis: mixing the collected solid materials with deionized water according to a feed liquid ratio of 1:15-30, hydrolyzing under the conditions of heating and pressurizing and ultrasonic assistance, and collecting hydrolysate;
s9, removing impurities and sterilizing: filtering and removing impurities from the collected hydrolysate, and performing ozone sterilization to obtain the high metasilicate water concentrate.
2. The method of claim 1, wherein in step S1, the temperature of the refrigeration is 3-6 ℃.
3. The method of claim 1, wherein the amount of tidal water in step S3 and step S4 is 30% of the total mass of the fermentation reactor.
4. The method according to claim 1, wherein in step S4, the core temperature is controlled at 45 ℃ and the fermentation time is 20 days.
5. The method of claim 1, wherein in step S5, the temperature of the drying is 85 ℃.
6. The method for processing aqueous high metasilicate concentrate according to claim 1, wherein in step S7, the carbonization conditions are as follows: the carbonization temperature is 300-600 ℃, and the carbonization time is 3-5h.
7. The method for processing aqueous high metasilicate concentrate according to claim 1, wherein in step S8, the hydrolysis conditions are: the ultrasonic power is 78-130w, the hydrolysis pressure is 0.5-0.7MPa, the hydrolysis temperature is 70-90 ℃, and the hydrolysis time is 20-60min.
8. The method for processing a water concentrate of high metasilicate according to claim 1, wherein in step S9, the hydrolysate is filtered and decontaminated sequentially by a quartz sand filter, a manganese sand filter, an activated carbon filter, an ultrafiltration and RO membrane combined separation device.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310697939.7A CN116548614A (en) | 2023-06-13 | 2023-06-13 | Processing method of high metasilicate water concentrate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310697939.7A CN116548614A (en) | 2023-06-13 | 2023-06-13 | Processing method of high metasilicate water concentrate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN116548614A true CN116548614A (en) | 2023-08-08 |
Family
ID=87500216
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202310697939.7A Pending CN116548614A (en) | 2023-06-13 | 2023-06-13 | Processing method of high metasilicate water concentrate |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN116548614A (en) |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20090142819A1 (en) * | 2007-12-03 | 2009-06-04 | 1695492 Ontario Inc. D.B.A. Global-Meridian Technology Group | Methods for co-production of ethanol and silica from equisetum |
| WO2010012124A1 (en) * | 2008-07-30 | 2010-02-04 | 福又达股份有限公司 | A method for preparing a product containing silicon from plant |
| BRPI0903040A2 (en) * | 2009-08-10 | 2011-04-12 | Maria De Fatima Tonon | process for ethanol and silica production from rice husk and straw |
| CN102389107A (en) * | 2011-07-25 | 2012-03-28 | 吉林大学 | Method for preparing orthosilicic acid extracting solution and silicon supplement by using silicon-rich plants |
| CN103156029A (en) * | 2013-03-31 | 2013-06-19 | 天益食品（徐州）有限公司 | Fermented burdock tea |
| CN103976104A (en) * | 2014-05-28 | 2014-08-13 | 江南大学 | Method for processing fermented burdock tea |
| CN108455745A (en) * | 2018-03-20 | 2018-08-28 | 朱瑞东 | Preparation method, system and the water-soluble silicon element concentrate of water-soluble silicon element concentrate |
| CN110604310A (en) * | 2019-10-29 | 2019-12-24 | 朱瑞东 | System and method for extracting food-grade water-soluble silicon element from rice hulls |
| KR20210008191A (en) * | 2019-07-10 | 2021-01-21 | (주)비티팜 | Functional food composition and functional composition comprising extract containing water-soluble silicon |
-
2023
- 2023-06-13 CN CN202310697939.7A patent/CN116548614A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20090142819A1 (en) * | 2007-12-03 | 2009-06-04 | 1695492 Ontario Inc. D.B.A. Global-Meridian Technology Group | Methods for co-production of ethanol and silica from equisetum |
| WO2010012124A1 (en) * | 2008-07-30 | 2010-02-04 | 福又达股份有限公司 | A method for preparing a product containing silicon from plant |
| BRPI0903040A2 (en) * | 2009-08-10 | 2011-04-12 | Maria De Fatima Tonon | process for ethanol and silica production from rice husk and straw |
| CN102389107A (en) * | 2011-07-25 | 2012-03-28 | 吉林大学 | Method for preparing orthosilicic acid extracting solution and silicon supplement by using silicon-rich plants |
| CN103156029A (en) * | 2013-03-31 | 2013-06-19 | 天益食品（徐州）有限公司 | Fermented burdock tea |
| CN103976104A (en) * | 2014-05-28 | 2014-08-13 | 江南大学 | Method for processing fermented burdock tea |
| CN108455745A (en) * | 2018-03-20 | 2018-08-28 | 朱瑞东 | Preparation method, system and the water-soluble silicon element concentrate of water-soluble silicon element concentrate |
| KR20210008191A (en) * | 2019-07-10 | 2021-01-21 | (주)비티팜 | Functional food composition and functional composition comprising extract containing water-soluble silicon |
| CN110604310A (en) * | 2019-10-29 | 2019-12-24 | 朱瑞东 | System and method for extracting food-grade water-soluble silicon element from rice hulls |
Non-Patent Citations (2)
| Title |
|---|
| 王丹: "硅提高烟草幼苗抗盐性的效果及作用机理", 《中国优秀硕士学位论文全文数据库 农业科技辑》, no. 1, 15 January 2023 (2023-01-15), pages 047 - 947 * |
| 黄建平: "含硅植物笔管草用水提取最适宜条件的研究", 《中草药》, 15 August 1985 (1985-08-15), pages 15 - 16 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP4521447B2 (en) | Method for producing enzyme-containing health food and health food | |
| CN101643767B (en) | Method for preparing almond peptide from almond dregs | |
| CN104286247A (en) | Preparation method of detoxified gingko tea | |
| CN106901363A (en) | A kind of preparation method of olive pomace ferment | |
| CN108719976A (en) | A kind of walnut grouts ferment production method | |
| CN109486604A (en) | A kind of preparation method of Stauntonia latifolia fruit wine | |
| KR101697107B1 (en) | Method for Preparing of Beverage Fermented by Lactic Acid Bacteria using Grain Syrup and Beverage Fermented by Lactic Acid Bacteria thereof | |
| CN106036610A (en) | Selenium-enriched blueberry fruit powder product and preparation method thereof | |
| CN111955721A (en) | Gastrodia elata edible fungus flavor polyphenol liquid plant enzyme formula and preparation method thereof | |
| CN107114643B (en) | Red date health concentrated juice and preparation method thereof | |
| CN117801967B (en) | Method for culturing Eurotium cristatum and application | |
| CN103497883B (en) | Ginseng healthy acetic acid drink and production method thereof | |
| CN104997096A (en) | Chinese fevervine sour soup beverage and preparation method thereof | |
| CN110353051A (en) | A kind of low purine soybean milk powder and preparation method thereof | |
| CN108719941A (en) | The method to be made soy sauce using olive fruit juice | |
| CN116548614A (en) | Processing method of high metasilicate water concentrate | |
| CN105779255A (en) | Honey vinegar and preparing method thereof | |
| CN102311909A (en) | Preparation method of watermelon fruit vinegar containing citrulline and propolis | |
| CN107981280A (en) | A kind of production method of marinated Radix Folium Allii tuberosi | |
| CN106539075A (en) | A kind of preparation method of efficient absorption sea cucumber nutrient buccal tablet | |
| CN111411140A (en) | Furic acid and preparation method thereof | |
| CN112826082A (en) | Preparation method of mushroom enzyme | |
| CN112273646A (en) | Method for preparing ginger enzyme by fermenting ginger slices | |
| KR100903848B1 (en) | Method for concentrated separation of fiber from mushroom | |
| CN108272051B (en) | Preparation method of mulberry leaf pickled vegetables fermented by composite probiotics |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |