CN116530725A - Filter stick for increasing milk fragrance for cigarettes, preparation method and cigarettes - Google Patents

Filter stick for increasing milk fragrance for cigarettes, preparation method and cigarettes Download PDF

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Publication number
CN116530725A
CN116530725A CN202310479952.5A CN202310479952A CN116530725A CN 116530725 A CN116530725 A CN 116530725A CN 202310479952 A CN202310479952 A CN 202310479952A CN 116530725 A CN116530725 A CN 116530725A
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CN
China
Prior art keywords
filter stick
cigarette
cigarettes
vanillin
filter
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202310479952.5A
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Chinese (zh)
Inventor
邱光明
朱丛戎
赵玉轩
周远祥
何蓉
任志刚
刘如灿
陶文生
李朝荣
倪博
钱旎
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chongqing China Tobacco Industry Co Ltd
Original Assignee
Chongqing China Tobacco Industry Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chongqing China Tobacco Industry Co Ltd filed Critical Chongqing China Tobacco Industry Co Ltd
Priority to CN202310479952.5A priority Critical patent/CN116530725A/en
Publication of CN116530725A publication Critical patent/CN116530725A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/02Manufacture of tobacco smoke filters
    • A24D3/0229Filter rod forming processes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/02Manufacture of tobacco smoke filters
    • A24D3/0204Preliminary operations before the filter rod forming process, e.g. crimping, blooming
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/061Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking

Abstract

The invention belongs to the technical field of cigarette filter sticks, and in particular relates to a filter stick for increasing milk fragrance for cigarettes, a preparation method and cigarettes. The circumference of the filter stick body is 24+/-0.2 mm, the suction resistance is 3800+/-265 Pa, the hardness is more than or equal to 84%, the length is 120+/-0.5 mm, the roundness is less than or equal to 0.35mm, and the weight is 0.76+/-0.3 g/branch; the tow specification of the filter stick body is 3.0Y35000d, and the molding paper specification of the filter stick body is 25g/m 2 X26.5mm×6000CU, by dissolving essence in glycerol, and adding the glycerol mixture with essence into the above tow. The invention dissolves the food grade essence in the glycerol for producing the filter stick, so that the essence can be uniformly distributed in the filter stick, and the smoke generated during the combustion of the cigarette can increase the aroma of the smoke by adsorption and entrainment modes when the cigarette passes through the flavoring filter stick, therebyAnd adding milk flavor to the cigarette product.

Description

Filter stick for increasing milk fragrance for cigarettes, preparation method and cigarettes
Technical Field
The invention belongs to the technical field of cigarette filter sticks, and particularly relates to a filter stick for increasing milk fragrance for cigarettes, a preparation method and cigarettes.
Background
In the traditional cigarette product design, the process point of increasing the cigarette aroma is mainly in the flavoring link of the cut tobacco making process. The principle is that essence is sprayed on the surfaces of tobacco shreds, so that the tobacco shreds absorb essence solution, and then the essence and the tobacco shreds participate in combustion and release fragrance when the cigarettes are combusted. Although the traditional flavoring mode can increase the fragrance of cigarettes to a certain extent, the uncertain factors are insufficient expression and uncontrollable expression of the released fragrance and the amount of fragrance after the essence participates in combustion. Meanwhile, on the aspect of releasing the pack-opening incense, the pack-opening incense of the cigarettes produced in the traditional flavoring mode is mainly the cigarette incense, and the fragrance release of the added essence cannot be completely shown.
Along with the development of technology, the cigarette flavoring adopts the traditional modes, such as filter stick flavoring, cigarette paper flavoring and the like. In the perfuming of cigarette filter sticks, common perfuming modes include a perfume bead filter stick, a granule filter stick, a gel filter stick, a perfume line filter stick and the like; for example, patent publication number CN216821738U discloses a filter rod with cooling and flavoring functions, which comprises a core body and heat-insulating molding paper covering the core body, wherein the core body comprises a filtering section, a cooling section, a flavoring section and a diversion section which are connected in sequence, porous bars are arranged in the cooling section in a matching way, and the porous bars comprise a plurality of cooling channels for flue gas to pass through; the flavoring section is internally provided with a flavoring bar loaded with essence and spice in a matching way.
The proposal of the patent provides filter sticks capable of perfuming aiming at the defects of the prior art, but the perfuming modes of the filter sticks increase the fragrance of cigarettes to different degrees, but the technology and equipment for producing the filter sticks have higher requirements; meanwhile, the material cost for producing the filter stick is increased.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide a filter stick for increasing the milk fragrance for cigarettes, a preparation method and cigarettes, wherein food-grade essence is dissolved in glycerol for producing the filter stick, so that the essence can be uniformly distributed in the filter stick, and smoke generated during the combustion of the cigarettes is increased by adsorption and entrainment during the flavoring of the filter stick, so that the milk fragrance is increased for cigarette products.
The invention solves the technical problems by the following technical means:
the filter stick for increasing milk fragrance for the cigarettes comprises a filter stick body, wherein the filter stick body comprises a silk bundle and forming paper, and a mixture of spice and glycerol is added into the silk bundle.
Further, the circumference of the filter stick body is 24+/-0.2 mm, the suction resistance is 3800+/-265 Pa, the hardness is more than or equal to 84%, the length is 120+/-0.5 mm, the roundness is less than or equal to 0.35mm, and the weight is 0.76+/-0.3 g/count.
Further, the tow specification of the filter stick body is 3.0Y35000d, and the molding paper specification of the filter stick body is 25g/m 2 ×26.5mm×6000CU。
Further, the perfume is vanillin, the added amount of vanillin is 1.3-2 ug/branch, and the added amount of glycerin is 60+/-3.0 mg/branch.
Further, the preparation method of the milk flavor increasing filter stick for the cigarettes comprises the following steps of:
s1, preparing a silk bundle: firstly, taking vanillin according to a certain proportion, adding the vanillin into glycerin, and uniformly stirring to obtain a mixture;
s2, adding the glycerol mixture dissolved with the essence into a silk bundle according to a proportion, wherein the specification of the silk bundle is 3.0Y35000d, the addition amount of vanillin is 1.3-2 ug/branch, and the addition amount of glycerol is 60+/-3.0 mg/branch;
s3, adopting the specification of 25g/m 2 The filter stick is prepared by molding paper with the length of multiplied by 26.5mm and the length of multiplied by 6000CU, the circumference of the filter stick is 24+/-0.2 mm, the suction resistance is 3800+/-265 Pa, the hardness is more than or equal to 84 percent, the length is 120+/-0.5 mm, the roundness is less than or equal to 0.35mm, and the weight is 0.76+/-0.3 g/branch;
s4, cutting the filter stick prepared in the step S3 into six sections to obtain the filter stick required by a single cigarette
In a second aspect, the invention discloses a preparation method of a filter stick for increasing milk flavor for cigarettes, which is characterized by comprising the following steps of: the essence is dissolved in glycerin, and then the glycerin mixture in which the essence is dissolved is added to the above-mentioned tow. The preparation method of the technical scheme ensures that the addition of the spice is easy to implement, the filter stick production is convenient, and facility equipment required by the filter stick production is not required to be increased.
In a third aspect, the invention also discloses a cigarette, and the cigarette uses the filter stick or the preparation method of the filter stick. Experiments show that the cigarette produced by the flavored filter stick has 300% of the milk aroma index in sense.
The beneficial effects of the invention are as follows:
1. according to the invention, the food-grade essence vanillin is firstly dissolved in glycerin for producing the filter stick, so that the essence can be uniformly distributed in the filter stick, and smoke generated during cigarette combustion is increased in an adsorption and entrainment mode when the filter stick is flavored, so that the effect of increasing the milk fragrance of a cigarette product is remarkable; the circumference of the filter stick combined with the invention is 24+/-0.2 mm, the suction resistance is 3800+/-265 Pa, the hardness is more than or equal to 84%, the length is 120+/-0.5 mm, the roundness is less than or equal to 0.35mm, the weight is 0.76+/-0.3 g/branch, the tow specification is 3.0Y35000d, and the molding paper specification of the filter stick body is 25g/m 2 By the arrangement of the special technical characteristics and the mutual matching of the special technical characteristics and the spice, the experiment shows that the cigarette produced by the perfuming filter stick of the invention has the sensory effectThe milk fragrance index is increased by 300 percent, which is far higher than the milk fragrance in the prior art.
2. When the filter stick is produced, the vanillin is firstly dissolved in the glycerin for producing the filter stick, and then the glycerin is added into the silk bundle of the filter stick body, so that compared with the prior art, the vanillin is added in a microcapsule, chitosan and other modes, the adding is simpler, the adding of the spice is easy to implement, the filter stick production is convenient, and facility equipment required for producing the filter stick is not required to be increased, so that the production cost of the filter stick is reduced.
3. The glycerol is colorless odorless transparent viscous liquid, and can not influence the properties of vanillin, so that the milk flavor of vanillin is more pure; in addition, the glycerol is used as an organic matter, and can adsorb some harmful substances such as nicotine and the like in the smoke, so that the health injury of the smoke to a smoker is reduced.
4. The added amount of vanillin in each cigarette is 1.3-2 ug/cigarette, and the special vanillin adding method, the preparation method of the filter stick and the structural property of the filter stick are adopted, so that the transfer rate of vanillin reaches more than 17%, and compared with the prior art, the transfer rate of vanillin is obviously improved, and the use amount of vanillin in cigarette production can be reduced, thereby reducing the cigarette cost.
5. The cigarette produced by adopting the filter stick production mode has higher market acceptance than other existing technologies, and can be widely popularized and used by consumers.
Drawings
FIG. 1 is a graph showing semi-quantitative results of vanillin in an example of the invention.
Detailed Description
The present invention will be described in detail with reference to the following examples and drawings.
Example 1,
The embodiment is a filter stick for increasing milk fragrance for cigarettes, which comprises a filter stick body, wherein the filter stick body comprises a silk bundle and forming paper, and a mixture of spice and glycerol is added in the silk bundle. The circumference of the filter stick body is 24+/-0.2 mm, the suction resistance is 3800+/-265 Pa, and the hardness is more than or equal to84%, length 120+ -0.5 mm, roundness less than or equal to 0.35mm, weight 0.76+ -0.3 g/branch. The tow specification of the filter stick body is 3.0Y35000d, and the molding paper specification of the filter stick body is 25g/m 2 X 26.5mm x 6000CU. The perfume is vanillin, the adding amount of vanillin is 1.3-2 ug/branch, and the adding amount of glycerin is 60+/-3.0 mg/branch.
EXAMPLE 2,
This example is a method for preparing a milk flavor-enhancing filter stick for cigarettes, according to the requirements described in example 1, a filter stick body having a circumference of 24.+ -. 0.2mm, a suction resistance of 3800.+ -. 265Pa, a hardness of 84% or more, a length of 120.+ -. 0.5mm, a roundness of 0.35mm or less, and a weight of 0.76.+ -. 0.3 g/count is prepared, the tow specification of the filter stick body is 3.0Y35000d, and the molding paper specification of the filter stick body is 25g/m 2 X 26.5mm x 6000CU. During the preparation of the silk bundle, essence is firstly dissolved in glycerin, and then the glycerin mixture dissolved with the essence is added into the silk bundle, wherein the addition amount of vanillin is 1.3-2 ug/branch, and the addition amount of glycerin is 60+/-3.0 mg/branch.
The filter rod prepared in example 2 was cut into 6 pieces in a six-cut manner, and one cigarette was prepared for each filter rod. And carrying out sensory evaluation on the prepared cigarettes by adopting a Chinese style cigarette sensory evaluation method, wherein the evaluation result is shown in a table 1.
Table 1 sensory evaluation results of the release of the cigarette flavors
As can be seen from Table 1, the product rolled after the flavoring filter stick is adopted increases 1 minute on the milk flavor index of the flavor style, the flavoring is very obvious, the baking flavor and the sweet flavor are respectively increased by 0.3 minute, the flavoring is more obvious, and the flavor is slightly reduced on the tobacco flavor and the fragrance of the flue-cured tobacco; the sweet taste is obviously increased in taste style; the aroma and the richness are obviously improved on the smoke characteristics, and the fineness and the softness are reduced; the irritation is slightly increased in comfort characteristics. In the aspect of pack fragrance opening, the fragrance of the filter stick cigarette sample before fragrance adding takes tobacco fragrance as a main body, and the fragrance of the filter stick sample after fragrance adding takes elegant milk fragrance as a main body.
And then detecting smoke of the prepared cigarettes, and carrying out smoking experiments on samples before and after the cigarettes are flavored by adopting a Cerulean SM450 linear type smoking machine to analyze conventional change of the smoke before and after the cigarettes are flavored. Suction method according to ISO3308-2012: intermittent 60s, suction capacity 35mL, suction 2s, suction count 5, results are shown in Table 2:
table 2 smoke analysis and detection results
Parameters (parameters) Before perfuming After perfuming
Number of suction ports 5.2 mouth/cig 5.0 mouth/cig
Total particulate matter TPM 14.9 mouth/cig 14.8 mouth/cig
Moisture content 2.23 mouth/cig 2.34 mouth/cig
Saline-alkali 0.81 mouth/cig 0.79 mouth/cig
Tar oil 11.8 mouth/cig 12.8 mouth/cig
Note that: because the cigarette filter stick is flavored, the cigarettes are not balanced when the cigarettes are smoked.
The results from table 2 above show that: the difference of the indexes of the suction port number, the total particulate matters, the moisture and the nicotine is very small before and after the flavoring of the filter stick, and the tar index is increased to a certain extent. On the overall index, the conventional index of the smoke changes less before and after the filter stick is flavored.
The prepared cigarettes are subjected to essence release results, and the essence release results are specifically shown as follows: according to the ISO3308-2012 method, smoke is trapped on cigarette samples of the flavored filter stick samples and the non-flavored filter stick samples, organic solvent extraction is carried out on the trapped Cambridge filter discs, smoke component analysis and target perfume raw material (vanillin) semi-quantitative analysis are carried out on the extract by utilizing GC/MS, and the release effect of the cigarette essence before and after flavoring in the smoking process of the cigarette is studied. The smoke components of the samples after treatment are compared and analyzed, and the smoke components of the sample cigarette before flavoring and the smoke components of the sample cigarette after flavoring are basically consistent, and no obvious difference exists in vanillin release, and the detailed view is shown in figure 1.
The treated samples were subjected to semi-quantitative analysis of vanillin release amounts of 4.967ug and 5.253ug, respectively, and the vanillin amount of the flavored sample cigarettes was increased by 0.286ug, as detailed in table 3.
TABLE 3 semi-quantitative results of vanillin
Name of the name Front half quantitative result of perfuming (ug) Front half quantitative result of perfuming (ug)
Vanillin 4.967 5.253
From the analysis, the food-grade essence vanillin is firstly dissolved in the glycerin for producing the filter stick, so that the essence can be uniformly distributed in the filter stick, and the smoke generated during the combustion of the cigarette can be increased in fragrance by adsorption and entrainment during the flavoring of the filter stick, so that the effect of increasing the milk fragrance of the cigarette product is remarkable; the circumference of the filter stick combined with the invention is 24+/-0.2 mm, the suction resistance is 3800+/-265 Pa, the hardness is more than or equal to 84%, the length is 120+/-0.5 mm, the roundness is less than or equal to 0.35mm, the weight is 0.76+/-0.3 g/branch, the tow specification is 3.0Y35000d, and the molding paper specification of the filter stick body is 25g/m 2 By the arrangement of the special technical characteristics and the mutual matching of the special technical characteristics and the spice, experiments show that the cigarette produced by the flavoring filter stick has 300 percent of the increase of the milk aroma index in sense.
In addition, the present example calculates the vanillin transfer rate of the application: detecting vanillin increment of 0.284 ug in 5 cigarette smoke, wherein vanillin increment of 0.286/5=0.0572 ug in 1 cigarette smoke; 2ug of vanillin is added to 6 cigarettes, and 0.333ug of vanillin is added to 1 cigarette; the transfer rate was calculated as: vanillin increment in 1 cigarette smoke/vanillin addition amount of 1 cigarette= 17.166%. Thus, the transfer rate of vanillin reaches 17.166% by adopting the method of the invention.
However, in the prior art, for example, in the text of "influence of vanillin on volatile components in main stream smoke of cigarettes" in the 6 th period of the fifth volume of the journal of food safety quality detection ", the transfer rate of vanillin in the main stream smoke of cigarettes is 4.08%; for another example, the application publication number is CN111394182A, the transfer rate of ethyl vanillin in a patent of a flavor composition for bursting beads, a flavor base module for bursting beads, a cigarette bursting beads and a bursting bead cigarette which are used for highlighting milk flavor and bean flavor is only 1.15%; and in the patent with application publication number of CN111394178A, named as a milk-flavored and bean-flavored base module for cigarettes, essence and cigarettes, the transfer rate of vanillin is 6.25%.
Therefore, according to the analysis results, the vanillin addition method, the preparation method of the filter stick and the structural property of the filter stick are adopted, so that the transfer rate of vanillin is obviously improved compared with the prior art, the use amount of vanillin in cigarette production can be reduced, and the cigarette cost is reduced.
The above embodiments are only for illustrating the technical solution of the present invention and not for limiting the same, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications and equivalents may be made thereto without departing from the spirit and scope of the technical solution of the present invention, which is intended to be covered by the scope of the claims of the present invention. The technology, shape, and construction parts of the present invention, which are not described in detail, are known in the art.

Claims (8)

1. A filter stick for increasing milk fragrance for cigarettes is characterized in that: the filter stick comprises a filter stick body, wherein the filter stick body comprises a silk bundle and forming paper, and a mixture of spice and glycerol is added into the silk bundle.
2. A milk flavored filter stick for cigarettes according to claim 1, wherein: the circumference of the filter stick body is 24+/-0.2 mm, the suction resistance is 3800+/-265 Pa, the hardness is more than or equal to 84%, the length is 120+/-0.5 mm, the roundness is less than or equal to 0.35mm, and the weight is 0.76+/-0.3 g/count.
3. A milk flavored filter stick for cigarettes according to claim 2, wherein: the tow specification of the filter stick body is 3.0Y35000d, and the molding paper specification of the filter stick body is 25g/m 2 ×
26.5mm×6000CU。
4. A milk flavored filter stick for cigarettes according to claim 3, wherein: the perfume is vanillin, the adding amount of vanillin is 1.3-2 ug/branch, and the adding amount of glycerin is 60+/-3.0 mg/branch.
5. A preparation method of a cigarette filter stick with milk flavor increasing function is characterized by comprising the following steps: a flavor is dissolved in glycerin, and then a flavor-dissolved glycerin mixture is added to the tow of claim 1.
6. The method for preparing the cigarette milk flavor increasing filter stick according to claim 5, wherein the method comprises the following steps: the steps include the steps of (a) providing a first step,
s1, preparing a silk bundle: firstly, taking vanillin according to a certain proportion, adding the vanillin into glycerin, and uniformly stirring to obtain a mixture;
s2, adding the glycerol mixture dissolved with the essence into a silk bundle according to a proportion, wherein the specification of the silk bundle is 3.0Y35000d, the addition amount of vanillin is 1.3-2 ug/branch, and the addition amount of glycerol is 60+/-3.0 mg/branch;
s3, adopting the specification of 25g/m 2 The filter stick is prepared by molding paper with the length of multiplied by 26.5mm and the length of multiplied by 6000CU, the circumference of the filter stick is 24+/-0.2 mm, the suction resistance is 3800+/-265 Pa, the hardness is more than or equal to 84 percent, the length is 120+/-0.5 mm, the roundness is less than or equal to 0.35mm, and the weight is 0.76+/-0.3 g/branch;
s4, cutting the filter stick prepared in the step S3 into six sections to obtain the filter stick required by a single cigarette.
7. A cigarette, characterized in that: the cigarette comprising the filter rod of claim 1.
8. A cigarette, characterized in that: the cigarette comprises the preparation method of the filter stick of claim 5.
CN202310479952.5A 2023-04-28 2023-04-28 Filter stick for increasing milk fragrance for cigarettes, preparation method and cigarettes Pending CN116530725A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202310479952.5A CN116530725A (en) 2023-04-28 2023-04-28 Filter stick for increasing milk fragrance for cigarettes, preparation method and cigarettes

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202310479952.5A CN116530725A (en) 2023-04-28 2023-04-28 Filter stick for increasing milk fragrance for cigarettes, preparation method and cigarettes

Publications (1)

Publication Number Publication Date
CN116530725A true CN116530725A (en) 2023-08-04

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Application Number Title Priority Date Filing Date
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Country Status (1)

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