CN115844776A - Preparation method of long-acting and lasting anti-allergic hair care solution for pets - Google Patents

Preparation method of long-acting and lasting anti-allergic hair care solution for pets Download PDF

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CN115844776A
CN115844776A CN202211299175.8A CN202211299175A CN115844776A CN 115844776 A CN115844776 A CN 115844776A CN 202211299175 A CN202211299175 A CN 202211299175A CN 115844776 A CN115844776 A CN 115844776A
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周剑
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Ningbo Ruisong Biological Technology Co ltd
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Abstract

The invention discloses a preparation method of a long-acting and lasting pet antiallergic hair care solution, wherein the addition amount of a Japanese magnolia flower bud extract, a Japanese lithospermum petal extract and a Japanese kaki extract in the long-acting and lasting pet antiallergic hair care solution is 1-5%, and the adopted extraction methods are respectively pressurized fluid extraction, pressurized fluid extraction and microwave-assisted extraction. The Magnolia japonica pistil extract, the Lithospermum japonicum petal extract and the persimmon Queen extract have rich vitamins B5 and E, amino acids, multiple trace elements, phenols, triterpenoid saponins, tannins and the like, small-molecular vitamins B5 and E and amino acids are injected into the root of pet hair through rubbing and washing so as to achieve the effect of moistening the hair, large-molecular phenols, triterpenoid saponins, tannins and the like and allergens have the effects of oxidation and the effects of negative charges carried by surfactants and positive and negative charges carried by the allergens, and the synergistic effect between the large-molecular phenols, the triterpenoid saponins, the tannins and the allergens can enable the allergenic proteins to lose effectiveness and be removed, so that the good effects of washing-free, safety, long-acting, lasting, anti-allergy, effective molecule locking and moistening the pet hair are achieved.

Description

Preparation method of long-acting and lasting anti-allergic hair care solution for pets
Technical Field
The invention belongs to the field of pet hair care, and particularly relates to a preparation method of a long-acting and lasting anti-allergic hair care solution for pets.
Background
With the development of society and the continuous change of life concept and the continuous change of family member constitution, more and more families for raising pets, cats and dogs are provided, and the lives of pets and people are close to each other. At present, pet hair care products on the market mostly take fungi and bacteria resisting cats and dogs per se as main materials, the report of the care products for inhibiting the pet allergens is less, some families are forbidden to nurture pets due to the existence of family members allergic to the pets, so how to prepare a product which can realize the nourishing of the hair roots of the pets without washing and only by wiping, can also play the anti-allergy effect, and realizes the long-acting, lasting, washing-free, anti-allergy and moistening of the pet hair is a problem to be solved urgently in the existing market.
Disclosure of Invention
Aiming at the existing problems, the invention takes the Japanese magnolia flower stamen extract, the Japanese lithospermum petal extract and the Japanese kaki extract as raw materials, and realizes the good effects of no-washing, anti-allergy and pet hair moistening through the synergistic effect of the effective components of the three.
In order to achieve the above purpose of the present invention, the present invention provides the following technical solutions:
a preparation method of a long-acting and durable anti-allergic hair care solution for pets is characterized by comprising the following steps: the addition amount of the Japanese magnolia flower bud extract, the Japanese lithospermum petal extract and the Japanese kaki extract in the long-acting and lasting anti-allergic hair care solution for pets is 1-5 percent respectively.
A preparation method of a long-acting and durable anti-allergic hair care solution for pets comprises the extraction methods of a Japanese magnolia flower stamen extract, a Japanese petrosal petal extract and a Japanese kaki extract, namely, pressurized fluid extraction and microwave-assisted extraction.
The extraction method of the Japanese magnolia flower stamen extract comprises the following steps: crushing and grinding dried Japanese Maolan pistil until the granularity is lower than 100 meshes, placing the crushed Japanese Maolan pistil and a proper amount of quartz sand in an extraction tank, placing the extraction tank in a pressurized fluid extraction instrument, taking absolute ethyl alcohol as an extraction solvent, performing cyclic extraction for 2 times at the extraction temperature of 190 ℃ and the extraction pressure of 8.5MPa for 10min, performing reduced pressure distillation on the obtained extracting solution, recovering the ethyl alcohol, concentrating and drying to obtain Japanese Maolan pistil extract powder.
The extraction method of the Jatropha curcas petal extract comprises the following steps: pulverizing dried petals of Nippon Oldhamiz to particle size of less than 100 meshes, mixing with appropriate amount of quartz sand, placing in an extraction tank, placing in a pressurized fluid extraction apparatus, extracting with dichloromethane as extraction solvent at 90 deg.C under 10.5MPa for 10min for 2 times, distilling the extractive solution under reduced pressure, concentrating, and drying to obtain extract powder.
The extraction method of the kaki comprises the following steps: crushing and grinding dried Japanese persimmon of the King to the granularity of less than 40 meshes, putting a proper amount of the dried Japanese persimmon of the King into a microwave synthesis extraction bottle, adding absolute ethyl alcohol into the mixture at a ratio of 1 to 20g/mL, setting the microwave power to be 500W, reacting at 65 ℃ for 10min, centrifuging the reaction liquid for 5min at a ratio of 10000r/min, taking the supernatant, distilling the supernatant under reduced pressure, concentrating and drying to obtain the Japanese persimmon extract powder of the King.
The long-acting and lasting pet anti-allergic hair care solution comprises the following components in parts by weight: 5 to 20 percent of phenoxyethanol, 1 to 5 percent of glycerin, 1 to 5 percent of panthenol, 1 to 3 percent of quaternary ammonium salt-27, 1 to 3 percent of quaternary ammonium salt-22, 1 to 5 percent of Japanese magnolia flower bud extract powder, 1 to 5 percent of Japanese petrosal petal extract powder, 1 to 5 percent of Japanese persimmon king extract powder, 0.5 to 3 percent of allantoin, 0.1 to 0.2 percent of hydrogenated lecithin, 0.5 to 5 percent of hydroxyethyl hydrolyzed collagen, 0.5 to 5 percent of hydroxypropyl trimethyl ammonium hydrolyzed wheat protein, 0.5 to 8 percent of stearin, 0.05 to 3 percent of methyl dibromoglutaronitrile and the balance of water. Preferably 15% phenoxyethanol, 3% glycerin, 4% panthenol, 3% quaternary ammonium salt-27, 3% quaternary ammonium salt-22, 5% japanese magnolia flower bud extract powder, 5% japanese bergamot petal extract powder, 5% japanese persimmon kaki extract powder, 2% allantoin, 0.1% hydrogenated lecithin, 2% hydroxyethyl hydrolyzed collagen, 3% hydroxypropyl trimethyl ammonium hydrolyzed wheat protein, 2% stearin, 2% methyl dibromoglutaronitrile, and the balance water, in parts by mass.
The preparation method of the long-acting and durable anti-allergic hair care solution for pets comprises the following steps:
1) Mixing phenoxyethanol, glycerol, panthenol, quaternary ammonium salt-27, quaternary ammonium salt-22, hydroxyethyl hydrolyzed collagen, hydroxypropyl trimethyl ammonium hydrolyzed wheat protein, and water, heating to 40-65 deg.C, and stirring for 3-5min;
2) Heating allantoin and hydrogenated lecithin to 60-95 deg.C, and stirring for 15-30min;
3) Pumping the step (1) into the step (2), mixing, stirring uniformly, adding stearylamine, and stirring for 3-5 minutes;
4) Cooling to below 45 deg.C under stirring, adding flos Magnoliae extract powder, japanese petroselinum petal extract powder, japanese kaki extract powder, methyl dibromoglutaronitrile, oleum Eucalypti, and hinoki oil;
5) Continuously stirring and cooling, discharging and filling after the inspection is qualified.
The invention takes the Japanese magnolia flower bud extract, the Japanese lithospermum petal extract and the Japanese kaki extract as raw materials, rich vitamins B5, E, amino acid, a plurality of trace elements, phenols, triterpenoid saponin, tannin and the like extracted from the raw materials are extracted, small molecular vitamins B5, E and amino acid are injected into the root of the pet hair through rubbing and washing so as to play a role in moistening the hair, large molecular phenols, triterpenoid saponin, tannin and the like and the allergen play a role in oxidation and the positive and negative charges between the negative charges carried by the surfactant and the allergen, and the synergistic effect between the large molecular phenols, triterpenoid saponin, tannin and the allergen can lead the allergen to lose efficacy and remove the double antiallergic effect, thereby realizing the good effects of no washing, safety, long-acting, durability, antianaphylaxis and pet hair moistening, and having wide application prospects in the field of pet care solution and the market segmentation.
Drawings
FIG. 1 is a graph showing the antiallergic effect of long-acting, long-lasting pet antiallergic hair care solutions with different ratios in examples 1 to 5 of the present invention on dermatophagoides pteronyssinus allergen protein Der p 1;
FIG. 2 is a graph of the antiallergic performance of the long-acting, long-lasting pet antiallergic hair care solutions of examples 1 to 5 of the present invention against house dust mite allergen protein Der f1 at different ratios;
FIG. 3 is a graph showing the antiallergic properties of long-acting, long-lasting pet antiallergic hair care solutions with different ratios of parts in examples 1-5 of the present invention on cat dander allergen protein Fel d 1;
FIG. 4 is a graph of the antiallergic properties of the long-acting, long-lasting pet antiallergic hair care solutions of examples 1-5 of the present invention against dog dander allergen protein Can f1 at different ratios;
FIG. 5 is a graph of the anti-allergic and persistent performance of the long-acting and persistent pet anti-allergic hair care solution on dermatophagoides pteronyssinus allergen protein Der p1 in example 5 of the present invention;
FIG. 6 is a chart of the anti-allergic durability of the long-lasting and durable pet anti-allergic hair care solution to dermatophagoides pteronyssinus allergen protein Der f1 in example 5 of the present invention;
FIG. 7 is a graph of the anti-allergic durability of a long-lasting, long-lasting pet anti-allergic hair care solution to cat dander allergen protein Fel d1 in example 5 of the present invention;
FIG. 8 is a graph of the anti-allergic durability of the long-lasting, long-lasting pet anti-allergic hair care solution to dog dander allergen protein Can f1 of example 5 of the present invention.
Detailed Description
The method of the present invention will be described in detail with reference to specific examples, which are carried out on the premise of the technical solution of the present invention, but the scope of the present invention is not limited to the following examples.
Example 1
Crushing and grinding dried Japanese Maolan pistil until the granularity is lower than 100 meshes, placing the crushed Japanese Maolan pistil and a proper amount of quartz sand in an extraction tank, placing the extraction tank in a pressurized fluid extraction instrument, taking absolute ethyl alcohol as an extraction solvent, performing cyclic extraction for 2 times at the extraction temperature of 190 ℃ and the extraction pressure of 8.5MPa for 10min, performing reduced pressure distillation on the obtained extracting solution, recovering the ethyl alcohol, concentrating and drying to obtain Japanese Maolan pistil extract powder; crushing and grinding dried petals of the Nippon rock microscope by adopting pressurized fluid until the granularity is lower than 100 meshes, placing the crushed petals of the Nippon rock microscope and a proper amount of quartz sand in an extraction tank, placing the extraction tank in a pressurized fluid extraction instrument, taking dichloromethane as an extraction solvent, performing cyclic extraction for 2 times at the extraction temperature of 90 ℃, the extraction pressure of 10.5MPa and the extraction time of 10min, distilling the obtained extract under reduced pressure, concentrating and drying to obtain Nippon rock microscope petal extract powder; crushing and grinding dried persimmons of Japan Tianwang by adopting a microwave-assisted extraction method until the granularity is lower than 40 meshes, putting a proper amount of the dried persimmons of Japan Tianwang into a microwave synthesis extraction bottle, adding absolute ethyl alcohol into the mixture at a ratio of 1; mixing 15% phenoxyethanol, 3% glycerin, 4% panthenol, 1% quaternary ammonium salt-27, 1% quaternary ammonium salt-22, 2% hydroxyethyl hydrolyzed collagen, 3% hydroxypropyl trimethyl ammonium hydrolyzed wheat protein, and 57.9% water, heating to 40-65 deg.C, and stirring for 3-5min; heating 2% allantoin and 0.1% hydrogenated lecithin to 60-95 deg.C, and stirring for 15-30min; mixing the two solutions, stirring uniformly, adding 2% ammonium stearate, and stirring for 3-5 minutes; cooling to below 45 deg.C under stirring, adding 1% of flos Magnoliae extract powder, 1% of Japanese Ottelia petal extract powder, 1% of Japanese Kazuki extract powder, 2% of methyl dibromoglutaronitrile, 2% of oleum Eucalypti, and 2% of hinoki oil; and continuously stirring and cooling to obtain the long-acting and lasting anti-allergic hair care solution for the pets.
Example 2
Crushing and grinding dried Japanese Maolan pistil until the granularity is lower than 100 meshes, placing the crushed Japanese Maolan pistil and a proper amount of quartz sand in an extraction tank, placing the extraction tank in a pressurized fluid extraction instrument, taking absolute ethyl alcohol as an extraction solvent, performing cyclic extraction for 2 times at the extraction temperature of 190 ℃ and the extraction pressure of 8.5MPa for 10min, performing reduced pressure distillation on the obtained extracting solution, recovering the ethyl alcohol, concentrating and drying to obtain Japanese Maolan pistil extract powder; crushing and grinding dried petals of the Nippon rock microscope by adopting pressurized fluid until the granularity is lower than 100 meshes, placing the crushed petals of the Nippon rock microscope and a proper amount of quartz sand in an extraction tank, placing the extraction tank in a pressurized fluid extraction instrument, taking dichloromethane as an extraction solvent, performing cyclic extraction for 2 times at the extraction temperature of 90 ℃, the extraction pressure of 10.5MPa and the extraction time of 10min, distilling the obtained extract under reduced pressure, concentrating and drying to obtain Nippon rock microscope petal extract powder; crushing and grinding dried persimmons of Japan Tianwang by adopting a microwave-assisted extraction method until the granularity is lower than 40 meshes, putting a proper amount of the dried persimmons of Japan Tianwang into a microwave synthesis extraction bottle, adding absolute ethyl alcohol into the mixture at a ratio of 1; mixing 15% phenoxyethanol, 3% glycerin, 4% panthenol, 1% quaternary ammonium salt-27, 1% quaternary ammonium salt-22, 2% hydroxyethyl hydrolyzed collagen, 3% hydroxypropyl trimethyl ammonium hydrolyzed wheat protein, and 51.9% water, heating to 40-65 deg.C, and stirring for 3-5min; heating 2% allantoin and 0.1% hydrogenated lecithin to 60-95 deg.C, stirring for 15-30min; mixing the two solutions, stirring uniformly, adding 2% ammonium stearate, and stirring for 3-5 minutes; stirring and cooling to below 45 deg.C, adding 3% of Japanese Maolan pistil extract powder, 3% of Japanese petrosal petal extract powder, 3% of Japanese Kazuki extract powder, 2% of methyl dibromoglutaronitrile, 2% of eucalyptus oil, and 2% of hinoki oil; and continuously stirring and cooling to obtain the long-acting and lasting anti-allergic hair care solution for the pets.
Example 3
Crushing and grinding dried Japanese Maolan pistil until the granularity is lower than 100 meshes, placing the crushed Japanese Maolan pistil and a proper amount of quartz sand in an extraction tank, placing the extraction tank in a pressurized fluid extraction instrument, taking absolute ethyl alcohol as an extraction solvent, performing cyclic extraction for 2 times at the extraction temperature of 190 ℃ and the extraction pressure of 8.5MPa for 10min, performing reduced pressure distillation on the obtained extracting solution, recovering the ethyl alcohol, concentrating and drying to obtain Japanese Maolan pistil extract powder; crushing and grinding dried Marasmius androsaceus petals by adopting pressurized fluid until the granularity is less than 100 meshes, placing the crushed Marasmius androsaceus petals and a proper amount of quartz sand into an extraction tank, placing the extraction tank into a pressurized fluid extraction instrument, taking dichloromethane as an extraction solvent, performing cyclic extraction for 2 times at the extraction temperature of 90 ℃, the extraction pressure of 10.5MPa and the extraction time of 10min, and performing reduced pressure distillation, concentration and drying on the obtained extract to obtain Marasmius androsaceus petal extract powder; crushing and grinding dried persimmons of Japan Tianwang by adopting a microwave-assisted extraction method until the granularity is lower than 40 meshes, putting a proper amount of the dried persimmons of Japan Tianwang into a microwave synthesis extraction bottle, adding absolute ethyl alcohol into the mixture at a ratio of 1; mixing 15% phenoxyethanol, 3% glycerin, 4% panthenol, 1% quaternary ammonium salt-27, 1% quaternary ammonium salt-22, 2% hydroxyethyl hydrolyzed collagen, 3% hydroxypropyl trimethyl ammonium hydrolyzed wheat protein, and 45.9% water, heating to 40-65 deg.C, and stirring for 3-5min; heating 2% allantoin and 0.1% hydrogenated lecithin to 60-95 deg.C, and stirring for 15-30min; mixing the two solutions, uniformly stirring, adding 2% ammonium stearate, and stirring for 3-5 minutes; cooling to 45 deg.C under stirring, adding 5% of Japanese Maolan pistil extract powder, 5% of Japanese Marasmius petal extract powder, 5% of Japanese Kazuki extract powder, 2% of methyl dibromoglutaronitrile, 2% of oleum Eucalypti, and 2% of cedar oil; and continuously stirring and cooling to obtain the long-acting and lasting anti-allergic hair care solution for the pets.
Example 4
Crushing and grinding dried Japanese Maolan pistil until the granularity is less than 100 meshes, placing the crushed Japanese Maolan pistil and a proper amount of quartz sand in an extraction tank, placing the extraction tank in a pressurized fluid extraction instrument, taking absolute ethyl alcohol as an extraction solvent, performing cyclic extraction for 2 times at the extraction temperature of 190 ℃ under the extraction pressure of 8.5MPa for 10min, performing reduced pressure distillation on the obtained extract, recovering the ethyl alcohol, and concentrating and drying to obtain Japanese Maolan pistil extract powder; crushing and grinding dried petals of the Nippon rock microscope by adopting pressurized fluid until the granularity is lower than 100 meshes, placing the crushed petals of the Nippon rock microscope and a proper amount of quartz sand in an extraction tank, placing the extraction tank in a pressurized fluid extraction instrument, taking dichloromethane as an extraction solvent, performing cyclic extraction for 2 times at the extraction temperature of 90 ℃, the extraction pressure of 10.5MPa and the extraction time of 10min, distilling the obtained extract under reduced pressure, concentrating and drying to obtain Nippon rock microscope petal extract powder; crushing and grinding dried persimmons of Japan Tianwang by adopting a microwave-assisted extraction method until the granularity is lower than 40 meshes, putting a proper amount of the dried persimmons of Japan Tianwang into a microwave synthesis extraction bottle, adding absolute ethyl alcohol into the mixture at a ratio of 1; mixing 15% phenoxyethanol, 3% glycerin, 4% panthenol, 2% quaternary ammonium salt-27, 2% quaternary ammonium salt-22, 2% hydroxyethyl hydrolyzed collagen, 3% hydroxypropyl trimethyl ammonium hydrolyzed wheat protein, and 43.9% water, heating to 40-65 deg.C, and stirring for 3-5min; heating 2% allantoin and 0.1% hydrogenated lecithin to 60-95 deg.C, and stirring for 15-30min; mixing the two solutions, uniformly stirring, adding 2% ammonium stearate, and stirring for 3-5 minutes; cooling to 45 deg.C under stirring, adding 5% of Japanese Maolan pistil extract powder, 5% of Japanese petrosal petal extract powder, 5% of Japanese Kazuki extract powder, 2% of methyl dibromoglutaronitrile, 2% of oleum Eucalypti, and 2% of hinoki oil; and continuously stirring and cooling to obtain the long-acting and lasting anti-allergic hair care solution for the pets.
Example 5
Crushing and grinding dried Japanese Maolan pistil until the granularity is less than 100 meshes, placing the crushed Japanese Maolan pistil and a proper amount of quartz sand in an extraction tank, placing the extraction tank in a pressurized fluid extraction instrument, taking absolute ethyl alcohol as an extraction solvent, performing cyclic extraction for 2 times at the extraction temperature of 190 ℃ under the extraction pressure of 8.5MPa for 10min, performing reduced pressure distillation on the obtained extract, recovering the ethyl alcohol, and concentrating and drying to obtain Japanese Maolan pistil extract powder; crushing and grinding dried petals of the Nippon rock microscope by adopting pressurized fluid until the granularity is lower than 100 meshes, placing the crushed petals of the Nippon rock microscope and a proper amount of quartz sand in an extraction tank, placing the extraction tank in a pressurized fluid extraction instrument, taking dichloromethane as an extraction solvent, performing cyclic extraction for 2 times at the extraction temperature of 90 ℃, the extraction pressure of 10.5MPa and the extraction time of 10min, distilling the obtained extract under reduced pressure, concentrating and drying to obtain Nippon rock microscope petal extract powder; crushing and grinding dried persimmons of Japan Tianwang by adopting a microwave-assisted extraction method until the granularity is lower than 40 meshes, putting a proper amount of the dried persimmons of Japan Tianwang into a microwave synthesis extraction bottle, adding absolute ethyl alcohol into the mixture at a ratio of 1; mixing 15% phenoxyethanol, 3% glycerin, 4% panthenol, 3% quaternary ammonium salt-27, 3% quaternary ammonium salt-22, 2% hydroxyethyl hydrolyzed collagen, 3% hydroxypropyl trimethyl ammonium hydrolyzed wheat protein, and 41.9% water, heating to 40-65 deg.C, and stirring for 3-5min; heating 2% allantoin and 0.1% hydrogenated lecithin to 60-95 deg.C, and stirring for 15-30min; mixing the two solutions, uniformly stirring, adding 2% ammonium stearate, and stirring for 3-5 minutes; cooling to 45 deg.C under stirring, adding 5% of Japanese Maolan pistil extract powder, 5% of Japanese petrosal petal extract powder, 5% of Japanese Kazuki extract powder, 2% of methyl dibromoglutaronitrile, 2% of oleum Eucalypti, and 2% of hinoki oil; and continuously stirring and cooling to obtain the long-acting and lasting anti-allergic hair care solution for the pets.
The test method comprises the following steps: by using
Figure BDA0003903892140000081
(Luminex) method to detect anti-allergic effects. />

Claims (7)

1. A preparation method of a long-acting and durable anti-allergic hair care solution for pets is characterized by comprising the following steps: the addition amount of the Japanese Maolan pistil extract, the Japanese vetiver petal extract and the Japanese kaki extract in the long-acting and lasting anti-allergic hair care solution for pets is 1-5 percent respectively.
2. The method for preparing a long-acting and durable anti-allergic hair care solution for pets according to claim 1, wherein the method comprises the following steps: the extraction methods of the Magnolia japonica pistil extract, the Pyrola japonica petal extract and the Kazuki kaki extract are respectively pressurized fluid extraction, pressurized fluid extraction and microwave-assisted extraction.
3. The method for preparing a long-acting and durable anti-allergic hair care solution for pets according to claim 2, wherein the method comprises the following steps: the extraction method of the Japanese magnolia flower stamen extract comprises the following steps: crushing and grinding dried Japanese Maolan pistil until the granularity is lower than 100 meshes, placing the crushed Japanese Maolan pistil and a proper amount of quartz sand in an extraction tank, placing the extraction tank in a pressurized fluid extraction instrument, taking absolute ethyl alcohol as an extraction solvent, performing cyclic extraction for 2 times at the extraction temperature of 190 ℃ and the extraction pressure of 8.5MPa for 10min, performing reduced pressure distillation on the obtained extracting solution, recovering the ethyl alcohol, concentrating and drying to obtain Japanese Maolan pistil extract powder.
4. The method for preparing a long-acting and durable anti-allergic hair care solution for pets according to claim 2, wherein the method comprises the following steps: the extraction method of the Jatropha curcas petal extract comprises the following steps: pulverizing dried petals of Nippon Oldhamiz to particle size of less than 100 meshes, mixing with appropriate amount of quartz sand, placing in an extraction tank, placing in a pressurized fluid extraction apparatus, extracting with dichloromethane as extraction solvent at 90 deg.C under 10.5MPa for 10min for 2 times, distilling the extractive solution under reduced pressure, concentrating, and drying to obtain extract powder.
5. The method for preparing a long-acting and durable anti-allergic hair care solution for pets according to claim 2, wherein the method comprises the following steps: the extraction method of the kaki comprises the following steps: crushing and grinding dried persimmons of Japan Tianwang to the particle size of less than 40 meshes, putting a proper amount of the dried persimmons of Japan Tianwang in a microwave synthesis extraction bottle, adding absolute ethyl alcohol into the mixture at the ratio of 1 to 20g/mL, setting the microwave power to be 500W, reacting at the temperature of 65 ℃ for 10min, carrying out centrifugation treatment on the reaction liquid at the ratio of 10000r/min for 5min, taking supernatant, carrying out reduced pressure distillation, concentrating and drying to obtain the extract powder of the persimmons of Japan Tianwang.
6. The preparation method of the long-acting and lasting pet antiallergic hair care solution is characterized in that the long-acting and lasting pet antiallergic hair care solution comprises the following components in parts by weight: 0.5-2% phenoxyethanol, 1-5% glycerin, 1-5% panthenol, 1-3% polyquaternium-27, 1-3% polyquaternium-22, 1-3% polyquaternium-33, 0.5-2% green tea extract, 1-5% Japanese Maolan pistil extract powder, 1-5% Japanese petrosal petal extract powder, 1-5% Japanese Kao persimmon extract powder, 0.5-3% allantoin, 0.1-5% hydrogenated lecithin, 1-5% phytosterol, 0.5-5% stearyltrimethylammonium hydroxyethyl hydrolyzed collagen, 0.5-5% hydrolyzed keratin, 0.5-8% squalane, 0.05-3% methyldibromopentadinitrile, 1-2% eucalyptus oil, 1-2% hinoki oil, and the balance water.
7. A method of preparing a long-lasting, long-lasting pet anti-allergic hair care solution according to any of claims 1 to 6, comprising the steps of:
1) Mixing phenoxyethanol, glycerol, panthenol, quaternary ammonium salt-27, quaternary ammonium salt-22, hydroxyethyl hydrolyzed collagen, hydroxypropyl trimethyl ammonium hydrolyzed wheat protein and water, heating to 40-65 deg.C, and stirring for 3-5min;
2) Heating allantoin and hydrogenated lecithin to 60-95 deg.C, and stirring for 15-30min;
3) Pumping the step (1) into the step (2), mixing, stirring uniformly, adding stearylamine, and stirring for 3-5 minutes;
4) Cooling to below 45 deg.C under stirring, adding flos Magnoliae extract powder, japanese petroselinum petal extract powder, japanese kaki extract powder, methyl dibromoglutaronitrile, oleum Eucalypti, and hinoki oil;
5) Continuously stirring and cooling, discharging and filling after being inspected to be qualified.
CN202211299175.8A 2022-10-24 2022-10-24 Preparation method of long-acting and lasting anti-allergic hair care solution for pets Pending CN115844776A (en)

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Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113388459A (en) * 2021-05-26 2021-09-14 宁波芮颂生物科技有限公司 Preparation method and application of cat and dog allergen-resistant finishing composition solution

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113388459A (en) * 2021-05-26 2021-09-14 宁波芮颂生物科技有限公司 Preparation method and application of cat and dog allergen-resistant finishing composition solution

Non-Patent Citations (4)

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Title
国家标准化管理委员会: "伴侣动物(宠物)用品安全技术要求", 15 March 2024, pages: 13 *
国家食品药品监督管理总局: "化妆品安全技术规范", 30 November 2015, pages: 116 *
王刚力: "化妆品安全性评价方法及实例", 29 February 2020, 中国医药科技出版社, pages: 211 - 212 *
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