CN115813006A - Electronic cigarette liquid capable of improving fruit aroma and preparation method thereof - Google Patents

Electronic cigarette liquid capable of improving fruit aroma and preparation method thereof Download PDF

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CN115813006A
CN115813006A CN202211088422.XA CN202211088422A CN115813006A CN 115813006 A CN115813006 A CN 115813006A CN 202211088422 A CN202211088422 A CN 202211088422A CN 115813006 A CN115813006 A CN 115813006A
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electronic cigarette
essential oil
fruit
liquid
improving
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CN202211088422.XA
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CN115813006B (en
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胡磊
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Dongguan Hongfu Biological Technology Co ltd
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Dongguan Hongfu Biological Technology Co ltd
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Abstract

The application is suitable for the technical field of electronic cigarettes and discloses an electronic cigarette liquid capable of improving fruit fragrance and a preparation method thereof, wherein the electronic cigarette liquid comprises the following raw material components in percentage by weight: 0.07-2.2% of nicotine, 6-30.4% of fruit essential oil, 0.3-1.5% of acetoin, 0.1-2.4% of maxolidene, 0.001-1.7% of fruit flavor substance, (2, 3, 5) -trimethyl pyrazine, 0.003-0.01% of peppermint oil and 60-82% of solvent. This application has added acetoin, masonya lactone and fruity flavor material in fruity flavor type electron cigarette liquid, each component synergism, and the fruity flavor smell obviously promotes, the richness of fragrance increase, and the raw materials in this application are general easily available, and the nature is stable, and the allotment is simple, has wide application prospect.

Description

Electronic cigarette liquid capable of improving fruit aroma and preparation method thereof
Technical Field
The application relates to the technical field of electronic cigarettes, in particular to electronic cigarette liquid capable of improving fruit fragrance and a preparation method thereof.
Background
In recent years, along with the continuous enhancement of the cigarette control strength at home and abroad, the production, sale and use population of the traditional cigarette is more and more limited. Electronic cigarettes are widely concerned and researched as possible substitute products of traditional cigarettes, and the development of the electronic cigarettes is extremely rapid. The smoking taste of the electronic cigarette is very important for product popularization, the smoking taste of the electronic cigarette is diversified and developed on the basis of simulating the fragrance of the traditional cigarette, and tobacco oil with various types of fragrance is developed.
The fruit aroma exists widely in food and beverage industries, and has extremely high acceptance degree. The fruity electronic cigarette liquid is based on fruit aroma and covers aroma and aroma of different fruits, but the sensory quality of the current fruity electronic cigarette is poor during smoking, particularly in the aspects of fruity aroma, richness and the like, so that the electronic cigarette liquid capable of improving the fruit aroma is required to be provided.
Disclosure of Invention
The application aims at solving at least one of the technical problems existing in the prior art, and therefore the application provides the electronic cigarette liquid capable of improving the fruit fragrance.
The application provides an electronic cigarette liquid capable of improving fruit aroma, which comprises the following raw material components in percentage by weight:
Figure BDA0003832925140000011
Figure BDA0003832925140000021
more specifically, in the above technical solution, the fruit essential oil includes one or more of apple essential oil, pear essential oil, banana essential oil, pineapple essential oil, strawberry essential oil, orange essential oil, lemon essential oil, and grape essential oil.
More specifically, in the above technical scheme, the fruity substance is selected from one or more of benzyl butyrate, trigonella foenum-graecum lactone and benzyl benzoate.
More specifically, in the technical scheme, the weight ratio of the benzyl butyrate, the trigonella foenum-graecum lactone and the benzyl benzoate is (0.2-0.5) to (0.34-0.67) to ((0.004-0.03).
More specifically, in the above technical solution, the peppermint oil is at least one of spearmint peppermint oil and peppermint oil.
More specifically, in the above technical solution, the solvent includes: at least one of ethanol, water, menthol, propylene glycol, 1, 2-propylene glycol, glycerol, diethylene glycol, triethylene glycol, and glycerol triacetate.
More specifically, in the above technical solution, the electronic cigarette further includes 0.001 to 0.005% of a preservative by weight percentage.
More specifically, in the technical scheme, the preservative is p-hydroxybenzoate.
The application also provides a preparation method of the electronic cigarette liquid, which comprises the following steps: mixing the raw materials in the electronic cigarette liquid according to the weight percentage.
This application protects the application of above-mentioned electron tobacco juice in improving electron cigarette fruit is fragrant simultaneously.
Compared with the prior art, the embodiment of the application has at least one of the following beneficial effects:
this application has added acetoin, masonya lactone and fruity flavor material in fruity flavor type electron cigarette liquid, each component synergism, and the fruity flavor smell obviously promotes, the richness of fragrance increase, and the raw materials in this application are general easily available, and the nature is stable, and the allotment is simple, has wide application prospect. In addition, various raw materials are coordinated and matched, so that the natural feeling and the penetrability of the electronic cigarette liquid can be improved, and the flavor and the richness of the fruit are comprehensively improved.
Detailed Description
The technical solutions in the present application are clearly and completely described below by specific examples. It should be understood that the detailed description and specific examples, while indicating the embodiments described in this section, are intended for purposes of illustration only and are not intended to limit the scope of the disclosure.
It will be appreciated by those skilled in the art that the following examples are illustrative of the present application only and should not be taken as limiting the scope of the present application. The examples do not specify particular techniques or conditions, and are performed according to the techniques or conditions described in the literature in the art or according to the product specifications. The materials or equipment used are not indicated by manufacturers, and all are conventional products available by purchase.
The application provides an electronic cigarette liquid capable of improving fruit aroma, which comprises the following raw material components in percentage by weight:
Figure BDA0003832925140000031
the fruit essential oil is obtained by separating lemon and citrus peel, squeezing and filtering pulp, concentrating, freeze drying pulp residue, and pulverizing; adding water into the peel, carrying out ultrasonic crushing treatment, carrying out enzymolysis, and distilling by using steam to obtain the fruit essential oil.
Acetoin is often applied to beverages and snacks with cream taste, and the maosolides have the fragrance of milk oil, coconut and the like, and the two ingredients have synergistic effect with fruit essential oil and other components, so that the fruit fragrance in the electronic cigarette liquid is obviously improved, and the fragrance richness is increased.
The fruit flavor can be further improved by adding a proper amount of (2, 3, 5) -trimethyl pyrazine, and the mint oil can improve the reduction degree of the electronic cigarette liquid, so that the electronic cigarette liquid has fresh fruit flavor and mouthfeel.
In some embodiments, the fruit essential oil comprises one or more of apple essential oil, pear essential oil, banana essential oil, pineapple essential oil, strawberry essential oil, citrus essential oil, lemon essential oil, grape essential oil.
In some embodiments, the fruity substance is selected from one or more of benzyl butyrate, fenugreek lactone, and benzyl benzoate, which can further enhance the fruity odor of the e-liquid.
In some embodiments, the weight ratio of benzyl butyrate, trigonella foenum-graecum lactone, and benzyl benzoate is (0.2-0.5): (0.34-0.67): (0.004-0.03).
In some embodiments, the peppermint oil is at least one of spearmint peppermint oil, peppermint oil.
In some embodiments, the solvent comprises: at least one of ethanol, water, menthol, propylene glycol, 1, 2-propylene glycol, glycerol, diethylene glycol, triethylene glycol, and glycerol triacetate, wherein the water is preferably distilled water.
In some embodiments, the e-cigarette further comprises 0.001-0.005% by weight of a preservative, wherein the preservative extends the shelf life of the e-cigarette liquid.
In some embodiments, the preservative is a paraben.
The application also provides a preparation method of the electronic cigarette liquid, which comprises the following steps: the raw materials in the electronic cigarette liquid are mixed according to the weight percentage, the flavor of the electronic cigarette liquid prepared by the method is obviously improved, the richness of the flavor is increased, and the sensory quality of a user is also improved.
This application protects the application of above-mentioned electron tobacco juice in improving electron cigarette fruit is fragrant simultaneously.
The present application is further described with reference to the following specific examples.
Example 1
The electronic cigarette liquid capable of improving the fruity flavor is prepared by mixing the following raw materials in percentage by weight:
nicotine 1.3%, lemon essential oil 16.4%, acetoin 0.6%, maxolidene 0.5%, benzyl butyrate 0.6%, (2, 3, 5) -trimethylpyrazine 0.005%, peppermint oil 7.9%, 1, 2-propanediol 55%, and diethylene glycol 17.695%.
Example 2
The electronic cigarette liquid capable of improving the fruity flavor is prepared by mixing the following raw materials in percentage by weight:
1.1% of nicotine, 17.64% of grape essential oil, 0.9% of acetoin, 1.1% of maxolidene, 0.8% of fenugreek lactone, 0.004% of (2, 3, 5) -trimethyl pyrazine, 8.3% of peppermint oil, 35.2% of propylene glycol and 34.956% of glycerol.
Example 3
The electronic cigarette liquid capable of improving the fruity flavor is prepared by mixing the following raw materials in percentage by weight:
nicotine 0.88%, strawberry essential oil 17.01%, acetoin 1.2%, maxonolide 1.7%, benzyl benzoate 0.01%, (2, 3, 5) -trimethylpyrazine 0.005%, peppermint oil 10.3%, propylene glycol 40.23% and menthol 28.665%.
Example 4
The electronic cigarette liquid capable of improving the fruity flavor is prepared by mixing the following raw materials in percentage by weight:
1.04% of nicotine, 18.64% of pineapple essential oil, 1.4% of acetoin, 2.3% of maxolidene, 0.2% of benzyl butyrate, 0.01% of (2, 3, 5) -trimethyl pyrazine, 12.4% of peppermint oil, 35.41% of propylene glycol and 28.6% of triethylene glycol.
Comparative example 1
The electronic cigarette liquid is prepared by mixing the following raw materials in percentage by weight:
1.3% of nicotine, 16.4% of lemon essential oil, 0.5% of maxolidene, 0.6% of benzyl butyrate, (2, 3, 5) -trimethyl pyrazine 0.005%, 7.9% of peppermint oil, 55.3% of 1, 2-propylene glycol and 17.995% of diethylene glycol.
Comparative example 2
The electronic cigarette liquid is prepared by mixing the following raw materials in percentage by weight:
1.1% of nicotine, 17.64% of grape essential oil, 0.9% of acetoin, 0.8% of fenugreek lactone, 0.004% of (2, 3, 5) -trimethyl pyrazine, 8.3% of peppermint oil, 36.2% of propylene glycol and 35.056% of glycerol.
Comparative example 3
The electronic cigarette liquid is prepared by mixing the following raw materials in percentage by weight:
nicotine 0.88%, strawberry essential oil 17.01%, benzyl benzoate 0.01%, (2, 3, 5) -trimethylpyrazine 0.005%, peppermint oil 10.3%, propylene glycol 41.63%, and menthol 30.165%.
The weight percentages of acetoin and maxonolide in examples 1-4 increased gradually, no acetoin was added in comparative example 1, no maxonolide was added in comparative example 2, and neither acetoin nor maxonolide was added in comparative example 3.
The electronic cigarette liquid is added into the electronic cigarette, 15 consumers perform sensory evaluation on the fruity flavor of the electronic cigarette, and the sensory evaluation is performed on six grades, namely first grade, second grade, third grade, fourth grade, fifth grade and sixth grade, wherein the sensory perception of each grade for the fruity flavor is shown in table 1. When 15 consumers evaluated the same sensory evaluation grade of the fruity flavor impression type by 90% or more, the evaluation is effective, otherwise, the evaluation is carried out again. After each consumer smokes the electronic cigarette for evaluation, the consumer rinses the mouth with clear water and takes a rest for ten minutes for next evaluation, and the evaluation results are shown in table 2.
TABLE 1
Stage number Fruit fragrance
First gear Is very fragrant and sweet
Second gear Graceful and moderate
Three-gear Fresh and sweet
Four-gear In general terms
Five-gear Is slightly light
Six-gear Too light
TABLE 2
Sample (I) Stage number
Example 1 Three-gear
Example 2 Second gear
Example 3 Second gear
Example 4 First gear
Comparative example 1 Four-gear
Comparative example 2 Four-gear
Comparative example 3 Five-gear
According to the evaluation results of table 1 and table 2 show, acetoin and maxolide have special advantage in the electron tobacco tar of this application, after the electron tobacco tar of this application adds acetoin and maxolide, each component synergism, fruit flavor information obviously promotes, and along with acetoin and the increase of percentage content of maxolide fruit in the electron tobacco juice, the experience of user fruit flavor in to the electron cigarette also rises gradually.
The evaluation method of the aroma richness is that 10 professionals in the panel of smoking are respectively used for carrying out quantitative evaluation on the aroma richness evaluation index of the electronic cigarette according to the quantitative table shown in the table 3, and the evaluation result is shown in the table 4.
TABLE 3
Sensory perception Has no feeling Weak (weak) Slightly weaker Average Is a little stronger High strength
Score of 0 2 4 6 8 10
TABLE 4
Figure BDA0003832925140000071
According to table 3 and table 4 show, after the electronic cigarette liquid adds acetoin and maxolide, the experience of tester to the fragrance richness of electronic cigarette is promoted, and along with the promotion of acetoin and maxolide weight percentage content, the experience of fragrance richness is also stronger and stronger, and consumer's experience is also promoted, has increased the taste that the electronic cigarette smoked.
The above-mentioned embodiments are only used for illustrating the technical solutions of the present application, and not for limiting the same; although the present application has been described in detail with reference to the foregoing embodiments, it should be understood by those of ordinary skill in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some technical features may be equivalently replaced; such modifications and substitutions do not depart from the spirit and scope of the embodiments of the present application, and they should be construed as being included in the present application.

Claims (10)

1. The electronic cigarette liquid capable of improving the fruit aroma is characterized by comprising the following raw material components in percentage by weight:
Figure FDA0003832925130000011
2. the electronic cigarette liquid capable of improving the fruit aroma according to claim 1, wherein the fruit essential oil comprises one or more of apple essential oil, pear essential oil, banana essential oil, pineapple essential oil, strawberry essential oil, orange essential oil, lemon essential oil and grape essential oil.
3. The liquid e-cigarette of claim 1, wherein the fruity material is selected from one or more of benzyl butyrate, trigonella foenum-graecum lactone, and benzyl benzoate.
4. The electronic cigarette liquid capable of improving the fruity flavor as claimed in claim 3, wherein the weight ratio of benzyl butyrate, trigonella foenum-graecum lactone and benzyl benzoate is (0.2-0.5) to (0.34-0.67) to (0.004-0.03).
5. The electronic cigarette liquid capable of improving the fruit aroma according to claim 1, wherein the mint oil is at least one of spearmint mint oil and peppermint oil.
6. The liquid e-cigarette capable of improving fruit aroma according to any one of claims 1-5, wherein the solvent comprises: at least one of ethanol, water, menthol, propylene glycol, 1, 2-propylene glycol, glycerol, diethylene glycol, triethylene glycol, and glycerol triacetate.
7. The liquid e-cigarette capable of improving fruit flavor according to any one of claims 1-5, wherein the e-cigarette further comprises 0.001-0.005% preservative by weight.
8. The liquid tobacco according to claim 7, wherein the preservative is parabens.
9. A preparation method of electronic cigarette liquid is characterized by comprising the following steps: mixing the raw materials in the electronic cigarette liquid according to any one of claims 1 to 8 in percentage by weight.
10. Use of the e-liquid of any one of claims 1 to 8 to enhance the fruity flavor of an e-cigarette.
CN202211088422.XA 2022-09-05 2022-09-05 Electronic cigarette liquid capable of improving fruit fragrance and preparation method thereof Active CN115813006B (en)

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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2113133C1 (en) * 1995-12-01 1998-06-20 Всероссийский научно-исследовательский институт пищевых ароматизаторов, кислот и красителей Food flavor with taste and aroma of tropical fruits
CN104768406A (en) * 2012-08-28 2015-07-08 亲切消费者有限公司 Nicotine composition
CN105368577A (en) * 2015-11-26 2016-03-02 上海应用技术学院 Strawberry essence and preparation method therefor
CN106820270A (en) * 2017-01-20 2017-06-13 深圳瀚星翔科技有限公司 A kind of electronic cigarette tobacco tar and preparation method thereof
CN108185539A (en) * 2018-03-21 2018-06-22 福建中烟工业有限责任公司 Electronic cigarette that a kind of aesthetic quality is improved and preparation method thereof
CN113558282A (en) * 2021-08-23 2021-10-29 深圳芳芯科技有限公司 Electronic cigarette liquid and atomization device containing same
CN114184690A (en) * 2020-09-14 2022-03-15 深圳波顿香料有限公司 Method for simultaneously determining butanedione, 2, 3-pentanedione and acetoin in electronic cigarette oil

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2113133C1 (en) * 1995-12-01 1998-06-20 Всероссийский научно-исследовательский институт пищевых ароматизаторов, кислот и красителей Food flavor with taste and aroma of tropical fruits
CN104768406A (en) * 2012-08-28 2015-07-08 亲切消费者有限公司 Nicotine composition
CN105368577A (en) * 2015-11-26 2016-03-02 上海应用技术学院 Strawberry essence and preparation method therefor
CN106820270A (en) * 2017-01-20 2017-06-13 深圳瀚星翔科技有限公司 A kind of electronic cigarette tobacco tar and preparation method thereof
CN108185539A (en) * 2018-03-21 2018-06-22 福建中烟工业有限责任公司 Electronic cigarette that a kind of aesthetic quality is improved and preparation method thereof
CN114184690A (en) * 2020-09-14 2022-03-15 深圳波顿香料有限公司 Method for simultaneously determining butanedione, 2, 3-pentanedione and acetoin in electronic cigarette oil
CN113558282A (en) * 2021-08-23 2021-10-29 深圳芳芯科技有限公司 Electronic cigarette liquid and atomization device containing same

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