CN115804733A - Gel-in-oil moisturizing composition and preparation method and application thereof - Google Patents
Gel-in-oil moisturizing composition and preparation method and application thereof Download PDFInfo
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- CN115804733A CN115804733A CN202211713108.6A CN202211713108A CN115804733A CN 115804733 A CN115804733 A CN 115804733A CN 202211713108 A CN202211713108 A CN 202211713108A CN 115804733 A CN115804733 A CN 115804733A
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- 230000003020 moisturizing effect Effects 0.000 title claims abstract description 53
- 239000000203 mixture Substances 0.000 title claims abstract description 46
- 238000002360 preparation method Methods 0.000 title abstract description 9
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 28
- 239000002994 raw material Substances 0.000 claims abstract description 24
- TXFPEBPIARQUIG-UHFFFAOYSA-N 4'-hydroxyacetophenone Chemical compound CC(=O)C1=CC=C(O)C=C1 TXFPEBPIARQUIG-UHFFFAOYSA-N 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- -1 polydimethylsiloxane Polymers 0.000 claims abstract description 19
- 239000004205 dimethyl polysiloxane Substances 0.000 claims abstract description 17
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 17
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- 229920002385 Sodium hyaluronate Polymers 0.000 claims abstract description 14
- 229940010747 sodium hyaluronate Drugs 0.000 claims abstract description 14
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims abstract description 14
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- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 description 2
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- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 description 2
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- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
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- OSCJHTSDLYVCQC-UHFFFAOYSA-N 2-ethylhexyl 4-[[4-[4-(tert-butylcarbamoyl)anilino]-6-[4-(2-ethylhexoxycarbonyl)anilino]-1,3,5-triazin-2-yl]amino]benzoate Chemical compound C1=CC(C(=O)OCC(CC)CCCC)=CC=C1NC1=NC(NC=2C=CC(=CC=2)C(=O)NC(C)(C)C)=NC(NC=2C=CC(=CC=2)C(=O)OCC(CC)CCCC)=N1 OSCJHTSDLYVCQC-UHFFFAOYSA-N 0.000 description 1
- 241000228245 Aspergillus niger Species 0.000 description 1
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- OVRNDRQMDRJTHS-FMDGEEDCSA-N N-acetyl-beta-D-glucosamine Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O OVRNDRQMDRJTHS-FMDGEEDCSA-N 0.000 description 1
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- FAPWYRCQGJNNSJ-UBKPKTQASA-L calcium D-pantothenic acid Chemical class [Ca+2].OCC(C)(C)[C@@H](O)C(=O)NCCC([O-])=O.OCC(C)(C)[C@@H](O)C(=O)NCCC([O-])=O FAPWYRCQGJNNSJ-UBKPKTQASA-L 0.000 description 1
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- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 description 1
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- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical group [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 description 1
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Abstract
The invention discloses a water-in-oil gel moisturizing composition and a preparation method and application thereof, wherein the water-in-oil gel moisturizing composition comprises the following raw materials: water, glycerin, butanediol, sodium hyaluronate, panthenol, lodestone, polyacryloyldimethyl taurinate ammonium, G57, polydimethylsiloxane, disteardimonium hectorite, isononyl isononanoate, hydrogenated polyisobutene, KSG-210, KF-6017, KF-6038, p-hydroxyacetophenone, 1,2-hexanediol. The water-in-oil gel system moisturizing composition is prepared by adopting the organic silicon emulsifier, and the moisturizing composition prepared by compounding the components has the characteristics of being fresh, cool, not sticky and easy to spread in the skin smearing process. After the skin moisturizing cream is applied, a thin oil film can be kept on the skin for a long time, and the water-locking and moisturizing capabilities of the skin are improved.
Description
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to a water-in-oil gel moisturizing composition and a preparation method and application thereof.
Background
With the continuous development of the cosmetic industry technology and the continuous change of the market trend. New challenges are posed to our formulation development. Products in the cosmetics market have been viewed as involving emulsifying systems having oil-in-water, water-in-oil, and water-in-oil gels, respectively. Both oil-in-water and water-in-oil systems are currently the most mature and can be accomplished by a wide variety of emulsifiers. As a novel emulsifying system, the hydrogel-in-oil emulsion is developed by selecting the traditional emulsifier on the market, and the selected emulsifier is single. The limitation on skin feel innovation is large. The existing market lacks compositions that utilize silicone emulsifiers to develop hydrogel-in-oil systems.
Disclosure of Invention
In order to overcome the defects of the prior art, one of the purposes of the invention is to provide a gel-in-oil moisturizing composition, two types of organic silicon of KF-6017 and KF-6038 are used as emulsifiers, so that organic silicon oil in a formula can be better compatible, the composition has the characteristics of refreshing, non-sticky and greasy skin feeling, good moisturizing effect and the like when being used on skin, and the singleness of the selection of the emulsifiers of the gel-in-oil system is eliminated; the second purpose of the invention is to provide a preparation method of the gel-in-oil moisturizing composition, the oil phase and the gel phase are mixed and emulsified by cold preparation, and the moisturizing composition can be obtained without homogeneous participation in the emulsification process; the invention also aims to provide the application of the gel-in-oil moisturizing composition, which can be used for preparing cosmetics and is suitable for all-skin use.
One of the purposes of the invention is realized by adopting the following technical scheme:
the water-in-oil gel moisturizing composition comprises the following raw materials in percentage by weight: 3 to 5 percent of glycerin, 3 to 5 percent of butanediol, 0.02 to 0.1 percent of sodium hyaluronate, 0.5 to 1 percent of panthenol, 0.5 to 1 percent of water-locking magnetite, 0.6 to 1 percent of polyacryloyldimethyl ammonium taurate, 0.4 to 0.7 percent of G57, 5 to 8 percent of polydimethylsiloxane, 0.2 to 0.5 percent of disteardimonium hectorite, 4 to 6 percent of isononyl isononanoate, 1 to 3 percent of hydrogenated polyisobutene, 0.3 to 3 percent of KSG-2101, 2 to 3 percent of KF-6017, 0.3 to 0.8 percent of KF-6038, 0.3 to 0.5 percent of p-hydroxyacetophenone, 0.4 to 0.6 percent of 1,2-hexanediol and the balance of water.
Preferably, the above water-in-oil gel moisturizing composition comprises the following raw materials in percentage by weight: 5% of glycerin, 3% of butanediol, 0.04% of sodium hyaluronate, 0.8% of panthenol, 0.8% of Magnetitum, 1% of polyacryloyldimethyl ammonium taurate, 0.5% of G57, 6.5% of polydimethylsiloxane, 0.3% of distearyl dimethyl ammonium hectorite, 5% of isononyl isononanoate, 2% of hydrogenated polyisobutene, 2.5% of KSG-210, 2.5% of KF-6017, 0.5% of KF-6038, 0.5% of p-hydroxyacetophenone, 0.5% of 1,2-hexanediol, and the balance of water.
Furthermore, the water-in-oil gel moisturizing composition also comprises 0.02-0.05% of an aromatizer, and preferably 0.03% of an aromatizer.
The second purpose of the invention is realized by adopting the following technical scheme:
the preparation method of the water-in-oil gel moisturizing composition comprises the following steps:
1) Respectively dividing each raw material into an A phase, a B phase and a C phase; wherein, the phase A is: water, glycerin, butanediol, sodium hyaluronate, ammonium polyacryloyldimethyl taurate, G57; the phase B is as follows: p-hydroxyacetophenone, 1,2-hexanediol; the phase C is as follows: panthenol and water-locking magnetite; the phase D is as follows: polydimethylsiloxane, disteardimonium hectorite, isononyl isononanoate, hydrogenated polyisobutene, KSG-210, KF-6017, KF-6038;
2) Adding the components of the phase A raw material into an emulsifying pot, stirring, heating, stirring and homogenizing until the material body is uniform, and keeping the temperature;
3) Weighing the components of the phase B raw material in a container, heating, adding the B raw material into the phase A after complete dissolution, uniformly stirring, and starting stirring and cooling;
4) Stirring and cooling the emulsion pot, adding the C phase components, and uniformly stirring to obtain the aqueous phase gel consisting of the A phase, the B phase and the C phase.
5) Weighing all the components of the D-phase raw material, placing the components in an oil phase pot, stirring and homogenizing until the material body is uniform; adding the phase D into the water-phase gel obtained in the step 4), stirring and mixing, cooling, filtering and discharging to obtain the water-in-oil gel moisturizing composition.
Furthermore, the raw materials of the water-in-oil gel moisturizing composition also comprise an E phase which is an aromatizer; and 5) adding the aqueous phase gel into the phase D, uniformly stirring, then adding the phase E, and uniformly stirring to obtain the water-in-oil gel moisturizing composition.
Further, the stirring time after the phase E is added is 5-10 min.
Further, in the step 2), the heating temperature is 80-85 ℃, and the heat preservation time is 10-15 min.
Further, in the step 3), heating to 60-65 ℃; in the step 5), the temperature is reduced to 38-40 ℃ and the material is discharged.
The third purpose of the invention is realized by adopting the following technical scheme:
the use of the above water-in-oil gel moisturizing composition for the preparation of a cosmetic. Cosmetic dosages include, but are not limited to, lotions, creams, and essences.
Compared with the prior art, the invention has the beneficial effects that:
(1) The moisturizing composition disclosed by the invention comprises the following main components: water, glycerin, butanediol, sodium hyaluronate, panthenol, lodestone, polyacryloyldimethyl taurinate ammonium, G57, polydimethylsiloxane, disteardimonium hectorite, isononyl isononanoate, hydrogenated polyisobutene, KSG-210, KF-6017, KF-6038, p-hydroxyacetophenone, 1,2-hexanediol. The moisturizing composition prepared by compounding the components has the characteristics of refreshing, no stickiness and easy spreading in the skin smearing process. After the skin moisturizing cream is applied, a thin oil film can be kept on the skin for a long time, and the water-locking and moisturizing capabilities of the skin are improved. The main technical raw materials are as follows:
KF-6017, KF-6038 and KSG-210 are compounded to be used as an emulsifier to prepare the skin feel which is high in stability, fresh, breathable and not sticky. The aqueous phase hydrogel prepared from the poly acryloyl dimethyl ammonium taurate, the G57 and the two thickening agents in a specific ratio can provide light and moist skin feel for a system and help the system to be stable. Three kinds of oil and fat of polydimethylsiloxane, isononyl isononanoate and hydrogenated polyisobutene are matched to form a layer of breathable film on the skin, so that the water locking and retaining capacity of the skin is improved. The moisturizing cream effectively improves the dry state of skin by matching glycerin, butanediol, sodium hyaluronate, panthenol, water-locking magnetite, micromolecules and macromolecules. The raw materials used in the gel-in-oil moisturizing composition are safe in components, do not contain toxic and harmful substances, and can be directly applied to the skin of all skin types.
Detailed Description
The present invention is further described below with reference to specific embodiments, and it should be noted that, without conflict, any combination between the embodiments or technical features described below may form a new embodiment.
The water-in-oil gel moisturizing composition comprises the following raw materials in percentage by weight: the balance of water, 3 to 5 percent of glycerin, 3 to 5 percent of butanediol, 0.02 to 0.1 percent of sodium hyaluronate, 0.5 to 1 percent of panthenol, 0.5 to 1 percent of magnetite, 0.6 to 1 percent of polyacryl dimethyl ammonium taurate, 0.4 to 0.7 percent of G57, 5 to 8 percent of polydimethylsiloxane, 0.2 to 0.5 percent of distearyl dimethyl ammonium hectorite, 4 to 6 percent of isononyl isononanoate, 1 to 3 percent of hydrogenated polyisobutene, 1 to 3 percent of KSG-210, 2 to 3 percent of KF-6017, 0.3 to 0.8 percent of KF-6038, 0.3 to 0.5 percent of p-hydroxyacetophenone and 0.4 to 0.6 percent of 1,2-hexanediol.
The functions and functions of the components are as follows:
the chemical name of glycerin is glycerol, which is a colorless, odorless, transparent and viscous liquid and is the most traditional moisturizing component of cosmetics. It has strong water absorption, and can moisturize skin by absorbing moisture in air, and also help skin lock moisture and prevent skin moisture from volatilizing.
Butanediol is a colorless and odorless transparent liquid, and has the characteristics of small irritation, refreshing skin feel and the like. Is often used as a humectant and solvent in cosmetics. The skin care product helps the skin to achieve the effects of moisturizing and moistening by adsorbing moisture and preventing the skin from losing. Meanwhile, the polyol also has the capability of inhibiting the growth of microorganisms and is often used as a preservative synergist.
Sodium hyaluronate is linear high molecular mucopolysaccharide, which is formed by repeating and connecting disaccharide units consisting of glucuronic acid and N-acetylglucosamine. The sodium hyaluronate can stay on the surface of the skin to form a polymer film, so that the polymer film has a sealing effect and can reduce the water loss of the skin to play a moisturizing effect. Sodium hyaluronate has a polysaccharide structure, and can combine water molecules through the action of hydrogen bonds to play a water replenishing effect. Is popular among people as a natural moisturizing factor.
Panthenol is a derivative of vitamin B5, also known as provitamin B5. It is a colorless, transparent, viscous paste with a slight characteristic odor. Panthenol has moisturizing, barrier improving, soothing, and healing effects in skin care products.
The water-locking magnet compound component comprises saccharide isomerate, water, citric acid and sodium citrate. The water-locking magnetite is an active ingredient of natural source, and the unique composition is very similar to carbohydrate in human skin. Therefore, the hydration degree and the water retention degree of the horny layer can be improved in a short time, and simultaneously, better hydration of epidermal cells can be facilitated. Has the functions of deeply moisturizing and improving skin barrier.
Polyacryloyldimethyltauric acid ammonium is a polymer based on sulfonated, lightly crosslinked acrylic acid, does not require neutralization and readily swells in cold water. As a thickener in cosmetics to help stabilize the formulation system. The excellent skin feeling experience has the characteristics of smoothness, lightness, no stickiness, etc.
The G57 compound component is sodium polyacrylate, C18-21 alkyl and tridecyl polyether-6. G57 is a high active content polymer dispersion. The emulsion stabilizer and the thickener are commonly used in cosmetics and can endow cream with light, refreshing, silky, non-sticky and satin-like skin feeling experience. Various conventional systems are suitable.
The chemical state of the polydimethylsiloxane is the dimethyl silicone oil, according to the difference of relative molecular mass, the appearance of the polydimethylsiloxane is from colorless and transparent volatile liquid to extremely high-viscosity liquid or silica gel, and the polydimethylsiloxane is tasteless, high in transparency, heat-resistant, cold-resistant, small in viscosity change along with temperature, waterproof and small in surface tension, and the dimethyl silicone oil is nontoxic and tasteless, and has physiological inertia and good chemical stability.
The disteardimonium hectorite has excellent thickening, dispersing and adsorbing capacity. The emulsion is often used as a thickening suspending agent in cosmetics, and can improve the rheological property and stability of the paste. Is mainly applied to a water-in-oil system.
Isononyl isononanoate is also known as synthetic silk oil. The unique multi-methyl branched chain structure endows the soft, silky and extremely soft hand feeling. Isononyl isononanoate as a fat-imparting agent can provide skin with a moist feeling, but does not give a greasy feeling after use. Has excellent compatibility and dispersibility, and can solve the problem that silicone oil is incompatible in a formula.
Hydrogenated polyisobutenes, also known as synthetic squalane, are colorless liquids with a slightly characteristic odor. It has the similar property with natural squalane and high cost performance. The hydrogenated polyisobutene has the characteristics of strong air permeability, moisture retention, moistening and the like.
The KSG-210 compound component comprises polydimethylsiloxane, polydimethylsiloxane PEG-10/15 cross-linked polymer, dipropylene glycol, sodium citrate and tocopherol (vitamin E). KSG-210 is a silicone elastomer with emulsifying capabilities that imparts a superior powder-like feel to the formulation.
KF-6017, INCI name: PEG-10 polydimethylsiloxane. The modified organic silicone oil containing polyoxyethylene groups in the molecules has excellent emulsifying capacity. Can prepare a fresh and stable W/Si system product.
KF-6038 compound component is lauryl PEG-9 dimethyl silicone ethyl dimethyl silicone, tocopherol (vitamin E). The modified organic silicone oil containing polyoxyethylene groups in the molecules has excellent emulsifying capacity. Can prepare a fresh and stable W/Si system product.
The p-hydroxyacetophenone is used as a preservative promoter and a chelating agent in cosmetics, has multiple effects of oxidation resistance, irritation resistance and the like, is effective to fungi, has strong killing capability to aspergillus niger, has an inhibiting effect on pseudomonas aeruginosa, is resistant to acid, alkali and high temperature, promotes the effects of various preservatives, has good compatibility with various cosmetic components, and can be widely used in cosmetics.
1,2-hexanediol, a diol, is a rapidly volatile solvent, is completely soluble in water, is used as an antibacterial agent, has a good antibacterial effect, and can also be used as a defoaming agent in the production process. Is mild to skin and has good safety performance.
Examples 1 to 3 and comparative examples 1 to 2
TABLE 1 formulation of materials of examples 1-3 and comparative examples 1-2
The preparation method of the gel-in-oil moisturizing composition comprises the following steps:
1) The raw materials are respectively divided into A phases: water, glycerol, butanediol, sodium hyaluronate, ammonium polyacryloyldimethyl taurate, G57; the phase B is as follows: p-hydroxyacetophenone, 1,2-hexanediol; the phase C is as follows: panthenol and Magnetitum; the phase D is as follows: polydimethylsiloxane, disteardimonium hectorite, isononyl isononanoate, hydrogenated polyisobutene, KSG-210, KF-6017, KF-6038; the phase E is as follows: an aromatizing agent;
2) Adding the A-phase raw material into an emulsifying pot, stirring, heating to 80-85 ℃, stirring, homogenizing until the material is uniform, and keeping the temperature for 10-15 minutes.
3) Weighing the components of the raw material of the phase B in a container, heating to 60-65 ℃, adding the components into the phase A after complete dissolution, and stirring uniformly. Stirring and cooling are started.
4) And (3) adding the C-phase components when the temperature of the emulsifying pot is reduced to 45 ℃ by stirring, and uniformly stirring to obtain the aqueous phase gel consisting of the A phase, the B phase and the C phase.
5) Weighing the components of the phase D raw material, and stirring and homogenizing in an oil phase pot until the material body is uniform. Adding phase D to step 4 to form an aqueous gel. Slowly adding the D phase into the water phase gel under rapid stirring, and stirring for 10-15 minutes at 50r/min after the D phase is completely added. Finally, E is added and stirring is continued for 5-10 minutes. Cooling to 40-38 deg.C, filtering and discharging.
Performance testing
1. Skin feel test
40 female volunteers of 25-45 year-old dry skin type were recruited, 10 testers were randomized per sample, and blind tests were performed on examples and comparative examples, which were tested 7 times in parallel per example and comparative example. After cleaning the face of a tester each time, 0.6g of the product is smeared on the face, and the product is scored for 1-10 minutes according to experience feeling, wherein evaluation items comprise spreadability, sticky feeling and moist feeling. And finally, taking the average value of each group by removing the highest score and the lowest score according to the scoring standard, wherein the higher the score is, the better the satisfaction is. Specific data are shown in table 1.
Table 1 experience data of skin feel of each group
| Number of groups | Spreadability | Sticky feeling | Moistening sensation |
| Example 1 | 9.3 | 8.7 | 9.0 |
| Example 2 | 8.0 | 8.5 | 8.2 |
| Example 3 | 8.2 | 8.6 | 8.3 |
| Comparative example 1 | 7.4 | 6.2 | 8.2 |
As shown in table 1, the skin feel score was highest among three dimensions of spreadability, sticky feel and moist feel in example 1, i.e., the overall skin feel was the best. Compared with the comparative example 1, the skin feeling of the gel-in-oil moisturizing composition prepared by the organic silicon emulsifier is better, and the oil is preferably selected for the gel-in-oil system.
2. Test of moisturizing Effect
The skin moisture content and the transdermal water loss were measured using a skin moisture test probe Corneometer CM 825 from CK, germany under (25. + -.1) ℃ C. And 65%. + -. 5% relative humidity. 10 female volunteers 25-45 years old were recruited, 0.6g of the product was applied to the face after cleaning the face, and the skin moisture content was tested 30 minutes, 2 hours, 4 hours later.
TABLE 2 moisture content of skin after 30min, 2h, 4h of spread product
As can be seen from Table 2, the products of examples 1-3 had higher skin moisture content after being applied for 30min, 2h and 4h than comparative example 1, indicating that the products of examples 1-3 had better moisturizing performance than comparative example 1.
The above embodiments are only preferred embodiments of the present invention, and the protection scope of the present invention is not limited thereby, and any insubstantial changes and substitutions made by those skilled in the art based on the present invention are within the protection scope of the present invention.
Claims (10)
1. The water-in-oil gel moisturizing composition is characterized by comprising the following raw materials in percentage by weight: 3 to 5 percent of glycerin, 3 to 5 percent of butanediol, 0.02 to 0.1 percent of sodium hyaluronate, 0.5 to 1 percent of panthenol, 0.5 to 1 percent of water-locking magnetite, 0.6 to 1 percent of polyacryloyldimethyl ammonium taurate, 0.4 to 0.7 percent of G, 5 to 8 percent of polydimethylsiloxane, 0.2 to 0.5 percent of disteardimonium hectorite, 4 to 6 percent of isononyl isononanoate, 1 to 3 percent of hydrogenated polyisobutene, 1 to 3 percent of KSG-210, 2 to 3 percent of KF-6017, 0.3 to 0.8 percent of KF-6038, 0.3 to 0.5 percent of p-hydroxyacetophenone, 0.4 to 0.6 percent of 1,2-hexanediol and the balance of water.
2. The water-in-oil gel moisturizing composition of claim 1, comprising the following raw materials in weight percent: 5% of glycerin, 3% of butanediol, 0.04% of sodium hyaluronate, 0.8% of panthenol, 0.8% of Magnetitum, 1% of polyacryloyldimethyl taurate, 0.5% of G57, 6.5% of polydimethylsiloxane, 0.3% of distearyl dimethyl ammonium hectorite, 5% of isononyl isononanoate, 2% of hydrogenated polyisobutene, KSG-2102.5%, 2.5% of KF-6017, 0.5% of KF-6038, 0.5% of p-hydroxyacetophenone, 0.5% of 1,2-hexanediol, and the balance of water.
3. The water-in-oil gel moisturizing composition of claim 1 or 2, further comprising 0.02 to 0.05% of an aroma-imparting agent.
4. The water-in-oil gel moisturizing composition of claim 1 or 2, further comprising 0.03% of an aroma-imparting agent.
5. A method of preparing a water-in-oil gel moisturizing composition of any of claims 1 to 4, comprising the steps of:
1) Respectively dividing each raw material into an A phase, a B phase and a C phase; wherein, the phase A is: water, glycerin, butanediol, sodium hyaluronate, ammonium polyacryloyldimethyl taurate, G57; the phase B is as follows: p-hydroxyacetophenone, 1,2-hexanediol; the phase C is as follows: panthenol and water-locking magnetite; the phase D is as follows: polydimethylsiloxane, disteardimonium hectorite, isononyl isononanoate, hydrogenated polyisobutene, KSG-210, KF-6017, KF-6038;
2) Adding the components of the phase A raw material into an emulsifying pot, stirring, heating, stirring and homogenizing until the material body is uniform, and keeping the temperature;
3) Weighing the components of the phase B raw material in a container, heating, adding the B raw material into the phase A after complete dissolution, uniformly stirring, and starting stirring and cooling;
4) Stirring and cooling the mixture in an emulsifying pot, adding the C-phase components, and uniformly stirring to obtain a water-phase gel consisting of the A-phase, the B-phase and the C-phase;
5) Weighing all the components of the D-phase raw material, placing the components in an oil phase pot, stirring and homogenizing until the material body is uniform; adding the phase D into the water-phase gel obtained in the step 4), stirring and mixing, cooling, filtering and discharging to obtain the water-in-oil gel moisturizing composition.
6. The method of preparing a water-in-oil gel moisturizing composition of claim 5, wherein the raw materials of the water-in-oil gel moisturizing composition further comprise an E phase, wherein the E phase is an aromatizer; and 5) adding the aqueous phase gel into the phase D, uniformly stirring, then adding the phase E, and uniformly stirring to obtain the water-in-oil gel moisturizing composition.
7. The method for preparing a water-in-oil gel moisturizing composition of claim 6, wherein the stirring time after the addition of phase E is 5 to 10min.
8. The method for preparing a water-in-oil gel moisturizing composition of claim 6, wherein in step 2), the heating temperature is 80-85 ℃ and the holding time is 10-15 min.
9. The method for preparing a water-in-oil gel moisturizing composition of claim 6, wherein in step 3), the temperature is raised to 60-65 ℃; in the step 5), the temperature is reduced to 38-40 ℃ and the material is discharged.
10. Use of the water-in-oil gel moisturizing composition of any of claims 1 to 4, wherein the water-in-oil gel moisturizing composition is used to prepare a cosmetic.
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