CN115737721A

CN115737721A - Prickly ash foot bath bag and preparation method thereof

Info

Publication number: CN115737721A
Application number: CN202211478900.8A
Authority: CN
Inventors: 何苗; 严政伟
Original assignee: Sichuan Jiaoao Food Technology Co ltd
Current assignee: Sichuan Jiaoao Food Technology Co ltd
Priority date: 2022-11-23
Filing date: 2022-11-23
Publication date: 2023-03-07

Abstract

The application discloses a pepper foot bath bag and a preparation method thereof, relates to the technical field of medical and health-care products, and aims to solve the technical problems of complex components and high cost of the existing foot bath bag. The foot bath bag for the peppers is composed of pepper powder, pepper leaf powder and pricklyash seed powder which are subjected to wall breaking treatment; wherein the mixing weight ratio of the pepper powder, the pepper leaf powder and the pricklyash seed powder is 2-4; the particle diameters of the pepper powder, the pepper leaf powder and the pepper powder are all below 100nm, and the wall breaking rate is at least more than 98%.

Description

Prickly ash foot bath bag and preparation method thereof

Technical Field

The application relates to the technical field of medical health-care products, in particular to a pepper foot bath bag and a preparation method thereof.

Background

Traditional Chinese medicine pedicure is a traditional Chinese medicine external treatment method which is guided by the basic theory of traditional Chinese medicine, and is used for acting on the meridians, acupuncture points and reflecting areas of the feet of a human body by one or more methods of massage, acupuncture, scraping, cupping, pasting, bathing and the like so as to adjust qi, blood and body fluids of the human body and viscera meridians and collaterals of the human body and achieve the purposes of disease prevention and health care. However, the existing foot bath powder is prepared by compounding dozens of traditional Chinese medicines, and has complex components, high cost and limited curative effect.

Therefore, a foot bath bag with simple components, high use safety and obvious effect is needed.

Disclosure of Invention

The application mainly aims to provide a pepper foot bath bag and a preparation method thereof, and aims to solve the technical problems of complex components and high cost of the existing foot bath bag.

In order to solve the above technical problem, an embodiment of the present application provides: a foot bath bag containing fructus Zanthoxyli comprises wall-broken fructus Zanthoxyli powder, folium Zanthoxyli powder and semen Zanthoxyli powder; wherein the mixing weight ratio of the pepper powder, the pepper leaf powder and the pricklyash seed powder is 2-4; the particle diameters of the pepper powder, the pepper leaf powder and the pepper powder are all below 100nm, and the wall breaking rate is at least more than 98%.

As some optional embodiments of the present application, the wall breaking process comprises the following steps:

respectively carrying out common crushing treatment on the peppers, the pepper leaves and the pricklyash seeds, and crushing to 30-45 meshes to respectively obtain first pepper powder, first pepper leaf powder and first pricklyash seed powder;

carrying out superfine grinding treatment on the first pepper powder, the first pepper leaf powder and the first pepper powder, and grinding to 30-60 mu m to obtain a second pepper powder, a second pepper leaf powder and a second pepper seed powder respectively;

performing ball milling and crushing treatment on the second pepper powder, the second pepper leaf powder and the second pepper powder to obtain a third pepper powder, a third pepper leaf powder and a third pepper powder, wherein the crushing treatment is less than 1000 nm;

and carrying out high-pressure homogenizing and crushing treatment on the third pepper powder, the third pepper leaf powder and the third pepper powder, and crushing to be less than 100nm to obtain a fourth pepper powder, a fourth pepper leaf powder and a fourth pepper powder.

As some optional embodiments of the present application, the treatment temperature of the micronization treatment is 30-40 ℃ and the treatment time is 4-5 hours.

As some optional embodiments of the present application, the treatment temperature of the ball milling and grinding treatment is 30-40 ℃, and the treatment time is 8-9 h.

As some optional embodiments of the present application, the treatment pressure of the high-pressure homogenizing and crushing treatment is 30-45 MPa, the treatment temperature is 30-40 ℃, the homogenizing times are 4-5 times, and the time for homogenizing each time is 25min.

As some optional embodiments of the application, when the foot bath bag is used, warm water with the temperature of 35-50 ℃ is added.

In order to solve the above technical problem, an embodiment of the present application further provides: a preparation method of the pepper foot bath bag comprises the following steps:

screening and obtaining pepper, pepper leaves and pepper seeds based on a preset screening standard;

respectively performing wall breaking treatment on the zanthoxylum, the zanthoxylum leaves and the zanthoxylum seeds to obtain zanthoxylum powder, zanthoxylum leaf powder and zanthoxylum seed powder;

mixing the pepper powder, the pepper leaf powder and the pricklyash seed powder according to a preset mixing weight ratio to obtain foot bath powder;

packaging the foot bath powder to obtain a first foot bath bag; and if the first foot bath bag meets the preset weight tolerance standard, successfully checking and accepting to obtain a finished product of the foot bath bag.

As some optional embodiments of this application, the broken wall processing is respectively carried out based on pricklyash peel, pricklyash leaf and pricklyash seed to obtain pricklyash peel powder, pricklyash leaf powder and pricklyash seed powder, including:

carrying out superfine grinding treatment on the first pepper powder, the first pepper leaf powder and the first prickly ash seed powder, and grinding to 30-60 mu m to obtain a second pepper powder, a second pepper leaf powder and a second prickly ash seed powder respectively;

and performing high-pressure homogenizing and crushing treatment on the third Chinese prickly ash powder, the third Chinese prickly ash leaf powder and the third prickly ash seed powder, and crushing the powder to be less than 100nm to obtain fourth Chinese prickly ash powder, fourth Chinese prickly ash leaf powder and fourth prickly ash seed powder.

As some optional embodiments of the present application, the foot bath powder is packaged to obtain a first foot bath bag; if the first foot bath bag meets the preset weight tolerance standard, the acceptance is successful, and a foot bath bag finished product is obtained, wherein the method comprises the following steps:

weighing the foot bath powder based on the target weight value of the finished foot bath bag product, and packaging to obtain a first foot bath bag;

weighing the first foot bath bag to obtain a weight value of the first foot bath bag;

if the weight value of the first foot bath bag meets the preset weight tolerance standard, the acceptance check is successful, and a finished product of the foot bath bag is obtained.

As some optional embodiments of the present application, the weight value of the finished foot bath bag satisfies the following relation:

X＝A+y

wherein X is expressed as a weight value of the finished footbath bag; a is expressed as a target weight value of the finished foot bath bag; y is a preset weight tolerance standard and takes the value of 0.2-1 g.

Compared with the prior art, the foot bath bag disclosed by the embodiment of the application is composed of the Chinese prickly ash powder, the Chinese prickly ash leaf powder and the pricklyash seed powder which are subjected to wall breaking treatment; wherein the mixing weight ratio of the pepper powder, the pepper leaf powder and the pricklyash seed powder is 2-4; the particle diameters of the pepper powder, the pepper leaf powder and the pricklyash seed powder are all below 100nm, and the wall breaking rate is at least more than 98%. It can be seen that the foot bath bag is simple in components and only comprises pepper powder, pepper leaf powder and pricklyash seed powder. Moreover, the pepper powder, the pepper leaf powder and the pricklyash seed powder are subjected to wall breaking treatment, and the failure of bioactive components caused by overheating can not occur in the treatment process, so that the medicinal property of the foot bath bag is improved. Secondly, particularly, the method of the embodiment of the application carries out wall breaking treatment on the pepper, the pepper leaves and the zanthoxylum seeds, so that the pepper, the pepper leaves and the zanthoxylum seeds are unpacked and then placed into a foot bath container when in use, and warm water with the temperature of 35-50 ℃ is added to dissolve out effective substances in the pepper powder, the pepper leaf powder and the zanthoxylum seed powder so as to achieve the expected effect; the foot bath bag does not need to be soaked or boiled by boiling water when in use like the existing foot bath bag, thereby effectively avoiding the accidents of scalding and the like, and greatly improving the use safety.

Drawings

FIG. 1 is a schematic flow diagram of a wall breaking process according to an embodiment of the present application;

fig. 2 is a schematic flow chart of preparation of the zanthoxylum bungeanum foot bath bag according to the embodiment of the application.

Detailed Description

It should be understood that the specific embodiments described herein are merely illustrative of and not restrictive on the broad application.

In daily life, people feel careless in diet and wear, so that the dampness in the body is too heavy and is yin pathogen, and the shoes have the characteristics of damaging yang qi, blocking qi activity, being sticky and lingering. In the field of traditional Chinese medicine, the foot is considered as the origin and termination point of the three yin and yang meridians of foot, and has close relationship with all viscera and meridians of the whole body. Therefore, the stimulation of feet can play the roles of adjusting the functions of viscera and strengthening physique. Traditional Chinese medicine pedicure is a traditional Chinese medicine external treatment method which is guided by the basic theory of traditional Chinese medicine, and is used for acting on the meridians, acupuncture points and reflecting areas of the feet of a human body by one or more methods of massage, acupuncture, scraping, cupping, pasting, bathing and the like so as to adjust qi, blood and body fluids of the human body and viscera meridians and collaterals of the human body and achieve the purposes of disease prevention and health care.

At present, most of the traditional Chinese medicine components in the market are directly ground and mixed for use, for example, the components of pepper, ginger, folium artemisiae argyi and the like are compounded to enhance the drug effect. However, the inventor researches and discovers that if the pepper can be properly treated during the initial treatment to ensure that the bioactive components are effective, and the pepper, the pepper leaves and the pricklyash seeds are mixed according to a special proportion, only the pepper, the pepper leaves and the pricklyash seeds are used as the components.

However, how to furthest retain effective bioactive components of the lavipeditum powder when the pericarpium zanthoxyli, the semen zanthoxyli and the folium zanthoxyli are crushed to prepare the lavipeditum powder is a problem which needs to be solved urgently at present. Thereby providing a footbath bag with simple components, good drug effect and higher use safety.

Based on this, the main solutions of the embodiments of the present application are:

a foot bath bag containing fructus Zanthoxyli comprises wall-broken fructus Zanthoxyli powder, folium Zanthoxyli powder and semen Zanthoxyli powder; wherein the mixing weight ratio of the pepper powder, the pepper leaf powder and the pricklyash seed powder is 2-4; the particle diameters of the pepper powder, the pepper leaf powder and the pricklyash seed powder are all below 100nm, and the wall breaking rate is at least more than 98%.

Researches show that the main components of the volatile oil in the peel of the pepper are limonene accounting for 25.10 percent of the total oil, 1, 8-cineole accounting for 21.98 percent of the total oil, myrcene accounting for 11.99 percent of the total oil, and the volatile oil also contains alpha-pinene, beta-pinene, sabinene, perillene, linalool, estragole and the like. The pericarp also contains vanilline, skimmianine, ruthenamine, and dehydroicilin. It has effect in resisting formation of experimental gastric ulcer in animals; the composition has bidirectional regulation effect on the small intestine of an animal in vitro, and is excited in a small dose and inhibited in a large dose; has analgesic and anti-inflammatory effects; the volatile oil has certain inhibiting and killing effects on 11 dermatophytes and 4 deep fungi, wherein the Microsporum lanuginosum and Trichophyton rubrum are most sensitive and can kill scabies and mites. Secondly, the zanthoxylum bungeanum maxim is used as an accessory drug of the zanthoxylum bungeanum maxim, is used as a seed of the zanthoxylum bungeanum maxim, and is bitter and cold in nature. It enters lung, kidney and bladder meridians. Has the functions of inducing diuresis to alleviate edema, descending qi and relieving asthma. It is suitable for edema, distention and fullness, cough and asthma due to phlegm and retained fluid. Furthermore, the pricklyash peel leaves contain a small amount of volatile oil and horse chestnut bark element dimethyl ether. The fruit contains volatile oil and pungent pepper extract. The volatile oil contains limonene, linalool and linalool acetate; it has effects of dispelling pathogenic wind and cold, invigorating stomach and expelling parasites, eliminating dampness and relieving diarrhea, promoting blood circulation and dredging channels, and can be used for treating traumatic injury, rheumatalgia, blood stasis pain, amenorrhea, hemoptysis, hematemesis, arthrolithiasis and parasitosis.

Therefore, in the specific application, the zanthoxylum bungeanum leaves and the zanthoxylum bungeanum seeds are subjected to wall breaking treatment instead of simple crushing treatment, so that the bioactive ingredients in the prepared foot bath bag are ensured to be effective, and the expected effects such as conditioning viscera or dispelling wind and removing dampness and the like are achieved after foot bath.

In a specific application, in order to achieve the above technical effect, as shown in fig. 1, in some embodiments of the present application, the wall breaking process includes the following steps:

and S01, respectively carrying out common crushing treatment on the peppers, the pepper leaves and the pricklyash seeds, and crushing to 30-45 meshes to respectively obtain first pepper powder, first pepper leaf powder and first pricklyash seed powder.

In specific application, in the common crushing treatment process, the inactivation of effective biological components in the pepper, the pepper leaves and the pepper seeds caused by excessive crushing is avoided.

And S02, carrying out superfine grinding treatment on the first pepper powder, the first pepper leaf powder and the first prickly ash seed powder, and grinding to 30-60 mu m to obtain a second pepper powder, a second pepper leaf powder and a second prickly ash seed powder respectively.

In specific application, the treatment temperature of the superfine grinding treatment is 30-40 ℃, and the treatment time is 4-5 h.

And S03, performing ball milling and crushing treatment on the second Chinese prickly ash powder, the second Chinese prickly ash leaf powder and the second prickly ash seed powder, and crushing the powder to be less than 1000nm to obtain third Chinese prickly ash powder, third Chinese prickly ash leaf powder and third prickly ash seed powder.

In the specific application, the treatment temperature of the ball milling and crushing treatment is 30-40 ℃, and the treatment time is 8-9 h.

And step S04, performing high-pressure homogenizing and crushing treatment on the third Chinese prickly ash powder, the third Chinese prickly ash leaf powder and the third prickly ash seed powder, and crushing the powder to be less than 100nm to obtain fourth Chinese prickly ash powder, fourth Chinese prickly ash leaf powder and fourth prickly ash seed powder.

In the specific application, the treatment pressure of the high-pressure homogenizing and crushing treatment is 30-45 Mpa, the treatment temperature is 30-40 ℃, the homogenizing times are 4-5 times, and the homogenizing time is 25min each time.

The existing pepper powder is generally crushed by a common machine, fiber substances in the pepper are difficult to crush, and a large amount of waste slag is obtained by crushing, so that the waste of raw materials is caused. The fiber substances in the paprika powder, the pepper leaf powder and the pricklyash seed powder obtained after the wall breaking treatment are crushed to the greatest extent, so that the obtained powder is fine and smooth, and the waste of resources is reduced when the powder is applied to health care or medicine. And by the wall breaking technology, the utilization rate of the pepper raw material is improved, the same effect can be achieved when the amount of the pepper raw material is less than or equal to that of the original formula, and raw materials can be saved by about 45-80%. Furthermore, the powder obtained by the wall breaking technology is directly put into warm water at 35-50 ℃ without being boiled or soaked by boiled water when in use; thereby improving the safety in the using process.

In order to solve the above technical problem, as shown in fig. 2, an embodiment of the present application further provides: a preparation method of the pepper foot bath bag comprises the following steps:

and S10, screening the pepper, the pepper leaves and the pepper seeds based on preset screening standards to obtain the raw materials of the foot bath bag.

In specific application, screening rules can be preset according to actual requirements, and pepper, pepper leaves and pepper seeds are respectively screened and respectively collected as required by the application, so that the subsequent preparation steps are facilitated. And after the pepper is collected, storing the pepper, the pepper leaves and the pepper seeds according to a preset storage management system respectively.

And S20, respectively performing wall breaking treatment on the peppers, the pepper leaves and the pricklyash seeds to obtain pepper powder, pepper leaf powder and pricklyash seed powder.

In specific application, the wall breaking treatment is respectively carried out on the basis of the zanthoxylum bungeanum, the zanthoxylum bungeanum leaves and the zanthoxylum bungeanum seeds to obtain the zanthoxylum bungeanum powder, the zanthoxylum bungeanum leaf powder and the zanthoxylum bungeanum seeds powder, and the wall breaking treatment comprises the following steps: and S01, respectively carrying out common crushing treatment on the peppers, the pepper leaves and the pricklyash seeds, and crushing to 30-45 meshes to respectively obtain first pepper powder, first pepper leaf powder and first pricklyash seed powder. Wherein, in the common crushing treatment process, the inactivation of effective biological components in the pepper, the pepper leaves and the pepper seeds caused by excessive crushing is avoided. And S02, carrying out superfine grinding treatment on the first pepper powder, the first pepper leaf powder and the first prickly ash seed powder, and grinding to 30-60 mu m to obtain a second pepper powder, a second pepper leaf powder and a second prickly ash seed powder respectively. Wherein the treatment temperature of the superfine grinding treatment is 30-40 ℃, and the treatment time is 4-5 h. And S03, performing ball milling and crushing treatment on the second Chinese prickly ash powder, the second Chinese prickly ash leaf powder and the second prickly ash seed powder, and crushing the powder to be less than 1000nm to obtain third Chinese prickly ash powder, third Chinese prickly ash leaf powder and third prickly ash seed powder. Wherein the treatment temperature of the ball milling and crushing treatment is 30-40 ℃, and the treatment time is 8-9 h. And S04, performing high-pressure homogenizing and crushing treatment on the third Chinese prickly ash powder, the third Chinese prickly ash leaf powder and the third prickly ash seed powder, and crushing to be less than 100nm to obtain fourth Chinese prickly ash powder, fourth Chinese prickly ash leaf powder and fourth prickly ash seed powder. Wherein the treatment pressure of the high-pressure homogenizing and crushing treatment is 30-45 Mpa, the treatment temperature is 30-40 ℃, the homogenizing times are 4-5 times, and the homogenizing time is 25min each time.

In specific application, the pepper powder, the pepper leaf powder and the pricklyash seed powder obtained after the wall breaking treatment are respectively stored by using sealed bags.

The fiber substances in the paprika powder, the pepper leaf powder and the pricklyash seed powder obtained after the wall breaking treatment are crushed to the maximum extent, so that the obtained powder is fine and smooth, and the waste of resources is reduced when the powder is applied to health care or medicine. Moreover, by the wall breaking technology, the utilization rate of the pepper raw material is improved, the same effect can be achieved when the amount of the pepper raw material is less than or equal to that of the original formula, and raw materials can be saved by about 45-80%.

And S30, mixing the pepper powder, the pepper leaf powder and the pricklyash seed powder according to a preset mixing weight ratio to obtain the foot bath powder.

In the specific application, the mixing weight ratio of the pepper powder, the pepper leaf powder and the pricklyash seed powder is 2-4; the particle diameters of the pepper powder, the pepper leaf powder and the pepper powder are all below 100nm, and the wall breaking rate is at least more than 98%.

When the powder foot bath bag obtained by the wall breaking technology is used, boiling water is not needed for decoction or soaking, and the powder foot bath bag is directly placed in warm water at 35-50 ℃; thereby improving the safety in the using process.

Step S40, packaging the foot bath powder to obtain a first foot bath bag; and if the first foot bath bag meets the preset weight tolerance standard, successfully checking and accepting to obtain a finished product of the foot bath bag.

In specific application, the foot bath powder is packaged to obtain a first foot bath bag; if the first foot bath bag meets the preset weight tolerance standard, the acceptance is successful, and a foot bath bag finished product is obtained, wherein the method comprises the following steps: weighing the foot bath powder based on the target weight value of the finished foot bath bag product, and packaging to obtain a first foot bath bag; weighing the first foot bath bag to obtain a weight value of the first foot bath bag; if the weight value of the first foot bath bag meets the preset weight tolerance standard, the acceptance is successful, and a finished product of the foot bath bag is obtained.

Wherein, the weight value of the finished product of the foot bath bag satisfies the following relational expression:

X＝A+y

wherein X represents the weight value of the finished foot bath bag; a is expressed as a target weight value of the finished foot bath bag; y is expressed as a preset weight tolerance standard and is 0.2-1 g.

In specific application, the foot bath bag is divided into an inner package and an outer package when being packaged, wherein:

the internal packaging means that proportioned powder is put into a hopper of a full-automatic three-edge packaging machine, the packaging machine automatically packages, and the finished product of the powder package needs to be subjected to first piece weight measurement (positive tolerance is 0.2-1 g) and appearance sealing inspection.

The external packaging means that the material bag and the parchment paper are filled into the bottom cover according to requirements, the upper cover is covered to confirm that the quantity of the filled materials cannot be wrong; if 6 small bags of foot bath bags are put into one box, namely the dosage of 6 times of foot bath can be put according to actual requirements, the 6 small bags are only exemplified in the application.

In the specific application, after the inner package and the outer package are completed, the automatic flow code spraying equipment is used for printing codes, whether the code spraying is correct and clear is checked, and then the finished box of the foot bath bag is obtained.

And (3) putting the finished product box into a POF film bag and packaging by using a sealing machine, wherein the sealing is required to be free of damage, the wrinkle-free surface is clean and free of oil stains, and unqualified products are required to be removed in time when being found. And (4) putting the packaged POF film bag into a transmission belt of a thermal shrinkage film machine, and inspecting whether the appearance of a finished product is flat, free of wrinkles and damage at an outlet. If the two codes are consistent, manual box sealing and code printing processes are carried out, the sealing requirement is flat, no wrinkles exist, and the code printing is correct and clear.

After the above process is completed, the product can be put into a warehouse for standby after passing quality inspection by a quality inspector.

The foot bath bag and the preparation method thereof are described in detail with reference to specific examples as follows:

example 1

Step 1, screening and obtaining pepper, pepper leaves and pepper seeds based on preset screening standards;

step 2, respectively carrying out common crushing treatment on the peppers, the pepper leaves and the pricklyash seeds, and crushing the peppers, the pepper leaves and the pricklyash seeds into 32 meshes to respectively obtain first pepper powder, first pepper leaf powder and first pricklyash seed powder; carrying out superfine grinding treatment on the first pepper powder, the first pepper leaf powder and the first pepper seed powder, and grinding to 55 mu m to respectively obtain a second pepper powder, a second pepper leaf powder and a second pepper seed powder; performing ball milling and crushing treatment on the second Chinese prickly ash powder, the second Chinese prickly ash leaf powder and the second prickly ash seed powder, and crushing the powder to be less than 1000nm to obtain third Chinese prickly ash powder, third Chinese prickly ash leaf powder and third prickly ash seed powder; and performing high-pressure homogenizing and crushing treatment on the third Chinese prickly ash powder, the third Chinese prickly ash leaf powder and the third prickly ash seed powder, and crushing the powder to be less than 100nm to obtain fourth Chinese prickly ash powder, fourth Chinese prickly ash leaf powder and fourth prickly ash seed powder.

Step 3, mixing the fourth pepper powder, the fourth pepper leaf powder and the fourth pepper powder according to a preset mixing weight ratio to obtain foot bath powder; wherein the mixing weight ratio of the fourth pepper powder, the fourth pepper leaf powder and the fourth pepper powder is 2;

step 4, weighing the foot bath powder based on the target weight value of the finished foot bath bag product, and packaging to obtain a first foot bath bag; weighing the first foot bath bag to obtain a weight value of the first foot bath bag; if the weight value of the first foot bath bag meets the preset weight tolerance standard of 0.2-1g, the acceptance is successful, and a finished product of the foot bath bag is obtained.

Example 2

step 2, respectively carrying out common crushing treatment on the peppers, the pepper leaves and the pricklyash seeds, and crushing to 37 meshes to respectively obtain first pepper powder, first pepper leaf powder and first pricklyash seed powder; carrying out superfine grinding treatment on the first pepper powder, the first pepper leaf powder and the first pepper seed powder, and grinding to 40 mu m to obtain a second pepper powder, a second pepper leaf powder and a second pepper seed powder respectively; performing ball milling and crushing treatment on the second pepper powder, the second pepper leaf powder and the second pepper powder to obtain a third pepper powder, a third pepper leaf powder and a third pepper powder, wherein the crushing treatment is less than 1000 nm; and carrying out high-pressure homogenizing and crushing treatment on the third pepper powder, the third pepper leaf powder and the third pepper powder, and crushing to be less than 100nm to obtain a fourth pepper powder, a fourth pepper leaf powder and a fourth pepper powder.

Step 3, mixing the fourth pepper powder, the fourth pepper leaf powder and the fourth pepper powder according to a preset mixing weight ratio to obtain foot bath powder; wherein the mixing weight ratio of the fourth pepper powder, the fourth pepper leaf powder and the fourth pepper powder is 3;

Example 3

step 2, respectively carrying out common crushing treatment on the peppers, the pepper leaves and the pricklyash seeds, and crushing to 43 meshes to respectively obtain first pepper powder, first pepper leaf powder and first pricklyash seed powder; carrying out superfine grinding treatment on the first pepper powder, the first pepper leaf powder and the first pepper seed powder, and grinding to 31 mu m to obtain a second pepper powder, a second pepper leaf powder and a second pepper seed powder respectively; performing ball milling and crushing treatment on the second pepper powder, the second pepper leaf powder and the second pepper powder to obtain a third pepper powder, a third pepper leaf powder and a third pepper powder, wherein the crushing treatment is less than 1000 nm; and carrying out high-pressure homogenizing and crushing treatment on the third pepper powder, the third pepper leaf powder and the third pepper powder, and crushing to be less than 100nm to obtain a fourth pepper powder, a fourth pepper leaf powder and a fourth pepper powder.

Comparative example 1

step 2, respectively carrying out common crushing treatment on the peppers, the pepper leaves and the pepper seeds, and crushing to 40 meshes to respectively obtain first pepper powder, first pepper leaf powder and first pepper seed powder; .

Step 3, mixing the first pepper powder, the first pepper leaf powder and the first pepper seed powder according to a preset mixing weight ratio to obtain foot bath powder; wherein the mixing weight ratio of the first pepper powder, the first pepper leaf powder and the first pepper seed powder is 3;

Experimental example 1

100 patients with fever (the main clinical manifestations are fever (the body temperature is 38.4-41.3 ℃), aversion to cold, aversion to wind, no sweat, polydipsia, floating pulse, body pain in middle and old aged patients, soreness of limbs, cough and pharyngalgia in children cases), 50 men and 50 women; mean age (27 ± 3) years.

The patients are divided into 2 groups, and the age, sex, etiology, course of disease, clinical manifestation and difference of fever degree of the 2 groups of patients have no significant meaning (P is more than 0.05) and are comparable. Wherein, the patients in the experimental example group are treated by transfusion, anti-infection, support and the like according to the medical advice according to the requirements of the illness state, and are subjected to foot bath by using the foot bath bag prepared in the embodiment 3; the patients in the comparative example group are treated according to medical advice, infusion, infection resistance, support and the like according to the disease condition, and are subjected to foot bath by using the foot bath bag prepared in the comparative example 1.

The specific foot bath method comprises the following steps: putting a foot bath bag into warm water with the temperature of 35-50 ℃ to carry out foot bath; the water consumption for foot bath is only required when the water level reaches the position of the shank; the lasting time of each foot bath is determined according to the physique and the illness state of the patient, the physique is strong, the obese patient performs foot bath for more than 20 minutes until the forehead slightly generates heat and perspires, and the emaciation and infirm patient performs foot bath for more than 10 minutes and the forehead slightly sweats; generally, each patient takes foot bath once a day, and the patient with body temperature not obviously lowered after sweating of individual foot bath can take foot bath for the second time the next day, and the foot bath time is properly prolonged, and the sweat amount is increased. Before operation, the aim of foot bath is explained for patients and family members, cooperation is achieved, a door window is closed to avoid wind, and the patients are encouraged to drink 300-1000 mL of warm boiled water in the foot bath process to promote forehead sweating; when the patient feels dysphoria with feverish sensation, the forehead is applied with cold towel and the replacement is frequently carried out, so as to relieve the uncomfortable feeling of the head. After the foot bath is finished, sweat is wiped off by a dry towel in time, the patient can change clothes, lie in bed for rest, keep out wind and keep warm, and measure the body temperature again after 1 hour, so that the patient is encouraged to drink warm boiled water more to supplement body fluid.

And (3) evaluating the curative effect: the treatment effect of 2 patients was evaluated in 72 hours. The body temperature is reduced to below 37.5 ℃, repeated fever, aversion to cold, aversion to wind, headache, sore throat, body pain and limb ache can not disappear within 72 hours, and cough can be cured; the body temperature is reduced to below 37.5 ℃, repeated fever, aversion to cold, aversion to wind, headache, sore throat, body pain and limb ache are not caused in 72 hours, and the cough is relieved obviously; the body temperature did not drop or increased, or fever was repeated within 72 hours, and other symptoms were not relieved and were ineffective. The efficacy of 2 groups was compared and is shown in table 1 below.

Table 1:

group of	Number of examples	Recovery method	Show effect	Invalidation	Total effective
						Group of embodiments	50	36	12	2	96％
Comparative example group	50	23	19	8	84％

From the above table, the foot bath bag provided by the scheme of the application has a better curative effect on the patient with exogenous fever.

Experimental example 2

The specific components in the foot bath bag described in the present application were analyzed using a headspace solid phase microextraction-gas chromatography-mass spectrometry detection method.

The experimental method is as follows: a65 mu mPDMS/DVB extraction fiber head is selected, the sampling amount is 0.6g, the extraction temperature is 60 ℃, the extraction time is 15min, and the desorption time is 3min. GC conditions were as follows: HP-5MS quartz capillary column (30 m × 0.25mm,0.25 μm); carrier gas: high-purity He; flow rate: 0.8mL/min; sample inlet temperature: 230 ℃; temperature rising procedure: heating to 230 ℃ at a speed of 10 ℃/min from 50 ℃, and keeping for 3min. MS conditions: an EI source; the ion source temperature is 230 ℃; ionization voltage 70eV; the temperature of a four-level bar is 150 ℃; the scanning mass range is 35-550m/z.

The foot bath bag mainly comprises the components of pepper powder, pepper leaf powder and pricklyash seed powder, so that the foot bath bag contains a large amount of linalool and limonene. Linalool (Linalool) is also called Linalool, galois, linalool and the like, has strong and sweet wood green smell, is similar to the fragrance of rosewood, is more similar to the green fragrance of green tea just coming out of a furnace, not only has the fragrance of lilac, lily of the valley and roses, but also has the fragrance of costus and fruits, is soft in fragrance, is slightly raised and well-developed, is not very durable, and can eliminate indoor uncomfortable smell. Linalool is a terpene compound, and has good antibacterial activity against Escherichia coli, proteus, campylobacter enteronitis, staphylococcus, saccharomyces cerevisiae, micrococcus albus, aspergillus niger, agar, etc. The application of linalool to white mice in experimental models has been reported since ancient times in foreign folks, and the results of the drug administration of linalool to white mice indicate that the central nervous system including sleep, anticonvulsant and hypothermia has the phenomenon of dose-dependent increase. In addition, linalool vapor affects the brain through olfaction, has significant anxiolytic properties, and unlike anxiolytic drugs, linalool acts systemically. Linalool and its content are key to the bath lotion's diaphoresis and exterior syndrome relieving (fever, convulsion, bacterial infection are western medicine symptoms corresponding to the common cold syndrome due to wind-cold in traditional Chinese medicine).

The Chinese prickly ash has the functions of warming the middle-jiao and relieving pain; it has the actions of removing dampness, stopping diarrhea, killing parasites and relieving itching, and is mainly indicated for abdominal cold pain, ascarid abdominal pain, vomiting and diarrhea, cough and cough due to lung cold, toothache due to dental caries, pruritus vulvae, leukorrhagia, eczema and skin pruritus due to deficiency-cold of spleen and stomach. The main component of the volatile oil in the peel of the pricklyash peel is limonene (limonene) accounting for 25.10 percent of the total oil quantity, and the volatile oil of the fruit of the pricklyash peel accounts for 7.30 percent. From the above disclosure, limonene and its content are very important for bath liquid to exert the effects of inducing sweat and relieving exterior syndrome (cough and asthma are western medicine symptoms corresponding to the wind-cold type common cold in traditional Chinese medicine).

The foot bath packs prepared in examples 1 to 3 and comparative example 1, in which linalool and limonene contents are as shown in table 2 below, were used.

Table 2:

examples	Example 1	Example 2	Example 3	Comparative example 1
					Linalool content	0.93	0.91	0.96	0.40
Limonene content	0.35	0.38	0.37	0.08

It can be seen that the linalool and limonene content in the foot bath bag prepared by the wall-breaking method is obviously higher than that in the foot bath bag obtained by ordinary crushing. That is to say, according to the application, the zanthoxylum bungeanum leaves and the zanthoxylum bungeanum seeds are subjected to wall breaking treatment instead of simple crushing treatment, so that the biological active ingredients in the prepared foot bath bag are ensured to be effective, and the expected effects such as viscera conditioning or wind dispelling, dampness removing and the like are achieved after foot bath.

The above description is only a preferred embodiment of the present application, and not intended to limit the scope of the present application, and all the equivalent structures or equivalent processes that can be directly or indirectly applied to other related technical fields by using the contents of the specification and the drawings of the present application are also included in the scope of the present application.

Claims

1. A foot bath bag with pepper is characterized in that the foot bath bag is composed of pepper powder, pepper leaf powder and pricklyash seed powder which are subjected to wall breaking treatment; wherein the mixing weight ratio of the pepper powder, the pepper leaf powder and the pricklyash seed powder is 2-4; the particle diameters of the pepper powder, the pepper leaf powder and the pepper powder are all below 100nm, and the wall breaking rate is at least more than 98%.

2. The pepper foot bath bag according to claim 1, wherein the wall breaking treatment comprises the following steps:

respectively carrying out common crushing treatment on the peppers, the pepper leaves and the pepper seeds, and crushing to 30-45 meshes to respectively obtain first pepper powder, first pepper leaf powder and first pepper seed powder;

3. The pepper foot bath bag according to claim 2, wherein the superfine grinding treatment is carried out at the treatment temperature of 30-40 ℃ for 4-5 h.

4. The pepper foot bath bag according to claim 2, wherein the ball milling and crushing treatment is carried out at a temperature of 30-40 ℃ for 8-9 h.

5. The pepper foot bath bag according to claim 2, wherein the high-pressure homogenizing and crushing treatment is carried out at a treatment pressure of 30-45 Mpa, a treatment temperature of 30-40 ℃ and a homogenizing time of 4-5 times, and each homogenizing time is 25min.

6. The pepper foot bath bag according to any one of claims 1-5, wherein when in use, warm water at 35-50 ℃ is added.

7. A preparation method of the pepper foot bath bag as defined in any one of claims 1-5, which is characterized by comprising the following steps:

8. The preparation method of the pepper foot bath bag according to claim 7, wherein the wall breaking treatment is performed on the pepper, the pepper leaves and the zanthoxylum seeds respectively to obtain pepper powder, pepper leaf powder and zanthoxylum seed powder, and comprises the following steps:

9. The preparation method of the pepper foot bath bag according to claim 7, wherein the foot bath powder is packaged to obtain a first foot bath bag; if the first foot bath bag meets the preset weight tolerance standard, the acceptance is successful, and a foot bath bag finished product is obtained, wherein the method comprises the following steps:

weighing the foot bath powder based on a target weight value of a finished foot bath bag product, and packaging to obtain a first foot bath bag;

10. The preparation method of the wind-dispelling and dehumidifying foot bath bag according to claim 9, wherein the weight value of the finished product of the foot bath bag satisfies the following relational expression:

X＝A+y

wherein X is expressed as a weight value of the finished footbath bag; a is expressed as a target weight value of the finished foot bath bag; y is expressed as a preset weight tolerance standard and is 0.2-1 g.