CN115721757A - Rattan aromatherapy liquid base material and rattan aromatherapy liquid - Google Patents
Rattan aromatherapy liquid base material and rattan aromatherapy liquid Download PDFInfo
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- CN115721757A CN115721757A CN202211659832.5A CN202211659832A CN115721757A CN 115721757 A CN115721757 A CN 115721757A CN 202211659832 A CN202211659832 A CN 202211659832A CN 115721757 A CN115721757 A CN 115721757A
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Abstract
The invention relates to a rattan aromatherapy liquid base material and rattan aromatherapy liquid, wherein the rattan aromatherapy liquid base material comprises the following components in percentage by mass: 98.0-99.9% of diluent component and 0.1-2% of special component, wherein the diluent component comprises the following components in percentage by mass: ISOPAR L10-90%, ISOPAR M10-90%; the special component comprises the following components in percentage by mass: 0.1-0.5% of patchouli oil, 0.1-0.3% of ambergris root, 0.1-0.3% of methyl cedryl ketone and 0.1-0.3% of Shumuxiang. The rattan aromatherapy liquid base material and the rattan aromatherapy liquid provided by the invention can achieve the effect of accurately controlling the volatilization duration time, have consistent fragrance effect in the using process and have excellent market application prospect.
Description
Technical Field
The invention relates to the technical field of liquid aromatherapy, in particular to a rattan aromatherapy liquid base material and rattan aromatherapy liquid.
Background
The finished liquid rattan aromatherapy liquid product is a household product which is quite popular at present and has the effects of improving air, delighting body and mind and the like by diffusing liquid fragrance into the air through a certain carrier (white vine, willow/vine, reed and the like).
The rattan volatile liquid, also known as air fragrance, incense liquid and rattan perfume, is generally used for matching with rattan to prepare rattan aromatherapy, and can automatically absorb and uniformly emit fragrance for a long time by using the rattan as a fragrance-emitting medium. The traditional perfume generally disperses fragrance directly through air holes, the fragrance is quickly volatilized in the air, and the fragrance is not lasting, so the rattan champignon is a very popular environment-friendly air freshening article and furniture living article in countries such as Europe, america, japan and Korean.
The common liquid rattan incense finished product consists of the following parts:
1. a container: usually a glass bottle, a ceramic bottle or a plastic bottle;
2. rattan: usually white vine, willow/vine, reed, etc.;
3. aromatherapy essential oil: mixing natural essential oil or mixed essence;
4. the volatile liquid base material formula comprises: diluent component and special component.
DPM (dipropylene glycol monomethyl ether) is popular in the market as a rattan volatile liquid base material, and has irritation to respiratory tract, a low flash point of 47.9 ℃ and potential safety hazard. Patent application CN108969788A discloses a rattan incense liquid with lasting fragrance, which comprises the following components in percentage by weight: 3 to 5 percent of essential oil, 3 to 5 percent of polyvinyl alcohol, 3 to 5 percent of flavor fixative additive, 0.5 to 1.2 percent of methyl salicylate, 1.5 to 2 percent of trans-cinnamic aldehyde, 0.8 to 1.2 percent of antioxidant, 0.5 to 1 percent of preservative, and the balance of water, and the proposal adopts water as a base material, but has the following problems although the cost is low: (1) the using environment is limited, the system (2) is easy to freeze and solidify at low temperature and is easy to be polluted by microorganism and mildewed and smelly.
Disclosure of Invention
The invention aims to solve the potential safety hazard problem of the conventional rattan volatile liquid, and provides a rattan aromatherapy liquid base material which can control the volatilization rate of the liquid aromatherapy liquid and ensure that the fragrance can be kept consistent from initial duration to complete volatilization.
In the invention, the isoparaffin is used as a base solvent, and the method has the advantages of high purity, high flash point, little smell, good baking effect, low price and the like. And the product is stable in storage, does not delaminate or precipitate, and can exert the aromatherapy effect for a long time.
The inventor thinks that the technical core of the finished product of the liquid rattan incense is mainly concentrated on the essential oil and the volatile liquid base material, and the essential oil and the volatile liquid base material are well compatible with each other, so that a better effect can be exerted. The aromatherapy essential oil consists of various spices, about 3090 daily-use spices used globally have different volatilization speeds, so that the volatilization speeds of different aromatherapy essential oils are different, and the volatilization speed of the liquid rattan aromatherapy is directly influenced. The service life of the finished fragrant essential oil products with different fragrance types can be different under the condition of the same specification, volatile liquid base material and the same fragrance adding amount. Moreover, even if the same aromatherapy essential oil is prepared from different perfume components and components with small molecular weight, the volatilization speed is high; the components with large molecular weight and slow volatilization speed cause the problem of large difference of fragrance before and after the liquid rattan aromatherapy finished product.
Therefore, the invention develops a brand-new rattan aromatherapy liquid base material, develops rattan aromatherapy liquid with high matching degree based on the rattan aromatherapy liquid base material, and can independently select the service life of the liquid rattan aromatherapy finished product within 10 days to 100 days or even longer time by matching the base material formula with the aromatherapy essential oil. The two are matched, the volatilization duration of the liquid rattan aromatherapy finished product can reach the expected service life by easily adjusting the formula proportion, and the error of different batches does not exceed 3 days. And the aromatherapy essential oil is volatilized uniformly, and the front and back fragrance keeps consistent effect.
The specific scheme is as follows:
a rattan aromatherapy liquid base material comprises the following components in percentage by mass: 98.0-99.9 percent of diluent and 0.1-2 percent of special component, wherein,
the diluent comprises the following components in percentage by mass: ISOPAR L10-90%, ISOPAR M10-90%;
the special component comprises the following components in percentage by mass: 0.1-0.5% of patchouli oil, 0.1-0.3% of ambergris root, 0.1-0.3% of methyl cedryl ketone and 0.1-0.3% of Shumuxiang.
Further, the rattan aromatherapy liquid base material consists of 98.5-99.5% of diluent components and 0.5-1.5% of special component components according to mass percentage;
the diluent comprises 60-90% of ISOPAR L and 10-40% of ISOPAR M in percentage by mass, preferably 80-85% of ISOPAR L and 10-15% of ISOPAR M.
Further, the special component comprises the following components in percentage by mass: 0.2 to 0.4 percent of patchouli oil, 0.1 to 0.3 percent of ambergris root, 0.1 to 0.2 percent of methyl cedryl ketone and 0.1 to 0.2 percent of Shumuxiang.
The invention also provides a preparation method of the rattan aromatherapy liquid, the rattan aromatherapy liquid containing the rattan aromatherapy liquid base material is adopted, and the preparation method further comprises an aromatherapy essential oil component, 10g of the aromatherapy essential oil component volatilizes in a surface dish for 1-90 days at room temperature until the residual 5g of the aromatherapy essential oil component is left, the rattan aromatherapy liquid is obtained after the aromatherapy essential oil and the rattan aromatherapy liquid base material are mixed according to different proportions, and the regulation of the volatilization speed of the rattan aromatherapy liquid is realized by regulating and controlling the proportion of the aromatherapy essential oil component and the rattan aromatherapy liquid base material.
Further, the mass ratio of the essential oil component to the rattan aromatherapy liquid base material is 1-20%:80 to 90 percent.
Further, the essential oil for aromatherapy comprises the following components in percentage by mass:
further, the aromatherapy essential oil comprises the following components in percentage by mass:
the invention also provides the rattan aromatherapy liquid prepared by the preparation method of the rattan aromatherapy liquid, the rattan aromatherapy liquid is used at room temperature, the volatilization duration is 30-100 days, and the fragrance effects of the volatilization day 1 and the last 1 day are basically consistent.
The invention also discloses a liquid rattan aromatherapy finished product which comprises the rattan aromatherapy liquid base material or the rattan aromatherapy liquid prepared by the preparation method of the rattan aromatherapy liquid.
Has the advantages that:
the rattan aromatherapy liquid base material can regulate and control aromatherapy essential oils with different volatilization speeds to achieve the expected volatilization speed, for example, for slowly volatilizing aromatherapy essential oil and quickly volatilizing aromatherapy essential oil, rattan aromatherapy liquid products with the same volatilization speed can be achieved by adopting the rattan aromatherapy liquid base material with a proper proportion, which shows that the rattan aromatherapy liquid base material plays a decisive role in the volatilization speed of the whole rattan aromatherapy liquid product.
Secondly, the volatile liquid base material components ISOPAR L and ISOPAR M used by the product have the advantages of stable formula, no layering, no residue, high flash point, high purity, high flash point, small smell, good baking effect, low price and the like.
In addition, in the invention, by comparing 2 different aromatherapy essential oils and matching with the rattan aromatherapy liquid base material, different volatilization speeds can be achieved, for example, complete volatilization can be realized at room temperature for 30 days or 60 days respectively.
Furthermore, the rattan aromatherapy liquid base material can stabilize the lock-controlled fragrance, and the fragrance of the bottle opening for the first time is basically consistent with the fragrance of the fragrance to be completely released, wherein the basic consistency refers to the effect which is difficult to distinguish in the sense of fragrance tasters.
In a word, the rattan aromatherapy liquid base material system, the aromatherapy essential oil raw material system and the rattan aromatherapy liquid obtained by combining the rattan aromatherapy liquid base material system and the aromatherapy essential oil raw material system can achieve the effects of accurately controlling volatilization duration time, achieving expected service life and ensuring consistent fragrance.
Detailed Description
Preferred embodiments of the present invention will be described in more detail below. While the following describes preferred embodiments of the present invention, it should be understood that the present invention may be embodied in various forms and should not be limited by the embodiments set forth herein. The examples do not specify particular techniques or conditions, and are performed according to the techniques or conditions described in the literature in the art or according to the product specifications. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products commercially available. In the following examples, "%" means weight percent, unless otherwise specified.
The test methods used below included:
volatile base diluent component volatilization rate test:
test field: incense evaluation chamber with specification of 3m long, 3m wide and 2.7m high enclosed space
Test room temperature: 25 deg.C
Test materials: rattan material: reed pole
The number of the rattan: 5 root of Chinese goldthread
Length of exposed opening of the rattan: 10 cm
Volume of fragrance liquid: 100 ml of
The description criteria for the evaporation rate in the examples are: the test takes 10g of the material to volatilize in a watch glass at room temperature until 5g of the material remains, wherein the speed is fast within 1-30 days, the medium speed is medium within 30-60 days, and the slow speed is slow within more than 60 days.
EXAMPLE 1 study of volatilization Rate of base Material
In the rattan aromatherapy liquid base material, the main volatilization function is the diluent component, and the diluent components with different proportions are prepared and the volatilization speeds are shown in table 1.
TABLE 1 dilution composition volatilization speedometer
| Volatile liquid base material | ISOPAR L：ISOPAR M | Duration of volatilization/day |
| Diluent No. 1 | Pure ISOPAR L | 10 |
| Diluent No. 2 | 09:01 | 34 |
| Diluent No. 3 | 08:02 | 54 |
| Diluent No. 4 | 07:03 | 76 |
| Diluent No. 5 | 06:04 | 100 |
Therefore, the same fragrance liquid of 100 ml, along with the increase of the proportion of ISOPAR M, the volatilization duration of the volatile liquid base material can be from 10 to 100 days, even longer, and the longer the service life of the finished product of the liquid rattan fragrance is.
Examples 2-5 preparation of rattan aromatherapy liquid base
Weighing the raw materials according to the dosage in the table 2, and mixing to obtain the rattan aromatherapy liquid base material.
TABLE 2 rattan aromatherapy liquid base material formula (quality percentage)
| Components | Example 2 | Example 3 | Example 4 | Example 5 |
| ISOPAR L | 79.20 | 82.17 | 89.10 | 92.07 |
| ISOPAR M | 19.80 | 16.83 | 9.90 | 6.93 |
| Patchouli oil | 0.30 | 0.30 | 0.30 | 0.30 |
| Amur saussurea root | 0.20 | 0.20 | 0.20 | 0.20 |
| Methyl cedryl ketone | 0.20 | 0.20 | 0.20 | 0.20 |
| ShumuFragrant composition | 0.30 | 0.30 | 0.30 | 0.30 |
| Is totaled | 100 | 100 | 100 | 100 |
Example 6 preparation of Slow volatile aromatherapy essential oil
Weighing the raw materials according to the table 3, mixing uniformly to prepare the essential oil 1#, wherein the preparation method of the essential oil refers to the conventional essential oil preparation process.
TABLE 3 champignon essential oil 1# formulation (weight percent)
Essential oil 1#: the formula is judged to be the volatile slow-aroma essential oil formula through the raw materials.
Example 7 preparation of fast volatile aromatherapy essential oil
Weighing the raw materials according to the table 4, mixing uniformly to prepare the essential oil 2#, wherein the preparation method of the essential oil refers to the conventional essential oil preparation process.
TABLE 4 champignon essential oil 2# formulation (weight percent)
Essential oil 2#: the formula is a formula of the quick-volatilization champignon essential oil according to judgment of volatilization speed of the raw materials.
Example 8
The essential oils 1# and 2# prepared in examples 6 and 7 are respectively adopted, the volatilization duration time of different fragrance types is required to be 60 days, and the error before and after the liquid rattan fragrance finished product with different fragrance types is completely volatilized cannot exceed 3 days.
The formula of the finished product of No. 1-1 liquid rattan aromatherapy product comprises the following components: aromatherapy essential oil 2#10wt%, rattan aromatherapy liquid base material prepared in example 2 90wt% (ISOPAR L: ISOPAR M = 8;
the formula of the 2-1 # liquid rattan aromatherapy finished product comprises the following components: aromatherapy essential oil 1#, 10%, example 3 volatile base formulation 90% (ISOPAR L: ISOPAR M = 8.3.
The 2 liquid rattan aromatherapy finished products are respectively evaluated, and the evaluation results are shown in table 5.
Table 5 example 8 evaluation of fragrance results table
The experiment shows that the rattan aromatherapy liquid base material system, the aromatherapy essential oil raw material system and the rattan aromatherapy liquid obtained by combining the rattan aromatherapy liquid base material system and the aromatherapy essential oil raw material system can achieve the effects of accurately controlling volatilization duration time, achieving expected service life and ensuring consistent fragrance.
Example 9
The essential oils 1# and 2# prepared in examples 6 and 7 are respectively adopted, the volatilization duration time of different fragrance types is required to be 30 days, and the error before and after the finished product of the liquid rattan incense with different fragrance types volatilizes completely can not exceed 3 days.
The formula of the finished product of No. 1-2 liquid rattan incense comprises: aromatherapy essential oil No. 2#10wt%, rattan aromatherapy liquid base material prepared in example 4 (diluent No. 2: ISOPAR L: ISOPAR M = 9;
the formula of the 2-2 # liquid rattan aromatherapy finished product comprises the following components: aromatherapy essential oil 1#10wt%, rattan aromatherapy liquid base 90wt% prepared in example 5 (ISOPAR L: ISOPAR M = 9.3.
The 2 liquid rattan aromatherapy finished products are respectively evaluated, and the evaluation results are shown in table 6.
Table 6 example 9 evaluation of fragrance results table
The experiment shows that the rattan aromatherapy liquid base material system, the aromatherapy essential oil raw material system and the rattan aromatherapy liquid obtained by combining the rattan aromatherapy liquid base material system and the aromatherapy essential oil raw material system can achieve the effects of accurately controlling volatilization duration time, achieving expected service life and ensuring consistent fragrance.
The preferred embodiments of the present invention have been described in detail, however, the present invention is not limited to the specific details of the above embodiments, and various simple modifications may be made to the technical solution of the present invention within the technical idea of the present invention, and these simple modifications are all within the protection scope of the present invention.
It should be noted that the various features described in the above embodiments may be combined in any suitable manner without departing from the scope of the invention. The invention is not described in detail in order to avoid unnecessary repetition.
In addition, any combination of the various embodiments of the present invention is also possible, and the same should be considered as the disclosure of the present invention as long as it does not depart from the spirit of the present invention.
Claims (9)
1. A rattan aromatherapy liquid base material is characterized in that: the composite material comprises the following components in percentage by mass: 98.0-99.9 percent of diluent and 0.1-2 percent of special component, wherein,
the diluent comprises the following components in percentage by mass: ISOPAR L10-90%, ISOPAR M10-90%;
the special component comprises the following components in percentage by mass: 0.1-0.5% of patchouli oil, 0.1-0.3% of ambergris root, 0.1-0.3% of methyl cedryl ketone and 0.1-0.3% of Shumuxiang.
2. The rattan aromatherapy liquid base according to claim 1, characterized in that: the rattan aromatherapy liquid base material consists of 98.5-99.5% of diluent and 0.5-1.5% of special component in percentage by mass;
the diluent comprises 60-90% of ISOPAR L and 10-40% of ISOPAR M in percentage by mass, preferably 80-85% of ISOPAR L and 10-15% of ISOPAR M.
3. The rattan aromatherapy liquid base according to claim 2, characterized in that: the special component comprises the following components in percentage by mass: 0.2 to 0.4 percent of patchouli oil, 0.1 to 0.3 percent of ambergris root, 0.1 to 0.2 percent of methyl cedryl ketone and 0.1 to 0.2 percent of Shumuxiang.
4. A preparation method of rattan aromatherapy liquid is characterized by comprising the following steps: the rattan aromatherapy liquid containing the rattan aromatherapy liquid base material according to any one of claims 1 to 3 is adopted, and the rattan aromatherapy liquid further comprises an aromatherapy essential oil component, 10g of the aromatherapy essential oil component volatilizes in a surface dish for 1-90 days at room temperature until 5g of the aromatherapy essential oil component remains, the rattan aromatherapy liquid is obtained after the aromatherapy essential oil and the rattan aromatherapy liquid base material are mixed according to different proportions, and the volatilization speed of the rattan aromatherapy liquid is regulated and controlled by regulating and controlling the proportion of the aromatherapy essential oil component and the rattan aromatherapy liquid base material.
5. The preparation method of the rattan aromatherapy liquid according to claim 4, characterized by: the mass ratio of the aromatherapy essential oil component to the rattan aromatherapy liquid base material is 1-20%:80 to 90 percent.
6. The preparation method of the rattan aromatherapy liquid according to claim 5, characterized by: the aromatherapy essential oil comprises the following components in percentage by mass:
the total amount is 100%.
7. The preparation method of the rattan aromatherapy liquid according to claim 5, characterized by: the aromatherapy essential oil comprises the following components in percentage by mass:
the total amount is 100%.
8. The rattan aromatherapy liquid prepared by the preparation method of the rattan aromatherapy liquid according to any one of claims 4 to 7, characterized in that: when the rattan aromatherapy liquid is used at room temperature, the volatilization duration is 30-100 days, and the fragrance effect of the volatilization day 1 and the fragrance effect of the last 1 day are basically consistent.
9. A liquid rattan incense product comprising the rattan incense liquor base of any one of claims 1-3, or
Comprising the rattan aromatherapy liquid prepared by the preparation method of the rattan aromatherapy liquid according to any one of claims 4 to 7,
or comprises the rattan aromatherapy liquid according to claim 8.
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| CN202211659832.5A CN115721757A (en) | 2022-12-23 | 2022-12-23 | Rattan aromatherapy liquid base material and rattan aromatherapy liquid |
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| CN202211659832.5A CN115721757A (en) | 2022-12-23 | 2022-12-23 | Rattan aromatherapy liquid base material and rattan aromatherapy liquid |
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| CN115721757A true CN115721757A (en) | 2023-03-03 |
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| CN202211659832.5A Pending CN115721757A (en) | 2022-12-23 | 2022-12-23 | Rattan aromatherapy liquid base material and rattan aromatherapy liquid |
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