CN115674824A - Preparation method of glass fiber cloth - Google Patents
Preparation method of glass fiber cloth Download PDFInfo
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- CN115674824A CN115674824A CN202211230451.5A CN202211230451A CN115674824A CN 115674824 A CN115674824 A CN 115674824A CN 202211230451 A CN202211230451 A CN 202211230451A CN 115674824 A CN115674824 A CN 115674824A
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- glass fiber
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- cloth
- drying
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- 239000004744 fabric Substances 0.000 title claims abstract description 89
- 239000003365 glass fiber Substances 0.000 title claims abstract description 82
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 238000001035 drying Methods 0.000 claims abstract description 43
- 239000011347 resin Substances 0.000 claims abstract description 39
- 229920005989 resin Polymers 0.000 claims abstract description 39
- 239000002253 acid Substances 0.000 claims abstract description 29
- 239000004816 latex Substances 0.000 claims abstract description 28
- 229920000126 latex Polymers 0.000 claims abstract description 28
- 238000004140 cleaning Methods 0.000 claims abstract description 18
- 238000002386 leaching Methods 0.000 claims abstract description 15
- 239000000835 fiber Substances 0.000 claims abstract description 12
- 239000011248 coating agent Substances 0.000 claims abstract description 9
- 238000000576 coating method Methods 0.000 claims abstract description 9
- 238000005096 rolling process Methods 0.000 claims abstract description 9
- 238000002791 soaking Methods 0.000 claims abstract description 9
- 238000005406 washing Methods 0.000 claims abstract description 9
- 238000004804 winding Methods 0.000 claims abstract description 3
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 36
- 239000000843 powder Substances 0.000 claims description 24
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 18
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical group Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 16
- 239000008367 deionised water Substances 0.000 claims description 16
- 229910021641 deionized water Inorganic materials 0.000 claims description 16
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 16
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 16
- 239000002994 raw material Substances 0.000 claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 239000007822 coupling agent Substances 0.000 claims description 14
- 229910021426 porous silicon Inorganic materials 0.000 claims description 10
- 125000000217 alkyl group Chemical group 0.000 claims description 8
- 239000000706 filtrate Substances 0.000 claims description 8
- 239000000047 product Substances 0.000 claims description 8
- 239000003795 chemical substances by application Substances 0.000 claims description 6
- 230000000149 penetrating effect Effects 0.000 claims description 6
- 238000000034 method Methods 0.000 claims 7
- 230000009286 beneficial effect Effects 0.000 abstract 1
- 239000001913 cellulose Substances 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- 150000002191 fatty alcohols Chemical class 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000012466 permeate Substances 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 238000005299 abrasion Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000010292 electrical insulation Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a preparation method of glass fiber cloth, which comprises the following steps: s1, preparing glass fiber grey cloth by using glass fiber yarns; s2, adhering the glass fiber grey cloth to a yarn winding cloth through wear-resistant latex after antistatic coating, and drying; s3, carrying out acid leaching treatment on the glass fiber grey cloth obtained in the step S2; s4, cleaning and drying the acid leached glass fiber grey cloth, and then soaking the glass fiber grey cloth in a wear-resistant resin solution; and S5, washing, drying and rolling the fiber cloth soaked in the wear-resistant resin solution to obtain a finished product. The invention has the beneficial effects that: the glass fiber grey cloth is adhered with the yarn woven cloth through the wear-resistant latex, so that the connection strength is enhanced, the wear resistance is improved, and the grey cloth is soaked in the acid leaching and wear-resistant resin solution, so that the strength and the wear resistance of the glass fiber cloth are greatly improved.
Description
Technical Field
The invention relates to a preparation method of glass fiber, in particular to a preparation method of glass fiber cloth.
Background
The glass fiber is an inorganic non-metallic material with excellent performance, and has the advantages of high temperature resistance, non-combustion, corrosion resistance, good heat insulation and sound insulation, high tensile strength and good electrical insulation compared with organic fiber. As a very important metal substitute material, the material has wide application prospect in the fields of buildings, ships, chemical pipelines, automobiles, aviation and the like. The glass fiber cloth is a fabric made of glass fibers, and has the excellent performances of high strength, stable size, high temperature resistance and the like. However, the conventional glass fiber cloth has poor abrasion resistance and is easily damaged after long-term use, so that the service life is shortened.
Disclosure of Invention
The invention aims to provide a preparation method of glass fiber cloth, which solves the problems that the existing glass fiber cloth is poor in wear resistance and easy to damage after being used for a long time, and the service life is shortened.
The purpose of the invention is realized by the following technical scheme:
a preparation method of glass fiber cloth comprises the following steps:
s1, preparing glass fiber grey cloth by using glass fiber yarns;
s2, adhering the glass fiber grey cloth to a yarn winding cloth through wear-resistant latex after antistatic coating, and drying;
s3, carrying out acid leaching treatment on the glass fiber grey cloth obtained in the step S2;
s4, cleaning and drying the glass fiber grey cloth subjected to acid leaching treatment, and then soaking the glass fiber grey cloth in a wear-resistant resin solution;
and S5, washing, drying and rolling the fiber cloth soaked in the wear-resistant resin solution to obtain a finished product.
Further, the wear-resistant latex in the step S2 is composed of the following raw materials in parts by weight: 80-90 parts of latex, 10-15 parts of wear-resistant micro powder and 1-3 parts of penetrating agent.
Further, in the step S3, the acid filtrate is hydrochloric acid solution with the concentration of 4-6mol/L, the treatment temperature is 70-90 ℃, and the treatment time is 6-10h.
Further, in the step S4, the wear-resistant resin solution is composed of the following raw materials in parts by weight: 50-60 parts of resin, 3-5 parts of penetrating agent, 1-3 parts of coupling agent, 2-5 parts of porous silicon, 20-30 parts of wear-resistant micro powder and 85-95 parts of deionized water.
Further, the wear-resistant micro powder is superfine calcium carbonate powder, and the penetrating agent is fatty alcohol-polyoxyethylene ether.
Further, the coupling agent is an alkyl coupling agent.
Further, the cleaning in the step S4 adopts deionized water for cleaning, the drying temperature is 105-110 ℃, and the drying time is 20-30min.
The invention has the following advantages:
the glass fiber grey cloth is pasted with the gauze cloth through the wear-resistant latex, the connection strength is enhanced, the wear resistance is improved, the grey cloth is leached by acid to enable the internal structure to be in a porous shape and then is soaked in the wear-resistant resin solution, the porous silicon increases the adsorption of superfine calcium carbonate powder and permeates into cellulose and the porous structure under the action of the fatty alcohol polyoxyethylene ether, the fiber yarns and the resin enhance the structural strength under the action of the coupling agent, the precipitation of the superfine calcium carbonate powder is inhibited at the same time, and the strength and the wear resistance of the glass fiber cloth are greatly improved.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention more apparent, the embodiments of the present invention will be described in detail and completely with reference to the accompanying drawings.
Thus, the following detailed description of embodiments of the invention is not intended to limit the scope of the invention as claimed, but is merely representative of selected embodiments of the invention. All other embodiments, which can be obtained by a person skilled in the art without any inventive step based on the embodiments of the present invention, are within the scope of the present invention.
It should be noted that the embodiments and features of the embodiments of the present invention may be combined with each other without conflict.
Example 1
A preparation method of glass fiber cloth comprises the following steps:
s1, preparing glass fiber grey cloth by using glass fiber yarns;
s2, adhering and drying the glass fiber grey cloth after antistatic coating through wear-resistant latex, wherein the wear-resistant latex is prepared from the following raw materials in parts by weight: 85 parts of latex, 15 parts of superfine calcium carbonate powder and 3 parts of fatty alcohol-polyoxyethylene ether;
s3, carrying out acid leaching treatment on the glass fiber grey cloth obtained in the step S2 for 6 hours, wherein acid filtrate is hydrochloric acid solution with the concentration of 4mol/L, the treatment temperature is 80 ℃, and the treatment time is 10 hours;
s4, cleaning and drying the glass fiber grey cloth subjected to acid leaching treatment, and then soaking the glass fiber grey cloth in a wear-resistant resin solution, wherein the cleaning is performed by using deionized water, the drying temperature is 110 ℃, the drying time is 20min, and the wear-resistant resin solution is prepared from the following raw materials in parts by weight: 55 parts of resin, 5 parts of fatty alcohol-polyoxyethylene ether, 1 part of alkyl coupling agent, 5 parts of porous silicon, 30 parts of superfine calcium carbonate powder and 95 parts of deionized water;
and S5, washing, drying and rolling the fiber cloth soaked in the wear-resistant resin solution to obtain a finished product.
Example 2
A preparation method of glass fiber cloth comprises the following steps:
s1, preparing glass fiber grey cloth by using glass fiber yarns;
s2, adhering the glass fiber grey cloth to a gauze through wear-resistant latex after antistatic coating, and drying, wherein the wear-resistant latex is prepared from the following raw materials in parts by weight: 80 parts of latex, 10 parts of superfine calcium carbonate powder and 1 part of fatty alcohol-polyoxyethylene ether;
s3, carrying out acid leaching treatment on the glass fiber grey cloth obtained in the step S2 for 8 hours, wherein acid filtrate is hydrochloric acid solution with the concentration of 4mol/L, the treatment temperature is 70 ℃, and the treatment time is 8 hours;
s4, cleaning and drying the glass fiber grey cloth after the acid leaching treatment, and then soaking the glass fiber grey cloth in a wear-resistant resin solution, wherein the cleaning is performed by using deionized water, the drying temperature is 105 ℃, the drying time is 30min, and the wear-resistant resin solution comprises the following raw materials in parts by weight: 50 parts of resin, 3 parts of fatty alcohol-polyoxyethylene ether, 1 part of alkyl coupling agent, 2 parts of porous silicon, 20 parts of superfine calcium carbonate powder and 85 parts of deionized water;
and S5, washing, drying and rolling the fiber cloth soaked in the wear-resistant resin solution to obtain a finished product.
Example 3
A preparation method of glass fiber cloth comprises the following steps:
s1, preparing glass fiber grey cloth by using glass fiber yarns;
s2, adhering the glass fiber grey cloth to a gauze through wear-resistant latex after antistatic coating, and drying, wherein the wear-resistant latex is prepared from the following raw materials in parts by weight: 90 parts of latex, 12 parts of superfine calcium carbonate powder and 2 parts of fatty alcohol-polyoxyethylene ether;
s3, carrying out acid leaching treatment on the glass fiber grey cloth obtained in the step S2 for 6 hours, wherein acid filtrate is hydrochloric acid solution with the concentration of 6mol/L, the treatment temperature is 90 ℃, and the treatment time is 8 hours;
s4, cleaning and drying the acid leached glass fiber grey cloth, then soaking in a wear-resistant resin solution, cleaning by using deionized water, wherein the drying temperature is 108 ℃, the drying time is 26min, and the wear-resistant resin solution comprises the following raw materials in parts by weight: 60 parts of resin, 4 parts of fatty alcohol-polyoxyethylene ether, 3 parts of alkyl coupling agent, 4 parts of porous silicon, 27 parts of superfine calcium carbonate powder and 88 parts of deionized water;
and S5, washing, drying and rolling the fiber cloth soaked in the wear-resistant resin solution to obtain a finished product.
Example 4
A preparation method of glass fiber cloth comprises the following steps:
s1, preparing glass fiber grey cloth by using glass fiber yarns;
s2, adhering and drying the glass fiber grey cloth after antistatic coating through wear-resistant latex, wherein the wear-resistant latex is prepared from the following raw materials in parts by weight: 86 parts of latex, 14 parts of superfine calcium carbonate powder and 3 parts of fatty alcohol-polyoxyethylene ether;
s3, carrying out acid leaching treatment on the glass fiber grey cloth obtained in the step S2 for 7 hours, wherein acid filtrate is hydrochloric acid solution with the concentration of 5mol/L, the treatment temperature is 87 ℃, and the treatment time is 7 hours;
s4, cleaning and drying the acid leached glass fiber grey cloth, then soaking in a wear-resistant resin solution, cleaning by using deionized water, wherein the drying temperature is 106 ℃, the drying time is 30min, and the wear-resistant resin solution comprises the following raw materials in parts by weight: 58 parts of resin, 3 parts of fatty alcohol-polyoxyethylene ether, 2 parts of alkyl coupling agent, 5 parts of porous silicon, 30 parts of superfine calcium carbonate powder and 92 parts of deionized water;
and S5, washing, drying and rolling the fiber cloth soaked in the wear-resistant resin solution to obtain a finished product.
Example 5
A preparation method of glass fiber cloth comprises the following steps:
s1, preparing glass fiber grey cloth by using glass fiber yarns;
s2, adhering and drying the glass fiber grey cloth after antistatic coating through wear-resistant latex, wherein the wear-resistant latex is prepared from the following raw materials in parts by weight: 89 parts of latex, 11 parts of superfine calcium carbonate powder and 1 part of fatty alcohol-polyoxyethylene ether;
s3, carrying out acid leaching treatment on the glass fiber grey cloth obtained in the step S2 for 9 hours, wherein acid filtrate is hydrochloric acid solution with the concentration of 4mol/L, the treatment temperature is 72 ℃, and the treatment time is 9 hours;
s4, cleaning and drying the glass fiber grey cloth subjected to acid leaching treatment, then soaking in a wear-resistant resin solution, cleaning by using deionized water, wherein the drying temperature is 109 ℃, the drying time is 24min, and the wear-resistant resin solution comprises the following raw materials in parts by weight: 56 parts of resin, 5 parts of fatty alcohol-polyoxyethylene ether, 3 parts of alkyl coupling agent, 4 parts of porous silicon, 24 parts of superfine calcium carbonate powder and 93 parts of deionized water;
and S5, washing, drying and rolling the fiber cloth soaked in the wear-resistant resin solution to obtain a finished product.
Example 6
A preparation method of glass fiber cloth comprises the following steps:
s1, preparing glass fiber grey cloth by using glass fiber yarns;
s2, adhering the glass fiber grey cloth to a gauze through wear-resistant latex after antistatic coating, and drying, wherein the wear-resistant latex is prepared from the following raw materials in parts by weight: 90 parts of latex, 10 parts of superfine calcium carbonate powder and 3 parts of fatty alcohol-polyoxyethylene ether;
s3, carrying out acid leaching treatment on the glass fiber grey cloth obtained in the step S2 for 9 hours, wherein acid filtrate is hydrochloric acid solution with the concentration of 4mol/L, the treatment temperature is 76 ℃, and the treatment time is 10 hours;
s4, cleaning and drying the glass fiber grey cloth after the acid leaching treatment, and then soaking the glass fiber grey cloth in a wear-resistant resin solution, wherein the cleaning is performed by using deionized water, the drying temperature is 110 ℃, the drying time is 30min, and the wear-resistant resin solution comprises the following raw materials in parts by weight: 60 parts of resin, 3 parts of fatty alcohol-polyoxyethylene ether, 2 parts of alkyl coupling agent, 5 parts of porous silicon, 30 parts of superfine calcium carbonate powder and 90 parts of deionized water;
and S5, washing, drying and rolling the fiber cloth soaked in the wear-resistant resin solution to obtain a finished product.
The glass fiber grey cloth is pasted with the gauze cloth through the wear-resistant latex, the connection strength is enhanced, the wear resistance is improved, the grey cloth is leached by acid to enable the internal structure to be in a porous shape and then is soaked in the wear-resistant resin solution, the porous silicon increases the adsorption of superfine calcium carbonate powder and permeates into cellulose and the porous structure under the action of the fatty alcohol polyoxyethylene ether, the fiber yarns and the resin enhance the structural strength under the action of the coupling agent, the precipitation of the superfine calcium carbonate powder is inhibited at the same time, and the strength and the wear resistance of the glass fiber cloth are greatly improved.
Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described in the foregoing embodiments, or equivalents may be substituted for elements thereof.
Claims (7)
1. The preparation method of the glass fiber cloth is characterized by comprising the following steps: the method comprises the following steps:
s1, preparing glass fiber grey cloth by using glass fiber yarns;
s2, adhering the glass fiber grey cloth to a yarn winding cloth through wear-resistant latex after antistatic coating, and drying;
s3, carrying out acid leaching treatment on the glass fiber grey cloth obtained in the step S2;
s4, cleaning and drying the acid leached glass fiber grey cloth, and then soaking the glass fiber grey cloth in a wear-resistant resin solution;
and S5, washing, drying and rolling the fiber cloth soaked in the wear-resistant resin solution to obtain a finished product.
2. The method for preparing glass fiber cloth according to claim 1, wherein: the wear-resistant latex in the step S2 is prepared from the following raw materials in parts by weight: 80-90 parts of latex, 10-15 parts of wear-resistant micro powder and 1-3 parts of penetrating agent.
3. The method for preparing glass fiber cloth according to claim 1, wherein: in the step S3, the acid filtrate is hydrochloric acid solution with the concentration of 4-6mol/L, the treatment temperature is 70-90 ℃, and the treatment time is 6-10h.
4. The method for preparing glass fiber cloth according to claim 1, wherein: in the step S4, the wear-resistant resin solution is prepared from the following raw materials in parts by weight: 50-60 parts of resin, 3-5 parts of penetrating agent, 1-3 parts of coupling agent, 2-5 parts of porous silicon, 20-30 parts of wear-resistant micro powder and 85-95 parts of deionized water.
5. The method for preparing glass fiber cloth according to claim 2 and 4, wherein: the wear-resistant micro powder is superfine calcium carbonate powder, and the penetrating agent is fatty alcohol-polyoxyethylene ether.
6. The method for preparing glass fiber cloth according to claim 4, wherein: the coupling agent is an alkyl coupling agent.
7. The method for preparing glass fiber cloth according to claim 1, wherein: and in the step S4, the cleaning is carried out by using deionized water, the drying temperature is 105-110 ℃, and the drying time is 20-30min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211230451.5A CN115674824A (en) | 2022-09-30 | 2022-09-30 | Preparation method of glass fiber cloth |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211230451.5A CN115674824A (en) | 2022-09-30 | 2022-09-30 | Preparation method of glass fiber cloth |
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| CN115674824A true CN115674824A (en) | 2023-02-03 |
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| CN202211230451.5A Pending CN115674824A (en) | 2022-09-30 | 2022-09-30 | Preparation method of glass fiber cloth |
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Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101654834A (en) * | 2009-07-10 | 2010-02-24 | 江苏恒州特种玻璃纤维材料有限公司 | High silica glass fiber mesh cloth and production technique thereof |
| CN107245882A (en) * | 2017-05-24 | 2017-10-13 | 浙江凯澳新材料有限公司 | A kind of production technology of wear-resisting glass-fiber-fabric |
| CN107376509A (en) * | 2017-08-21 | 2017-11-24 | 营口凯悦滤业科技有限公司 | The preparation method of the superfine modified glass fiber filter material of fluorine silica |
| CN107651854A (en) * | 2017-10-24 | 2018-02-02 | 内江市旭日环境科技有限公司 | A kind of novel glass fiber |
| CN109137545A (en) * | 2018-07-25 | 2019-01-04 | 合肥神舟建筑集团有限公司 | A kind of preparation method of fiberglass gridding cloth |
| CN109648961A (en) * | 2019-01-14 | 2019-04-19 | 河南凯辉实业有限公司 | A kind of grinding tempered glass functional carpet and preparation method thereof |
| CN112575589A (en) * | 2020-12-11 | 2021-03-30 | 九江鑫星玻纤材料有限公司 | High-wear-resistance glass fiber cloth and preparation method thereof |
| WO2022011873A1 (en) * | 2020-07-16 | 2022-01-20 | 抚顺天成环保科技有限公司 | High-temperature-resistant glass fiber woven fabric and preparation method therefor |
-
2022
- 2022-09-30 CN CN202211230451.5A patent/CN115674824A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101654834A (en) * | 2009-07-10 | 2010-02-24 | 江苏恒州特种玻璃纤维材料有限公司 | High silica glass fiber mesh cloth and production technique thereof |
| CN107245882A (en) * | 2017-05-24 | 2017-10-13 | 浙江凯澳新材料有限公司 | A kind of production technology of wear-resisting glass-fiber-fabric |
| CN107376509A (en) * | 2017-08-21 | 2017-11-24 | 营口凯悦滤业科技有限公司 | The preparation method of the superfine modified glass fiber filter material of fluorine silica |
| CN107651854A (en) * | 2017-10-24 | 2018-02-02 | 内江市旭日环境科技有限公司 | A kind of novel glass fiber |
| CN109137545A (en) * | 2018-07-25 | 2019-01-04 | 合肥神舟建筑集团有限公司 | A kind of preparation method of fiberglass gridding cloth |
| CN109648961A (en) * | 2019-01-14 | 2019-04-19 | 河南凯辉实业有限公司 | A kind of grinding tempered glass functional carpet and preparation method thereof |
| WO2022011873A1 (en) * | 2020-07-16 | 2022-01-20 | 抚顺天成环保科技有限公司 | High-temperature-resistant glass fiber woven fabric and preparation method therefor |
| CN112575589A (en) * | 2020-12-11 | 2021-03-30 | 九江鑫星玻纤材料有限公司 | High-wear-resistance glass fiber cloth and preparation method thereof |
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