CN115590135B - Essence and application thereof, and carbonated beverage containing essence - Google Patents

Essence and application thereof, and carbonated beverage containing essence Download PDF

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Publication number
CN115590135B
CN115590135B CN202211247597.0A CN202211247597A CN115590135B CN 115590135 B CN115590135 B CN 115590135B CN 202211247597 A CN202211247597 A CN 202211247597A CN 115590135 B CN115590135 B CN 115590135B
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essence
oil
percent
flavored
carbonated beverage
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CN115590135A (en
Inventor
陈雄
常旋
徐春明
赵华杰
叶田
王根女
沈国
张佳靓
陈佳
吴庆龙
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Hengfeng Food Technology Co ltd
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Hengfeng Food Technology Co ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52Adding ingredients
    • A23L2/56Flavouring or bittering agents
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52Adding ingredients
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/52Adding ingredients
    • A23L2/54Mixing with gases
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20Synthetic spices, flavouring agents or condiments
    • A23L27/24Synthetic spices, flavouring agents or condiments prepared by fermentation

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Biotechnology (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

The invention discloses essence and application thereof, and a carbonated beverage containing the essence, wherein the essence comprises an oil fermentation base material, the oil fermentation base material is prepared by fermenting oil with aspergillus oryzae, the essence is used for preparing the carbonated beverage, the ingredients of the carbonated beverage comprise the essence, and the essence accounts for not more than 0.05 per mill of the mass of the carbonated beverage. The invention has the advantages of enhancing the carbonic acid stimulation taste of the gas-containing beverage, having no influence on the flavor of the beverage, slowing down the degassing speed of carbon dioxide in the beverage, and the like.

Description

Essence and application thereof, and carbonated beverage containing essence
Technical Field
The invention belongs to the technical field of food additives, and particularly relates to essence and application thereof, and a carbonated beverage containing the essence.
Background
Carbonated beverages, sparkling wines and the like with carbon dioxide gas added thereto are highly favored by consumers. Carbon dioxide is added to the beverage under pressurized conditions, so that the content of carbon dioxide is reduced with the increase of the storage time of the beverage, the rapid degassing of the beverage under normal pressure after uncapping, and the like, resulting in reduced stimulation of carbonic acid. In order to maintain or enhance the taste of carbonic acid, the prior art has mainly been disclosed to solve the problem by adding spicy substances, bitter substances or cool substances to the beverage, such as the addition of capsicum extract, pepper extract, ginger extract, mountain pepper extract, peppermint components, etc. as disclosed in CN105491893 a. Such materials, while providing a stimulating mouthfeel, are different from carbon dioxide, in that they provide a stimulating oral cavity with low flavor thresholds and even low levels of these ingredients added to the beverage can affect the flavor of the beverage itself.
Disclosure of Invention
The invention aims to solve the problems in the background technology and provides essence, application thereof and a carbonated beverage containing the essence.
In order to achieve the above purpose, the invention provides an essence, wherein the essence comprises a grease fermentation base material, and the grease fermentation base material is prepared by fermenting grease by aspergillus oryzae.
Preferably, the oil is at least one of almond oil, sesame oil, peanut oil, sunflower oil, soybean oil, walnut oil, coconut oil, palm oil, octyl, capric glyceride or butter.
Preferably, the fat is coconut oil or caprylic/capric glyceride.
Preferably, the specific preparation method of the oil fermentation base material comprises the following steps: mixing oil and water, sterilizing, inoculating Aspergillus oryzae, aerobic fermenting at 20-40deg.C for 48 hr, and centrifuging to obtain upper oil phase as oil fermentation base material.
Preferably, the specific preparation method of the oil fermentation base material comprises the following steps: glucose is dissolved in water and then mixed with grease, after sterilization, aspergillus oryzae is inoculated, aerobic fermentation is carried out for 48 hours at the temperature of 20-40 ℃, and the upper oil phase is centrifugally taken as the grease fermentation base material.
Preferably, the essence further comprises a stabilizer, wherein the stabilizer is at least one of agar, polydextrose, xanthan gum, gellan gum or shellac, and the stabilizer can slow down the degassing speed of carbon dioxide in the carbonated beverage to a certain extent.
Preferably, the essence consists of the following components in percentage by mass: 0.01-1% of oil fermentation base stock, 2-20% of emulsifying agent, 0-80% of auxiliary emulsifying agent, 0-6% of perfume base, 0-10% of weighting agent, 0-0.5% of acidity regulator, 0-0.2% of preservative and the balance of water, wherein the perfume base is at least one of lemon flavor, sweet orange flavor, wen Dan flavor, grapefruit flavor, strawberry flavor, cola flavor, ginger flavor, walnut flavor, cream flavor, milk flavor, butter flavor or condensed milk flavor, the emulsifying agent is at least one of modified starch, polyglycerol fatty acid ester, mono-diglycerol fatty acid ester, succinic acid monoglyceride, polyglycerol ricinoleate, tween, span, octyl, capric acid glyceride, sucrose fatty acid ester, sodium caseinate or enzymatic hydrolysis soybean lecithin, the auxiliary emulsifying agent is at least one of glycerol, propylene glycol or ethanol, the weighting agent is rosin glyceride or acetic acid isobutyric acid sucrose ester, the acidity regulator is at least one of citric acid, malic acid or phosphoric acid, and the preservative is sodium benzoate or sodium benzoate.
Preferably, the essence consists of the following components in parts by weight: the oil fermentation base material comprises, by weight, 0.01-1% of an oil fermentation base material, 2-20% of an emulsifying agent, 0-80% of a co-emulsifying agent, 0-6% of a perfume base, 0-10% of a weighting agent, 0-0.5% of an acidity regulator, 0.01-5% of a stabilizer, 0-0.2% of a preservative and the balance of water, wherein the perfume base is at least one of lemon-flavored essence, orange-flavored essence, civilian-flavored essence, grapefruit-flavored essence, strawberry-flavored essence, cola-flavored essence, ginger-flavored essence, walnut-flavored essence, cream-flavored essence, milk-flavored essence, butter-flavored essence or condensed milk-flavored essence, the emulsifying agent is at least one of modified starch, polyglycerol fatty acid ester, mono-diglycerol fatty acid ester, succinic acid monoglyceride, polyglycerol ricinoleate, tween, span, octyl, capric acid glyceride, sucrose fatty acid ester, sodium caseinate or soybean lecithin, the co-emulsifying agent is at least one of glycerol, propylene glycol or ethanol, the weighting agent is rosin glyceride or sucrose acetate, the acidity regulator is at least one of citric acid, sodium benzoate or potassium phosphate, and the preservative is sodium benzoate or sodium benzoate.
The invention also provides application of the essence in preparing carbonated beverage.
The invention also provides a carbonated beverage, the ingredients of the carbonated beverage comprise the essence, and the essence accounts for not more than 0.05 per mill of the mass of the carbonated beverage.
The invention has the following beneficial effects:
1) According to the invention, aspergillus oryzae is used for fermenting grease, the grease fermentation base material contains natural saturated methyl ketone such as 2-heptanone, 2-nonanone, 2-undecanone, 2-tridecanone, 2-pentadecanone and the like, alcohol and acid, and trace components such as 8-nonene-2-ketone and the like, the components can play a role in a certain carbonic acid stimulation sense, and the carbonic acid stimulation sense can be effectively enhanced by using the grease fermentation base material to prepare essence and then apply the essence to the gas-containing beverage, and meanwhile, the flavor of the fermentation base material is covered due to emulsification embedding, so that the influence on the flavor of the beverage is avoided within the range of effectively enhancing the carbonic acid stimulation sense.
2) According to the invention, the grease fermentation base material obtained by fermenting grease by aspergillus oryzae is added into the gas-containing beverage after being prepared into essence, so that obvious carbonic acid can be endowed with a stimulated taste, and the degassing speed of carbon dioxide after uncapping is slowed down, thereby maintaining and enhancing the carbonic acid taste of the gas-containing beverage and improving the drinking feeling.
The features and advantages of the present invention will be described in detail by way of example with reference to the accompanying drawings.
Drawings
FIG. 1 is a graph showing the change in the amount of carbon dioxide lost after uncapping of various carbonated beverage samples in accordance with an embodiment of the present invention.
Detailed Description
The present invention will be further illustrated by the following specific examples, which are given for illustration of the present invention only and are not intended to be limiting, and the total mass of the essence in the following examples and comparative examples is 1 kg.
Example 1
The essence in the embodiment comprises the following components in percentage by mass: 1g of grease fermentation base stock, 99g of octyl and capric glyceride, 25g of modified starch, 3.5g of citric acid, 1.5g of sodium benzoate and 870g of water.
The specific preparation method of the oil fermentation base material in the embodiment comprises the following steps: mixing 500g of octyl and decyl glyceride, 50g of glucose and 450g of water, dissolving glucose in the water, mixing with the octyl and decyl glyceride, sterilizing, inoculating Aspergillus oryzae, performing aerobic fermentation at 35 ℃ for 48h, and centrifuging to obtain an upper oil phase to obtain the oil fermentation base material.
This example presents a carbonated beverage with 0.05% of the essence of this example added.
Example 2
The essence in the embodiment comprises the following components in percentage by mass: 1g of grease fermentation base stock, 99g of octyl and capric glyceride, 25g of modified starch, 25g of polydextrose, 3.5g of citric acid, 1.5g of sodium benzoate and 845g of water.
The specific preparation method of the fat fermentation base in this example is the same as that in example 1.
This example presents a carbonated beverage with 0.05% of the essence of this example added.
Example 3
The essence in the embodiment comprises the following components in percentage by mass: 0.1g of grease fermentation base stock, 99.9g of caprylic/capric glyceride, 100g of sucrose acetate isobutyrate, 60g of polyglycerol fatty acid ester, 540g of glycerol and 200g of water.
The specific preparation method of the oil fermentation base material in the embodiment comprises the following steps: taking 500g of coconut oil, 60g of glucose and 440g of water, dissolving glucose in the water, mixing with the coconut oil, sterilizing, inoculating Aspergillus oryzae, performing aerobic fermentation at 40 ℃ for 48 hours, and centrifuging to obtain an upper oil phase to obtain the oil fermentation base material.
This example presents a carbonated beverage with 0.05% of the essence of this example added.
Example 4
The essence in the embodiment comprises the following components in percentage by mass: 0.5g of oil fermentation base stock, 99.5g of lemon flavor essence, 20g of rosin glyceride, 60g of sucrose acetate isobutyrate, 50g of modified starch and 770g of water.
The specific preparation method of the oil fermentation base material in the embodiment comprises the following steps: taking 600g of palm oil, 60g of glucose and 340g of water, dissolving glucose in the water, mixing with the palm oil, sterilizing, inoculating Aspergillus oryzae, performing aerobic fermentation at 40 ℃ for 48 hours, and centrifuging to obtain an upper oil phase to obtain the oil fermentation base material.
This example presents a carbonated beverage with 0.05% of the essence of this example added.
Example 5
The essence in the embodiment comprises the following components in percentage by mass: 0.5g of oil fermentation base stock, 50.5g of cream flavor essence, 149g of caprylic/capric glyceride, 50g of modified starch and 750g of water.
The specific preparation method of the oil fermentation base material in the embodiment comprises the following steps: taking 600g of anhydrous cream, 60g of glucose and 340g of water, dissolving glucose in the water, mixing with the anhydrous cream, sterilizing, inoculating Aspergillus oryzae, performing aerobic fermentation at 40 ℃ for 48h, and centrifuging to obtain an upper oil phase to obtain the oil fermentation base material.
This example presents a carbonated beverage with 0.03% of the essence of this example added.
Example 6
The essence in the embodiment comprises the following components in percentage by mass: 0.5g of oil fermentation base stock, 50.5g of cream flavor essence, 149g of caprylic/capric glyceride, 50g of modified starch, 30g of shellac and 720g of water.
The specific preparation method of the fat fermentation base material in this example is the same as that in example 5.
This example presents a carbonated beverage to which 0.04% of the essence of this example is added.
Comparative example 1
The essence in the comparative example consists of the following components in percentage by mass: 99g of octyl and decyl glyceride, 25g of modified starch, 3.5g of citric acid, 1.5g of sodium benzoate and 871g of water.
Experiment of influence of essence on carbon dioxide degassing speed and carbonic acid taste in carbonic acid beverage
The formulations of 1L carbonated beverages prepared from the essence of the same amount of example 1, example 2, example 3 and comparative example 1 at an addition ratio of 0.05% were shown in Table 1 below:
Table 1 sample formulation of essence-added carbonated beverage
In this experiment, the essence of example 1, example 2, example 3 and comparative example 1 was added to the carbonated beverages of sample 1, sample 2, sample 3 and sample 4 in equal amounts, respectively, and no essence was added to the blank samples. And (3) sealing and filling the prepared five carbonated beverage samples into beverage bottles of the same model, simultaneously unscrewing the bottle caps of the five beverage bottles, standing, continuously weighing at intervals of 1h, and evaluating the degassing speed of carbon dioxide in the carbonated beverage by taking the weight reduction quantity of the beverage samples as the quality of the carbon dioxide overflowed from the beverage, wherein the carbon dioxide loss quantity in the carbonated beverage is shown in figure 1.
As can be seen from FIG. 1, the loss amount of carbon dioxide in sample 1, sample 2, sample 3 and sample 4 is significantly lower than that of the blank sample, the carbon dioxide loss rate of the blank sample is 0.147g/h, the carbon dioxide loss rate of sample 1 is 0.077g/h, the carbon dioxide loss rate of sample 2 is 0.040g/h, the carbon dioxide loss rate of sample 3 is 0.068g/h, and the carbon dioxide loss rate of sample 4 is 0.096g/h, as calculated by fitting. Therefore, the essence can slow down the degassing speed of carbon dioxide in the carbonated beverage to less than half, and the stabilizer and the oil fermentation base material in the essence play a remarkable role in slowing down the degassing speed of the carbon dioxide in the carbonated beverage, so that the carbonated taste of the carbonated beverage is maintained.
Selecting 20 testers, training the carbonated taste evaluation standard of the carbonated beverages of the testers to ensure that the testers score the carbonated taste of different carbonated beverages according to the same standard, equally dividing the 20 testers into five groups, respectively evaluating and scoring the carbonated beverages of the sample 1, the sample 2, the sample 3, the sample 4 and the blank sample at different times after uncapping, and calculating the average value of scoring conditions of the testers of each group, wherein the specific evaluation results are shown in the following table 2:
Table 2 sample evaluation results
Time (h) Blank space Sample 1 Sample 2 Sample 3 Sample 4
0 (Just uncap) 8.0 8.6 8.3 8.3 8.1
2 4.7 7.5 7.6 7.6 5.0
4 3.3 7.0 7.1 7.1 4.3
6 3.2 6.3 6.7 6.7 3.5
Note that: the scoring criteria for the sample evaluation were as follows: the score of 1-9 indicates the strength of carbonic acid, the lower the score, the weaker the carbonic acid, 1 indicates the weakest carbonic acid, and 9 indicates the strongest carbonic acid.
As can be seen from table 2, the carbonic acid feeling of all samples was relatively high just after the cover was opened, and the carbonic acid taste was gradually weakened due to continuous overflow of carbon dioxide in each sample, and the carbonic acid taste of sample 1, sample 2, and sample 3 added with the essence of the present invention was stronger than the carbonic acid taste of the blank sample and sample 4 without the essence at each time point, and the carbonic acid taste of sample 1, sample 2, and sample 3 added with the essence of the present invention was significantly higher than the carbonic acid taste of the blank sample and sample 4 without the essence even after the cover was opened for 6 hours. Therefore, the essence added with the oil fermentation base material has a certain reinforcing effect on the carbonic acid feel of the carbonated beverage.
The above embodiments are illustrative of the present invention, and not limiting, and any simple modifications of the present invention fall within the scope of the present invention.

Claims (1)

1. A carbonated beverage, characterized by: the components of the carbonated beverage comprise emulsified essence, wherein the emulsified essence accounts for not more than 0.05 per mill of the carbonated beverage in mass percent, and the emulsified essence consists of the following components in parts by weight: 0.01 to 1 percent of oil fermentation base stock, 2 to 20 percent of emulsifying agent, 0 to 80 percent of auxiliary emulsifying agent, 0 to 6 percent of oil-soluble perfume base, 0 to 10 percent of weighting agent, 0 to 0.5 percent of acidity regulator, 0.01 to 5 percent of stabilizing agent, 0 to 0.2 percent of preservative and the balance of water, wherein the oil fermentation base stock is prepared by fermenting oil by aspergillus oryzae, the oil is coconut oil or palm oil or octyl, capric glyceride or butter, the stabilizing agent is at least one of agar, polydextrose, xanthan gum, gellan gum or lac gum, the emulsifying agent is at least one of modified starch, polyglycerol fatty acid ester, mono-diglycerol fatty acid ester, succinic acid monoglyceride, polyglycerol ricinoleate, tween, span, octyl, capric glyceride, sucrose fatty acid ester, sodium caseinate or enzymatic hydrolysis soybean phosphatide, the oil-soluble perfume base is at least one of lemon-flavored essence, sweet orange-flavored essence, civilian-flavored essence, grapefruit-flavored essence, strawberry-flavored essence, cola-flavored essence, ginger-flavored essence, walnut-flavored essence, cream-flavored essence, milk-flavored essence, butter-flavored essence or condensed milk-flavored essence, the auxiliary emulsifier is at least one of glycerol, propylene glycol or ethanol, the weighting agent is rosin glyceride or sucrose acetate isobutyrate, the acidity regulator is at least one of citric acid, sodium citrate, malic acid or phosphoric acid, the preservative is sodium benzoate, potassium sorbate or nisin, and the specific preparation method of the oil fermentation base material comprises the following steps: glucose is dissolved in water and then mixed with grease, after sterilization, aspergillus oryzae is inoculated, aerobic fermentation is carried out for 48 hours at the temperature of 20-40 ℃, and the upper oil phase is centrifugally taken as the grease fermentation base material.
CN202211247597.0A 2022-10-12 2022-10-12 Essence and application thereof, and carbonated beverage containing essence Active CN115590135B (en)

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Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4957862A (en) * 1989-02-27 1990-09-18 Sanofi Microbiological process for the preparation of methyl ketones
CN102057047A (en) * 2008-06-03 2011-05-11 玛奈·菲尔萨公司 Method for producing natural 9-decen-2-one by bioconverting undecylenic acid using a mold, and use in the perfume and food flavoring fields
JP2013121323A (en) * 2011-12-09 2013-06-20 Taiyo Kagaku Co Ltd Carbonic acid feeling applying agent
CN105491893A (en) * 2013-09-04 2016-04-13 长谷川香料株式会社 Carbonation enhancer
WO2016208527A1 (en) * 2015-06-26 2016-12-29 アサヒ飲料株式会社 Packaged carbonated beverage and quality improvement method for packaged carbonated beverage
CN106387835A (en) * 2016-08-31 2017-02-15 恒枫食品科技有限公司 Preparation method of emulsifying essence
JP2019062867A (en) * 2017-10-05 2019-04-25 曽田香料株式会社 Carbonated feeling enhancing agent
CN111150043A (en) * 2020-01-16 2020-05-15 恒枫食品科技有限公司 Milk flavor essence and preparation method thereof
CN111758875A (en) * 2020-07-30 2020-10-13 东莞波顿香料有限公司 Opacifier and preparation method and application thereof
CN112021546A (en) * 2020-09-04 2020-12-04 恒枫食品科技有限公司 Preparation method of almond-flavored essence
CN113892626A (en) * 2021-08-23 2022-01-07 华百仕(河北)食品科技有限公司 Paste-like orange essence and preparation method and application thereof

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4957862A (en) * 1989-02-27 1990-09-18 Sanofi Microbiological process for the preparation of methyl ketones
CN102057047A (en) * 2008-06-03 2011-05-11 玛奈·菲尔萨公司 Method for producing natural 9-decen-2-one by bioconverting undecylenic acid using a mold, and use in the perfume and food flavoring fields
JP2013121323A (en) * 2011-12-09 2013-06-20 Taiyo Kagaku Co Ltd Carbonic acid feeling applying agent
CN105491893A (en) * 2013-09-04 2016-04-13 长谷川香料株式会社 Carbonation enhancer
WO2016208527A1 (en) * 2015-06-26 2016-12-29 アサヒ飲料株式会社 Packaged carbonated beverage and quality improvement method for packaged carbonated beverage
CN106387835A (en) * 2016-08-31 2017-02-15 恒枫食品科技有限公司 Preparation method of emulsifying essence
JP2019062867A (en) * 2017-10-05 2019-04-25 曽田香料株式会社 Carbonated feeling enhancing agent
CN111150043A (en) * 2020-01-16 2020-05-15 恒枫食品科技有限公司 Milk flavor essence and preparation method thereof
CN111758875A (en) * 2020-07-30 2020-10-13 东莞波顿香料有限公司 Opacifier and preparation method and application thereof
CN112021546A (en) * 2020-09-04 2020-12-04 恒枫食品科技有限公司 Preparation method of almond-flavored essence
CN113892626A (en) * 2021-08-23 2022-01-07 华百仕(河北)食品科技有限公司 Paste-like orange essence and preparation method and application thereof

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