CN115584178A - Water-based release printing coating material and preparation method thereof - Google Patents
Water-based release printing coating material and preparation method thereof Download PDFInfo
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- CN115584178A CN115584178A CN202211281936.7A CN202211281936A CN115584178A CN 115584178 A CN115584178 A CN 115584178A CN 202211281936 A CN202211281936 A CN 202211281936A CN 115584178 A CN115584178 A CN 115584178A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D139/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/20—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes for coatings strippable as coherent films, e.g. temporary coatings strippable as coherent films
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/20—Diluents or solvents
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
Abstract
The invention discloses a water-based release printing coating material, which comprises the following components: cationic acrylic acid, a color fixing agent, organosilicon and a wetting agent. The invention also discloses a preparation method of the coating material, which comprises the following steps: mixing the above materials. According to the water-based release printing coating material and the preparation method thereof, the materials of the printing coating and the release coating are combined into one, and the water-based release printing coating can be formed on PET through one-time coating, so that the coating process is simplified, the working efficiency is improved, and all the materials are environment-friendly and safe water-based materials; the hot-pressed picture can be suitable for producing hot-pressed pictures in various printing modes such as printing, spray painting, silk-screen printing and the like, the patterns and colors of the hot-pressed pictures are variable, the chromaticity is full, and the hot-pressed pictures can be cold-torn and hot-torn when subjected to high-temperature heat transfer.
Description
Technical Field
The invention relates to the technical field of material preparation, in particular to a water-based release printing coating material and a preparation method thereof.
Background
The pyrograph is also called pyrograph, or the heat transfer printing paper is a printing process which prints a pattern on a base material, and then transfers the pattern to a printing stock by heating with a pyrograph machine or an electric iron. Because of its low cost and simple operation, the pyrograph product has been widely used by more and more garment factories, printing factories, case factories and the like. In daily life, a plurality of products related to pyrograph are printed, including clothes T-shirt printing, jigsaw puzzle, pillow, mouse pad, ceramic, mug, case, towel, gift bag and the like, and the pyrograph process is used for printing a plurality of products.
In the traditional pyrograph industry, a release layer is coated on corona PET (polyethylene terephthalate) and dried to form a release film; and curing the release film for a certain time, coating an ink absorption layer, and drying to form the release printing film. Printing ink on the release printing film by screen printing, scattering hot-melt adhesive powder when the ink is not dry, and drying to finish the manufacture of the pyrograph. The ink is transferred to a printing stock by a thermal transfer printing mode, the process is labor-consuming and time-consuming, and release layers and the ink of different manufacturers cannot be mixed.
The traditional pyrography industry mostly adopts screen printing, each pattern of the screen printing needs to be manufactured with a screen printing plate independently, and only single color can be printed at a time, so that the difficulty of multicolor overprinting and gradient color printing is increased, most pyrography products on the market have single pattern, color and the like, and color deviation possibly occurs before and after pyrography to influence the color reduction degree; meanwhile, the ink absorption performance of the release printing film is not ideal, the ink is easy to flow out after printing the ink, and the film is easy to stick powder in the powder spraying process, so that the edge of a printed pattern is irregular and shrunk; because the ink absorption layer contains a large amount of powder, the powder is easy to fall after drying, the pollution to printing stocks is possible to be caused, and the release printing film is easy to absorb moisture after being stored for a long time.
As the release layer used by a plurality of pyrograph manufacturers is made of an oily material, the release layer can be left with solvent after being baked at high temperature in the manufacturing process, so that pungent smell is generated, and potential safety hazard and environmental protection problems exist. In order to thoroughly solve the environmental protection problem, all the materials used should be water-based environment-friendly materials, so as to solve the problem of solvent residue.
Along with the improvement of living standard of people, the quality requirement of used articles for daily use is continuously improved, but the traditional pyrograph manufacturing has single color, pattern and the like due to the limitation of the printing process, the transitional color is not easy to realize, and meanwhile, the production process has potential safety hazard and environmental protection problems. Therefore, through process improvement, environmental protection and good-quality pyrograph printing modes gradually become development trends, and coatings capable of printing pyrographs also have a large market demand.
Disclosure of Invention
The invention mainly aims to provide a water-based release printing coating material, which solves the problems of environmental pollution and poor performance of the existing release printing coating material.
The invention also aims to provide a preparation method of the water-based release printing coating material, which solves the problem that the preparation and use steps are complicated when the existing release printing layer material needs to be prepared respectively and independently.
In order to achieve the above purpose, the first technical scheme adopted by the invention is as follows: the water-based release printing coating material is characterized by comprising the following components: cationic acrylic acid, a color fixing agent, organic silicon and a wetting agent.
Preferably, the components are as follows according to the mass ratio: 10-15 parts of cationic acrylic acid, 15-30 parts of a color fixing agent, 5-10 parts of organic silicon and 0.1-0.3 part of a wetting agent.
Further, the aqueous release printing coating material also comprises the following components: a slow-drying agent.
Further, the aqueous release printing coating material also comprises the following components: and (4) defoaming agent.
Further, the aqueous release printing coating material also comprises the following components: fumed silica and polyethylene wax.
Further, the aqueous release printing coating material also comprises the following components: a thickening agent.
Further, the aqueous release printing coating material also comprises the following components: and (3) a curing agent.
The second technical scheme adopted by the invention is as follows: a preparation method of a water-based release printing coating material comprises the steps of mixing and uniformly stirring cationic acrylic acid, a color fixing agent, organic silicon, a wetting agent, a slow drying agent, a defoaming agent, fumed silica, polyethylene wax, a thickening agent and a curing agent to obtain the water-based release printing coating material.
Further, mixing and stirring the cationic acrylic acid, the color fixing agent, the organic silicon, the wetting agent, the slow drying agent, the defoaming agent, the fumed silica and the polyethylene wax uniformly, filtering, adding the thickening agent and the curing agent, and continuously stirring uniformly to obtain the water-based release printing coating material.
Compared with the prior art, the invention has the following beneficial effects: according to the water-based release printing coating material and the preparation method thereof, the materials of the printing coating and the release coating are combined into a whole, and the water-based release printing coating can be formed on PET through one-time coating, so that the coating process is simplified, the working efficiency is improved, and all the used materials are environment-friendly and safe water-based materials; the hot-pressed picture can be suitable for producing hot-pressed pictures in various printing modes such as printing, spray painting, silk-screen printing and the like, the patterns and colors of the hot-pressed pictures are variable, the chromaticity is full, and the hot-pressed pictures can be cold-torn and hot-torn when subjected to high-temperature heat transfer.
Detailed Description
The invention discloses a water-based release printing coating material, which comprises the following components: cationic acrylic acid, a color fixing agent, organic silicon and a wetting agent.
The invention uses cation acrylic emulsion as film forming matter; the addition of the fixing agent can ensure that the printed patterns and colors are firm and durable, and illustratively, the fixing agent can be selected from poly dimethyl diallyl ammonium chloride; the addition of the organic silicon can ensure that the dried coating has release performance, and the coating is soft, elastic and smooth and has excellent handfeel. Illustratively, the silicone may be selected from silicone resin-modified polysiloxanes; the wetting agent is used for adjusting the surface tension of the coating made of the material, so that the liquid coating is more easily wetted and soaked on the solid base material. Illustratively, the wetting agent can be selected from polyether modified siloxane, and the specific model can be BYK-349 and the like.
In order to meet environmental and safety requirements, the present invention utilizes deionized water as a diluent.
Preferably, the components are respectively as follows according to the mass ratio: 10-15 parts of cationic acrylic acid, 15-30 parts of a color fixing agent, 5-10 parts of organic silicon and 0.1-0.3 part of a wetting agent; also comprises 20-56 parts of deionized water.
Further, in order to prevent the water-based release printing coating from being dried too fast locally, so as to cause the occurrence of skinning, plate blocking and the like, a slow drying agent is added into the water-based release printing coating material. Illustratively, the slow-drying agent may be propylene glycol methyl ether. The addition amount of the slow drying agent can be adjusted according to selected substances and coating characteristics, and the mass ratio of the slow drying agent taking propylene glycol methyl ether as the slow drying agent is 2-5 parts.
Further, in order to inhibit or eliminate air bubbles generated in the process of preparing the aqueous release printing coating material, the aqueous release printing coating material of the invention is also added with a defoaming agent. Illustratively, the defoaming agent can be a defoaming polysiloxane solution with the mass ratio of 0.1-0.3, and the specific model can be BYK-094 and the like.
Further, the aqueous release printing coating material of the invention also comprises the following components: fumed silica and polyethylene wax. The softening point of the polyethylene wax is 80-100 ℃, the fumed silica and the polyethylene wax can ensure that the dried coating is wear-resistant and scratch-resistant, and the ink absorption is improved, wherein the mass ratio of the fumed silica is 6-7, and the mass ratio of the polyethylene wax is 5-10.
Further, in order to adjust the viscosity of the coating material liquid of the present invention, the aqueous release printing coating material of the present invention further comprises the components: the mass ratio of the thickening agent is 0.3-0.5. Illustratively, the thickener is preferably an associative polyurethane-based thickener.
Further, in order to improve the resistance of the aqueous release printing coating, the aqueous release printing coating material of the invention also comprises the following components: and the mass ratio of the curing agent is 2-5. Preferably, the curing agent is an isocyanate curing agent, further is a blocked isocyanate curing agent, and specifically can be a curing agent of bayer 2706, 2794 and other types.
Specifically, the water-based release printing coating material of the invention has at least the following advantages:
1. the material can combine a printing coating and a release coating into a whole, and a release printing film can be formed on PET through one-time coating, so that the coating process is simplified, and the working efficiency is improved;
2. the release printing film produced by the coating material can be used for printing various simple or complex patterns by using printing modes such as printing, spray painting, silk-screen printing and the like, has full pattern chromaticity and high color reduction degree, and does not deviate color after high-temperature heat transfer printing;
3. the release printing film produced by the coating material disclosed by the invention does not stick hot-melt adhesive powder, only the hot-melt adhesive powder remains on a printed matter after a powder spraying-powder shaking process, and a printing stock cannot be polluted by thermal transfer printing;
4. the coating supported by the coating material has less powder, excellent coating effect and difficult moisture absorption, powder falling and the like;
5. the coating material is a water-based material, and distilled water is used as a diluent, so that the coating is safe and environment-friendly;
6. the pyrograph made of the coating material can be released at high temperature (hot tearing) or at normal temperature (cold tearing), and has wide application fields.
The invention also discloses a preparation method of the water-based release printing coating material, which specifically comprises the following steps:
mixing and stirring deionized water, cationic acrylic acid, a color fixing agent, organic silicon, a wetting agent, a slow drying agent, a defoaming agent, fumed silica and polyethylene wax uniformly, filtering, adding a thickening agent, stirring, and adding a curing agent in the stirring process until the stirring is uniform, thus obtaining the water-based release printing coating material.
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be obtained by a person skilled in the art without making any creative effort based on the embodiments in the present invention, belong to the protection scope of the present invention.
Example 1
The embodiment discloses a preparation method of an aqueous release printing coating material, which specifically comprises the following steps:
adding 10kg of cationic acrylic emulsion into 20kg of deionized water, placing the mixture on a stirrer, adjusting the stirring speed to 500r/min, then adding 5kg of organic silicon resin modified polysiloxane, 15kg of polydimethyldiallylammonium chloride, 2kg of propylene glycol methyl ether, 0.1kg of BYK-094 type defoaming agent, 0.1kg of BYK-349 type wetting agent, 6kg of fumed silica and 5kg of polyethylene wax, stirring for 30min, filtering with 80-mesh filter cloth to remove impurities, then adding 0.3kg of associative polyurethane thickener, stirring, adding 2kg of Bayer 2706 type curing agent in the stirring process, and continuing stirring until the mixture is uniform, thus obtaining the waterborne release printing coating material.
Example 2
The embodiment discloses a preparation method of an aqueous release printing coating material, which specifically comprises the following steps:
adding 12kg of cationic acrylic emulsion into 25kg of deionized water, then placing the mixture on a stirrer, adjusting the stirring speed to 500r/min, then adding 6kg of organic silicon resin modified polysiloxane, 18kg of polydimethyldiallylammonium chloride, 3kg of propylene glycol methyl ether, 0.15kg of BYK-094 type defoaming agent, 0.1kg of BYK-349 type wetting agent, 6kg of fumed silica and 6kg of polyethylene wax, stirring for 30min, filtering with 80-mesh filter cloth to remove impurities, then adding 0.35kg of associative polyurethane thickener, stirring, adding 2.5kg of Bayer 2794 type curing agent in the stirring process, and continuously stirring until the mixture is uniform, thus obtaining the waterborne release printing coating material.
Example 3
The embodiment discloses a preparation method of an aqueous release printing coating material, which specifically comprises the following steps:
adding 12kg of cationic acrylic emulsion into 32kg of deionized water, then placing the mixture on a stirrer, adjusting the stirring speed to 300r/min, then adding 6kg of organic silicon resin modified polysiloxane, 20kg of poly dimethyl diallyl ammonium chloride, 3.5kg of propylene glycol methyl ether, 0.2kg of BYK-094 type defoaming agent, 0.2kg of BYK-349 type wetting agent, 8kg of fumed silica and 6.5kg of polyethylene wax, stirring for 40min, filtering with 80-mesh filter cloth to remove impurities, then adding 0.35kg of associative polyurethane thickener, stirring, adding 3kg of Bayer 2706 type curing agent in the stirring process, and continuously stirring until the mixture is uniform to obtain the water-based release printing coating material.
Example 4
The embodiment discloses a preparation method of an aqueous release printing coating material, which specifically comprises the following steps:
adding 13kg of cationic acrylic emulsion into 45kg of deionized water, then placing the mixture on a stirrer, adjusting the stirring speed to 500r/min, then adding 8kg of organic silicon resin modified polysiloxane, 24kg of polydimethyldiallyl ammonium chloride, 3.5kg of propylene glycol methyl ether, 0.2kg of BYK-094 type defoaming agent, 0.3kg of BYK-349 type wetting agent, 6.6kg of fumed silica and 8kg of polyethylene wax, stirring for 30min, filtering with 80-mesh filter cloth to remove impurities, then adding 0.5kg of associated polyurethane thickening agent, stirring, adding 4kg of Bayer 2706 type curing agent in the stirring process, and continuously stirring until the mixture is uniform to obtain the waterborne release printing coating material.
Example 5
The embodiment discloses a preparation method of an aqueous release printing coating material, which specifically comprises the following steps:
adding 15kg of cationic acrylic emulsion into 56kg of deionized water, then placing the mixture on a stirrer, adjusting the stirring speed to be 450r/min, then adding 10kg of organic silicon resin modified polysiloxane, 28kg of polydimethyldiallylammonium chloride, 4.5kg of propylene glycol methyl ether, 0.3kg of BYK-094 type defoaming agent, 0.25kg of BYK-349 type wetting agent, 7kg of fumed silica and 10kg of polyethylene wax, stirring for 35min, filtering with 80-mesh filter cloth to remove impurities, then adding 0.5kg of associative polyurethane thickener, stirring, adding 5kg of Bayer 2794 type curing agent in the stirring process, and continuing stirring until the mixture is uniform, thus obtaining the water-based release printing coating material.
When the water-based release printing coating is manufactured, the water-based release printing coating material is coated on corona PET for one time. The waterborne release printing coating can meet the following requirements:
1. the hot stamping is carried out for 5 to 10 seconds at the high temperature of 180 ℃;
2. the printed color has good reducibility, no distortion and clear and natural margin;
3. ensuring good matte degree after hot stamping;
4. the coating is not stained with hot melt powder, does not get damp, is scratch resistant, and is not easy to oxidize in the placing process.
Through experiments, the clothes printed with the aqueous release printing coating can meet European Union washing standards: 3-5% of laundry detergent is added into water at 60 ℃, the laundry detergent is washed for 4 hours and 4 times by a single machine, and printed coatings on clothes are not decolored and cracked, so that the requirements of European Union washing standards are met.
It should be noted that, in this document, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (9)
1. The water-based release printing coating material is characterized by comprising the following components: cationic acrylic acid, a color fixing agent, organosilicon and a wetting agent.
2. The aqueous release printing coating material according to claim 1, wherein the components are respectively as follows according to mass ratio: 10-15 parts of cationic acrylic acid, 15-30 parts of a color fixing agent, 5-10 parts of organic silicon and 0.1-0.3 part of a wetting agent.
3. The aqueous release print coating material according to claim 1 or 2, further comprising the components: a slow drying agent.
4. The aqueous release print coating material according to claim 1 or 2, further comprising the components: and (4) defoaming agent.
5. The aqueous release print coating material according to claim 1 or 2, further comprising the components: fumed silica and polyethylene wax.
6. The aqueous release print coating material according to claim 1 or 2, further comprising the components: a thickening agent.
7. The aqueous release print coating material according to claim 1 or 2, further comprising the components: and (3) a curing agent.
8. The preparation method of the water-based release printing coating material is characterized by mixing and uniformly stirring cationic acrylic acid, a color fixing agent, organic silicon, a wetting agent, a slow drying agent, a defoaming agent, fumed silica, polyethylene wax, a thickening agent and a curing agent to obtain the water-based release printing coating material.
9. The preparation method as claimed in claim 8, characterized in that the aqueous release printing coating material is obtained by mixing and stirring the cationic acrylic acid, the color fixing agent, the organic silicon, the wetting agent, the slow drying agent, the defoaming agent, the fumed silica and the polyethylene wax uniformly, then filtering, adding the thickening agent, stirring, and adding the curing agent in the stirring process until the stirring is uniform.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202211281936.7A CN115584178A (en) | 2022-10-19 | 2022-10-19 | Water-based release printing coating material and preparation method thereof |
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| CN202211281936.7A CN115584178A (en) | 2022-10-19 | 2022-10-19 | Water-based release printing coating material and preparation method thereof |
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Cited By (1)
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| CN116790165A (en) * | 2023-06-30 | 2023-09-22 | 常州勤邦新材料科技有限公司 | Coating composition for receiving and transferring aqueous pigment ink and film prepared from coating composition |
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