CN115531977A - Liquid-residue separator for extracting polyisoprene from dandelion and separation method thereof - Google Patents
Liquid-residue separator for extracting polyisoprene from dandelion and separation method thereof Download PDFInfo
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- CN115531977A CN115531977A CN202211523370.4A CN202211523370A CN115531977A CN 115531977 A CN115531977 A CN 115531977A CN 202211523370 A CN202211523370 A CN 202211523370A CN 115531977 A CN115531977 A CN 115531977A
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
- B01D36/04—Combinations of filters with settling tanks
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/96—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor in which the filtering elements are moved between filtering operations; Particular measures for removing or replacing the filtering elements; Transport systems for filters
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
The invention relates to the field of polyisoprene extraction and separation, in particular to a liquid-residue separator for extracting polyisoprene from dandelion and a separation method thereof. The clamping mechanism can be repeatedly separated through the curved surface sliding strip in the separation process to replace the filtering paper, and the curved surface sliding strip is reset and waits for the next replacement of the filtering paper under the guiding action of the rail limiting plate after the replacement is finished, so that the filtering paper is repeatedly prevented from being damaged due to pulling in the translation process, the repeated filtration cannot be continued, and the thoroughness in the separation process is effectively ensured.
Description
Technical Field
The invention relates to the field of polyisoprene extraction and separation, in particular to a liquid-residue separator for extracting polyisoprene from dandelion and a separation method thereof.
Background
The dandelion is a Chinese medicinal material used as both medicine and food, has rich bioactive components, high nutritive value, wide distribution and rich germplasm resources. The dandelion flavone, polyphenol and polysaccharide substances have the health care effects of resisting oxidation and aging, resisting tumors, improving immunity, inhibiting bacteria in a broad spectrum and the like, and are high-quality and safe functional additives for medicines, foods and the like.
Disclosure of Invention
The invention aims to solve the problems in the background art and provides a liquid-residue separator for extracting polyisoprene from dandelion and a separation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
the utility model provides a liquid residue separator that polyisoprene was used is drawed to dandelion, includes separation end jar, divides liquid top jar and initial solid ring, initial solid ring can cup joint the outside at separation end jar and divide liquid top jar through the screw thread, the outer wall of separation end jar has cup jointed the intermediate ring through the screw thread, the inner wall welding of intermediate ring has the scraping ring, the inside of separation end jar is equipped with heat transfer mechanism, the intermediate ring outer wall cup joints and is fixed with separation owner grillage, one side outer wall welding of separation owner grillage has the bull stick, the opposite side of bull stick is equipped with supporting mechanism, bull stick one side outer wall is equipped with paper changing mechanism, the top outer wall of bull stick has the rail limiting plate through the screw connection, one side outer wall that separation owner grillage was kept away from to the rail has the fixed strip through the screw connection, the top outer wall welding of fixed strip has balanced locating piece, the top outer wall of fixed strip has the curved surface draw runner through sliding connection, the curved surface draw runner keeps away from one side outer wall of separation owner grillage and has seted up the spacing groove, the both sides outer wall of balanced locating piece is provided with the reset spring between the inner wall that the corresponding with the spacing groove respectively, the separation end jar is equipped with the pressure release movable block, the inboard card is held to the separation end jar inboard movable block that presses.
In the liquid residue separator for extracting polyisoprene from dandelion, the heat transfer mechanism comprises a heat transfer cylinder plate and an electric connection plate, the heat transfer cylinder plate is welded on the inner wall of the separation bottom tank, the electric connection plate is inserted in the outer wall of the top of the separation bottom tank, an inner movable groove is formed in the separation bottom tank, a heat release plate is inserted in the inner movable groove, the outer wall of one side of the electric connection plate is electrically connected with two strip-type fixed conducting strips, a first movable conducting plate and a second movable conducting plate are respectively welded on the inner wall of the heat release plate, a reset spring is fixed between the outer wall of one side of each of the first movable conducting plate and the second movable conducting plate and the inner wall of the inner movable groove, and the first movable conducting plate and the second movable conducting plate are respectively in fixed contact with the corresponding strip-type fixed conducting strips.
In foretell liquid sediment separator that polyisoprene was used is drawed to dandelion, trade paper mechanism and include first filter paper section of thick bamboo, second filter paper section of thick bamboo and filter the note paper, a lateral wall of bull stick is pegged graft and is had two rotary columns and run through the opposite side that extends to the bull stick, and two rotary column symmetric distribution is at the both ends of bull stick, first filter paper section of thick bamboo and second filter paper section of thick bamboo cup joint respectively and fix in the corresponding rotary column outside, first filter paper section of thick bamboo and second filter paper section of thick bamboo outside all wrap up same filter the note paper, every the bull stick all cup joints and is fixed with the commentaries on classics fluted disc, and the commentaries on classics fluted disc is located the inside of bull stick, two same cingulum is cup jointed to the commentaries on classics fluted disc outside, and any one of commentaries on classics pole one side outer wall welding has the transmission button.
In the liquid residue separator for extracting polyisoprene from dandelion, two through holes are formed in the separation main plate frame, the outer side pressure release movable block and the inner side pressure release movable block are inserted into the corresponding through holes, and a butting groove is formed in one side wall of the inner side pressure release movable block, which is far away from the outer side pressure release movable block.
In foretell liquid sediment separator that polyisoprene was used is drawed to dandelion, there is the rail groove to seted up near one side outer wall of separation mainboard frame to the rail limiting plate, there is the rail limiting plate one side outer wall near separation mainboard frame to be connected with the gear post through the bearing, insection and cingulum mesh on the gear post mutually, the bottom outer wall welding of curved surface draw runner has the fixed sleeve post, peg graft in the bottom of fixed sleeve post has the post of living, be provided with balance spring between one side outer wall of post of living and the inner wall of fixed sleeve post, the bottom outer wall welding of post of living has insection card strip, and insection card strip meshes with the gear post mutually, insection card strip is close to one side outer wall welding of rail limiting plate has the track draw runner, and the track draw runner is located the track inslot portion slides.
In foretell liquid sediment separator that polyisoprene was used is drawed to dandelion, card is held the mechanism and is included two half snap rings, the spout has all been seted up to outside pressure release loose piece and the relative one side outer wall of inboard pressure release loose piece, two half snap ring is pegged graft inside the spout that corresponds, every the strip is held to the all welding of internal perisporium of half snap ring, every the periphery wall of half snap ring with correspond fixed mounting has a plurality of extrusion springs between the internal perisporium of spout, outside pressure release loose piece and the relative one side outer wall of inboard pressure release loose piece all weld have support the piece, every support one side outer wall of piece with be fixed with pressure release spring between the separation mainboard frame, two outer card grooves have been seted up to the outer wall symmetry of dividing the liquid top jar, every the card is held the strip and can the joint correspond inside the outer card groove.
In foretell liquid sediment separator that polyisoprene was used is drawed to dandelion, vary voltage mechanism includes a pressure section of thick bamboo and top cap, the top cap passes through the screw thread and pegs graft in minute liquid overhead tank, a vary voltage section of thick bamboo pegs graft inside the top cap and runs through, a plurality of extraction holes have been seted up to a vary voltage section of thick bamboo one side outer wall that is close to the separation end jar, a vary voltage section of thick bamboo inner wall has passive board and driving plate through sliding connection respectively, the inner wall welding of a vary voltage section of thick bamboo has the stationary ring board, be equipped with a plurality of answer springs between passive board and the stationary ring board, one side outer wall that the stationary ring board was kept away from to the driving plate bonds and has a plurality of rubber columns, and rubber column and extraction hole one-to-one.
In the liquid residue separator for extracting polyisoprene from dandelion, the outer wall of one side, away from the drawing hole, of the driving plate is welded with the variable pressure rod, the variable pressure rod penetrates through the variable pressure cylinder and extends to the outside, the outer wall of the other side of the variable pressure rod is bonded with the pressing sheet, the outside of the variable pressure cylinder is sleeved with the rotating ring through threads, and the rotating ring is connected with the outer wall of one side of the top cover through sliding.
In foretell liquid residue separator that polyisoprene was used is drawed to dandelion, supporting mechanism includes spliced pole and mobile jib, the spliced pole rotates the inside of pegging graft at the mobile jib, the spliced pole welding is kept away from at the bull stick one side outer wall of separation mobile jib frame, one side outer wall welding that the bull stick was kept away from has the upset turn-button, the outer wall of mobile jib has cup jointed respectively and has put board and bearing plate, and the bearing plate is located and puts the board under.
Compared with the prior art, the liquid-residue separator for extracting polyisoprene from dandelion has the advantages that:
1. the clamping mechanism can be repeatedly separated through the curved surface sliding strip in the separation process so as to be used for replacing the filtering paper, and after the replacement is finished, the curved surface sliding strip is reset and waits for the next replacement of the filtering paper under the guiding action of the rail limiting plate, so that the filtering paper is prevented from being damaged due to pulling in the translation process repeatedly in the replacement process, the repeated filtration cannot be continued, and the thoroughness in the separation process is effectively ensured;
2. the pressure inside the pressure-changing cylinder is changed by repeatedly controlling the pressure-changing rod, so that the repeated liquid-extracting process is realized, the separation effect of filtrate and filter residue in the separation bottom tank is accelerated, when the transmission knob is rotated to replace paper for filtration, the internal pressure is balanced with the atmospheric pressure when the liquid-separating top tank and the separation bottom tank are separated, the whole active plate of the pressing sheet is released, the pressure-changing cylinder is restored to the initial state under the action of the return spring, the repeated liquid-extracting is facilitated, the filtrate and the liquid residue in the separation bottom tank are completely separated, and the separation thoroughness is improved;
3. before staging, directly pressing down the whole sealed pressure swing cylinder after standing treatment, completely isolating and taking out supernatant liquid, ensuring that liquid slag can be completely separated from mixed liquid, and then completely separating the liquid slag to obtain the purest extracting solution by matching the operation of replacing filter paper for multiple times with repeated pumping pressure, so that the complete separation of the liquid slag and the extracting solution is effectively realized, and the efficiency of subsequently extracting polyisoprene is obviously improved;
in conclusion, the invention can directly centrifuge the mixed solution and pour the mixed solution into the device, completely separate the extracting solution and the residues for the first time, and can completely separate the liquid residues and the extracting solution by matching with the subsequent repeated operation of replacing the filter paper and extracting the pressure, and simultaneously, the concentration of the extracted solution before and after separation is not influenced, the completeness of the liquid residues and the extracted solution is effectively ensured, and the direct operation of extracting the polyisoprene for the subsequent time is convenient.
Drawings
FIG. 1 is a schematic diagram of the overall structure of a liquid-residue separator for extracting polyisoprene from dandelion provided by the present invention;
FIG. 2 is a schematic sectional perspective view of a liquid-residue separator for extracting polyisoprene from dandelion provided by the present invention;
FIG. 3 is an enlarged view of the structure of portion A of FIG. 2;
FIG. 4 is a schematic sectional perspective view of a heat transfer mechanism in a liquid-residue separator for extracting polyisoprene from dandelion provided by the present invention;
FIG. 5 is a schematic perspective view of the inner part of a pressure cylinder in a liquid-residue separator for extracting polyisoprene from dandelion provided by the present invention;
FIG. 6 is a schematic perspective view of a paper changing mechanism in a liquid-residue separator for extracting polyisoprene from dandelion provided by the present invention;
FIG. 7 is an enlarged view of the structure of portion B of FIG. 6;
FIG. 8 is a schematic perspective view of a retaining mechanism in a liquid-residue separator for extracting polyisoprene from dandelion provided by the present invention;
FIG. 9 is a schematic perspective view of an intermediate ring in a liquid-residue separator for extracting polyisoprene from dandelion provided by the present invention;
FIG. 10 is a schematic view of a disassembled three-dimensional structure of a retaining mechanism in a liquid-residue separator for extracting polyisoprene from dandelion provided by the invention;
FIG. 11 is an enlarged view of the structure of portion C of FIG. 10;
FIG. 12 is a schematic view of a three-dimensional disassembled structure of an inner side pressure release loose piece, a curved surface clamping strip and a connecting piece thereof in a liquid residue separator for extracting polyisoprene from dandelion provided by the invention;
FIG. 13 is a schematic view of a disassembled three-dimensional structure of a catching mechanism in a liquid-residue separator for extracting polyisoprene from dandelion provided by the present invention;
FIG. 14 is a schematic perspective view of a toothed fastener strip and a connecting piece thereof in a liquid-residue separator for extracting polyisoprene from dandelion provided by the invention;
FIG. 15 is a schematic perspective sectional view of another connection state of a bottom separating tank and a top separating tank in a liquid-residue separator for extracting polyisoprene from dandelion provided by the present invention;
FIG. 16 is a schematic perspective view of another connected separation bottom tank and separation top tank in a liquid residue separator for extracting polyisoprene from dandelion.
In the figure: 1. separating the bottom tank; 10. an outer clamping groove; 11. an inner movable groove; 12. initial ring fixing; 2. a liquid separation top tank; 4. a rotating rod; 41. separating the mainboard frame; 410. a through hole; 411. an intermediate ring; 412. scraping rings; 42. a rail limiting plate; 421. a track groove; 422. a gear post; 5. a main rod; 51. placing a plate; 52. a bearing plate; 53. turning over the knob; 531. connecting columns; 60. a half snap ring; 601. clamping the strip; 61. an outer pressure relief loose piece; 62. an inner pressure release loose piece; 621. a chute; 622. a resisting block; 623. a pressure-releasing spring; 624. a compression spring; 625. a butt joint groove; 64. a curved surface slider; 641. fixing the sleeve column; 642. a plunger; 643. a balance spring; 65. a fixing strip; 66. a balance positioning block; 67. the insection clamping strip; 671. a rail slide post; 68. a return spring; 69. a limiting groove; 71. turning the column; 711. a first filter paper cartridge; 712. a second filter paper cylinder; 713. a transmission turn button; 714. a rotary fluted disc; 72. filtering paper; 74. a toothed belt; 8. a top cover; 81. tabletting; 82. a variable compression bar; 83. a pressure changing cylinder; 831. a passive plate; 832. a driving plate; 833. drawing the hole; 834. a rubber column; 835. a stationary ring plate; 836. a return spring; 84. rotating the ring; 9. a power connection plate; 91. strip-type fixed conducting strips; 911. a first movable conductive plate; 921. a second movable conductive plate; 93. a heat releasing plate; 94. a return spring; 95. a heat transfer cartridge plate.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.
In the description of the present invention, it is to be understood that the terms "upper", "lower", "front", "rear", "left", "right", "top", "bottom", "inner", "outer", and the like, indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, are merely for convenience in describing the present invention and simplifying the description, and do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus, should not be construed as limiting the present invention.
Referring to fig. 1-16, a liquid residue separator for extracting polyisoprene from dandelion and a separation method thereof, comprises a separation bottom tank 1, a liquid separation top tank 2 and an initial solid ring 12, wherein the initial solid ring 12 can be sleeved outside the separation bottom tank 1 and the liquid separation top tank 2 through threads, the outer wall of the separation bottom tank 1 is sleeved with a middle ring 411 through threads, the inner wall of the middle ring 411 is welded with a scraping ring 412, the inside of the separation bottom tank 1 is provided with a heat transfer mechanism, the outer wall of the middle ring 411 is sleeved and fixed with a separation main plate frame 41, the outer wall of one side of the separation main plate frame 41 is welded with a rotating rod 4, the other side of the rotating rod 4 is provided with a supporting mechanism, the outer wall of one side of the rotating rod 4 is provided with a paper changing mechanism, the outer wall of the top of the rotating rod 4 is connected with a limiting plate rail 42 through a screw, the outer wall of one side of the rail limiting plate 42, which is far away from the separation main plate frame 41, is connected with a fixing strip 65 through a screw, the outer wall of the top of the fixing strip 65 is welded with a balance positioning block 66, the outer wall of the top of the fixing strip 65 is connected with a curved surface slide strip 64 through a sliding way, a limiting groove 69 is formed in the outer wall of one side of the curved surface slide strip 64, which is far away from the separation main plate frame 41, the balance positioning block 66 is positioned in the limiting groove 69 to slide, a restoring spring 68 is arranged between the inner walls, which correspond to the limiting groove 69, of the outer walls of the two sides of the balance positioning block 66 respectively, an outer side pressure release movable block 61 and an inner side pressure release movable block 62 are inserted into the separation main plate frame 41 respectively, the outer side pressure release movable block 61 and the inner side pressure release movable block 62 are respectively provided with a clamping mechanism, and one side of the separating top tank 2, which is far away from the separating bottom tank 1, is provided with a pressure transformation mechanism.
Specifically, when fine separation is performed, pressure releasing and sealing operations need to be repeated for multiple times, and then when the top liquid separating tank 2 is separated from the bottom separating tank 1, the outer pressure releasing movable block 61 and the inner pressure releasing movable block 62 need to be jacked up by translation of the curved surface slide bar 64, the curved surface structure arranged at the top of the curved surface slide bar 64 enables the curved surface slide bar 64 to jack up the outer pressure releasing movable block 61 and the inner pressure releasing movable block 62 no matter which side of the length direction of the fixed bar 65 translates, the fixed top liquid separating tank 2 and the bottom separating tank 1 are synchronously driven to be separated for a short time, a plurality of restoring springs 68 are in a stressed state when the curved surface slide bar 64 moves, when the curved surface slide bar 64 is not bound, the restoring springs 68 are restored to a balanced state from the stressed state to reset the curved surface slide bar 64, and the most sunken part of the curved surface slide bar 64 is in contact with the inner pressure releasing movable block 62 during reset, so that the outer pressure releasing movable block 61 and the inner pressure releasing movable block 62 are restored to an initial state.
The variable pressure mechanism includes a variable pressure cylinder 83 and a top cover 8, the top cover 8 is inserted in the top separating tank 2 through threads, the variable pressure cylinder 83 is inserted inside the top cover 8 and penetrates through the variable pressure cylinder, the variable pressure cylinder 83 is close to one side outer wall of the bottom separating tank 1 and is provided with a plurality of drawing holes 833, the inner wall of the variable pressure cylinder 83 is respectively connected with a driven plate 831 and an active plate 832 through sliding, the inner wall of the variable pressure cylinder 83 is welded with a fixed annular plate 835, a plurality of return springs 836 are arranged between the driven plate 831 and the fixed annular plate 835, one side outer wall of the active plate 832 far away from the fixed annular plate 835 is bonded with a plurality of rubber columns 834, the rubber columns 834 correspond to the drawing holes 833 one to one, one side outer wall of the active plate 832 far away from the drawing holes 833 is welded with a variable pressure rod 82, the variable pressure rod 82 penetrates through the variable pressure cylinder 83 and extends to the outside, the other side outer wall of the variable pressure rod 82 is bonded with a pressing sheet 81, the outside of the variable pressure cylinder 83 is sleeved with a rotating ring 84 through threads, and one side outer wall of the rotating ring 84 and the top cover 8 is connected through sliding.
The external thread of the thin end of the variable pressure cylinder 83 is screwed with the rotary ring 84, the whole variable pressure cylinder 83 can be moved to the position jointed with the top liquid separating tank 2 by rotating the rotary ring 84 for six circles, so that the top liquid separating tank 2 is kept in a closed state, and the variable pressure cylinder 83 can be restored to the initial position by reversely rotating the rotary ring 84 for six circles.
Specifically, initial solid ring 12 is used for carrying on when preliminary separation of stewing with separating end jar 1 and separating liquid top jar 2 through the screw cup joint at the depressed part between them, makes separating end jar 1 and separating liquid top jar 2 fixed, the state of the inside original paper of a vary voltage section of thick bamboo 83 this moment is: the return spring 836 is in an unstressed state; the rubber column 834 is inserted into the corresponding drawing hole 833 to enable the transformer cylinder 83 to be in a sealed state; the driven plate 831 is attached to the inner wall of the pressure-changing cylinder 83 provided with the drawing hole 833; the driving plate 832 is closely attached to the driven plate 831.
With further reference to fig. 16, after standing completely, the rotating ring 84 is rotated to enable the variable pressure cylinder 83 to move towards the inside of the liquid separation top tank 2, until the peripheral wall of the variable pressure cylinder 83 is attached to the inner peripheral wall of the liquid separation top tank 2, so that the liquid separation top tank 2 is separated from the space inside the separation bottom tank 1, wherein the thread pitch at the position above the variable pressure cylinder 83 influences the speed of moving down the variable pressure cylinder 83 when the rotating ring 84 is rotated, the variable pressure cylinder 83 slowly presses down, part of the clear liquid above the separation bottom tank 1 can be pressed into the inside of the liquid separation top tank 2, and the dandelion powder precipitated at the bottom cannot be brought into the inside of the liquid separation top tank 2 by the fluid, so that the dandelion liquid residue and the primary complete separation of the extracting solution are realized.
The heat transfer mechanism comprises a heat transfer barrel plate 95 and an electric connection plate 9, the heat transfer barrel plate 95 is welded on the inner wall of the separation bottom tank 1, the electric connection plate 9 is inserted into the outer wall of the top of the separation bottom tank 1, an inner movable groove 11 is formed in the separation bottom tank 1, a heat release plate 93 is inserted into the inner movable groove 11, the outer wall of one side of the electric connection plate 9 is electrically connected with two strip-type fixed conducting plates 91, a first movable conducting plate 911 and a second movable conducting plate 921 are welded on the inner wall of the heat release plate 93 respectively, a reset spring 94 is fixed between the outer wall of one side of the first movable conducting plate 911 and the second movable conducting plate 921 and the inner wall of the inner movable groove 11, and the first movable conducting plate 911 and the second movable conducting plate 921 are in contact with the corresponding strip-type fixed conducting plates 91 respectively.
With specific reference to fig. 3 and 4, when the power connection plate 9 is powered on, the first movable conductive plate 911 and the second movable conductive plate 921 are powered on through the strip type fixed conductive plate 91, the first movable conductive plate 911 and the second movable conductive plate 921 are respectively fixed on the inner side of the heat release plate 93, and the heat release plate 93 is powered on to release heat, so that the inside of the separation bottom tank 1 is heated and dried; the heat releasing plate 93 can be easily jogged in the separating bottom tank 1 for balancing partial air pressure change in the separating bottom tank 1, the return spring 94 is used for returning the heat releasing plate 93 to a balanced position, the jogged heat releasing plate 93 can also drive the first movable conductive plate 911 and the second movable conductive plate 921 which are fixed with the jogged heat releasing plate 93 to move, so that the heat releasing plate can be in a state of not contacting with the two strip-type fixed conductive plates 91, at the moment, the first movable conductive plate 911 and the second movable conductive plate 921 are respectively not conducted with the corresponding strip-type fixed conductive plates 91, the heat releasing plate 93 cannot be electrified to release heat, and the balanced heat releasing plate 93 can enable the first movable conductive plate 911 and the second movable conductive plate 921 to be respectively conducted with the corresponding strip-type fixed conductive plates 91.
The paper changing mechanism comprises a first filter paper cylinder 711, a second filter paper cylinder 712 and filter paper 72, two rotary columns 71 are inserted into one side wall of the rotary rod 4 and extend to the other side of the rotary rod 4 in a penetrating mode, the two rotary columns 71 are symmetrically distributed at two ends of the rotary rod 4, the first filter paper cylinder 711 and the second filter paper cylinder 712 are fixedly sleeved outside the corresponding rotary columns 71 respectively, the same filter paper 72 wraps the first filter paper cylinder 711 and the second filter paper cylinder 712, a rotary toothed disc 714 is fixedly sleeved on each rotary rod 4, the rotary toothed disc 714 is located inside the rotary rod 4, the same toothed belt 74 is sleeved outside the two rotary toothed discs 714, and a transmission rotary button 713 is welded on the outer wall of one side of any rotary column 71.
With particular reference to fig. 1 and 6, rotating the transmission knob 713 rotates the rotary column 71 to drive the second filter paper cylinder 712 to rotate, and the corresponding toothed belt 74 engaged with the rotary toothed disc 714 enables the first filter paper cylinder 711 on the other rotary column 71 to rotate synchronously, so that the filter paper 72 translates between the top liquid separating tank 2 and the middle ring 411, the transmission knob 713 rotates three times to drive the filter paper 72 located at the clamping position to completely separate and re-enter the roll, and the new filter paper 72 enters the clamping position to wait for downward movement of the filter work.
Two through holes 410 are formed in the separation mainboard frame 41, the outer side pressure release movable block 61 and the inner side pressure release movable block 62 are inserted into the corresponding through holes 410, a butting groove 625 is formed in one side wall, away from the outer side pressure release movable block 61, of the inner side pressure release movable block 62, and the inner wall of the top of the butting groove 625 is in contact with the curved surface arranged at the top of the curved surface slide bar 64.
Specifically, when the toothed belt 74 moves, the gear column 422 is driven to rotate, so that the toothed rack bar 67 also engaged with the toothed rack bar is driven to move, the curved surface slide bar 64 is driven to translate, in the process, the rail slide column 671 is always located inside the rail groove 421 to slide, the unstressed state of the balance spring 643 can ensure that the toothed rack bar 67 is engaged with the gear column 422, when the rail slide column 671 is located in the long linear rail of the rail groove 421, the balance spring 643 is in a stretched state, when the rail slide column 671 is located in the end linear rail of the rail groove 421, the balance spring 643 is in a compressed state, and the toothed rack bar 67 is disengaged from the gear column 422, when the rail slide column 671 moves to the edge position of the rail groove 421, the balance spring 643 returns to the unstressed state from the slightly stretched state to slightly lift the rail slide column 671, and because each return spring 68 when the rail slide column 671 moves to the edge position of the rail groove 421 is in the unbalanced state, the stretched or the compressed state of the return spring 68 is released, so that the toothed rack bar 67 and the central slide column 671 and the return to the central slide column 671 moves to the central curved surface groove 421 until the central slide column comes into the central groove 421, and the central slide column comes into the central slide bar 67 is not to return to the central groove 421, and the central slide bar 67.
The clamping mechanism comprises two half clamping rings 60, sliding grooves 621 are formed in the outer wall of one side, opposite to the outer side pressure release movable block 61 and the inner side pressure release movable block 62, the two half clamping rings 60 are inserted into the corresponding sliding grooves 621 in an inserted mode, clamping strips 601 are welded to the inner peripheral wall of each half clamping ring 60, a plurality of extrusion springs 624 are fixedly installed between the outer peripheral wall of each half clamping ring 60 and the inner peripheral wall of the corresponding sliding groove 621, abutting blocks 622 are welded to the outer wall of one side, opposite to the outer side pressure release movable block 61 and the inner side pressure release movable block 62, pressure release springs 623 are fixed between the outer wall of one side of each abutting block 622 and the separation main plate frame 41, two outer clamping grooves 10 are symmetrically formed in the outer wall of the liquid separation top tank 2, and each clamping strip 601 can be clamped inside the corresponding outer clamping groove 10.
Specifically referring to fig. 1, 8 and 10, the outer pressure-releasing movable block 61 and the inner pressure-releasing movable block 62 penetrate through corresponding through holes 410 formed in the separation main plate frame 41, wherein the abutting blocks 622 and the half clasps 60 are respectively located at two sides of the separation main plate frame 41, and the pressure-releasing springs 623 between the abutting blocks 622 and the separation main plate frame 41 are used for clamping the filter paper 72 so that the separating top can 2 clamped by the half clasps 60 is always close to the middle ring 411, and then when the outer pressure-releasing movable block 61 and the inner pressure-releasing movable block 62 are pressed by the pressure-releasing springs 623, the separating top can 2 clamped by the half clasps 60 is slightly lifted, so that the filter paper 72 is not clamped, and the filter paper 72 can also move.
Further, two half snap rings 60 are used for centre gripping liquid separation top jar 2, and wherein hold strip 601 and can correspond the outer draw-in groove 10 of card in liquid separation top jar 2 both sides, and when liquid separation top jar 2 was inserted, extrusion spring 624 slightly contracts, until holding strip 601 card income outer draw-in groove 10, extrusion spring 624 application of force is fixed liquid separation top jar 2 through half snap ring 60.
The supporting mechanism comprises a connecting column 531 and a main rod 5, the connecting column 531 is rotatably inserted into the main rod 5, the connecting column 531 is welded on the outer wall of one side, away from the separation main rod frame 41, of the rotating rod 4, the connecting column 531 is welded on the outer wall of one side, away from the rotating rod 4, of the rotating rod 4, is provided with a turnover rotating button 53, the outer wall of the main rod 5 is respectively sleeved with a placing plate 51 and a bearing plate 52, and the bearing plate 52 is located under the placing plate 51.
Referring specifically to fig. 1, the bearing plate 52 of bottom is used for supporting whole device, places the board 51 and can place separation end jar 1 or divide liquid top jar 2 alone, and spliced pole 531 is pegged graft and is run through the inside of mobile jib 5, and the rotation of upset turn-knob 53 can drive spliced pole 531 and the rotation of fixed bull stick 4 to invert whole fixed separation end jar 1 and divide liquid top jar 2.
The working principle is as follows:
when in use, the initial fixed ring 12 is firstly fixed with the bottom separating bottom tank 1, then the top separating tank 2 is screwed in and fixed into a whole, then the top cover 8 is opened to introduce dandelion sample liquid to be separated, the pressure-changing cylinder 83 is not contacted with the top separating tank 2 when standing, the rotating ring 84 is rotated after standing is finished to enable the pressure-changing cylinder 83 to be contacted with the top separating tank 2, then the top separating tank 2 is screwed out to pour clear liquid out and independently place, the initial fixed ring 12 is taken out, the bottom separating tank 1 is fixed in the middle ring 411, the rotating ring 84 is rotated until the pressure-changing cylinder 83 is not contacted with the top separating tank 2, the top separating tank 2 is inserted until the clamping strip 601 is clamped into the outer clamping groove 10, then the pressing sheet 81 is simply pressed, at the moment, the driven plate 831 is driven to move downwards to reduce the air pressure in the top separating tank 2, moisture in the bottom separating tank 1 is pumped into the top separating tank 2 from the top through the filtering paper 72, when the pressing sheet 81 is released and the transmission rotating button 713 is rotated, the return spring 836 returns to lift the driving plate 832, the filter paper 72 moves, the transmission rotating button 713 drives the rotating column 71 to rotate, the meshed gear column 422 rotates along with the gear belt 74, the meshed insection clamping strip 67 moves to enable the curved surface sliding strip 64 at the top to slide and jack up the clamping mechanism, so that the pressure is relieved, the filter paper 72 also moves horizontally, when the filter paper 72 moves, the scraper ring 412 acts on the filter paper 72, liquid residues on the surface of the filter paper 72 are still retained in the separating bottom tank 1, and finally the curved surface sliding strip 64 resets to wait for the next transmission, so that the filter paper 72 is replaced, the repeated suction filtration effect is realized, the dandelion liquid residues are completely separated, the mixed liquid is retained, and the polyisoprene is completely extracted.
The separation method of the liquid residue for extracting polyisoprene from the taraxacum officinale in any embodiment comprises the following steps:
s1, weighing 25g of an air-dried dandelion sample, adding 200mL of NaOH solution with the mass fraction of 10%, ultrasonically crushing for 4h under the condition of 30Hz, pouring the sample subjected to ultrasonic treatment into a centrifuge tube, centrifuging for 2min at the normal temperature under the condition of 5000r/min, discarding supernatant, adding distilled water into the centrifuge tube, continuing centrifuging, and repeating the centrifuging conditions until the pH is = 7;
s2, after the last centrifugation, pouring the mixed liquid into a separation bottom tank 1 and a liquid separation top tank 2 fixed by an initial fixed ring 12, screwing a top cover 8, standing for 30min, rotating a rotating ring 84 six times, screwing out the liquid separation top tank 2, pouring out the upper layer liquid for independent storage, taking out the initial fixed ring 12, screwing the separation bottom tank 1 into a middle ring 411, rotating the rotating ring 84 six times, inserting the liquid separation top tank 2 into a semi-clamping ring 60, and rotating and turning a rotating button 53 to invert the separation bottom tank;
s3, rotating the transmission knob 713 for three circles after standing for 30min, repeating the operation for 3-4 times, pulling the outer side pressure release movable block 61 outwards, taking out the separation liquid in the liquid separation top tank 2, and placing the separation liquid separately for later use;
s4, pressing the pressing sheet 81 to the horizontal height position of the bearing plate 52, enabling the driven plate 831 to move downwards under the action of negative pressure, enabling the mixed liquid in the separation bottom tank 1 to flow into the top liquid separation tank 2 under the filtering effect of the filtering paper 72 in the process, rotating the transmission rotating button 713 for three circles after pressing for 2-3min, replacing the filtering paper 72, and repeating the operation of pressing the pressing sheet 81 after the bottom pressing sheet 81 is reset;
and S5, repeating the operation in the step S4 for 5 times, taking out the separation liquid in the top liquid separation tank 2, putting the separation liquid in the step S3, rotating the turnover button 53 to enable the bottom separation tank 1 to be positioned at the bottom, and electrifying the electric plate 9 for drying to obtain completely separated liquid residues.
Further, unless otherwise specifically stated or limited, the above-described fixed connection is to be understood in a broad sense, and may be, for example, welded, glued, or integrally formed as is conventional in the art.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (9)
1. The utility model provides a liquid sediment separator that polyisoprene was used is extracted to dandelion, includes separation end jar (1), divides liquid top jar (2) and initial solid ring (12), its characterized in that: initial solid ring (12) can cup joint the outside at separation end jar (1) and separating top jar (2) through the screw thread, the outer wall of separation end jar (1) has cup jointed intermediate ring (411) through the screw thread, the inner wall welding of intermediate ring (411) has scraping ring (412), the inside of separation end jar (1) is equipped with heat transfer mechanism, intermediate ring (411) outer wall cup joints and is fixed with separation mainboard frame (41), one side outer wall welding of separation mainboard frame (41) has bull stick (4), the opposite side of bull stick (4) is equipped with supporting mechanism, bull stick (4) one side outer wall is equipped with paper changing mechanism, the top outer wall of bull stick (4) has rail limiting plate (42) through the screw connection, one side outer wall that separation mainboard frame (41) was kept away from to rail limiting plate (42) has fixed strip (65) through the screw connection, the top outer wall welding of fixed strip (65) has balanced locating piece (66), the top outer wall of fixed strip (65) has curved surface draw runner (64) through sliding connection, one side outer wall that separation mainboard frame (41) kept away from separation mainboard frame (41) has seted up one side has balanced locating piece (69) and has the inside pressure groove (69) and has the pressure limiting block (69), the inboard spacing groove (69) is provided with the pressure spring (69) respectively and the pressure clamp block (62) and the outside of the pressure clamp (69), the inboard side of the pressure block (69) and the pressure clamp (62) The outer side pressure release movable block (61) and the inner side pressure release movable block (62) are respectively provided with a clamping mechanism, and one side of the liquid separation top tank (2) far away from the separation bottom tank (1) is provided with a pressure changing mechanism.
2. The liquid-residue separator for extracting polyisoprene from dandelion as claimed in claim 1, wherein: the heat transfer mechanism comprises a heat transfer barrel plate (95) and an electric connection plate (9), the heat transfer barrel plate (95) is welded on the inner wall of the separation bottom tank (1), the electric connection plate (9) is inserted into the outer wall of the top of the separation bottom tank (1), an inner movable groove (11) is formed in the separation bottom tank (1), a heat release plate (93) is inserted into the inner movable groove (11), the outer wall of one side of the electric connection plate (9) is electrically connected with two strip type fixed conducting plates (91), the inner wall of the heat release plate (93) is respectively welded with a first movable conducting plate (911) and a second movable conducting plate (921), a reset spring (94) is fixed between the outer wall of one side of the first movable conducting plate (911) and the outer wall of one side of the second movable conducting plate (921) and the inner wall of the inner movable groove (11), and the first movable conducting plate (911) and the second movable conducting plate (921) are respectively contacted with the corresponding strip type fixed conducting plates (91).
3. The liquid-residue separator for extracting polyisoprene from dandelion as claimed in claim 1, wherein: paper changing mechanism includes first filter paper tube (711), second filter paper tube (712) and filters paper (72), a lateral wall of bull stick (4) is pegged graft and is had two rotary columns (71) and runs through the opposite side that extends to bull stick (4), and two rotary columns (71) symmetric distribution is at the both ends of bull stick (4), first filter paper tube (711) and second filter paper tube (712) cup joint respectively and fix in corresponding rotary column (71) outside, first filter paper tube (711) and second filter paper tube (712) outside all wrap up same filter paper (72), every rotary rod (4) all cup joint and are fixed with commentaries on classics fluted disc (714), and commentaries on classics fluted disc (714) are located the inside of bull stick (4), two same cingulum (74) have been cup jointed to changeing fluted disc (714) outside, arbitrary one side outer wall welding of rotary column (71) has transition knob (713).
4. The liquid-residue separator for extracting polyisoprene from dandelion as claimed in claim 1, wherein: two through holes (410) are formed in the separation mainboard frame (41), the outer side pressure release movable block (61) and the inner side pressure release movable block (62) are inserted into the corresponding through holes (410), and a butting groove (625) is formed in one side wall, far away from the outer side pressure release movable block (61), of the inner side pressure release movable block (62).
5. The liquid-residue separator for extracting polyisoprene from dandelion as claimed in claim 1, wherein: there has been track groove (421) to have been seted up to one side outer wall that has had close to separation mainboard frame (41) rail limiting plate (42), there has gear column (422) to have one side outer wall that has close to separation mainboard frame (41) rail limiting plate (42) through the bearing connection, insection and cingulum (74) on gear column (422) mesh mutually, the welding of the bottom outer wall of curved surface draw runner (64) has fixed set post (641), it has loose column (642) to peg graft in the bottom of fixed set post (641), be provided with between one side outer wall of loose column (642) and the inner wall of fixed set post (641) balancing spring (643), the welding of the bottom outer wall of loose column (642) has insection draw runner (67), and insection draw runner (67) mesh mutually with gear column (422), insection draw runner (67) are close to one side outer wall welding of rail limiting plate (42) and have track draw runner (671), and track draw runner (671) are located the inside slip of track groove (421).
6. The liquid-residue separator for extracting polyisoprene from dandelion as claimed in claim 1, wherein: the mechanism is held to card includes two half snap rings (60), spout (621) have all been seted up to outside pressure release loose piece (61) and the relative one side outer wall of inboard pressure release loose piece (62), two spout (621) that correspond is pegged graft inside half snap ring (60), every the internal perisporium of half snap ring (60) all welds and holds strip (601), every the periphery wall of half snap ring (60) and corresponding fixed mounting has a plurality of extrusion spring (624) between the internal perisporium of spout (621), outside pressure release loose piece (61) and the relative one side outer wall of inboard pressure release loose piece (62) all weld and support piece (622), every support one side outer wall of piece (622) with be fixed with pressure release spring (623) between separation main plate frame (41), two outer draw-in groove (10) have been seted up to the outer wall symmetry of dividing liquid top jar (2), every the strip (601) is held the joint and is corresponding inside outer draw-in groove (10).
7. The liquid-residue separator for extracting polyisoprene from dandelion as claimed in claim 1, wherein: the variable pressure mechanism includes a variable pressure cylinder (83) and a top cover (8), top cover (8) are pegged graft in separating a jar (2) through the screw thread, a variable pressure cylinder (83) are pegged graft inside top cover (8) and are run through, a variable pressure cylinder (83) have been seted up a plurality of holes (833) of taking out near one side outer wall of separating end jar (1), a variable pressure cylinder (83) inner wall has passive plate (831) and driving plate (832) through sliding connection respectively, the inner wall welding of a variable pressure cylinder (83) has fixed crown plate (835), be equipped with a plurality of answer spring (836) between passive plate (831) and fixed crown plate (835), one side outer wall that driving plate (832) kept away from fixed crown plate (835) bonds and has a plurality of rubber columns (834), and rubber column (834) and take out hole (833) one-to-one.
8. The liquid-residue separator for extracting polyisoprene from dandelion as claimed in claim 7, wherein: the outer wall of one side of the driving plate (832) far away from the drawing hole (833) is welded with a pressure-changing rod (82), the pressure-changing rod (82) penetrates through a pressure-changing cylinder (83) and extends to the outside, the outer wall of the other side of the pressure-changing rod (82) is bonded with a pressing sheet (81), the outside of the pressure-changing cylinder (83) is sleeved with a rotating ring (84) through threads, and the rotating ring (84) is connected with the outer wall of one side of the top cover (8) in a sliding mode.
9. The liquid-residue separator for extracting polyisoprene from dandelion as claimed in claim 1, wherein: the supporting mechanism includes spliced pole (531) and mobile jib (5), spliced pole (531) are rotated and are pegged graft in the inside of mobile jib (5), spliced pole (531) welding is kept away from in bull stick (4) one side outer wall of separation mobile jib frame (41), one side outer wall welding that bull stick (4) were kept away from in spliced pole (531) has upset turn-button (53), the outer wall of mobile jib (5) has been cup jointed respectively and has been put board (51) and bearing plate (52), and bearing plate (52) are located and put board (51) under.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211523370.4A CN115531977B (en) | 2022-12-01 | 2022-12-01 | Liquid-residue separator for extracting polyisoprene from dandelion and separation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211523370.4A CN115531977B (en) | 2022-12-01 | 2022-12-01 | Liquid-residue separator for extracting polyisoprene from dandelion and separation method thereof |
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| CN115531977B CN115531977B (en) | 2023-03-10 |
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| DE202021103460U1 (en) * | 2020-08-13 | 2021-07-19 | Suzhou Jingtian Airen Environmental Technology Co., Ltd. | Oil-water separator to facilitate the filtration of slag |
| CN113716761A (en) * | 2021-11-02 | 2021-11-30 | 烟台洁通水处理技术有限公司 | Separating liquid ultrafiltration desiliconization equipment of steam generator |
| CN113941180A (en) * | 2021-11-15 | 2022-01-18 | 洛阳万基铝加工有限公司 | Automatic paper system that trades of aluminium foil mill filter |
| CN216023439U (en) * | 2021-11-09 | 2022-03-15 | 山东初饮生物科技有限公司 | Slurry-residue separation device for yoghourt processing |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN204233864U (en) * | 2014-09-26 | 2015-04-01 | 中色科技股份有限公司 | A kind of location of the filtration paper roll for plate filter modifying device |
| DE202021103460U1 (en) * | 2020-08-13 | 2021-07-19 | Suzhou Jingtian Airen Environmental Technology Co., Ltd. | Oil-water separator to facilitate the filtration of slag |
| CN113716761A (en) * | 2021-11-02 | 2021-11-30 | 烟台洁通水处理技术有限公司 | Separating liquid ultrafiltration desiliconization equipment of steam generator |
| CN216023439U (en) * | 2021-11-09 | 2022-03-15 | 山东初饮生物科技有限公司 | Slurry-residue separation device for yoghourt processing |
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