CN115491772A - Method for preparing degradable Jujun grass fiber material - Google Patents

Method for preparing degradable Jujun grass fiber material Download PDF

Info

Publication number
CN115491772A
CN115491772A CN202211315147.0A CN202211315147A CN115491772A CN 115491772 A CN115491772 A CN 115491772A CN 202211315147 A CN202211315147 A CN 202211315147A CN 115491772 A CN115491772 A CN 115491772A
Authority
CN
China
Prior art keywords
hay
cooking
preparing
fiber
fiber material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202211315147.0A
Other languages
Chinese (zh)
Inventor
叶彬
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fuzhou Zhirui Enterprise Management Co ltd
Original Assignee
Fuzhou Zhirui Enterprise Management Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fuzhou Zhirui Enterprise Management Co ltd filed Critical Fuzhou Zhirui Enterprise Management Co ltd
Priority to CN202211315147.0A priority Critical patent/CN115491772A/en
Publication of CN115491772A publication Critical patent/CN115491772A/en
Pending legal-status Critical Current

Links

Classifications

    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01CCHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
    • D01C1/00Treatment of vegetable material
    • D01C1/02Treatment of vegetable material by chemical methods to obtain bast fibres

Landscapes

  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Molecular Biology (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Textile Engineering (AREA)
  • Paper (AREA)
  • Chemical And Physical Treatments For Wood And The Like (AREA)

Abstract

The invention discloses a method for preparing a degradable Jujun grass fiber material, which comprises the following steps: obtaining Jujun grass hay or fresh Jujun grass, mechanically cutting the Jujun grass hay into a grass section with the length of 15cm-25cm by using a machine, carrying out vibration screening and dust removal on the cut hay, removing impurities and dust attached to the hay, and rolling and cracking the hay for later use; preparing a soaking solution, soaking the prepared hay, taking out the hay after soaking for a period of time, washing the hay with clear water, and draining for later use; preparing a cooking liquid, adding the drained pennisetum hydridum in the step S2 into the cooking liquid, and cooking for 3-4 hours at the temperature of 95-100 ℃ and under normal pressure; acid washing the fiber obtained after cooking, measuring the pH value of the solution by using a pH meter or pH test paper until the pH value is neutral, kneading the fiber, rinsing the fiber by using clear water, heating the fiber to 40-50 ℃ after the fiber is kneaded to be completely dispersed, and soaking the fiber; and (4) drying the rinsed fiber under natural conditions or putting the fiber into a dryer for drying.

Description

Method for manufacturing degradable Jujun grass fiber material
Technical Field
The invention relates to the technical field of Jujun grass fiber materials, in particular to a method for manufacturing a degradable Jujun grass fiber material.
Background
At present, most textile fibers are prepared by extracting from bamboos, the production of the bamboo fibers basically adopts the procedures of cutting, slicing, green removing, yellow removing, cooking, rolling into bamboo tows and the like, the process of firstly forming the bamboo chips and then forming the bamboo fiber tows cannot be separated, the processing technology is laggard, the production efficiency is low, the function of processing equipment is single, and the waste of processing materials is serious. At present, the technology for preparing the bamboo fiber from the bamboo is in the starting stage, is not perfect, has low production efficiency, and has overhigh impurity content in the prepared bamboo fiber, so that the bamboo fiber can not be produced in a large scale.
The Jujun grass is a good raw material for preparing natural fiber, and the fiber material prepared from the Jujun grass has better air permeability, antibacterial property and radiation resistance than bamboo fiber.
According to the searched patent document with the publication number of CN106995939A, disclosed is a Megalobatrachus giganteus fibril chemically prepared by truncating Megalobatrachus giganteus, preparing a soaking solution to soak the Megalobatrachus giganteus fibril, taking out the soaked Megalobatrachus giganteus fibril, standing and cleaning the Megalobatrachus giganteus fibril, preparing a cooking solution to cook and stir the Megalobatrachus giganteus fibril, kneading, cleaning and airing the Megalobatrachus giganteus fibril to obtain the Megalobatrachus giganteus fibril with low impurity content. However, the Jujun grass raw material is adhered with dust and impurities when not used, and the Jujun grass raw material is not treated and directly soaked, so that the impurities and the dust are always adhered to the hay, the preparation of the fiber raw material is influenced, and the impurity content of the fiber material is high.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention provides the method for manufacturing the degradable Jujun grass fiber material, wherein the chopped hay is subjected to vibration screening for dedusting, impurities and dust attached to the hay are removed, the influence of the impurities and dust on cooking liquor, namely the preparation of the fiber material, can be avoided, the fiber material prepared by the scheme has low impurity content, and the finally prepared fiber material is relatively pure.
In order to solve the technical problems, the invention provides the following technical scheme: the method for manufacturing the degradable Jujun grass fiber material comprises the following steps:
s1, obtaining giant-mycorrhizal hay or fresh giant-mycorrhizal hay, mechanically cutting the giant-mycorrhizal hay into a grass section with the length of 15cm-25cm by using a machine, performing vibration screening and dust removal on the cut hay, removing impurities and dust attached to the hay, and then rolling and cracking the hay for later use;
s2, preparing a wetting solution, soaking the prepared hay, taking out the hay after soaking for a period of time, washing the hay with clear water, and draining for later use;
s3, preparing a cooking solution, namely adding the drained pennisetum hydridum in the step S2 into the cooking solution, and cooking for 3-4 hours at the temperature of 95-100 ℃ under normal pressure;
s4, carrying out acid washing on the fiber obtained after cooking, measuring the pH value of the solution by using a pH meter or pH test paper until the pH value is neutral, kneading the fiber, rinsing the fiber by using clear water, heating the fiber to 40-50 ℃ after the fiber is kneaded to be completely dispersed, and soaking the fiber;
and S5, airing the rinsed fibers under natural conditions or putting the fibers into a dryer for drying.
As a preferred technical scheme of the invention, when the hay is soaked, a plastic plate is pressed above the hay, so that the hay is completely immersed in the soaking liquid.
As a preferable technical scheme of the present invention, the preparation method of the soaking solution comprises: dissolving urea in water, stirring uniformly at about 40 ℃ to obtain 1-3% by mass of urea aqueous solution, immersing the truncated hay sections in the urea aqueous solution for 3-5 hours, taking out the immersed hay sections, standing for 1-3 hours, and washing the hay sections with clear water for later use.
As a preferable technical scheme of the invention, the preparation method of the cooking liquor comprises the following steps: water in weight ratio: sodium hydroxide: sodium sulfite: washing powder =1000:9:12:3 preparing cooking liquor, and uniformly stirring; the weight ratio of the cooking liquor is as follows: grass =5: (1-1.5), adding drained grass into the cooking liquor, cooking for 3-4 hours at the normal temperature of 95-100 ℃ and stirring.
As a preferred technical scheme of the invention, in the cooking process, a proper amount of water is supplemented every 20-25 minutes, and the quantity of the supplemented water is the quantity lost after cooking, so that the volume of the cooking liquor after water supplementation is the same as that of the original cooking liquor.
As a preferable technical scheme of the invention, after the heating is stopped after the cooking is finished, the solution is alkaline and has black color, and the black ink solution is processed to be neutral by acid washing.
As a preferred technical scheme of the invention, after the clean fiber is rinsed by using clean water, the pH value of the solution is measured again by using a pH meter or a pH test paper, so that errors are prevented.
As a preferred technical scheme of the invention, after the Jujun grass fiber material is prepared, the production wastewater is treated by a biochemical method, and is discharged after indexes in the wastewater reach the standard.
Compared with the prior art, the invention can achieve the following beneficial effects:
in the invention, the preparation method of the soaking liquid and the preparation method of the cooking liquid refer to the preparation method and the raw materials described in the patent document with the publication number of CN106995939A, and on the basis of the above-mentioned patent publications, the truncated hay is subjected to vibration screening for dust removal to remove impurities and dust attached to the hay, so that the influence of the impurities and dust on the cooking liquid, namely the preparation of the fiber material, can be avoided.
Detailed Description
The present invention will be further described with reference to specific embodiments for the purpose of facilitating an understanding of technical means, characteristics of creation, objectives and functions realized by the present invention, but the following embodiments are only preferred embodiments of the present invention, and are not intended to be exhaustive. Other embodiments obtained by persons skilled in the art without making creative efforts based on the embodiments in the implementation belong to the protection scope of the invention. The experimental methods in the following examples are conventional methods unless otherwise specified, and materials, reagents and the like used in the following examples are commercially available unless otherwise specified.
Example one
The invention provides a method for preparing a degradable Jujun grass fiber material, which comprises the following steps:
obtaining Jujun grass hay or fresh Jujun grass, mechanically cutting the Jujun grass hay into grass sections with the length of 15cm by using a machine, performing vibration screening and dust removal on the cut hay, removing impurities and dust attached to the hay, and then rolling and cracking the hay for later use;
dissolving urea in water, stirring uniformly at about 40 ℃ to obtain 1-3% by mass of urea aqueous solution, immersing the truncated hay sections in the urea aqueous solution for 3-5 hours, pressing and covering a plastic plate above the hay when the hay is immersed, so that the hay is completely immersed in the immersion liquid, taking out the immersed hay sections, standing for 1-3 hours, washing the hay sections with clear water, and draining for later use;
preparing a cooking liquor, wherein the weight ratio of water: sodium hydroxide: sodium sulfite: washing powder =1000:9:12:3 preparing cooking liquor, and uniformly stirring; the weight ratio of the cooking liquor is as follows: grass =5: (1-1.5), adding drained pennisetum hydridum into the cooking liquor, cooking for 3-4 hours at the temperature of 100 ℃ at normal temperature, stirring, and supplementing a proper amount of water every 20-25 minutes in the cooking process, wherein the water supplementing amount is the amount lost after cooking, so that the volume of the cooking liquor after water supplementing is the same as the volume of the original cooking liquor;
after the heating is stopped after the cooking is finished, the solution is alkaline, the color of the solution is black, the black ink solution is processed to be neutral by acid washing, the pH value of the solution is measured by using a pH meter or a pH test paper until the pH value is neutral, the fiber is kneaded, rinsed by using clear water, the pH value of the solution is measured again by using the pH meter or the pH test paper, the error is prevented, and after the fiber is kneaded to be completely dispersed, the solution is heated to 40-50 ℃ for soaking;
drying the rinsed fiber in the air under natural conditions or drying the fiber in a dryer;
after the Jujun grass fiber material is manufactured, the production wastewater is treated by a biochemical method, and is discharged when each index in the wastewater reaches the standard;
in the invention, the preparation method of the soaking solution and the preparation method of the cooking solution refer to the preparation method and raw materials described in the patent document with the publication number of CN106995939A, and on the basis of the above-mentioned patent publications, the chopped hay is subjected to vibration screening for dust removal to remove impurities and dust attached to the hay, so that the influence of the impurities and dust on the cooking solution, namely the preparation of the fiber material, can be avoided.
Example two
The invention provides a method for preparing a degradable Jujun grass fiber material, which comprises the following steps:
obtaining Jujun grass hay or fresh Jujun grass, mechanically cutting the Jujun grass hay into grass sections with the length of 20cm by using a machine, performing vibration screening and dust removal on the cut hay, removing impurities and dust attached to the hay, and then rolling and cracking the hay for later use;
dissolving urea in water, stirring uniformly at about 40 ℃ to obtain 1-3% by mass of urea aqueous solution, immersing the truncated hay sections in the urea aqueous solution for 3-5 hours, pressing and covering a plastic plate above the hay when the hay is immersed, so that the hay is completely immersed in the immersion liquid, taking out the immersed hay sections, standing for 1-3 hours, washing the hay sections with clear water, and draining for later use;
preparing a cooking liquor, wherein the weight ratio of water: sodium hydroxide: sodium sulfite: washing powder =1000:9:12:3 preparing cooking liquor, and uniformly stirring; the weight ratio of the cooking liquor is as follows: grass =5: (1-1.5) adding drained pennisetum sinese roxb into the cooking liquid, cooking for 3-4 hours at the temperature of 100 ℃ at normal temperature, stirring, and supplementing proper water every 20-25 minutes in the cooking process, wherein the water supplementing amount is the amount lost after cooking, so that the volume of the cooking liquid after water supplementing is the same as the volume of the original cooking liquid;
after the heating is stopped after the cooking is finished, the solution is alkaline, the color of the solution is black, the black ink solution is processed to be neutral by acid washing, the pH value of the solution is measured by using a pH meter or a pH test paper until the pH value is neutral, the fiber is kneaded, rinsed by using clear water, the pH value of the solution is measured again by using the pH meter or the pH test paper, the error is prevented, and after the fiber is kneaded to be completely dispersed, the solution is heated to 40-50 ℃ for soaking;
drying the rinsed fiber in the air under natural conditions or drying the fiber in a dryer;
after the Jujun grass fiber material is manufactured, the production wastewater is treated by a biochemical method, and is discharged when each index in the wastewater reaches the standard;
in the invention, the preparation method of the soaking solution and the preparation method of the cooking solution refer to the preparation method and raw materials described in the patent document with the publication number of CN106995939A, and on the basis of the above-mentioned patent publications, the chopped hay is subjected to vibration screening for dust removal to remove impurities and dust attached to the hay, so that the influence of the impurities and dust on the cooking solution, namely the preparation of the fiber material, can be avoided.
EXAMPLE III
The invention provides a method for preparing a degradable Jujun grass fiber material, which comprises the following steps:
obtaining Jujun grass hay or fresh Jujun grass, mechanically cutting the Jujun grass hay into a grass section with the length of 25cm by using a machine, carrying out vibration screening and dust removal on the cut hay, removing impurities and dust attached to the hay, and then rolling and cracking the hay for later use;
dissolving urea in water, stirring uniformly at about 40 ℃ to obtain 1-3% by mass of urea aqueous solution, immersing the truncated hay sections in the urea aqueous solution for 3-5 hours, pressing and covering a plastic plate above the hay when the hay is immersed, so that the hay is completely immersed in the immersion liquid, taking out the immersed hay sections, standing for 1-3 hours, washing the hay sections with clear water, and draining for later use;
preparing a cooking liquor, wherein the weight ratio of water: sodium hydroxide: sodium sulfite: washing powder =1000:9:12:3 preparing cooking liquor, and uniformly stirring; the weight ratio of the cooking liquor is as follows: grass =5: (1-1.5), adding drained pennisetum hydridum into the cooking liquor, cooking for 3-4 hours at the temperature of 100 ℃ at normal temperature, stirring, and supplementing a proper amount of water every 20-25 minutes in the cooking process, wherein the water supplementing amount is the amount lost after cooking, so that the volume of the cooking liquor after water supplementing is the same as the volume of the original cooking liquor;
after the heating is stopped after the cooking is finished, the solution is alkaline, the color of the solution is black, the black ink solution is processed to be neutral by acid washing, the pH value of the solution is measured by using a pH meter or a pH test paper until the pH value is neutral, the fiber is kneaded, rinsed by using clear water, the pH value of the solution is measured again by using the pH meter or the pH test paper, the error is prevented, and after the fiber is kneaded to be completely dispersed, the solution is heated to 40-50 ℃ for soaking;
drying the rinsed fiber in the air under natural conditions or drying the fiber in a dryer;
after the Jujun grass fiber material is manufactured, the production wastewater is treated by a biochemical method, and is discharged when each index in the wastewater reaches the standard;
in the invention, the preparation method of the soaking liquid and the preparation method of the cooking liquid refer to the preparation method and the raw materials described in the patent document with the publication number of CN106995939A, and on the basis of the above-mentioned patent publications, the truncated hay is subjected to vibration screening for dust removal to remove impurities and dust attached to the hay, so that the influence of the impurities and dust on the cooking liquid, namely the preparation of the fiber material, can be avoided.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (8)

1. The method for preparing the degradable Jujun grass fiber material is characterized in that: the method comprises the following steps:
s1, obtaining giant-mycorrhizal hay or fresh giant-mycorrhizal hay, mechanically cutting the giant-mycorrhizal hay into a grass section with the length of 15cm-25cm by using a machine, performing vibration screening and dust removal on the cut hay, removing impurities and dust attached to the hay, and then rolling and cracking the hay for later use;
s2, preparing a soaking solution, soaking the prepared hay, taking out the hay after soaking for a period of time, cleaning the hay with clear water, and draining the hay for later use;
s3, preparing a cooking solution, namely adding the drained pennisetum hydridum in the step S2 into the cooking solution, and cooking for 3-4 hours at the temperature of 95-100 ℃ under normal pressure;
s4, pickling the fibers obtained after cooking until the pH value is neutral, kneading the fibers, rinsing the fibers with clear water, heating the fibers to 40-50 ℃ after the fibers are kneaded to be completely dispersed, and soaking the fibers;
and S5, airing the rinsed fibers under natural conditions or putting the fibers into a dryer for drying.
2. The method for preparing the degradable pennisetum hydridum fiber material according to claim 1, wherein the method comprises the following steps: in the step S2, when the hay is soaked, a plastic plate is pressed and covered above the hay, so that the hay is completely immersed in the soaking liquid.
3. The method for preparing the degradable pennisetum hydridum fiber material according to claim 1, wherein the method comprises the following steps: the preparation method of the soaking solution comprises the following steps: dissolving urea in water, stirring uniformly at about 40 ℃ to obtain 1-3% by mass of urea aqueous solution, immersing the truncated hay sections in the urea aqueous solution for 3-5 hours, taking out the immersed hay sections, standing for 1-3 hours, and washing the hay sections with clear water for later use.
4. The method for preparing the degradable pennisetum hydridum fiber material according to claim 1, wherein the method comprises the following steps: the preparation method of the cooking liquor comprises the following steps: water in weight ratio: sodium hydroxide: sodium sulfite: washing powder =1000:9:12:3 preparing cooking liquor, and uniformly stirring; the weight ratio of the cooking liquor is as follows: grass =5: (1-1.5), adding drained grass into the cooking liquor, cooking for 3-4 hours at the normal temperature of 95-100 ℃ and stirring.
5. The method for preparing the degradable pennisetum hydridum fiber material according to claim 4, wherein the method comprises the following steps: in the cooking process, a proper amount of water is supplemented every 20-25 minutes, and the water supplementing amount is the amount lost after cooking, so that the volume of the cooking liquid after water supplementing is the same as that of the original cooking liquid.
6. The method for preparing the degradable pennisetum hydridum fiber material according to claim 1, wherein the method comprises the following steps: in the step S4, after the cooking is finished and the heating is stopped, the solution is alkaline and is black, and the black solution is processed to be neutral by acid washing.
7. The method for preparing the degradable pennisetum hydridum fiber material according to claim 1, wherein the method comprises the following steps: in the step S4, after the fibers are rinsed clean by using clean water, the pH value of the fibers is tested again to prevent errors.
8. The method for preparing the degradable pennisetum hydridum fiber material according to claim 1, wherein the method comprises the following steps: after the Jujun grass fiber material is manufactured, the production wastewater is treated by a biochemical method and is discharged after each index in the wastewater reaches the standard.
CN202211315147.0A 2022-10-26 2022-10-26 Method for preparing degradable Jujun grass fiber material Pending CN115491772A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202211315147.0A CN115491772A (en) 2022-10-26 2022-10-26 Method for preparing degradable Jujun grass fiber material

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202211315147.0A CN115491772A (en) 2022-10-26 2022-10-26 Method for preparing degradable Jujun grass fiber material

Publications (1)

Publication Number Publication Date
CN115491772A true CN115491772A (en) 2022-12-20

Family

ID=85114619

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202211315147.0A Pending CN115491772A (en) 2022-10-26 2022-10-26 Method for preparing degradable Jujun grass fiber material

Country Status (1)

Country Link
CN (1) CN115491772A (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101260629A (en) * 2007-03-08 2008-09-10 汪官久 Physical method ecological paper pulp production process
CN105019287A (en) * 2015-07-13 2015-11-04 四川省西龙生物质材料科技有限公司 Pulping method for obtaining high-performance fibers by using bamboo plants as raw materials
CN106958044A (en) * 2017-03-16 2017-07-18 王晓翔 The method that Juncao pulp fibres are produced using chemical method
CN106995939A (en) * 2017-03-16 2017-08-01 王晓翔 The method that Jujun grasses fibrillation is produced using chemical method

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101260629A (en) * 2007-03-08 2008-09-10 汪官久 Physical method ecological paper pulp production process
CN105019287A (en) * 2015-07-13 2015-11-04 四川省西龙生物质材料科技有限公司 Pulping method for obtaining high-performance fibers by using bamboo plants as raw materials
CN106958044A (en) * 2017-03-16 2017-07-18 王晓翔 The method that Juncao pulp fibres are produced using chemical method
CN106995939A (en) * 2017-03-16 2017-08-01 王晓翔 The method that Jujun grasses fibrillation is produced using chemical method

Similar Documents

Publication Publication Date Title
CN102041751B (en) High-temperature edible oil filter paper and manufacturing method thereof
CN109234826B (en) Method for preparing lyocell fibers by using bamboo as raw material
CN102492997B (en) Flash explosion and base boiling combined degumming method of natural bamboo fiber
CN1375578A (en) Bamboo fiber and its making process
CN101934545B (en) Method for manufacturing bamboo fibers
CN115491772A (en) Method for preparing degradable Jujun grass fiber material
CN106958044A (en) The method that Juncao pulp fibres are produced using chemical method
CN1217041C (en) Protein synthetic fiber and its production method
CN103484949A (en) Degumming process for mulberry fibers
CN110359305A (en) A kind of Pueraria lobota flaxen fiber bleaching processing method
CN109338495B (en) Method for preparing modal fiber by using reed straw as raw material
CN108588854A (en) A kind of preparation method of mulberry fibre
CN113279069A (en) Organic fiber material prepared from coconut fallen leaves
CN109267317A (en) A kind of high-quality modified silk fiber
KR100868889B1 (en) Manufacture of thread using grass fiber and thread manufactured by the same
CN109338481A (en) A kind of continuous degumming tech of pineapple flaxen fiber
CN113861429B (en) Modified polyvinylamine surface modified fiber material and preparation method thereof
CN110499395A (en) The extracting method of high yield pulp1 hemicellulose xylose
CN114808508B (en) Insulating paste and preparation method thereof
CN1876903A (en) Broussonetia papyrifera adhesive filament and preparation method thereof
CN114150521B (en) Preparation method of hemp-based lyocell fiber pulp
CN117487364B (en) Modified silk fibroin and preparation method thereof
CN114441259B (en) Method for evaluating reactivity of cellulose pulp and application thereof
CN109097838A (en) A kind of continuous Degumming method of pineapple flaxen fiber
CN102505148A (en) Sweetcane bark fiber and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination