CN113279069A - Organic fiber material prepared from coconut fallen leaves - Google Patents

Organic fiber material prepared from coconut fallen leaves Download PDF

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Publication number
CN113279069A
CN113279069A CN202110632883.8A CN202110632883A CN113279069A CN 113279069 A CN113279069 A CN 113279069A CN 202110632883 A CN202110632883 A CN 202110632883A CN 113279069 A CN113279069 A CN 113279069A
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coconut
fibers
leaves
fiber
drying
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陈传来
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Hainan Ruimin Agricultural Technology Co ltd
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Hainan Ruimin Agricultural Technology Co ltd
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Publication of CN113279069A publication Critical patent/CN113279069A/en
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    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01CCHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
    • D01C1/00Treatment of vegetable material

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  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Molecular Biology (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Textile Engineering (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention discloses an organic fiber material prepared from coconut fallen leaves, which comprises the following raw materials in part by weight: is composed of cellulose, lignin, pectin, hemicellulose, fat, wax and other substances, and comprises the following steps: firstly, collecting: picking coconut leaves from a coconut tree so as to facilitate subsequent processing operation and use, (II) drying: the collected coconut leaves are aired or are heated at high temperature through workshop equipment, and water flow in the coconut leaves is processed and lost. According to the organic fiber material prepared from the fallen coconut leaves, in the process of processing the coconut leaves, original dry coconut leaves are subjected to a series of steps of pickling, fiber beating, washing, alkali liquor boiling, bleaching, acid washing, oil feeding, drying and the like, and the coconut leaf fibers after chemical treatment are soft in texture, easy to bleach and dye, can be independently spun and can also be blended with fibers such as cotton and the like into yarns in different proportions so as to meet the requirements of wearability of different fabrics.

Description

Organic fiber material prepared from coconut fallen leaves
Technical Field
The invention relates to the technical field of wool weaving production, in particular to an organic fiber material prepared from coconut fallen leaves.
Background
The coconut palm plant is tall and big, arbor-shaped, 15-30 meters high, thick and strong stem, provided with annular leaf marks, thickened base, frequently clustered rootlet, thick petiole, axillary inflorescence, fruit egg-shaped or approximately spherical, fruit cavity containing endosperm, namely 'pulp' or kernel, embryo and juice coconut water, the flower and fruit period is mainly autumn, the coconut is originally produced in southeast Asia, Indonesia to Pacific Islands, islands in south China, Ranunculus semilands, Hainan, Taiwan and tropical regions in south Yunnan, the coconut leaf fiber has chemical components similar to hemp fiber and mainly comprises cellulose, lignin, pectin, hemicellulose, fat, wax and the like, wherein the cellulose content is the most and can reach 63 percent, but the cellulose content can slightly vary with different coconut varieties and producing places, and the content of the hemicellulose in the coconut leaf fiber is very low, therefore, the coconut leaf fiber has good mechanical properties, heat resistance and moisture resistance, and is measured to be long fiber with a multi-cell aggregation structure, wherein the length is about 10-25mm, the diameter is generally 100-450um, and the density is 1.12g/cm3, and a bundle of coconut leaf fibers contains 30-300 or more fiber cells.
The strength of the existing coconut fallen leaf fiber is not strong enough when in use, the hemp rope made of the fiber is not high enough in use strength, and the defects that the internal material is corroded to be damaged greatly and the service life is not long enough are caused by adopting other materials for mixing.
Disclosure of Invention
The invention aims to provide an organic fiber material made of coconut fallen leaves, so as to solve the problems that the strength of the coconut fallen leaves fiber is not strong enough when in use, the strength of hemp ropes made of the fiber is not high enough, and the materials in the coconut fallen leaves fiber are corroded to be damaged greatly and the service life is not long enough due to the fact that other materials are mixed.
In order to achieve the purpose, the invention provides the following technical scheme: an organic fiber material made from coconut fallen leaves comprises the following raw materials: is composed of cellulose, lignin, pectin, hemicellulose, fat, wax and other substances, and comprises the following steps:
firstly, collecting: picking the coconut leaves from the coconut tree so as to be convenient for subsequent processing, operation and use.
(II) drying: drying or carrying out high temperature heating through workshop appliance through the coconut leaf with gathering, processing the inside rivers of coconut leaf and run off, make the coconut leaf become the coconut leaf to carry out the processing in later stage and handle.
(III) pickling: in the fiber manufacturing industry, as a process of the preparation stage, the dried coconut leaf naked skin is soaked in a mixed solution of sulfuric acid and salt, so that the skin fiber can be developed, tanning materials can easily penetrate, the prepared fiber is soft and delicate, and common plants need to be soaked in acid to achieve the purpose of quick tanning.
(IV) fiber beating: decomposing the pickled coconut leaves, and dispersing the fibers of the coconut leaves to change the finished coconut leaves into one coconut leaf.
(V) water washing: the coconut leaf after the homogeneity passes through inside the water pump inflow washing pond, washes other magazines on coconut strip surface through the water washing bed in the pond, discharges through inside.
Boiling with alkali liquor: the coconut leaves after being washed are placed in the alkaline solution pool for boiling and extraction, the natural cellulose is a macromolecular compound, the processing performance and the reactivity can not meet the requirements of modern materials, cellulose macromolecules are changed into cellulose materials with smaller molecular weight, the reduction treatment mode has mild conditions and shorter time, the energy consumption is lower, meanwhile, certain relatively inert cellulose structures can be damaged, the reactivity of the cellulose is improved, and the alkali cellulose with better processing and reactivity is obtained.
(seventh) bleaching: the bleaching process is a process for decomposing and decoloring colored substances in the textile by chemical action to obtain the necessary whiteness of the textile.
(eighth) acid washing: and after bleaching, pickling the fiber, and taking out an oxide layer on the surface to enable the obtained fiber to be finer and finer.
(nine) oil feeding: oiling is carried out on the fibers at last, the bundling property of the fibers is improved, so that the generation of hairiness and hairline can be reduced, the strength of the tows can be increased, the weaving efficiency and quality are improved, meanwhile, the flexibility is improved, the tows are soft, the hand feeling is increased, the static electricity resistance is realized, and the weaving efficiency and quality are improved.
(ten) drying: the fiber is heated by a heat carrier, the moisture is evaporated to achieve a certain moisture content, the principle of moisture movement in the fiber is the same as that of wood, the plant fiber has the characteristics of heat sensitivity, fluffiness, fibrous shape, large surface area, easiness in dispersion and the like, generally, high-temperature airflow rapid drying is adopted, and the airflow drying is to mix wet fiber and a heat-carrying drying medium according to the solid fluidization principle to flow in a suspension state, so that the moisture in the wet fiber is gasified and then taken away by the heat-carrying medium, the purpose of drying the fiber is achieved, and finally, the intact fiber is obtained.
Preferably, the step (one) is to filter and sort the damaged and broken coconut leaves when collecting the coconut leaves.
Preferably, the step (two) is performed in a manner that the drying is performed so that the internal temperature is maintained at three hundred to four hundred degrees celsius, and the heat preservation is performed for one hour, and the number of times of drying cannot exceed three.
Preferably, in the step (three), when pickling is carried out, the time for the coconut leaves inside is not easy to be too long, otherwise, the fibers inside are easy to break.
Preferably, the step (IV) decomposes the fibers to nominally separate the fibers for further washing with water.
Preferably, in the step (v), the impurities on the surface are cleaned during the water washing, and then the impurities inside are discharged through the internal filtration.
Preferably, in the step (VI), strong base is dissolved in water with the temperature of 40-50 ℃, strong base solution with the concentration of 4-10% is prepared, and the plant fiber is soaked in the strong base solution for 8-12 hours.
Preferably, in the step (seven), during the bleaching of the fiber, natural or additional colored substances exist in the natural fiber, the natural fiber still remains after refining and needs bleaching for color removal, and some synthetic fibers are yellowed after heat setting treatment and also need bleaching, and an oxidation bleaching agent is commonly used.
Preferably, the fiber oiling rate in the step (eight) is the dry weight of the oiling agent on the chemical fibers accounting for the dry weight of the fibers after the oil removal, the oil content of the fibers is closely related to the spinnability of the fibers, the fibers with low oil content are easy to generate static electricity, and the fibers with too high oil content are easy to generate the sticking phenomenon, which all affect the normal operation of the textile production and processing.
Preferably, in the step (nine), when drying is performed, different temperatures are used according to different methods, high-temperature airflow is adopted for rapid drying, and airflow drying is performed by mixing wet fibers and a heat-carrying drying medium according to a solid fluidization principle, flowing in a suspension state, and taking away moisture in the wet fibers after gasification by the heat-carrying medium so as to achieve the purpose of drying the fibers.
Compared with the prior art, the invention has the beneficial effects that: the organic fiber material prepared from the coconut fallen leaves has the characteristics that the flexibility of internal fibers can be improved and the internal fiber strength can be improved when the organic fiber material is operated and manufactured, so that the internal connection of the fibers is tighter when the hemp ropes are manufactured, the connection tightness is improved, and the internal water absorption is stronger;
(1) when the hemp rope is decomposed, the alkaline scouring time inside the hemp rope is checked at any time, so that fiber impurities inside the hemp rope are cleaned more cleanly, the problem that the connection between the insides is not compact enough during manufacturing is avoided, the strength of the finally manufactured hemp rope is not high enough, and meanwhile, the heat resistance and the moisture resistance inside the hemp rope are high during manufacturing due to the fact that the content of the half fibers inside the hemp rope is not low.
(2) In the process of treating the coconut leaves, original dry coconut leaves are subjected to a series of steps of pickling, fiber beating, washing, alkali liquor scouring, bleaching, acid washing, oil feeding, drying and the like, and the coconut leaf fibers after chemical treatment are soft in texture, easy to bleach and dye, can be independently spun and can also be blended with fibers such as cotton and the like into yarns in different proportions so as to meet the requirements of the wearability of different fabrics.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example (b):
an organic fiber material made from coconut fallen leaves comprises the following raw materials: is composed of cellulose, lignin, pectin, hemicellulose, fat, wax and other substances, and comprises the following steps: the above production and its use are described in detail below:
firstly, collecting: picking the coconut leaves from the coconut tree so as to be convenient for subsequent processing, operation and use.
(II) drying: drying or carrying out high temperature heating through workshop appliance through the coconut leaf with gathering, processing the inside rivers of coconut leaf and run off, make the coconut leaf become the coconut leaf to carry out the processing in later stage and handle.
(III) pickling: in the fiber manufacturing industry, as a process of the preparation stage, the dried coconut leaf naked skin is soaked in a mixed solution of sulfuric acid and salt, so that the skin fiber can be developed, tanning materials can easily penetrate, the prepared fiber is soft and delicate, and common plants need to be soaked in acid to achieve the purpose of quick tanning.
(IV) fiber beating: decomposing the pickled coconut leaves, and dispersing the fibers of the coconut leaves to change the finished coconut leaves into one coconut leaf.
(V) water washing: the coconut leaf after the homogeneity passes through inside the water pump inflow washing pond, washes other magazines on coconut strip surface through the water washing bed in the pond, discharges through inside.
Boiling with alkali liquor: the coconut leaves after being washed are placed in the alkaline solution pool for boiling and extraction, the natural cellulose is a macromolecular compound, the processing performance and the reactivity can not meet the requirements of modern materials, cellulose macromolecules are changed into cellulose materials with smaller molecular weight, the reduction treatment mode has mild conditions and shorter time, the energy consumption is lower, meanwhile, certain relatively inert cellulose structures can be damaged, the reactivity of the cellulose is improved, and the alkali cellulose with better processing and reactivity is obtained.
(seventh) bleaching: the bleaching process is a process for decomposing and decoloring colored substances in the textile by chemical action to obtain the necessary whiteness of the textile.
(eighth) acid washing: and after bleaching, pickling the fiber, and taking out an oxide layer on the surface to enable the obtained fiber to be finer and finer.
(nine) oil feeding: oiling is carried out on the fibers at last, the bundling property of the fibers is improved, so that the generation of hairiness and hairline can be reduced, the strength of the tows can be increased, the weaving efficiency and quality are improved, meanwhile, the flexibility is improved, the tows are soft, the hand feeling is increased, the static electricity resistance is realized, and the weaving efficiency and quality are improved.
(ten) drying: the fiber is heated by a heat carrier, the moisture is evaporated to achieve a certain moisture content, the principle of moisture movement in the fiber is the same as that of wood, the plant fiber has the characteristics of heat sensitivity, fluffiness, fibrous shape, large surface area, easiness in dispersion and the like, generally, high-temperature airflow rapid drying is adopted, and the airflow drying is to mix wet fiber and a heat-carrying drying medium according to the solid fluidization principle to flow in a suspension state, so that the moisture in the wet fiber is gasified and then taken away by the heat-carrying medium, the purpose of drying the fiber is achieved, and finally, the intact fiber is obtained.
And (I) filtering and sorting damaged and broken coconut leaves when collecting the coconut leaves.
And (II) drying to keep the internal temperature at three hundred to four hundred ℃, and keeping the temperature for one hour, wherein the drying times cannot exceed three times.
In the step (III), when pickling is carried out, the time for the coconut leaves inside is not easy to overlook, otherwise, the fibers inside are easy to break.
And (IV) decomposing the fibers to obtain nominal single fibers so as to facilitate the next step of water washing.
And (V) cleaning impurities on the surface during water washing, and discharging the impurities inside through internal filtration.
Dissolving strong base in water at the temperature of 40-50 ℃, preparing strong base solution with the concentration of 4-10%, and soaking the plant fibers in the strong base solution for 8-12 hours.
And (seventhly) in the process of bleaching the fibers, natural or additional colored substances exist in the natural fibers, the natural fibers are still remained after refining and are bleached to be decolored, some synthetic fibers are yellowed after heat setting treatment and are also bleached, and an oxidation bleaching agent is usually used.
The oiling rate of the fibers in the step (eight) is the percentage of the dry weight of the oiling agent of the chemical fibers in the dry mass of the fibers after the oil removal agent is removed, the oil content of the fibers is closely related to the spinnability of the fibers, the fibers with low oil content are easy to generate static electricity, and the fibers with high oil content are easy to generate the adhesion phenomenon, so that the normal operation of the textile production and processing can be influenced.
And (ninth), during drying, different temperatures are used according to different methods, high-temperature airflow is adopted for rapid drying, and airflow drying is to mix wet fibers and a heat-carrying drying medium according to a solid fluidization principle to flow in a suspension state, so that moisture in the wet fibers is gasified and then taken away by the heat-carrying medium, and the purpose of drying the fibers is achieved.
It should also be noted that the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrase "comprising an … …" does not exclude the presence of other identical elements in the process, method, article, or apparatus that comprises the element.
Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that various changes in the embodiments and/or modifications of the invention can be made, and equivalents and modifications of some features of the invention can be made without departing from the spirit and scope of the invention.

Claims (10)

1. An organic fiber material made from coconut fallen leaves is characterized by comprising the following raw materials: is composed of cellulose, lignin, pectin, hemicellulose, fat, wax and other substances, and comprises the following steps:
firstly, collecting: picking coconut leaves from a coconut tree so as to facilitate subsequent processing, operation and use:
(II) drying: carry out the sunning or carry out high temperature heating through workshop appliance through the coconut leaf with gathering, process the inside rivers of coconut leaf and run off, make the coconut leaf become the coconut leaf to in the processing of carrying out the later stage:
(III) pickling: in the fiber manufacturing industry, as a process of the preparation stage, the dried coconut leaf naked skin is soaked in a mixed solution of sulfuric acid and salt, so that the skin fiber can be developed, tanning materials can easily penetrate, the prepared fiber is soft and delicate, and common plants need to be soaked in acid to achieve the purpose of quick tanning:
(IV) fiber beating: decomposing the pickled coconut leaves, and dispersing the fibers of the coconut leaves after the operation to change the finished coconut leaves into one coconut leaf:
(V) water washing: inside coconut leaf after the homogeneity passes through water pump inflow washing pond, washes coconut strip surperficial other magazines through the water washing bed in the pond, discharges through inside:
boiling with alkali liquor: the coconut leaf after will rinsing is put into the caustic soda pond inside and is cooked and draw, and natural cellulose is macromolecular compound, and processing property and reactivity can not satisfy modern material's demand, make the cellulose macromolecule become the less cellulose material of molecular weight, and the mode condition of reducing processing is mild, and the time is shorter relatively, and the energy consumption is lower can destroy some cellulose structures of relative inertia simultaneously, has improved the reactivity of cellulose, obtains processing and the better alkali cellulose of reactivity:
(seventh) bleaching: the bleaching is a process for decomposing and decoloring colored substances in the textile by chemical action to ensure that the textile obtains necessary whiteness:
(eighth) acid washing: after bleaching, the fiber is pickled, and an oxide layer on the surface is taken out, so that the obtained fiber is more fine:
(nine) oil feeding: oiling through last with the fibre, increasing fibrous beaming nature, can reduce the production of filoplume, filoplume like this, can increase the silk bundle intensity, improve and weave efficiency and quality, improve the compliance simultaneously, let the silk bundle soft, increase and feel, it is antistatic, improve and weave efficiency and quality:
(ten) drying: the fiber is heated by a heat carrier, the moisture is evaporated to achieve a certain moisture content, the principle of moisture movement in the fiber is the same as that of wood, the plant fiber has the characteristics of heat sensitivity, fluffiness, fibrous shape, large surface area, easiness in dispersion and the like, generally, high-temperature airflow rapid drying is adopted, and the airflow drying is to mix wet fiber and a heat-carrying drying medium according to the solid fluidization principle to flow in a suspension state, so that the moisture in the wet fiber is gasified and then taken away by the heat-carrying medium, the purpose of drying the fiber is achieved, and finally, the intact fiber is obtained.
2. The organic fibrous material of claim 1, wherein the organic fibrous material is prepared from coconut deciduous leaves: in the step (I), when collecting coconut leaves, damaged and broken coconut leaves are filtered and sorted.
3. The organic fibrous material of claim 1, wherein the organic fibrous material is prepared from coconut deciduous leaves: and (II) drying to keep the internal temperature at three hundred to four hundred ℃ and keeping the temperature for one hour, wherein the drying times cannot exceed three times.
4. The organic fibrous material of claim 1, wherein the organic fibrous material is prepared from coconut deciduous leaves: in the step (III), when pickling is carried out, the time for the coconut leaves inside is not easy to overlook, otherwise, the fibers inside are easy to break.
5. The organic fibrous material of claim 1, wherein the organic fibrous material is prepared from coconut deciduous leaves: and (IV) decomposing the fibers to obtain nominal single fibers so as to facilitate the next water washing.
6. The organic fibrous material of claim 1, wherein the organic fibrous material is prepared from coconut deciduous leaves: and (V) cleaning impurities on the surface in the water washing process, and discharging the impurities in the water washing process through internal filtration.
7. The organic fibrous material of claim 1, wherein the organic fibrous material is prepared from coconut deciduous leaves: dissolving strong base in water at the temperature of 40-50 ℃, preparing strong base solution with the concentration of 4-10%, and soaking the plant fibers in the strong base solution for 8-12 hours.
8. The organic fibrous material of claim 1, wherein the organic fibrous material is prepared from coconut deciduous leaves: in the step (VII), in the process of bleaching the fibers, natural or additional colored substances exist in the natural fibers, residues still remain after refining, the fibers can be decolored only by bleaching, and some synthetic fibers are yellowed after heat setting treatment and are also bleached, and an oxidation bleaching agent is commonly used.
9. The organic fibrous material of claim 1, wherein the organic fibrous material is prepared from coconut deciduous leaves: the oiling rate of the fibers in the step (eight) is the percentage of the dry weight of the oiling agent of the chemical fibers in the dry mass of the fibers after the oil removal agent is removed, the oil content of the fibers is closely related to the spinnability of the fibers, the fibers with low oil content are easy to generate static electricity, and the fibers with high oil content are easy to generate the adhesion phenomenon, so that the normal operation of the textile production and processing can be influenced.
10. The organic fibrous material of claim 1, wherein the organic fibrous material is prepared from coconut deciduous leaves: and (ninth) when drying, according to different methods, different temperatures are used, high-temperature airflow is adopted for rapid drying, and airflow drying is to mix wet fibers and a heat-carrying drying medium according to a solid fluidization principle to flow in a suspension state, so that moisture in the wet fibers is gasified and then taken away by the heat-carrying medium, and the purpose of drying the fibers is achieved.
CN202110632883.8A 2021-06-07 2021-06-07 Organic fiber material prepared from coconut fallen leaves Pending CN113279069A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113967956A (en) * 2021-11-04 2022-01-25 程栋 Novel material of palmaceae leaves and preparation method thereof

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CN105803538A (en) * 2016-05-17 2016-07-27 太仓市钱泾化纤厂 Chemical degumming technology for ramie for spinning ultra-fine yarn

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Publication number Priority date Publication date Assignee Title
CN113967956A (en) * 2021-11-04 2022-01-25 程栋 Novel material of palmaceae leaves and preparation method thereof

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Application publication date: 20210820