CN115400036A - 清洗料组合物 - Google Patents
清洗料组合物 Download PDFInfo
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- CN115400036A CN115400036A CN202210409660.XA CN202210409660A CN115400036A CN 115400036 A CN115400036 A CN 115400036A CN 202210409660 A CN202210409660 A CN 202210409660A CN 115400036 A CN115400036 A CN 115400036A
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- cleaning composition
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- UJMBCXLDXJUMFB-UHFFFAOYSA-K trisodium;5-oxo-1-(4-sulfonatophenyl)-4-[(4-sulfonatophenyl)diazenyl]-4h-pyrazole-3-carboxylate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)C1=NN(C=2C=CC(=CC=2)S([O-])(=O)=O)C(=O)C1N=NC1=CC=C(S([O-])(=O)=O)C=C1 UJMBCXLDXJUMFB-UHFFFAOYSA-K 0.000 description 1
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- LNRUEZIDUKQGRH-YZUCMPLFSA-N umbelliferose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O[C@@H]2[C@@H]([C@@H](O)[C@@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 LNRUEZIDUKQGRH-YZUCMPLFSA-N 0.000 description 1
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- 150000003722 vitamin derivatives Chemical class 0.000 description 1
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Abstract
清洗料组合物含有0.03质量%~0.4质量%的光亮性粉末、40质量%~95质量%的液态多元醇、0.1质量%~5质量%的增稠剂、和0.8质量%~10质量%的水。光亮性粉末中的粒子包含选自云母、二氧化硅、氧化铝、铝、滑石和玻璃中的板状基体、以及覆盖基体的至少一部分的选自二氧化钛和铁氧化物中的至少1种的覆盖层。
Description
相关申请
本发明主张基于日本专利申请:特愿2021-073479号(2021年4月23 日申请)的优先权,该申请的全部记载内容通过引用而整合记载到本说明书中进行记载。
技术领域
本公开涉及含有粉末的清洗料组合物。
背景技术
已知主要以清洗脸作为目的的清洗料、例如适于化妆料(彩妆)的清洗的清洗料(例如,参照专利文献1)。
在专利文献1中,记载了一种凝胶状皮肤清洗料,包含(A)以相对于皮肤清洗料为20质量%以上的混配比例包含甘油的多元醇40~95质量%、 (B)HLB为6~15的选自聚氧乙烯脂肪酸甘油酯、聚乙二醇单脂肪酸酯中的1种或2种以上非离子表面活性剂4~20质量%、(C)能够对高混配多元醇且低混配或不混配水的体系发挥增稠性的增稠剂0.1~5质量%、和(D) 水0~10质量%,粘度(B型粘度计,30℃)为10,000mPa·s以上。
现有技术文献
专利文献
专利文献1:日本特开2014-37404号公报
发明内容
发明所要解决的课题
以下分析是从本公开的观点考虑给出的。
在为了卸除画在脸上的彩妆而洗脸时,清洗者通常为了确认有没有彩妆的清洗残余而用镜子看自己的脸。此时,除去了彩妆的脸有时看起来气色差(肌肤暗)。特别是,由于直到即将洗脸前都看画了彩妆的脸,因此洗脸后的脸越发看起来气色差。感到自己的脸气色差的清洗者在洗脸后心情沮丧。
因此,要求卸除污垢,也同时在清洗了肌肤后,使清洗了的肌肤看起来气色好的清洗料组合物。
用于解决课题的方法
根据本公开的第1观点,提供一种清洗料组合物,含有0.03质量%~ 0.4质量%的光亮性粉末、40质量%~95质量%的液态多元醇、0.1质量%~ 5质量%的增稠剂和0.8质量%~10质量%的水。光亮性粉末中的粒子包含选自云母、二氧化硅、氧化铝、铝、滑石和玻璃中的板状基体,以及覆盖基体的至少一部分的选自二氧化钛和铁氧化物中的至少1种的覆盖层。
发明的效果
如果使用本公开的清洗料组合物清洗肌肤,则不仅卸除污垢,而且在清洗后,可以使清洗了的肌肤的颜色看起来好。
具体实施方式
以下记载上述各观点的优选的方案。
根据上述第1观点的优选的方案,板状基体为云母。覆盖层具有几何厚度60nm~100nm的二氧化钛层。
根据上述第1观点的优选的方案,覆盖层进一步具有覆盖二氧化钛层的至少一部分的铁氧化物层。
根据上述第1观点的优选的方案,粒子具有1μm~100μm的平均粒径。
根据上述第1观点的优选的方案,液态多元醇包含相对于清洗料组合物的质量为20质量%以上的甘油。
根据上述第1观点的优选的方案,液态多元醇进一步包含选自聚乙二醇、1,3-丁二醇、和双丙甘醇中的至少1种。
根据上述第1观点的优选的方案,清洗料组合物进一步包含0.8质量%~25质量%的水。
根据上述第1观点的优选的方案,清洗料组合物进一步包含1质量%~ 20质量%的表面活性剂。
根据上述第1观点的优选的方案,油性成分相对于清洗料组合物的质量为10质量%以下。
根据上述第1观点的优选的方案,清洗料组合物的粘度为1,000mPa·s 以上。
根据上述第1观点的优选的方案,清洗料组合物被应用于脸的清洗。
在以下说明中,POE为聚氧乙烯的简写,POP为聚氧丙烯的简写, POE或POP之后的括号内的数字表示该化合物中的POE基或POP基的平均加成摩尔数。
在本公开中所谓“有效质量”,是指能够产生由该化合物的添加带来的作用效果的量。
对本公开的第1实施方式涉及的清洗料组合物进行说明。
在本公开中所谓“液态”,是指在25℃下为液体、具有流动性。
本公开的清洗料组合物含有光亮性粉末、液态多元醇、和增稠剂。本公开的清洗料组合物优选为在大气压下在25℃下为液态组合物。
[光亮性粉末]
所谓光亮性粉末,是指具有珍珠样光泽或金属样光泽的粉末。例如,光亮性粉末是指通过光的干涉作用,根据观察角度而表现色彩不同的干涉色的粉末。在本公开的光亮性粉末中,也可以包含以珠光粉末、珠光颜料等这样的名称被称呼的粉末。
光亮性粉末中的粒子优选具有板状形状(薄片形状、鳞片形状、碎片 (flake)形状)。
光亮性粉末中的粒子可以具有选自云母(mica)、二氧化硅、氧化铝、铝、滑石和玻璃中的板状基体,以及覆盖基体的至少一部分的选自二氧化钛和铁氧化物中的至少1种的覆盖层。光亮性粉末例如可以为板状基体为云母、覆盖层为二氧化钛层的云母钛。云母可以为天然云母,也可以为合成云母。
覆盖云母的二氧化钛层的厚度可以根据作为目标的颜色来适当选择。干涉色优选为黄色(金色)。云母上的二氧化钛层的几何厚度例如可以为 60nm、70nm、或80nm以上。二氧化钛层的几何厚度例如可以为100nm 以下、90nm以下、或80nm以下。二氧化钛层的厚度例如可以通过透射型电子显微镜(TEM)测定。
覆盖层可以进一步具有覆盖二氧化钛层的至少一部分的铁氧化物层。例如,光亮性粉末可以为进一步用铁氧化物覆盖了云母钛的至少一部分的粒子。覆盖云母钛的铁氧化物相对于光亮性粉末的质量可以为1质量%以上。覆盖云母钛的铁氧化物相对于光亮性粉末的质量可以为20质量%以下。如果铁氧化物在上述范围,则在清洗后可以使肌肤看起来气色更好。
光亮性粉末可以具有例如1μm以上、5μm以上、10μm以上、15μm 以上、或20μm以上的平均粒径。光亮性粉末可以具有例如100μm以下、 90μm以下、80μm以下、70μm以下、或60μm以下的平均粒径。平均粒径例如可以通过激光衍射/散射型粒度分布计测定。
作为市售的光亮性粉末,可以使用例如,Colorona Sun Gold Sparkle Mp-29(メルク社)、Colorona Bright Gold(メルク社)、Colorona Red Gold(メルク社)、ColoronaPrecious Gold(メルク社)、CLOISONNE SPARKLE GOLD(BASF社)、GEMTONE AMBER(BASF社)、CLOISONNE GOLD(BASF社)、TIMICA BRILLIANT GOLD(BASF社)、 REFLECKS GILDED GOLD(BASF社)等。
光亮性粉末相对于清洗料组合物的质量,优选为0.03质量%以上,更优选为0.04质量%以上,进一步优选为0.05质量%以上。光亮性粉末相对于清洗料组合物的质量,可以为0.06质量%以上、0.08质量%以上、0.1 质量%以上、0.12质量%以上、0.15质量%以上、0.18质量%以上、或0.2 质量%以上。如果光亮性粉末小于0.03质量%则难以在清洗后感到肌肤的颜色变亮。光亮性粉末相对于清洗料组合物的质量,优选为0.4质量%以下,更优选为0.35质量%以下。光亮性粉末相对于清洗料组合物的质量,可以为0.3质量%以下、0.25质量%以下、0.2质量%以下、或0.15质量%以下。如果光亮性粉末超过0.4质量%则光亮性粉末易于沉降。
[液态多元醇]
液态多元醇优选为产生水合热的化合物。作为液态多元醇,可以举出例如,甘油、乙二醇、二甘醇、1,3-丁二醇、聚乙二醇、双甘油、双丙甘醇、二甘醇、1,6-己二醇、异戊二醇等。作为聚乙二醇,可以举出例如,PEG-400 等。
液态多元醇优选包含甘油。此外,液态多元醇除了甘油以外,还可以进一步包含选自聚乙二醇、1,3-丁二醇、和双丙甘醇中的至少1种。
液态多元醇相对于清洗料组合物的质量,优选为40质量%以上,更优选为50质量%以上,进一步优选为55质量%以上。液态多元醇相对于清洗料组合物的质量,可以为60质量%以上、65质量%以上、70质量%以上、75质量%以上、或80质量%以上。如果液态多元醇小于40质量%,则使用者在使用时不易获得由与水的混合引起的放热所带来的温感效果。液态多元醇相对于清洗料组合物的质量,优选为95质量%以下。液态多元醇相对于清洗料组合物的质量,可以为90质量%以下、85质量%以下、 80质量%以下、75质量%以下、70质量%以下、或65质量%以下。如果液态多元醇超过95质量%则不易获得充分的清洗力。
甘油相对于清洗料组合物的质量,优选为20质量%以上,更优选为 25质量%以上。甘油相对于清洗料组合物的质量,可以为30质量%以上、或35质量%以上。如果甘油小于20质量%,则获得充分的粘度变得困难。甘油相对于清洗料组合物的质量,可以为70质量%以下、60质量%以下、或50质量%以下。
[增稠剂]
增稠剂优选为在液态多元醇和水的含有率在本公开的范围内时能够发挥增稠效果的物质。增稠剂可以以成为与目的对应的所希望的粘度的方式添加。作为增稠剂,可举出例如,羧基乙烯基聚合物、藻酸钠、羟基乙基纤维素、黄原酸胶、透明质酸钠、琥珀酰聚糖、羧基甲基纤维素、聚丙烯酰胺、聚(丙烯酸-甲基丙烯酸烷基酯)、(二甲基丙烯酰胺/丙烯酰基二甲基牛磺酸Na)交联聚合物、聚(2-丙烯酰胺-2-甲基丙烷磺酸/乙烯基吡咯烷酮)、(丙烯酰基二甲基牛磺酸铵/甲基丙烯酸聚氧乙烯山萮醇聚醚-25)交联聚合物、 (聚氧乙烯癸基十四烷基醚/1,6-己二异氰酸酯/聚乙二醇11000共聚物、聚乙烯吡咯烷酮、氯化O-〔2-羟基-3-(三甲基铵基)丙基〕羟基乙基纤维素、氯化O-〔2-羟基-3-(三甲基铵基)丙基〕刺槐豆胶、乙烯基吡咯烷酮/甲基丙烯酸N,N-二甲基氨基乙酯/丙烯酸硬脂基酯/二丙烯酸三丙二醇酯共聚物、合成硅酸钠/镁等。其中,优选使用羧基乙烯基聚合物、(丙烯酰基二甲基牛磺酸铵/甲基丙烯酸聚氧乙烯山萮醇聚醚-25)交联聚合物、(二甲基丙烯酰胺/ 丙烯酰基二甲基牛磺酸钠)交联聚合物等。增稠剂可以使用1种或2种以上。
增稠剂相对于清洗料组合物的质量,优选为0.1质量%以上,更优选为0.2质量%以上。增稠剂相对于清洗料组合物的质量,可以为0.5质量%以上、或1质量%以上。如果增稠剂小于0.1质量%,则不能获得充分的粘度。增稠剂相对于清洗料组合物的质量,优选为5质量%以下,更优选为4质量%以下。增稠剂相对于清洗料组合物的质量,可以为3质量%以下,2质量%以下、1质量%以下、或0.5质量%以下。如果增稠剂超过5 质量%则使用者感到发粘感和皮膜感,得不到良好的使用感。
[水]
本公开的清洗料组合物可以进一步含有水。作为水,可以使用在化妆料、准药品等中使用的水,例如,可以使用纯化水、离子交换水、自来水等。
水相对于清洗料组合物的质量,优选为0.8质量%以上。水相对于清洗料组合物的质量,可以为1质量%以上、1.5质量%以上、或2质量%以上。如果水小于0.8质量%,则光亮性粉末的分散性降低。水相对于清洗料组合物的质量,优选为25质量%以下,更优选为20质量%以下,更优选为15质量%以下,更优选为10质量%以下。水相对于清洗料组合物的质量,可以为8质量%以下、5质量%以下、4质量%以下、或3质量%以下。如果水超过25质量%,则获得由多元醇带来的温感效果变难。
[表面活性剂]
本公开的清洗料组合物可以进一步含有表面活性剂。表面活性剂优选为HLB为6~15的选自聚氧乙烯脂肪酸甘油酯和聚乙二醇单脂肪酸酯中的 1种或2种以上非离子表面活性剂。如果HLB值小于6,则不易用水洗掉清洗料。如果HLB值超过15,则与彩妆化妆料中的油分的相容性变差,观察到不易获得清洗效果的倾向。HLB优选为9~14。HLB可以通过以下述式表示的川上式算出。在下述式中,MW表示亲水基部的分子量。MO 表示亲油基部的分子量。在HLB值中确认到加和性,将2种以上非离子性表面活性剂组合而使用的情况下的作为整体的HLB值由各自单独的表面活性剂的HLB值的加权平均表示。
HLB=7+11.7×log(MW/MO)
作为聚氧乙烯脂肪酸甘油酯,可举出例如,POE单异硬脂酸甘油酯 (3E.O.)(=单异硬脂酸PEG-3甘油酯)〔日本エマルジョン社制“EMALEXGWIS-103”,HLB=6〕、POE单异硬脂酸甘油酯(8E.O.)(=单异硬脂酸PEG-8甘油酯)〔日本エマルジョン社制“EMALEXGWIS-108”,HLB=10〕、POE(20)单异硬脂酸甘油酯(=单异硬脂酸PEG-20甘油酯)〔日本エマルジョン社制“EMALEXGWIS-120”, HLB=13〕、POE(7)椰油脂肪酸甘油酯(=椰油脂肪酸PEG-7甘油酯)〔コグニスジャパン社制“セチオールHE”,HLB=13〕、POE二异硬脂酸甘油酯(10E.O.)(=二异硬脂酸PEG-10甘油酯)〔日本エマルジョン社制“EMALEXGWIS-210EX”,HLB=7〕、POE二异硬脂酸甘油酯(10E.O.)(=二异硬脂酸PEG-10甘油酯)〔日本エマルジョン社制“EMALEXGWIS-210EX,HLB=7〕、POE三异硬脂酸甘油酯(20E.O.)(=三异硬脂酸PEG-20甘油酯)〔日本エマルジョン社制“EMALEXGWIS-320EX”,HLB=7〕等。
作为聚乙二醇单脂肪酸酯,可举出例如,单异硬脂酸聚乙二醇酯(6E.O.)(=单异硬脂酸PEG-6酯)〔日本エマルジョン社制“EMALEXPEIS-6EX”,HLB=9〕、单异硬脂酸聚乙二醇酯(10E.O.)(=单异硬脂酸PEG-10酯)〔日本エマルジョン社制“EMALEXPEIS-10EX”, HLB=11〕、单异硬脂酸聚乙二醇酯(12E.O.)(=单异硬脂酸聚乙二醇600 酯、单异硬脂酸PEG-12酯)〔日本エマルジョン社制“EMALEXPEIS-12EX”,HLB=12〕、单油酸聚乙二醇400酯〔HLB =11.4〕、单硬脂酸聚乙二醇400酯〔HLB=11.6〕等。
在使用聚氧乙烯脂肪酸甘油酯作为表面活性剂的情况下,使用了单脂肪酸作为脂肪酸时与使用了二脂肪酸、三脂肪酸等的情况相比,除了低温~中温区域中的稳定性这样的本发明效果以外,还可以获得高温下的稳定性效果。因此在也想要高温下的稳定性效果的情况下优选使用聚氧乙烯单脂肪酸甘油酯、聚乙二醇单脂肪酸酯。
表面活性剂相对于清洗料组合物的质量,优选为1质量%以上,更优选为2质量%以上。表面活性剂相对于清洗料组合物的质量,可以为3质量%以上、4质量%以上、5质量%以上、或6质量%以上。如果表面活性剂小于1质量%,则不能获得充分的清洗性。表面活性剂相对于清洗料组合物的质量,优选为20质量%以下,更优选为15质量%以下。表面活性剂相对于清洗料组合物的质量,可以为12质量%以下、或10质量%以下。如果表面活性剂超过20质量%则清洗力变得过强,使用者在清洗后感到紧绷感。
[油性成分]
本公开的清洗料组合物可以进一步含有油性成分。油性成分相对于清洗料组合物的质量,可以为0.1质量%以上、0.5质量%以上、1质量%以上、1.5质量%以上、或2质量%以上。油性成分相对于清洗料组合物的质量,优选为10质量%以下,更优选为8质量%以下。油性成分相对于清洗料组合物的质量,可以为5质量%以下、4质量%以下、或3质量%以下。如果油性成分超过10质量%,则产生发粘。
作为油性成分,可以使用例如,液体油脂、固体油脂、蜡(ワックス,wax)、蜡(ロウ)、烃、高级脂肪酸、高级醇、合成酯油、硅油等。
作为液体油脂,可举出例如,鳄梨油、山茶油、海龟油、澳洲坚果油、玉米油、貂油、橄榄油、菜籽油、蛋黄油、芝麻油、桃仁油、小麦胚芽油、山茶花油、蓖麻油、亚麻子油、红花油、棉籽油、紫苏油、豆油、花生油、茶籽油、榧子油、米糠油、白桐油、日本桐油、霍霍巴油、胚芽油、三甘油等。
作为固体油脂,可举出例如,可可脂、椰油、马脂、硬化椰油、棕榈油、牛脂、羊脂、硬化牛脂、棕榈仁油、猪脂、牛骨脂、木蜡仁油、硬化油、牛脚脂、木蜡、硬化蓖麻油等。
作为蜡,可举出例如,蜂蜡、小烛树蜡、棉蜡、巴西棕榈蜡、月桂蜡、虫白蜡、鲸蜡、褐煤蜡、米糠蜡、羊毛脂、木棉蜡、乙酰化羊毛脂、液态羊毛脂、甘蔗蜡、羊毛脂脂肪酸异丙酯、月桂酸己酯、还原羊毛脂、霍霍巴蜡、硬质羊毛脂、紫胶蜡、POE羊毛脂醇醚、POE羊毛脂醇乙酸酯、 POE胆固醇醚、羊毛脂脂肪酸聚乙二醇酯、POE氢化羊毛脂醇醚、例如液体石蜡、地蜡(ozocerite)、角鲨烷、姥鲛烷、石蜡、纯地蜡(Ceresine)、角鲨烯、矿脂、微晶蜡、费托蜡等。
作为蜡类,可举出例如,蜂蜡、小烛树蜡、棉蜡、巴西棕榈蜡、月桂蜡、虫白蜡、鲸蜡、褐煤蜡、米糠蜡、羊毛脂、木棉蜡、乙酰化羊毛脂、液态羊毛脂、甘蔗蜡、羊毛脂脂肪酸异丙酯、月桂酸己酯、还原羊毛脂、霍霍巴蜡、硬质羊毛脂、紫胶蜡、POE羊毛脂醇醚、POE羊毛脂醇乙酸酯、 POE胆固醇醚、羊毛脂脂肪酸聚乙二醇酯、POE氢化羊毛脂醇醚等。
作为烃油,可举出例如,液体石蜡、地蜡(ozocerite)、角鲨烷、姥鲛烷、石蜡、纯地蜡(Ceresine)、角鲨烯、矿脂、微晶蜡等。
作为高级脂肪酸,可举出例如,月桂酸、肉豆蔻酸、棕榈酸、硬脂酸、山萮酸、油酸、十一碳烯酸、妥尔油酸、异硬脂酸、亚油酸、亚麻酸、二十碳五烯酸(EPA)、二十二碳六烯酸(DHA)等。
作为高级醇,可以使用例如,直链醇(例如,月桂醇、鲸蜡醇、硬脂醇、山萮醇、肉豆蔻醇、油醇、十六醇十八醇混合物等);支链醇(例如,单硬脂基甘油醚(鲨肝醇)、2-癸基十四碳炔醇、羊毛脂醇、胆固醇、植物甾醇、己基十二烷醇、异硬脂醇、辛基十二烷醇等)等。
作为合成酯油,可举出肉豆蔻酸异丙酯、辛酸鲸蜡基酯、肉豆蔻酸辛基十二烷基酯、棕榈酸异丙酯、硬脂酸丁酯、月桂酸己酯、肉豆蔻酸肉豆蔻基酯、油酸癸酯、二甲基辛酸己基癸基酯、乳酸鲸蜡基酯、乳酸肉豆蔻基酯、乙酰化羊毛脂、硬脂酸异鲸蜡基酯、异硬脂酸异鲸蜡基酯、12-羟基硬脂酸胆甾烯基酯、二-2-乙基己酸乙二醇酯、二季戊四醇脂肪酸酯、单异硬脂酸N-烷基二醇酯、二癸酸新戊二醇酯、苹果酸二异硬脂基酯、二-2- 庚基十一烷酸甘油酯、三-2-乙基己酸三羟甲基丙烷、三异硬脂酸三羟甲基丙烷、四-2-乙基己酸季戊四醇酯、三-2-乙基己酸甘油酯、三辛酸甘油酯、三异棕榈酸甘油酯、三异硬脂酸三羟甲基丙烷、鲸蜡基2-乙基己酸酯、2- 乙基己基棕榈酸酯、三肉豆蔻酸甘油酯、三-2-庚基十一烷酸甘油酯、蓖麻油脂肪酸甲酯、油酸油基酯、乙酰甘油酯、棕榈酸2-庚基十一烷基酯、己二酸二异丁酯、N-月桂酰-L-谷氨酸-2-辛基十二烷基酯、己二酸二-2-庚基十一烷基酯、月桂酸乙酯、癸二酸二-2-乙基己基酯、肉豆蔻酸2-己基癸基酯、棕榈酸2-己基癸基酯、己二酸2-己基癸基酯、癸二酸二异丙酯、琥珀酸2-乙基己基酯、柠檬酸三乙酯等。
作为硅油,可举出二甲基聚硅氧烷、甲基氢聚硅氧烷、甲基苯基聚硅氧烷、硬脂氧基甲基聚硅氧烷、聚醚改性有机聚硅氧烷、氟烷基/聚氧化烯共改性有机聚硅氧烷、烷基改性有机聚硅氧烷、末端改性有机聚硅氧烷、氟改性有机聚硅氧烷、氨基改性有机聚硅氧烷、有机硅凝胶、丙烯酸系有机硅、三甲基甲硅烷氧基硅酸、有机硅RTV橡胶、环状五聚硅氧烷等有机硅化合物等。
[粘度]
本公开的清洗料组合物优选具有1,000mPa·s以上,更优选为 3,000mPa·s以上,更优选为5,000mPa·s以上,更优选为10,000mPa·s以上的粘度。本公开的清洗料组合物的粘度可以为15,000mPa·s以上、 20,000mPa·s以上、或25,000mPa·s以上。如果粘度小于1,000mPa·s,则光亮性粉末具有沉降倾向。本公开的清洗料组合物的粘度优选为 50,000mPa·s以下,更优选为40,000mPa·s以下。如果粘度超过 50,000mPa·s,则对肌肤的涂抹容易性降低。粘度可以在30℃下用布鲁克菲尔德型粘度计(锭子号6,转速10rpm)测定。
[其他]
本公开的清洗料组合物在不损害本公开的效果的范围内,可以根据需要适当含有其他成分,例如粉末、除上述以外的增稠剂、除上述以外的表面活性剂、水溶性醇、保湿剂、皮膜剂、油溶性紫外线吸收剂、水溶性紫外线吸收剂、多价螯合剂、氨基酸、有机胺、高分子乳液、pH调节剂、皮肤营养剂、维生素、抗氧化剂、抗氧化助剂、香料等。
作为粉末,可以使用例如,无机粉末(例如,滑石、高岭土、云母、绢云母(sericite)、白云母、金云母、合成云母、红云母、黑云母、锂云母、烧成云母、烧成滑石、蛭石、碳酸镁、碳酸钙、硅酸铝、硅酸钡、硅酸钙、硅酸镁、硅酸锶、钨酸金属盐、镁、二氧化硅、沸石、玻璃、硫酸钡、烧成硫酸钙(烧石膏)、磷酸钙、氟磷灰石、羟基磷灰石、陶瓷粉末、金属皂(例如,肉豆蔻酸锌、棕榈酸钙、硬脂酸铝)、氮化硼等);有机粉末(例如,聚酰胺树脂粉末(尼龙粉末)、聚乙烯粉末、聚甲基丙烯酸甲酯粉末、聚苯乙烯粉末、苯乙烯与丙烯酸的共聚物树脂粉末、苯胍胺树脂粉末、聚四氟乙烯粉末、纤维素粉末、有机硅树脂粉末、蚕丝粉末、羊毛粉末、氨基甲酸酯粉末等);无机白色颜料(例如,二氧化钛、氧化锌等);无机红色系颜料(例如,铁氧化物(氧化铁红)、钛酸铁等);无机褐色系颜料(γ-氧化铁等)、无机黄色系颜料(氧化铁黄、黄土等)、无机黑色系颜料(氧化铁黑、炭黑、低价氧化钛等)、无机紫色系颜料(例如,锰紫、钴紫等);无机绿色系颜料(例如,氧化铬、氢氧化铬、钛酸钴等);无机蓝色系颜料(例如,群青、藏青等);珠光颜料(例如,氧化钛覆盖云母、氧化钛覆盖氯氧化铋、氧化钛覆盖滑石、着色氧化钛覆盖云母、氯氧化铋、珠光石等);金属粉末颜料(例如,铝粉末、铜粉末等);锆、钡或铝色淀等有机颜料(例如,红色201号、红色202 号、红色204号、红色205号、红色220号、红色226号、红色228号、红色405号、橙色203号、橙色204号、黄色205号、黄色401号、和蓝色404号等有机颜料、红色3号、红色104号、红色106号、红色227号、红色230号、红色401号、红色505号、橙色205号、黄色4号、黄色5 号、黄色202号、黄色203号、绿色3号和蓝色1号等);天然色素(例如,叶绿素、β-胡萝卜素等);蜡粉末(例如,巴西棕榈蜡粉末等);淀粉粉末(例如,玉米淀粉粉末、米淀粉粉末等)等。
作为阴离子性表面活性剂,可以使用例如,脂肪酸皂(例如,月桂酸钠、棕榈酸钠等);高级烷基硫酸酯盐(例如,月桂基硫酸钠、月桂基硫酸钾等);烷基醚硫酸酯盐(例如,POE-月桂基硫酸三乙醇胺、POE-月桂基硫酸钠等); N-酰基肌氨酸(例如,月桂酰肌氨酸钠等);高级脂肪酸酰胺磺酸盐(例如, N-硬脂酰-N-甲基牛磺酸钠、N-肉豆蔻酰-N-甲基牛磺酸钠、椰油脂肪酸甲基牛磺酸钠、月桂基甲基牛磺酸钠等);磷酸酯盐(POE-油基醚磷酸钠、POE- 硬脂基醚磷酸等);磺基琥珀酸盐(例如,二-2-乙基己基磺基琥珀酸钠、单月桂酰单乙醇酰胺聚氧乙烯磺基琥珀酸钠、月桂基聚丙二醇磺基琥珀酸钠等);烷基苯磺酸盐(例如,线性十二烷基苯磺酸钠、线性十二烷基苯磺酸三乙醇胺、线性十二烷基苯磺酸等);高级脂肪酸酯硫酸酯盐(例如,硬化椰油脂肪酸甘油硫酸钠等);N-酰基谷氨酸盐(例如,N-月桂酰谷氨酸单钠、 N-硬脂酰谷氨酸二钠、N-肉豆蔻酰-L-谷氨酸单钠等);硫酸化油(例如,土耳其红油等);POE-烷基醚羧酸;POE-烷基烯丙基醚羧酸盐;α-烯烃磺酸盐;高级脂肪酸酯磺酸盐;仲醇硫酸酯盐;高级脂肪酸烷醇酰胺硫酸酯盐;月桂酰单乙醇酰胺琥珀酸钠;N-棕榈酰天冬氨酸二(三乙醇胺);酪蛋白钠等。
作为阳离子表面活性剂,可举出例如,烷基三甲基铵盐(例如,氯化硬脂基三甲基铵、氯化月桂基三甲基铵等);烷基吡啶盐(例如,氯化鲸蜡基吡啶等);二烷基二甲基铵盐(例如,氯化二硬脂基二甲基铵);氯化聚 (N,N’-二甲基-3,5-亚甲基哌啶);烷基季铵盐;烷基二甲基苄基铵盐;烷基异喹啉盐;二烷基吗啉盐;POE-烷基胺;烷基胺盐;多胺脂肪酸衍生物;戊醇脂肪酸衍生物;苯扎氯铵;苄索氯铵等。
作为两性表面活性剂,可举出例如,咪唑啉系两性表面活性剂(例如, 2-十一烷基-N,N,N-(羟基乙基羧基甲基)-2-咪唑啉钠、2-椰油酰基-2-咪唑啉氢氧化物-1-羧基乙氧基2钠盐等);甜菜碱系表面活性剂(例如,2-十七烷基-N-羧基甲基-N-羟基乙基咪唑啉甜菜碱、月桂基二甲基氨基乙酸甜菜碱、烷基甜菜碱、酰胺甜菜碱、磺基甜菜碱等)等。
作为亲水性非离子表面活性剂,可举出例如,POE-失水山梨糖醇脂肪酸酯(例如,POE-失水山梨糖醇单油酸酯、POE-失水山梨糖醇单硬脂酸酯、 POE-失水山梨糖醇单油酸酯、POE-失水山梨糖醇四油酸酯等);POE-山梨糖醇脂肪酸酯(例如,POE-山梨糖醇单月桂酸酯、POE-山梨糖醇单油酸酯、 POE-山梨糖醇五油酸酯、POE-山梨糖醇单硬脂酸酯等);POE-甘油脂肪酸酯(例如,POE-甘油单硬脂酸酯、POE-甘油单异硬脂酸酯、POE-甘油三异硬脂酸酯等POE-单油酸酯等);POE-脂肪酸酯(例如,POE-二硬脂酸酯、 POE-单二油酸酯、二硬脂酸乙二醇酯等);POE-烷基醚(例如,POE-月桂基醚、POE-油基醚、POE-硬脂基醚、POE-山萮基醚、POE-2-辛基十二烷基醚、POE-胆甾烷醇醚等);泊洛沙姆型(例如,泊洛沙姆等);POE/POP- 烷基醚(例如,POE/POP-鲸蜡基醚、POE/POP-2-癸基十四烷基醚、 POE/POP-单丁基醚、POE/POP-氢化羊毛脂、POE/POP-甘油醚等);四 POE/四POP-乙二胺缩合物(例如,テトロニック等);POE-蓖麻油硬化蓖麻油衍生物(例如,POE-蓖麻油、POE-硬化蓖麻油、POE-硬化蓖麻油单异硬脂酸酯、POE-硬化蓖麻油三异硬脂酸酯、POE-硬化蓖麻油单焦谷氨酸单异硬脂酸二酯、POE-硬化蓖麻油马来酸等);POE-蜂蜡/羊毛脂衍生物 (例如,POE-山梨糖醇蜂蜡等);链烷醇酰胺(例如,椰油脂肪酸二乙醇酰胺、月桂酸单乙醇酰胺、脂肪酸异丙醇酰胺等);POE-丙二醇脂肪酸酯;POE- 烷基胺;POE-脂肪酸酰胺;蔗糖脂肪酸酯;烷基乙氧基二甲基氧化胺;三油基磷酸等。
作为亲油性非离子表面活性剂,可举出例如,失水山梨糖醇脂肪酸酯 (例如,失水山梨糖醇单油酸酯、失水山梨糖醇单异硬脂酸酯、失水山梨糖醇单月桂酸酯、失水山梨糖醇单棕榈酸酯、失水山梨糖醇单硬脂酸酯、失水山梨糖醇倍半油酸酯、失水山梨糖醇三油酸酯、五-2-乙基己基酸二甘油失水山梨糖醇酯、四-2-乙基己基酸二甘油失水山梨糖醇酯等);甘油聚甘油脂肪酸酯(例如,单棉籽油脂肪酸甘油酯、单芥酸甘油酯、倍半油酸甘油酯、单硬脂酸甘油酯、α,α’-油酸焦谷氨酸甘油酯、单硬脂酸甘油苹果酸酯等);丙二醇脂肪酸酯(例如,单硬脂酸丙二醇酯等);硬化蓖麻油衍生物;甘油烷基醚等。
作为增稠剂,可举出例如,阿拉伯胶、角叉菜聚糖、刺梧桐树胶、黄蓍胶、角豆胶、榅桲籽(榅桲)、酪蛋白、糊精、明胶、果胶酸钠、藻酸钠、甲基纤维素、乙基纤维素、羧基甲基纤维素(CMC)、羟基乙基纤维素、羟基丙基纤维素、聚乙烯醇(PVA)、聚乙烯基甲基醚(PVM)、PVP(聚乙烯吡咯烷酮)、聚丙烯酸钠、羧基乙烯基聚合物、刺槐豆胶、瓜尔胶、酸豆籽胶、二烷基二甲基铵硫酸纤维素、黄原酸胶、硅酸铝镁、膨润土、锂蒙脱石、硅酸铝镁(ビーガム)、合成锂皂石、硅酸酐、牛磺酸酯系合成高分子、丙烯酸酯系合成高分子等。
作为水溶性醇,可以举出例如,选自低级醇、多元醇、多元醇聚合物、 2元的醇烷基醚类、2元醇烷基醚类、2元醇醚酯、甘油单烷基醚、糖醇、单糖、寡糖、多糖和它们的衍生物等中的至少1种。
作为低级醇,可举出例如,乙醇、丙醇、异丙醇、异丁醇、叔丁醇等。
作为多元醇,可举出例如,2元的醇(例如,乙二醇、丙二醇、1,3-丙二醇、1,2-丁二醇、1,3-丁二醇、1,4-丁二醇、2,3-丁二醇、1,5-戊二醇、2- 丁烯-1,4-二醇、己二醇、辛二醇等);3元的醇(例如,甘油、三羟甲基丙烷等);4元醇(例如,1,2,6-己烷三醇等季戊四醇等);5元醇(例如,木糖醇等); 6元醇(例如,山梨糖醇、甘露糖醇等);多元醇聚合物(例如,二甘醇、双丙甘醇、三甘醇、聚丙二醇、四甘醇、双甘油、聚乙二醇、三甘油、四甘油、聚甘油等);2元的醇烷基醚类(例如,乙二醇单甲基醚、乙二醇单乙基醚、乙二醇单丁基醚、乙二醇单苯基醚、乙二醇单己基醚、乙二醇单2-甲基己基醚、乙二醇异戊基醚、乙二醇苄基醚、乙二醇异丙基醚、乙二醇二甲基醚、乙二醇二乙基醚、乙二醇二丁基醚等);2元醇烷基醚类(例如,二甘醇单甲基醚、二甘醇单乙基醚、二甘醇单丁基醚、二甘醇二甲基醚、二甘醇二乙基醚、二甘醇丁基醚、二甘醇甲基乙基醚、三甘醇单甲基醚、三甘醇单乙基醚、丙二醇单甲基醚、丙二醇单乙基醚、丙二醇单丁基醚、丙二醇异丙基醚、双丙甘醇甲基醚、双丙甘醇乙基醚、双丙甘醇丁基醚等); 2元醇醚酯(例如,乙二醇单甲基醚乙酸酯、乙二醇单乙基醚乙酸酯、乙二醇单丁基醚乙酸酯、乙二醇单苯基醚乙酸酯、乙二醇二己二酸酯、乙二醇二琥珀酸酯、二甘醇单乙基醚乙酸酯、二甘醇单丁基醚乙酸酯、丙二醇单甲基醚乙酸酯、丙二醇单乙基醚乙酸酯、丙二醇单丙基醚乙酸酯、丙二醇单苯基醚乙酸酯等);甘油单烷基醚(例如,鲛肝醇、鲨油醇、鲨肝醇等);糖醇(例如,山梨糖醇、麦芽糖醇、麦芽三糖、甘露糖醇、蔗糖、赤藓醇、葡萄糖、果糖、淀粉分解糖、麦芽糖、木糖醇、淀粉分解糖还原醇等);乙交酯;四氢糠基醇;POE-四氢糠基醇;POP-丁基醚;POP/POE-丁基醚;三聚氧丙烯甘油醚;POP-甘油醚;POP-甘油醚磷酸;POP/POE-季戊四醇醚、聚甘油等。
作为单糖,可以举出例如,选自三碳糖(例如,D-甘油醛、二羟基丙酮等)、四碳糖(例如,D-赤藓糖、D-赤藓酮糖、D-苏糖、赤藓醇等)、五碳糖 (例如,L-阿拉伯糖、D-木糖、L-来苏糖、D-阿拉伯糖、D-核糖、D-核酮糖、 D-木酮糖、L-木酮糖等)、六碳糖(例如,D-葡萄糖、D-塔罗糖、D-阿洛酮糖、D-半乳糖、D-果糖、L-半乳糖、L-甘露糖、D-塔格糖等)、七碳糖(例如,庚醛糖、庚酮糖等)、八碳糖(例如,辛酮糖等)、脱氧糖(例如,2-脱氧 -D-核糖、6-脱氧-L-半乳糖、6-脱氧-L-甘露糖等)、氨基糖(例如,D-葡糖胺、 D-半乳糖胺、唾液酸、氨基糖醛酸、胞壁酸等)、糖醛酸(例如,D-葡糖醛酸、D-甘露糖醛酸、L-古洛糖醛酸、D-半乳糖醛酸、L-艾杜糖醛酸等)等中的至少1种。
作为寡糖,可以举出例如,选自蔗糖、龙胆三糖、伞形糖、乳糖、车前三糖、异剪秋罗糖类、α,α-海藻糖、棉子糖、剪秋罗糖类、石耳素、水苏糖、毛蕊花糖类等中的至少1种。
作为多糖,可以举出例如,选自纤维素、榅桲籽、硫酸软骨素、淀粉、半乳聚糖、硫酸皮肤素、糖原、阿拉伯胶、硫酸乙酰肝素、透明质酸、黄蓍胶、硫酸角质素、软骨素、黄原酸胶、硫酸粘液素、瓜尔胶、葡聚糖、硫酸角质、刺槐豆胶、琥珀酰葡聚糖、卡洛宁酸等中的至少1种。
作为其他多元醇,可以举出例如,选自聚氧乙烯甲基葡糖苷(グルカム E-10)、聚氧丙烯甲基葡糖苷(グルカムP-10)等中的至少1种。
作为天然的水溶性聚合物,可举出例如,植物系高分子(例如,阿拉伯胶、黄蓍胶、半乳聚糖、瓜尔胶、角豆胶、刺梧桐树胶、角叉菜聚糖、果胶、琼脂、榅桲籽(榅桲)、海藻胶(褐藻提取物)、淀粉(水稻、玉米、马铃薯、小麦)、甘草酸);微生物系高分子(例如,黄原酸胶、葡聚糖、琥珀酰葡聚糖、普鲁兰多糖等);动物系高分子(例如,胶原、酪蛋白、白蛋白、明胶等)等。
作为半合成的水溶性聚合物,可举出例如,淀粉系高分子(例如,羧基甲基淀粉、甲基羟基丙基淀粉等);纤维素系高分子(甲基纤维素、乙基纤维素、甲基羟基丙基纤维素、羟基乙基纤维素、纤维素硫酸钠、羟基丙基纤维素、羧基甲基纤维素、羧基甲基纤维素钠、结晶纤维素、纤维素末等);藻酸系高分子(例如,藻酸钠、藻酸丙二醇酯等)等。
作为保湿剂,可举出例如,聚乙二醇、丙二醇、甘油、1,3-丁二醇、木糖醇、山梨糖醇、麦芽糖醇、硫酸软骨素、透明质酸、硫酸粘液素、卡洛宁酸、缺端胶原、胆甾烯基-12-羟基硬脂酸酯、乳酸钠、胆汁酸盐、dl-吡咯烷酮羧酸盐、氧化烯衍生物、短链可溶性胶原、双甘油(EO)PO加成物、刺梨提取物、欧蓍草提取物、草木犀提取物等。
作为皮膜剂,可举出例如,阴离子性皮膜剂(例如,(甲基)丙烯酸/(甲基) 丙烯酸酯共聚物、甲基乙烯基醚/马来酸酐高聚合物等)、阳离子性皮膜剂(例如,阳离子化纤维素、二甲基二烯丙基氯化铵聚合物、二甲基二烯丙基氯化铵/丙烯酰胺共聚物等)、非离子性皮膜剂(例如,聚乙烯醇、聚乙烯吡咯烷酮、聚乙酸乙烯酯、聚丙烯酸酯共聚物、(甲基)丙烯酰胺、高分子有机硅、有机硅树脂、三甲基甲硅烷氧基硅酸等)。
作为水溶性紫外线吸收剂,可举出例如,二苯甲酮系紫外线吸收剂(例如,2-羟基-4-甲氧基二苯甲酮-5-磺酸盐等)、亚苄基樟脑系紫外线吸收剂(亚苄基樟脑磺酸、对苯二亚甲基二樟脑磺酸等)、苯基苯并咪唑系紫外线吸收剂(苯基苯并咪唑磺酸等)等。
作为多价螯合剂,可举出例如,1-羟基乙烷-1,1-二膦酸、1-羟基乙烷-1,1- 二膦酸四钠盐、乙二胺四乙酸二钠、乙二胺四乙酸三钠、乙二胺四乙酸四钠、柠檬酸钠、多磷酸钠、偏磷酸钠、葡糖酸、磷酸、柠檬酸、抗坏血酸、琥珀酸、乙二胺四乙酸、乙二胺羟基乙基三乙酸3钠等。
作为氨基酸,可举出例如,中性氨基酸(例如,苏氨酸、半胱氨酸等);碱性氨基酸(例如,羟基赖氨酸等)等。此外,作为氨基酸衍生物,可举出例如,酰基肌氨酸钠(月桂酰肌氨酸钠)、酰基谷氨酸盐、酰基β-丙氨酸钠、谷胱甘肽、吡咯烷酮羧酸等。
作为有机胺,可举出例如,单乙醇胺、二乙醇胺、三乙醇胺、吗啉、三异丙醇胺、2-氨基-2-甲基-1,3-丙烷二醇、2-氨基-2-甲基-1-丙醇等。
作为高分子乳液,可举出例如,丙烯酸系树脂乳液、聚丙烯酸乙酯乳液、丙烯酸系树脂液、聚丙烯酸系烷基酯乳液、聚乙酸乙烯酯树脂乳液、天然橡胶胶乳等。
作为pH调节剂,可举出例如,乳酸-乳酸钠、柠檬酸-柠檬酸钠、琥珀酸-琥珀酸钠等缓冲剂等。
作为维生素类,可举出例如,维生素A、B1、B2、B6、C、E及其衍生物、泛酸及其衍生物、生物素等。
作为抗氧化剂,可举出例如,生育酚类、二丁基羟基甲苯、丁基羟基茴香醚、没食子酸酯类等。
作为抗氧化助剂,可举出例如,磷酸、柠檬酸、抗坏血酸、马来酸、丙二酸、琥珀酸、富马酸、脑磷脂、六偏磷酸酯、肌醇六磷酸、乙二胺四乙酸等。
作为其他能够混配的成分,可举出例如,防腐剂(对羟基苯甲酸乙酯、对羟基苯甲酸丁酯、氯苯甘油醚、苯氧基乙醇等);消炎剂(例如,甘草酸衍生物、甘草亭酸衍生物、水杨酸衍生物、扁柏酚、氧化锌、尿囊素等);美白剂(例如,胎盘提取物、虎耳草提取物、熊果苷等);各种提取物(例如,黄檗、黄连、紫草、芍药、日本獐牙菜、桦树、药鼠尾草、枇杷、胡萝卜、芦荟、锦葵、鸢尾、葡萄、薏苡仁、丝瓜、百合、番红花、川芎、生姜、小连翘、红芒柄花、大蒜、辣椒、陈皮、当归、海藻等)、活化剂(例如,蜂王浆、感光素、胆固醇衍生物等);血液循环促进剂(例如,壬酸香草酰胺、烟酸苄酯、烟酸β-丁氧基乙酯、辣椒素、姜油酮、斑蝥酊、鱼石脂、单宁酸、α-龙脑、烟酸生育酚酯、肌醇六烟酸酯、环扁桃酯、桂利嗪、妥拉唑林、乙酰胆碱、维拉帕米、千金藤碱、γ-谷维素等);抗脂溢剂(例如,硫、二甲噻蒽等);抗炎剂(例如,凝血酸、硫代牛磺酸、亚牛磺酸等)等。
进一步,本公开的组合物也可以适当含有咖啡因、单宁、维拉帕米、凝血酸及其衍生物、甘草、木瓜、日本鹿蹄草等的各种生药提取物、生育酚乙酸酯、甘草次酸(グリチルレジン酸)、甘草酸及其衍生物或其盐等药剂、维生素C、抗坏血酸磷酸镁、抗坏血酸葡糖苷、熊果苷、曲酸等美白剂、精氨酸、赖氨酸等氨基酸及其衍生物。
本公开的清洗料组合物例如可以应用于脸用的清洗料等。
[制造方法]
对本公开的清洗料组合物的制造方法进行说明。本公开的清洗料组合物可以通过公知的方法制造。例如,可以通过将各成分混合来制造本公开的清洗料组合物。
在本公开的清洗料组合物中,有时相结构等不能通过组成来直接特定,或通过组成来直接特定不太实际。在这样的情况下,本公开的清洗料组合物应该被允许通过其制造方法来特定。
[使用方法]
本公开的清洗料组合物可以将清洗料组合物直接涂抹于肌肤而清洗肌肤,然后用水洗掉来使用。
如果使用本公开的清洗料组合物来清洗肌肤,则可以使洗掉后的肌肤看起来气色好。特别是,如果用本公开的清洗料组合物洗脸,则可以使脸色看起来好。
本公开的清洗料组合物如果涂抹于肌肤则多元醇与肌肤上的水分通过水合而发热。通过该温感效果(水合热),使用者在清洗时可以感到舒适感。此外,通过该温感效果,也可以易于卸除污垢。
本公开的清洗料组合物的液体部分具有透明性。本公开的清洗料组合物在透明的液体中光亮性粉末看起来亮,可以呈现漂亮的外观。
本公开的清洗料组合物具有高清洗性。本公开的清洗料组合物例如可以应用于化妆料用的清洗料(卸妆液)。
实施例
以下举例对本公开的清洗料组合物进行说明。然而,本公开的清洗料组合物不限定于以下例子。各表所示的各成分的含有率的单位为质量%。
[试验例1~35]
制作出表1~表7所示的试验例1~35涉及的清洗料组合物。关于各清洗料组合物,对洗完后的气色、光亮性粉末的分散性、清洗性、温感效果和外观进行了评价。以下显示各试验项目的评价基准。在表1~表7中显示各清洗料组合物的组成和评价。
[清洗后的肌肤的气色]
10名专门评审员将各试验例的清洗料组合物直接涂抹于脸,以擦蹭的方式清洗肌肤后,将清洗料用水洗掉,用毛巾将脸的水分除去。干燥后,确认了清洗后的脸的外观(气色)。根据评价人数而对于气色进行了评价。
A:评价为自然的颜色且看起来气色好的评审员为7名以上;
B:评价为自然的颜色且看起来气色好的评审员为4~6名;
C:评价为自然的颜色且看起来气色好的评审员为3名以下。
[光亮性粉末的分散性]
在制造清洗料组合物后,在室温环境下静置10天,对光亮性粉末的分散状态进行了确认。
A:光亮性粉末均匀地分散了;
B:光亮性粉末稍微沉降了;
C:光亮性粉末大量沉降了。
[清洗性]
脸上画了彩妆的10名专门评审员用各试验例的清洗料组合物洗脸,对彩妆的除去的程度进行了评价。根据评价人数而对于清洗性进行了评价。
A:感到可以充分地除去彩妆的评审员为7名以上;
B:感到可以充分地除去彩妆的评审员为4~6名;
C:感到可以充分地除去彩妆的评审员为3名以下。
[温感效果]
10名专门评审员将各试验例的清洗料组合物直接涂抹于脸而洗脸时,对温感效果进行了评价。根据评价人数而对于温感效果进行了评价。
A:感到具有充分的温感效果的评审员为7名以上;
B:感到具有充分的温感效果的评审员为4~6名;
C:感到具有充分的温感效果的评审员为3名以下。
[外观]
对清洗组合物的外观是否在除光亮性粉末以外的部分具有透明性进行了评价。
A:外观具有透明性;
B:外观稍微具有浑浊;
C:外观为白色。
[粘度]
粘度用30℃下的布鲁克菲尔德型粘度计(锭子编号6,转速10rpm)测定。
[试验例1~6]
改变光亮性粉末的种类和量而制作出清洗料组合物。对于未添加光亮性粉末的试验例1的清洗料组合物,评审员中多人感觉不到颜色的改善。另一方面,对于添加了光亮性粉末的试验例2~6的清洗料组合物,可以使感到了颜色的改善的评审员多。
试验例2~6的清洗料组合物的光亮性粉末的分散性及其外观也良好。此外,试验例2~6的清洗料组合物的清洗性也优异,使用者可以感到温感效果。
表1
[试验例7~14]
改变光亮性粉末的量而制作出清洗料组合物。在光亮性粉末为0.01质量%的试验例7和8中,评审员中多人感觉不到刚清洗后的颜色变亮。在光亮性粉末为0.5质量%的试验例13和14中,很多评审员感到刚清洗后的颜色变得不自然。此外,光亮性粉末的分散性也降低了。另一方面,在试验例9~12中,清洗后的肌肤的气色的评价良好。由此,可以认为光亮性粉末优选为0.03质量%以上,更优选为0.05质量%以上。此外,可以认为光亮性粉末优选为0.4质量%以下。
表2
表3
[试验例15~23]
制作出粘度不同的清洗料组合物。任一组合物都是评审员中多人可以感到在清洗后变为良好的肌肤的气色。
在粘度小于1,000mPa·s的试验例15~17中光亮性粉末沉降了。另一方面,在粘度为1,000mPa·s以上的试验例18~23中光亮性粉末的分散性被改善了。特别是,在5,000mPa·s以上的试验例21~23中未观察到光亮性粉末的沉降。由此,可以认为在提高光亮性粉末的分散性的情况下优选清洗料组合物的粘度为1,000mPa·s以上,优选为3,000mPa·s以上,更优选为5,000mPa·s以上。
表4
表5
[试验例24~35]
制作出水的量不同的清洗料组合物。任一组合物都是评审员中多人可以感到在清洗后变为良好的肌肤的气色。
在使水的量为30质量%的试验例33~35中,评审员中多人不能感到清洗时的温感效果。此外,在试验例33~35中,清洗料组合物的透明性降低了。由此,可以认为水优选为25质量%以下,优选为20质量%以下,更优选为15质量%以下,更优选为10质量%以下。
在使水的量为0.5质量%的试验例24和25中,光亮性粉末的分散性降低了。由此,可以认为在提高光亮性粉末的分散性的情况下水优选为0.8 质量%以上。
表6
表7
本发明的清洗料组合物虽然基于上述实施方式和实施例进行了说明,但不限定于上述实施方式和实施例,在本发明的范围内,并且基于本发明的基本技术思想,可以对各公开要素(包含权利要求书和说明书所记载的要素)包括各种变形、变更和改良。此外,在本发明的权利要求书的范围内,能够进行各公开要素的各种各样的组合/置换或选择。
本发明的进一步的课题、目的和方案(包括变更方案)也由包含权利要求书的本发明的全部公开事项明确了。
关于本书所记载的数值范围,即使在没有特别记载的情况下,也应该被解释为该范围内所包含的任意的数值或范围在本书中被具体记载。
上述实施方式的一部分或全部也能够如以下附记那样被记载,但不限定于以下记载。各附记也可以与权利要求书所记载的各权利要求组合。
[附记1]
清洗料组合物的使用方法,其中,使用本公开的清洗料组合物作为脸用的清洗料。
[附记2]
清洗料组合物的使用方法,其中,使用本公开的清洗料组合物作为化妆料除去清洗料。
[附记3]
本公开的清洗料组合物及其使用方法,光亮性粉末具有:
云母粒子、
覆盖上述云母粒子的至少一部分的几何厚度60nm~100nm的二氧化钛层、以及
覆盖上述二氧化钛层的至少一部分的铁氧化物层,
上述铁氧化物层相对于上述光亮性粉末的质量为1质量%~20质量%。
产业可利用性
本公开的清洗料组合物例如可以应用于对肌肤应用的清洗料、皮肤外用剂等。例如,本公开的清洗料组合物可以应用于卸妆液。
Claims (11)
1.一种清洗料组合物,含有
0.03质量%~0.4质量%的光亮性粉末、
40质量%~95质量%的液态多元醇、和
0.1质量%~5质量%的增稠剂,
所述光亮性粉末中的粒子包含
选自云母、二氧化硅、氧化铝、铝、滑石和玻璃中的板状基体,以及
覆盖所述基体的至少一部分的选自二氧化钛和铁氧化物中的至少1种的覆盖层。
2.根据权利要求1所述的清洗料组合物,
所述板状基体为云母,
所述覆盖层具有几何厚度60nm~100nm的二氧化钛层。
3.根据权利要求2所述的清洗料组合物,所述覆盖层进一步具有覆盖所述二氧化钛层的至少一部分的铁氧化物层。
4.根据权利要求1~3中任一项所述的清洗料组合物,所述粒子具有1μm~100μm的平均粒径。
5.根据权利要求1~4中任一项所述的清洗料组合物,所述液态多元醇包含相对于清洗料组合物的质量为20质量%以上的甘油。
6.根据权利要求5所述的清洗料组合物,所述液态多元醇进一步包含选自聚乙二醇、1,3-丁二醇、和双丙甘醇中的至少1种。
7.根据权利要求1~6中任一项所述的清洗料组合物,进一步包含0.8质量%~25质量%的水。
8.根据权利要求1~7中任一项所述的清洗料组合物,进一步包含1质量%~20质量%的表面活性剂。
9.根据权利要求1~8中任一项所述的清洗料组合物,油性成分相对于清洗料组合物的质量为10质量%以下。
10.根据权利要求1~9中任一项所述的清洗料组合物,其粘度为1,000mPa·s以上。
11.根据权利要求1~10中任一项所述的清洗料组合物,被应用于脸的清洗。
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