CN115367740A - Continuous preparation equipment and use method of vertical graphene - Google Patents
Continuous preparation equipment and use method of vertical graphene Download PDFInfo
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- CN115367740A CN115367740A CN202210993451.4A CN202210993451A CN115367740A CN 115367740 A CN115367740 A CN 115367740A CN 202210993451 A CN202210993451 A CN 202210993451A CN 115367740 A CN115367740 A CN 115367740A
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- C01—INORGANIC CHEMISTRY
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- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/182—Graphene
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Abstract
The invention discloses continuous preparation equipment for vertical graphene, which comprises a preparation machine and preparation boxes arranged on two sides of the preparation machine, wherein electric doors used for separating the preparation machine from the preparation boxes are arranged on two sides of the preparation machine, a guide rail is fixedly connected to the inner wall of the preparation machine, one end of the guide rail penetrates through and extends to an inner cavity of the preparation boxes, a substrate mounting frame is connected to the surface of the guide rail in a sliding mode, and a guide roller is connected to the surface of the substrate mounting frame in a rolling mode. This continuous preparation of perpendicular graphite alkene is equipped, when preparing, through basement mounting bracket and guide rail's cooperation, the material loading is carried out to the duplex position, when carrying out the material loading on one side, and the another side grows simultaneously, mutual noninterference between to it is effectual to keep warm.
Description
Technical Field
The invention relates to the technical field of graphene preparation, in particular to continuous preparation equipment and a use method of vertical graphene.
Background
The device and the method for continuously preparing the vertically oriented graphene in a large scale by using the plasmas according to the patent number CN112794316A have the following problems in use:
(1) The time of unloading can not process, need shut down and wait for a long time, can lead to a large amount of heat to run off to it is inefficient.
(2) The operator is easily scalded.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides continuous preparation equipment and a using method of vertical graphene, and solves the problems.
In order to realize the purpose, the invention is realized by the following technical scheme: the continuous preparation equipment for the vertical graphene comprises a preparation machine and preparation boxes arranged on two sides of the preparation machine, wherein electric doors used for separating the preparation machine from the preparation boxes are arranged on two sides of the preparation machine, a guide rail is fixedly connected to the inner wall of the preparation machine, one end of the guide rail penetrates through and extends to the inner cavity of the preparation boxes, substrate mounting frames are connected to the surface of the guide rail in a sliding mode, guide rollers are connected to the surface of the substrate mounting frames in a rolling mode, a driving wheel is rotatably connected to the inner cavity of the preparation boxes, a pull rope is connected to the surface of the driving wheel in a transmission mode, one end of the pull rope is fixedly connected to the surface of the substrate mounting frames, the two substrate mounting frames are provided, the two substrate mounting frames are fixedly connected through a connecting rope, an empty groove matched with the surface of the pull rope is formed in the inner cavity of each electric door, and a sealing plate which is driven by a lifting mechanism and matched with the empty groove is connected to the bottom of the inner cavity of each preparation box in a sliding mode;
the top of the preparation box is movably connected with a lifting cover, the surface of the preparation box is fixedly connected with a lifting cylinder, and the surface of a piston rod of the lifting cylinder is fixedly connected with the surface of the lifting cover.
As a further scheme of the invention: and a sealing strip sealed with the top of the preparation box is fixed at the bottom of the lifting cover.
As a further scheme of the invention: the bottom of the preparation box is fixedly connected with a fan and a hot storage box respectively, an air suction opening of the fan is communicated with the inner cavity of the preparation box, and an air outlet of the hot storage box is communicated with the inner cavity of the preparation box.
As a further scheme of the invention: the surface of basement mounting bracket rotates and is connected with the leading wheel, the surface and the surface roll connection of direction track of leading wheel.
As a further scheme of the invention: the inner cavity of the preparation box is fixedly connected with a motor for driving the driving wheel to rotate.
As a further scheme of the invention: a preparation mechanism is arranged in an inner cavity of the preparation machine.
The invention also discloses a use method of the continuous preparation equipment for the vertical graphene, which comprises the following steps:
firstly, mounting a substrate mounting frame on a guide rail in a preparation box and a preparation machine in advance, connecting two substrate mounting frames together through a connecting rope, wherein one substrate mounting frame is arranged in the preparation box, the other substrate mounting frame is arranged in the preparation machine, a motor door is closed, a sealing plate is lifted to separate the preparation box from the preparation machine, then a lifting cover at the top of the preparation box where the substrate mounting frame is located is opened, a substrate material is wound on a guide roller at the top of the substrate mounting frame, and then the lifting cover is closed;
step two, opening the electric door to lower the sealing plate, then driving the motor, driving the driving wheel to rotate by the motor to drive the pull rope to move, driving the substrate mounting rack positioned in the inner cavity of the preparation machine to move into another preparation box, and driving the substrate mounting rack positioned in the preparation box to move into the preparation machine for preparation through the connecting rope;
step three, the basement mounting bracket that does not twine the basement material this moment moves to the opposite side and prepares the incasement, through opening the lift cover, carry out the installation of basement material to the opposite side, then after the growth in the centre finishes, open the reverse starter motor of electrically operated gate, export the basement mounting bracket that finishes growing, grow the leading-in of not growing, then close the electrically operated gate, start the fan of preparing the bottom of the case portion after finishing growing, take out inside steam and send to the hot storage tank in and cool down, wait to put into the hot gas input in the hot storage tank behind the new basement material.
Compared with the prior art, the invention has the following beneficial effects:
1. according to the invention, during preparation, the substrate mounting rack and the guide rail are matched, feeding is carried out at double stations, while feeding is carried out at one side, the growth is carried out at the other side simultaneously, mutual interference is avoided, and the heat preservation effect is good.
2. According to the invention, the grown substrate mounting rack is output, the non-grown lead-in is grown, then the electric door is closed, the fan at the bottom of the preparation tank is started after the growth is finished, the internal hot air is pumped out and sent into the hot storage tank for cooling, and the hot air in the hot storage tank is input for hot air replacement after new substrate materials are placed, so that the energy is saved.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a structural cross-sectional view of the present invention;
FIG. 3 is an enlarged view of a portion of the invention at A in FIG. 2;
fig. 4 is a partial enlarged view of the invention at B in fig. 2.
In the figure: 1. preparing a machine; 2. a preparation box; 3. an electrically operated door; 4. a fan; 5. a hot storage tank; 6. a substrate mounting frame; 7. a guide rail; 8. a guide wheel; 10. a lifting cylinder; 11. a lifting cover; 12. a drive wheel; 13. a motor; 14. pulling a rope; 15. connecting ropes; 16. and a guide roller.
Detailed Description
To further illustrate the technical means and effects of the present invention adopted to achieve the predetermined objects, the following detailed description of the embodiments, structures, characteristics and effects according to the present invention will be made with reference to the accompanying drawings and preferred embodiments.
Referring to fig. 1-4, the present invention provides a technical solution: a continuous preparation device for vertical graphene comprises a preparation machine 1 and preparation boxes 2 arranged on two sides of the preparation machine 1, wherein electric doors 3 used for separating the preparation machine 1 from the preparation boxes 2 are arranged on two sides of the preparation machine 1, a guide rail 7 is fixedly connected to the inner wall of the preparation machine 1, one end of the guide rail 7 penetrates through and extends to the inner cavity of the preparation boxes 2, a substrate mounting frame 6 is connected to the surface of the guide rail 7 in a sliding manner, guide rollers 16 are connected to the surface of the substrate mounting frame 6 in a rolling manner, driving wheels 12 are rotatably connected to the inner cavity of the preparation boxes 2, pull ropes 14 are connected to the surfaces of the driving wheels 12 in a transmission manner, one ends of the pull ropes 14 are fixedly connected with the surfaces of the substrate mounting frame 6, the two substrate mounting frames 6 are fixedly connected with each other through connecting ropes 15, empty grooves matched with the surfaces of the pull ropes 14 are formed in the inner cavities of telescopic sections of the electric doors 3, the bottom of the inner cavity of the preparation box 2 is connected with a sealing plate which is driven by a lifting mechanism and is matched with the empty slot in a sliding way, the electric door 3 is opened to lower the sealing plate, then a motor 13 is driven, the motor 13 drives a driving wheel 12 to rotate to drive a pulling rope 14 to move, the substrate mounting rack 6 positioned in the inner cavity of the preparation machine 1 is driven to move into another preparation box 2, at the moment, the substrate mounting rack 6 positioned in the preparation box 2 is driven to move into the preparation machine 1 through a connecting rope 15 to prepare, at the moment, the substrate mounting rack 6 which is not wound with a substrate material moves into the preparation box 2 at the other side, the substrate material is mounted at the other side by opening a lifting cover 11, then after the middle growth is finished, the electric door 3 is opened to reversely start the motor 13, the substrate mounting rack 6 which is finished with growth is output, the introduction which is not finished with growth is carried out, and then the electric door 3 is closed, starting a fan 4 at the bottom of the preparation box 2 after growth is finished, pumping out internal hot air, sending the hot air into the hot storage box 5 for cooling, inputting the hot air into the hot storage box 5 after new base materials are put in, during preparation, through the matching of the base mounting frame 6 and the guide rail 7, feeding is carried out at double stations, and when feeding is carried out at one side, the other side grows simultaneously, the feeding does not interfere with each other, and the heat preservation effect is good;
the top of the preparation box 2 is movably connected with a lifting cover 11, the surface of the preparation box 2 is fixedly connected with a lifting cylinder 10, the surface of a piston rod of the lifting cylinder 10 is fixedly connected with the surface of the lifting cover 11, the substrate mounting frames 6 are mounted on the guide rails 7 in the preparation box 2 and the preparation machine 1 in advance, the two substrate mounting frames 6 are connected together through a connecting rope 15, one substrate mounting frame 6 is in the preparation box 2 at the moment, the other substrate mounting frame 6 is in the preparation machine 1, the electric door 3 is closed to lift the sealing plate to separate the preparation box 2 from the preparation machine 1 at the moment, then the lifting cover 11 at the top of the preparation box 2 where the substrate mounting frames 6 are located is opened, the substrate material is wound on a guide roller 16 at the top of the substrate mounting frames 6, and then the lifting cover 11 is closed.
A sealing strip for sealing the top of the preparation tank 2 is fixed to the bottom of the elevating cover 11.
Prepare the bottom of case 2 fixedly connected with fan 4 and hot storage box 5 respectively, the suction opening of fan 4 and prepare the inner chamber intercommunication of case 2, the air outlet of hot storage box 5 and prepare the inner chamber intercommunication of case 2.
The surface of the substrate mounting frame 6 is rotatably connected with a guide wheel 8, and the surface of the guide wheel 8 is in rolling connection with the surface of the guide track 7.
A motor 13 for driving the driving wheel 12 to rotate is fixedly connected with the inner cavity of the preparation box 2.
The preparation mechanism is arranged in the inner cavity of the preparation machine 1.
The invention also discloses a use method of the continuous preparation equipment for the vertical graphene, which comprises the following steps:
firstly, mounting substrate mounting frames 6 on guide rails 7 in a preparation box 2 and a preparation machine 1 in advance, connecting the two substrate mounting frames 6 together through a connecting rope 15, wherein one substrate mounting frame 6 is in the preparation box 2, then the other substrate mounting frame 6 is in the preparation machine 1, closing an electric door 3 to lift a sealing plate to separate the preparation box 2 from the preparation machine 1, then opening a lifting cover 11 at the top of the preparation box 2 where the substrate mounting frames 6 are located, winding a substrate material on guide rollers 16 at the top of the substrate mounting frames 6, and then closing the lifting cover 11;
step two, the electric door 3 is opened at the moment, the sealing plate is lowered, then the motor 13 is driven, the motor 13 drives the driving wheel 12 to rotate to drive the pull rope 14 to move, the substrate mounting frame 6 in the inner cavity of the preparation machine 1 is driven to move into the other preparation box 2, and at the moment, the substrate mounting frame 6 in the preparation box 2 is driven to move into the preparation machine 1 through the connecting rope 15 to prepare;
step three, the substrate mounting rack 6 which is not wound with the substrate material moves into the preparation box 2 on the other side, the substrate material is mounted on the other side by opening the lifting cover 11, then after the middle growth is finished, the electric door 3 is opened to reversely start the motor 13, the substrate mounting rack 6 which is finished with the growth is output, the non-grown guide-in is grown, then the electric door 3 is closed, the fan 4 at the bottom of the preparation box 2 after the growth is finished is started, the internal hot air is pumped out and sent to the hot storage box 5 to be cooled, and the hot air in the hot storage box 5 is input after the new substrate material is placed.
Although the present invention has been described with reference to the preferred embodiments, it should be understood that various changes, substitutions and alterations can be made herein without departing from the spirit and scope of the invention as defined by the appended claims.
Claims (7)
1. The utility model provides a continuous preparation of perpendicular graphite alkene is equipped, includes preparation machine (1) and sets up preparation case (2) in preparation machine (1) both sides, the both sides of preparation machine (1) all are provided with electrically operated gate (3) that are used for cutting off preparation machine (1) and preparation case (2), its characterized in that: the inner wall of the preparation machine (1) is fixedly connected with a guide rail (7), one end of the guide rail (7) penetrates through and extends to an inner cavity of the preparation box (2), the surface of the guide rail (7) is connected with a substrate mounting frame (6) in a sliding mode, the surface of the substrate mounting frame (6) is connected with a guide roller (16) in a rolling mode, the inner cavity of the preparation box (2) is connected with a driving wheel (12) in a rotating mode, the surface of the driving wheel (12) is connected with a pull rope (14) in a transmission mode, one end of the pull rope (14) is fixedly connected with the surface of the substrate mounting frame (6), the substrate mounting frames (6) are provided with two parts, the two substrate mounting frames (6) are fixedly connected through a connecting rope (15), an empty groove matched with the surface of the pull rope (14) is formed in an inner cavity of a telescopic section of the electric door (3), and a sealing plate which is driven by a lifting mechanism and is matched with the empty groove is connected to the bottom of the inner cavity of the preparation box (2) in a sliding mode;
the top of the preparation box (2) is movably connected with a lifting cover (11), the surface of the preparation box (2) is fixedly connected with a lifting cylinder (10), and the surface of a piston rod of the lifting cylinder (10) is fixedly connected with the surface of the lifting cover (11).
2. The continuous preparation equipment for vertical graphene according to claim 1, characterized in that: and a sealing strip sealed with the top of the preparation box (2) is fixed at the bottom of the lifting cover (11).
3. The continuous preparation equipment for vertical graphene according to claim 1, characterized in that: prepare the bottom of case (2) and be fixedly connected with fan (4) and hot storage tank (5) respectively, the suction opening of fan (4) and the inner chamber intercommunication of preparing case (2), the air outlet of hot storage tank (5) and the inner chamber intercommunication of preparing case (2).
4. The continuous preparation equipment of vertical graphene according to claim 1, characterized in that: the surface of the substrate mounting frame (6) is rotatably connected with a guide wheel (8), and the surface of the guide wheel (8) is in rolling connection with the surface of the guide track (7).
5. The continuous preparation equipment for vertical graphene according to claim 1, characterized in that: the inner cavity of the preparation box (2) is fixedly connected with a motor (13) for driving a driving wheel (12) to rotate.
6. The continuous preparation equipment of vertical graphene according to claim 1, characterized in that: the inner cavity of the preparation machine (1) is internally provided with a preparation mechanism.
7. A use method of a continuous preparation device for vertical graphene is characterized by comprising the following steps: the method comprises the following steps:
firstly, mounting a substrate mounting rack (6) on a guide rail (7) in a preparation box (2) and a preparation machine (1) in advance, connecting the two substrate mounting racks (6) together through a connecting rope (15), closing an electric door (3) to lift a sealing plate to separate the preparation box (2) from the preparation machine (1), then opening a lifting cover (11) at the top of the preparation box (2) where the substrate mounting racks (6) are located, winding a substrate material on a guide roller (16) at the top of the substrate mounting rack (6), and then closing the lifting cover (11);
secondly, the driving motor (13) drives the substrate mounting rack (6) in the preparation box (2) to move into the preparation machine (1) through the connecting rope (15) for preparation;
step three, the basement mounting bracket (6) that does not twine the basement material at this moment moves in the opposite side prepares case (2), through opening lift cover (11), the installation of basement material is carried out to the opposite side, then after the growth of centre finishes, open electrically operated gate (3) reverse starter motor (13), export basement mounting bracket (6) that finishes growing, the leading-in that will not grow grows, then close electrically operated gate (3), start fan (4) of preparing case (2) bottom after finishing growing, take out inside steam and send to hot storage tank (5) in and cool down, wait to put into the hot air input in new basement material after with hot storage tank (5).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210993451.4A CN115367740A (en) | 2022-08-18 | 2022-08-18 | Continuous preparation equipment and use method of vertical graphene |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210993451.4A CN115367740A (en) | 2022-08-18 | 2022-08-18 | Continuous preparation equipment and use method of vertical graphene |
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| Publication Number | Publication Date |
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| CN115367740A true CN115367740A (en) | 2022-11-22 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202210993451.4A Pending CN115367740A (en) | 2022-08-18 | 2022-08-18 | Continuous preparation equipment and use method of vertical graphene |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102492934A (en) * | 2011-12-26 | 2012-06-13 | 彭鹏 | Apparatus and method used for preparing graphene, and obtained graphene |
| CN211012499U (en) * | 2019-07-29 | 2020-07-14 | 丹阳市恒泰电炉有限公司 | Waste heat recovery device of reaction furnace for producing graphene three-dimensional structure powder |
| CN113619220A (en) * | 2021-08-04 | 2021-11-09 | 北京理工大学 | Preparation method of layered graphene/titanium composite material |
| US20220316053A1 (en) * | 2019-07-18 | 2022-10-06 | Institute of Metal Research Chinese Academy of Scienes | Hfcvd device used for continuous preparation of diamond thin film, and coating method thereof |
-
2022
- 2022-08-18 CN CN202210993451.4A patent/CN115367740A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102492934A (en) * | 2011-12-26 | 2012-06-13 | 彭鹏 | Apparatus and method used for preparing graphene, and obtained graphene |
| US20220316053A1 (en) * | 2019-07-18 | 2022-10-06 | Institute of Metal Research Chinese Academy of Scienes | Hfcvd device used for continuous preparation of diamond thin film, and coating method thereof |
| CN211012499U (en) * | 2019-07-29 | 2020-07-14 | 丹阳市恒泰电炉有限公司 | Waste heat recovery device of reaction furnace for producing graphene three-dimensional structure powder |
| CN113619220A (en) * | 2021-08-04 | 2021-11-09 | 北京理工大学 | Preparation method of layered graphene/titanium composite material |
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