CN115353768B - Color logo ink capable of not fading after long time and preparation method thereof - Google Patents
Color logo ink capable of not fading after long time and preparation method thereof Download PDFInfo
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- CN115353768B CN115353768B CN202211015932.4A CN202211015932A CN115353768B CN 115353768 B CN115353768 B CN 115353768B CN 202211015932 A CN202211015932 A CN 202211015932A CN 115353768 B CN115353768 B CN 115353768B
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/16—Writing inks
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention discloses a color logo ink which does not fade for a long time and a preparation method thereof, which relate to the technical field of ink and are prepared from the following components: pine smoke, pigment, modified bone glue, spice powder extract, pearl powder, surfactant, peppermint oil and deionized water; the color ink prepared by the invention can not fade for a long time, and the raw materials used by the invention do not generate pungent smell, accord with the safety standard, and are nontoxic and harmless.
Description
Technical Field
The invention belongs to the technical field of ink, and particularly relates to color logo ink which does not fade for a long time and a preparation method thereof.
Background
The ink is an ink stick used for ancient writing and drawing in China. The main raw materials of the ink are carbon black, pine smoke, gum and the like, and carbon elements exist in an amorphous state. The ink for writing by the writing brush can be produced by grinding inkstone with water in which a colloidal solution is present.
The invention provides a color ink composition for surface dyeing of high-cleanliness materials, which comprises raw materials including dye, organic solvent, resin, humectant and additive. Compared with the chemical coloring method in the prior art, the color ink composition is used for dyeing the surfaces of metal and other accessories, has the characteristics of simple operation process and equipment, quick coloring and good color fastness, and meets the use requirement of flexible color change when small-scale metal pieces are dyed in batches. The metal surface dyed by the method can be provided with richer color, uniform and bright color and strong fastness after being dyed. The raw materials used in the invention do not generate pungent odor, are in line with the safety standard, and are nontoxic and harmless.
Accordingly, there is a need for further improvements in the art.
Disclosure of Invention
The invention aims at solving the existing problems and provides a color logo which does not fade for a long time and a preparation method thereof.
The invention is realized by the following technical scheme:
the technical scheme adopted by the invention is as follows:
the color logo ink which is not faded after being used for a long time is prepared from the following components in parts by weight:
15-20 parts of pine smoke, 6-10 parts of pigment, 30-35 parts of modified bone glue, 0.1-0.3 part of spice powder extract, 1-2 parts of pearl powder, 2-4 parts of surfactant, 1.5-1.8 parts of peppermint oil and 6-10 parts of deionized water.
As a further technical scheme: the preparation method of the modified bone glue comprises the following steps:
(1) Adding rosin into ethanol solution, then adding sodium alginate, adjusting the temperature to 80 ℃, preserving heat and stirring for 30min, and then performing rotary evaporation and drying to obtain sodium alginate modified rosin;
(2) Glutaraldehyde is added into sodium alginate modified rosin, and then grinding treatment is carried out for 1 hour, so as to obtain composite rosin;
(3) Adding the prepared compound rosin into bone glue, continuously grinding for 4 hours, and standing for 2 hours to obtain the compound rosin.
As a further technical scheme: the mixing mass ratio of the rosin to the ethanol solution is 1:5;
the mass fraction of the ethanol solution is 25%.
As a further technical scheme: the mixing mass ratio of the rosin to the sodium alginate is 15:1.2.
As a further technical scheme: the mass ratio of the sodium alginate modified rosin to glutaraldehyde is 30:1.
As a further technical scheme: the mixing mass ratio of the composite rosin to the bone glue is 1:5.
As a further technical scheme: the pigment is one or more of red, yellow and blue.
As a further technical scheme: the preparation method of the spice powder extract comprises the following steps:
radix Arnebiae, herba Senecionis Scandentis, herba Speranskiae Tuberculatae, and rhizoma Zingiberis recens at a ratio of 3:1:2:1, after mixing in mass ratio, crushing to obtain mixed crushed materials;
mixing the mixed crushed materials with ethanol solution, stirring at 1200r/min for 1 hour, filtering to obtain filter residues and filtrate, mixing the filter residues with ethanol solution, stirring at 1500r/min for 1 hour, filtering, mixing the two filtrates, and spray drying to obtain spice powder extract;
the mass fraction of the ethanol solution is 75%;
the mixing mass ratio of the mixed crushed material to the ethanol solution is 1:10;
the mixing mass ratio of the filter residue to the ethanol solution is 1:6.
As a further technical scheme: the surfactant is sodium dodecyl sulfate.
A method for preparing color ink which does not fade after long time, comprising the following steps:
(1) Weighing the following components in parts by weight: pine smoke, pigment, modified bone glue, spice powder extract, pearl powder, surfactant, peppermint oil and deionized water;
(2) Sequentially adding the pine smoke, pigment, spice powder extract, pearl powder, peppermint oil and deionized water into a stirring device, and stirring for 30min at a rotating speed of 1000 r/min;
(3) Continuously adding the modified bone glue and the surfactant into the stirring device, and stirring for 2 hours at the rotating speed of 800r/min to obtain a mixture;
(4) Injecting the mixture into a mold, freezing and shaping, drying, and demolding.
According to the invention, through the modification treatment of the bone glue, the adhesive property of the bone glue can be greatly improved, so that pigment molecules can be better adsorbed, and the fading period of the color logo ink can be greatly prolonged.
According to the invention, the compound rosin can be chemically reacted with amino groups and the like in bone glue molecules to form a space three-dimensional network structure, so that the bonding property of the bone glue can be improved, a hydrophobic chain segment can be introduced, the water resistance of the bone glue is greatly improved, and the peptide bonds in peptide chains can be broken through the introduction of alginic acid ions, so that part of macromolecules are changed into small molecules, and then a cross-linking reaction is formed, and the bone glue becomes a linear structure, so that the bone glue molecule chain is obviously prolonged, and meanwhile, the bonding property is obviously enhanced.
By taking rosin as the raw material base of the modified bone glue, the performance of the bone glue can be improved, and meanwhile, the fragrance of the rosin can be added into the bone glue, so that the fragrance of the prepared color logo ink is further improved.
The prepared color logo ink has the advantages that the glossiness, ink color gradation and aroma of the prepared color logo ink can be enhanced by introducing the pearl powder and the spice powder extract, and the pearl powder is used as a filler to increase the adhesive force of bone glue to pigment, so that the color logo ink can resist fading. By modifying the bone glue and combining other components, the compactness of the prepared color ink block can be enhanced, so that the grinding can be better carried out.
Compared with the prior art, the invention has the following advantages:
the color ink prepared by the invention can not fade for a long time, and the raw materials used by the invention do not generate pungent smell, accord with the safety standard, and are nontoxic and harmless.
The invention combines a plurality of components, the writing performance of the prepared color ink is greatly improved, and the color ink has stronger paper surface adhesive force, and also has certain waterproof performance, does not change when meeting water, and can effectively prevent the phenomenon that the painting and calligraphy works are damaged by being mistakenly touched and hydrated.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely, and it is apparent that the described embodiments are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Example 1
The color logo ink which is not faded after being used for a long time is prepared from the following components in parts by weight:
15 parts of pine smoke, 6 parts of pigment, 30 parts of modified bone glue, 0.1 part of spice powder extract, 1 part of pearl powder, 2 parts of surfactant, 1.5 parts of peppermint oil and 6 parts of deionized water.
The preparation method of the modified bone glue comprises the following steps:
(1) Adding rosin into ethanol solution, then adding sodium alginate, adjusting the temperature to 80 ℃, preserving heat and stirring for 30min, and then performing rotary evaporation and drying to obtain sodium alginate modified rosin;
(2) Glutaraldehyde is added into sodium alginate modified rosin, and then grinding treatment is carried out for 1 hour, so as to obtain composite rosin;
(3) Adding the prepared compound rosin into bone glue, continuously grinding for 4 hours, and standing for 2 hours to obtain the compound rosin.
The mixing mass ratio of the rosin to the ethanol solution is 1:5;
the mass fraction of the ethanol solution is 25%.
The mixing mass ratio of the rosin to the sodium alginate is 15:1.2.
The mass ratio of the sodium alginate modified rosin to glutaraldehyde is 30:1.
The mixing mass ratio of the composite rosin to the bone glue is 1:5.
The pigment is one or more of red, yellow and blue.
The preparation method of the spice powder extract comprises the following steps:
radix Arnebiae, herba Senecionis Scandentis, herba Speranskiae Tuberculatae, and rhizoma Zingiberis recens at a ratio of 3:1:2:1, after mixing in mass ratio, crushing to obtain mixed crushed materials;
mixing the mixed crushed materials with ethanol solution, stirring at 1200r/min for 1 hour, filtering to obtain filter residues and filtrate, mixing the filter residues with ethanol solution, stirring at 1500r/min for 1 hour, filtering, mixing the two filtrates, and spray drying to obtain spice powder extract;
the mass fraction of the ethanol solution is 75%;
the mixing mass ratio of the mixed crushed material to the ethanol solution is 1:10;
the mixing mass ratio of the filter residue to the ethanol solution is 1:6.
The surfactant is sodium dodecyl sulfate.
A method for preparing color ink which does not fade after long time, comprising the following steps:
(1) Weighing the following components in parts by weight: pine smoke, pigment, modified bone glue, spice powder extract, pearl powder, surfactant, peppermint oil and deionized water;
(2) Sequentially adding the pine smoke, pigment, spice powder extract, pearl powder, peppermint oil and deionized water into a stirring device, and stirring for 30min at a rotating speed of 1000 r/min;
(3) Continuously adding the modified bone glue and the surfactant into the stirring device, and stirring for 2 hours at the rotating speed of 800r/min to obtain a mixture;
(4) Injecting the mixture into a mold, freezing and shaping, drying, and demolding.
Example 2
The color logo ink which is not faded after being used for a long time is prepared from the following components in parts by weight:
20 parts of pine smoke, 10 parts of pigment, 35 parts of modified bone glue, 0.3 part of spice powder extract, 2 parts of pearl powder, 4 parts of surfactant, 1.8 parts of peppermint oil and 10 parts of deionized water.
The preparation method of the modified bone glue comprises the following steps:
(1) Adding rosin into ethanol solution, then adding sodium alginate, adjusting the temperature to 80 ℃, preserving heat and stirring for 30min, and then performing rotary evaporation and drying to obtain sodium alginate modified rosin;
(2) Glutaraldehyde is added into sodium alginate modified rosin, and then grinding treatment is carried out for 1 hour, so as to obtain composite rosin;
(3) Adding the prepared compound rosin into bone glue, continuously grinding for 4 hours, and standing for 2 hours to obtain the compound rosin.
The mixing mass ratio of the rosin to the ethanol solution is 1:5;
the mass fraction of the ethanol solution is 25%.
The mixing mass ratio of the rosin to the sodium alginate is 15:1.2.
The mass ratio of the sodium alginate modified rosin to glutaraldehyde is 30:1.
The mixing mass ratio of the composite rosin to the bone glue is 1:5.
The pigment is one or more of red, yellow and blue.
The preparation method of the spice powder extract comprises the following steps:
radix Arnebiae, herba Senecionis Scandentis, herba Speranskiae Tuberculatae, and rhizoma Zingiberis recens at a ratio of 3:1:2:1, after mixing in mass ratio, crushing to obtain mixed crushed materials;
mixing the mixed crushed materials with ethanol solution, stirring at 1200r/min for 1 hour, filtering to obtain filter residues and filtrate, mixing the filter residues with ethanol solution, stirring at 1500r/min for 1 hour, filtering, mixing the two filtrates, and spray drying to obtain spice powder extract;
the mass fraction of the ethanol solution is 75%;
the mixing mass ratio of the mixed crushed material to the ethanol solution is 1:10;
the mixing mass ratio of the filter residue to the ethanol solution is 1:6.
The surfactant is sodium dodecyl sulfate.
A method for preparing color ink which does not fade after long time, comprising the following steps:
(1) Weighing the following components in parts by weight: pine smoke, pigment, modified bone glue, spice powder extract, pearl powder, surfactant, peppermint oil and deionized water;
(2) Sequentially adding the pine smoke, pigment, spice powder extract, pearl powder, peppermint oil and deionized water into a stirring device, and stirring for 30min at a rotating speed of 1000 r/min;
(3) Continuously adding the modified bone glue and the surfactant into the stirring device, and stirring for 2 hours at the rotating speed of 800r/min to obtain a mixture;
(4) Injecting the mixture into a mold, freezing and shaping, drying, and demolding.
Example 3
The color logo ink which is not faded after being used for a long time is prepared from the following components in parts by weight:
18 parts of pine smoke, 7 parts of pigment, 32 parts of modified bone glue, 0.2 part of spice powder extract, 1.5 parts of pearl powder, 3 parts of surfactant, 1.6 parts of peppermint oil and 8 parts of deionized water.
The preparation method of the modified bone glue comprises the following steps:
(1) Adding rosin into ethanol solution, then adding sodium alginate, adjusting the temperature to 80 ℃, preserving heat and stirring for 30min, and then performing rotary evaporation and drying to obtain sodium alginate modified rosin;
(2) Glutaraldehyde is added into sodium alginate modified rosin, and then grinding treatment is carried out for 1 hour, so as to obtain composite rosin;
(3) Adding the prepared compound rosin into bone glue, continuously grinding for 4 hours, and standing for 2 hours to obtain the compound rosin.
The mixing mass ratio of the rosin to the ethanol solution is 1:5;
the mass fraction of the ethanol solution is 25%.
The mixing mass ratio of the rosin to the sodium alginate is 15:1.2.
The mass ratio of the sodium alginate modified rosin to glutaraldehyde is 30:1.
The mixing mass ratio of the composite rosin to the bone glue is 1:5.
The pigment is one or more of red, yellow and blue.
The preparation method of the spice powder extract comprises the following steps:
radix Arnebiae, herba Senecionis Scandentis, herba Speranskiae Tuberculatae, and rhizoma Zingiberis recens at a ratio of 3:1:2:1, after mixing in mass ratio, crushing to obtain mixed crushed materials;
mixing the mixed crushed materials with ethanol solution, stirring at 1200r/min for 1 hour, filtering to obtain filter residues and filtrate, mixing the filter residues with ethanol solution, stirring at 1500r/min for 1 hour, filtering, mixing the two filtrates, and spray drying to obtain spice powder extract;
the mass fraction of the ethanol solution is 75%;
the mixing mass ratio of the mixed crushed material to the ethanol solution is 1:10;
the mixing mass ratio of the filter residue to the ethanol solution is 1:6.
The surfactant is sodium dodecyl sulfate.
A method for preparing color ink which does not fade after long time, comprising the following steps:
(1) Weighing the following components in parts by weight: pine smoke, pigment, modified bone glue, spice powder extract, pearl powder, surfactant, peppermint oil and deionized water;
(2) Sequentially adding the pine smoke, pigment, spice powder extract, pearl powder, peppermint oil and deionized water into a stirring device, and stirring for 30min at a rotating speed of 1000 r/min;
(3) Continuously adding the modified bone glue and the surfactant into the stirring device, and stirring for 2 hours at the rotating speed of 800r/min to obtain a mixture;
(4) Injecting the mixture into a mold, freezing and shaping, drying, and demolding.
Comparative example 1: the difference from example 1 is that the bone glue is not modified;
comparative example 2: the difference from example 1 is that rosin was replaced with starch in the bone glue modification;
test
The diffusivity of ten prescription pine ink obtained by test four is detected according to the current standard DB34/T1379-2020 (Anhui province local standard) of the Hui ink, and the method is as follows:
taking a proper amount of standard ink in a viscosity test, adding distilled water, and mixing according to a ratio of 1:25, preparing diluted ink in proportion, sucking 0.05mL of the diluted ink by using a suction pipe with a scale value of 0.01mL, vertically contacting a dropper with a filter paper surface to naturally suck the diluted ink into the filter paper for diffusion, measuring the outer circle diameter d1 of the ink mark by using a vernier caliper on two vertical lines passing through the center of a circle after the ink is naturally dried, and simultaneously, using distilled water to replace the diluted ink, and measuring the outer circle diameter d of the water mark according to the method.
The result is calculated according to the following formula:
wherein: diffusivity = d1/d x 100%;
d1: the diameter of the outer circle of the ink mark;
d: diameter of the excircle of distilled water;
the data obtained are as follows;
TABLE 1
| Diffusivity% | |
| Example 1 | 83.5 |
| Example 2 | 85.1 |
| Example 3 | 83.2 |
| Comparative example 1 | 63.5 |
| Comparative example 2 | 67.8 |
As can be seen from Table 1, the diffusivity of the color ink prepared by the method provided by the invention is obviously improved, and the writing smoothness is improved conveniently.
Writing the sample of the embodiment, and detecting the appearance;
TABLE 2
| Appearance of | |
| Example 1 | The surface is free from damage, smooth and crack |
| Example 2 | The surface is free from damage, smooth and crack |
| Example 3 | No surface damage and no lightSlip, no crack |
As can be seen from table 2, the color ink writing product prepared according to the present invention has an excellent appearance.
Fade detection (uv light exposure for 30 h):
TABLE 3 Table 3
| Fading | |
| Example 1 | Whether or not |
| Example 2 | Whether or not |
| Example 3 | Whether or not |
| Comparative example 1 | Obvious fading |
| Comparative example 2 | Obvious fading |
As can be seen from Table 3, the color ink prepared by the present invention has excellent color fastness and excellent color fastness.
The foregoing description of the preferred embodiments of the invention should not be taken as limiting the scope of the invention, which is defined by the appended claims, but rather by the description of the preferred embodiments, all changes and modifications that come within the meaning and range of equivalency of the claims are intended to be embraced therein.
Claims (8)
1. A color ink that does not fade for a long time, characterized by: the coating is prepared from the following components in parts by weight:
15-20 parts of pine smoke, 6-10 parts of pigment, 30-35 parts of modified bone glue, 0.1-0.3 part of spice powder extract, 1-2 parts of pearl powder, 2-4 parts of surfactant, 1.5-1.8 parts of peppermint oil and 6-10 parts of deionized water; the preparation method of the modified bone glue comprises the following steps:
(1) Adding rosin into ethanol solution, then adding sodium alginate, adjusting the temperature to 80 ℃, preserving heat and stirring for 30min, and then performing rotary evaporation and drying to obtain sodium alginate modified rosin;
(2) Glutaraldehyde is added into sodium alginate modified rosin, and then grinding treatment is carried out for 1 hour, so as to obtain composite rosin;
(3) Adding the prepared compound rosin into bone glue, continuously grinding for 4 hours, and standing for 2 hours to obtain the compound rosin;
the preparation method of the spice powder extract comprises the following steps:
radix Arnebiae, herba Senecionis Scandentis, herba Speranskiae Tuberculatae, and rhizoma Zingiberis recens at a ratio of 3:1:2:1, after mixing in mass ratio, crushing to obtain mixed crushed materials;
mixing the mixed crushed materials with ethanol solution, stirring at 1200r/min for 1 hour, filtering to obtain filter residues and filtrate, mixing the filter residues with ethanol solution, stirring at 1500r/min for 1 hour, filtering, mixing the two filtrates, and spray drying to obtain spice powder extract;
the mass fraction of the ethanol solution is 75%;
the mixing mass ratio of the mixed crushed material to the ethanol solution is 1:10;
the mixing mass ratio of the filter residue to the ethanol solution is 1:6.
2. A color ink of claim 1 which does not fade, wherein: the mixing mass ratio of the rosin to the ethanol solution is 1:5;
the mass fraction of the ethanol solution is 25%.
3. A color ink of claim 1 which does not fade, wherein: the mixing mass ratio of the rosin to the sodium alginate is 15:1.2.
4. A color ink of claim 1 which does not fade, wherein: the mass ratio of the sodium alginate modified rosin to glutaraldehyde is 30:1.
5. A color ink of claim 1 which does not fade, wherein: the mixing mass ratio of the composite rosin to the bone glue is 1:5.
6. A color ink of claim 1 which does not fade, wherein: the pigment is one or more of red, yellow and blue.
7. A color ink of claim 1 which does not fade, wherein: the surfactant is sodium dodecyl sulfate.
8. The method for preparing the color logo ink which is not fading after long time according to claim 1, wherein the method comprises the following steps: the method comprises the following steps:
(1) Weighing the following components in parts by weight: pine smoke, pigment, modified bone glue, spice powder extract, pearl powder, surfactant, peppermint oil and deionized water;
(2) Sequentially adding the pine smoke, pigment, spice powder extract, pearl powder, peppermint oil and deionized water into a stirring device, and stirring for 30min at a rotating speed of 1000 r/min;
(3) Continuously adding the modified bone glue and the surfactant into the stirring device, and stirring for 2 hours at the rotating speed of 800r/min to obtain a mixture;
(4) Injecting the mixture into a mold, freezing and shaping, drying, and demolding.
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