CN109504178A - A kind of production method of superelevation blackness prepared Chinese ink - Google Patents

A kind of production method of superelevation blackness prepared Chinese ink Download PDF

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Publication number
CN109504178A
CN109504178A CN201811640699.2A CN201811640699A CN109504178A CN 109504178 A CN109504178 A CN 109504178A CN 201811640699 A CN201811640699 A CN 201811640699A CN 109504178 A CN109504178 A CN 109504178A
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China
Prior art keywords
parts
chinese ink
prepared chinese
water
blackness
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CN201811640699.2A
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Chinese (zh)
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罗旭映
罗会坪
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Chongqing Technology and Business University
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Chongqing Technology and Business University
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Priority to CN201811640699.2A priority Critical patent/CN109504178A/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00Inks
    • C09D11/16Writing inks
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00Inks
    • C09D11/16Writing inks
    • C09D11/17Writing inks characterised by colouring agents

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inks, Pencil-Leads, Or Crayons (AREA)

Abstract

A kind of production method of superelevation blackness prepared Chinese ink, comprising the following steps: preliminary working-grinding-sunning-is stirred-blends-bottles.The beneficial effects of the present invention are: operation is easy, so that various substance collective effects, mutual cooperation in prepared Chinese ink, to have superelevation blackness, and the property write, fluency improve on rice paper, the length of lines has also obtained increasing significantly, and deep or light dry and wet is easily controllable, is suitble to use on various rice paper.

Description

A kind of production method of superelevation blackness prepared Chinese ink
Technical field
The present invention relates to ink areas, and in particular to a kind of production method of superelevation blackness prepared Chinese ink.
Background technique
Ink, one of Chinese tradition study articles, be write, drawing black pigment, after also include the red and black and various colours Ink, primary raw material are coal smoke, pine soot, glue etc., are presence of the carbon with noncrystalline kenel.Prepared Chinese ink is then traditional china ink stick grinding It forms, is that can produce by the grinding of inkstone water for brush writing, exists in water with the solution of colloid.
Existing prepared Chinese ink production technology emerges one after another, and is all changed substantially with traditional china ink stick method and is ground to prepared Chinese ink, basic skills It is that a traditional china ink stick is milled to dilute brewed, the extraction of black master batch is all also extracted using traditional pine soot and oil smoke Method, the prepared Chinese ink produced is easy burnt hair, that is, the black phenomenon of ash on rice paper, and the blackness of mass colour is very low, and prepared Chinese ink is in rice paper On be difficult to show required deep or light artistic effect.In addition, the raising of prepared Chinese ink blackness is all along with dense in prepared Chinese ink production and processing Degree is increased accordingly than also, and then affects operation fluency of the writing brush on rice paper, such as in order to pursue stream of the writing brush on rice paper Smooth property just necessarily reduces prepared Chinese ink concentration ratio, also just accordingly destroys mass colour blackness matter in this way, keep artistic expression spatial depth poor It is weary.
Summary of the invention
The object of the present invention is to provide a kind of production method of superelevation blackness prepared Chinese ink, ashless mass colour declines phenomenon after writing, And making prepared Chinese ink that there is superelevation blackness, the property write, fluency improve on rice paper, increase the length of lines significantly, deep or light dry It is wet controllable, it is suitble to use on various rice paper.
It is realized the purpose of the present invention is technical solution in this way, a kind of production method of superelevation blackness prepared Chinese ink, packet Include following steps:
Preliminary working: prepared Chinese ink material is poured into smokeless environment-friendly vertical counter-combustion boiler high temperature and pressure 10~20 minutes by S1;
S2, grinding: the material after taking out S1 processing pours into grinder, and fineness of grind to partial size is 85~350 nanometers;
S3, sunning: the materials'use drying equipment after taking out S2 processing is dried to 80% degree of drying;
Stirring: the material dried taking-up is poured into blender and stirred evenly by S4;
S5 is blent: the pure water of corresponding amount is added, stirs 10~20 minutes;
Bottling: S6 waits 5~bottling after ten minutes after the completion of stirring.
Wherein, bottling is bottled in S6 for artificial or auto-filling equipment, and it is preferable to use Ningbo prepared Chinese ink producers by the latter Auto-filling equipment.
In the present invention, the purpose that prepared Chinese ink material pours into smokeless environment-friendly vertical counter-combustion boiler high temperature and pressure is mainly increased in S1 Blacken the black effect of color masterbatch;Material after taking out S1 processing in S2 pours into grinder, and fineness of grind to partial size is 85~350 Nanometer improves the solubility of black master batch in water, has been correspondingly improved fluent writing performance while increasing effect; Sunning not only acts as the effect of cooling in S3, and the ingredient in prepared Chinese ink is made sufficiently to contact generation chemical reaction with air, increases It is strong to write brightness and blackness;Stirring in S4 is so that the substance in prepared Chinese ink is thoroughly mixed together, in progress and water after evenly mixing Blend and stir, waiting 5~10 minutes, i.e., do not generating reaction or the laggard luggage bottle of precipitating.Integrated operation is easy, makes Various substance collective effects, cooperate so that prepared Chinese ink in the present invention has superelevation blackness, and the property write, stream on rice paper Smooth property improves, and the length of lines has also obtained increasing significantly, and deep or light dry and wet is easily controllable, is suitble to use on various rice paper.
By adopting the above-described technical solution, the present invention has the advantage that: operation is easy, so that various in prepared Chinese ink Substance collective effect cooperates, so that there is superelevation blackness, and the property write, fluency improve on rice paper, the length of lines Also it has obtained increasing significantly, and deep or light dry and wet is easily controllable, has been suitble to use on various rice paper.
Specific embodiment
Below with reference to embodiment, the present invention is further illustrated.
Embodiment 1
A kind of production method of superelevation blackness prepared Chinese ink, which comprises the following steps:
Preliminary working: prepared Chinese ink material is poured into smokeless environment-friendly vertical counter-combustion boiler high temperature and pressure 10~20 minutes by S1;
S2, grinding: the material after taking out S1 processing pours into grinder, and fineness of grind to partial size is 85~350 nanometers;
S3, sunning: the materials'use drying equipment after taking out S2 processing is dried to 80% degree of drying;
Stirring: the material dried taking-up is poured into blender and stirred evenly by S4;
S5 is blent: the pure water of corresponding amount is added, stirs 10~20 minutes;
Bottling: S6 waits 5~bottling after ten minutes after the completion of stirring.
Prepared Chinese ink material includes the substance of following parts by weight in S1: 50~70 parts of high-carbon black pigment, water soluble acrylic acid rouge cream 4.5~5.5 parts of liquid, 4~5 parts of surfactant, 5.4~6.6 parts of dimethylolpropionic acid, environment-friendly water-based rosin resin 3.2~3.8 Part, 2.7~3.3 parts of gelatine, 3.8~4.6 parts of brightener, 1.8~2.2 parts of water softener, 2~2.4 parts of edible essence, aqueous defoaming 0.36~0.44 part of agent;450~550 parts of the pure water being added in S5.
Embodiment 2
A kind of production method of superelevation blackness prepared Chinese ink, which comprises the following steps:
Preliminary working: prepared Chinese ink material is poured into smokeless environment-friendly vertical counter-combustion boiler high temperature and pressure 10~20 minutes by S1;
S2, grinding: the material after taking out S1 processing pours into grinder, and fineness of grind to partial size is 85~350 nanometers;
S3, sunning: the materials'use drying equipment after taking out S2 processing is dried to 80% degree of drying;
Stirring: the material dried taking-up is poured into blender and stirred evenly by S4;
S5 is blent: the pure water of corresponding amount is added, stirs 10~20 minutes;
Bottling: S6 waits 5~bottling after ten minutes after the completion of stirring.
Prepared Chinese ink material includes the substance of following parts by weight in S1: 50 parts of high-carbon black pigment, water soluble acrylic acid fat liquor 4.5 Part, 4 parts of surfactant, 5.4 parts of dimethylolpropionic acid, 3.2 parts of environment-friendly water-based rosin resin, 2.7 parts of gelatine, brightener 3.8 Part, 1.8 parts of water softener, 2 parts of edible essence, 0.36 part of aqueous defoamer;450 parts of the pure water being added in S5.
Embodiment 3
Preliminary working: prepared Chinese ink material is poured into smokeless environment-friendly vertical counter-combustion boiler high temperature and pressure 10~20 minutes by S1;
S2, grinding: the material after taking out S1 processing pours into grinder, and fineness of grind to partial size is 85~350 nanometers;
S3, sunning: the materials'use drying equipment after taking out S2 processing is dried to 80% degree of drying;
Stirring: the material dried taking-up is poured into blender and stirred evenly by S4;
S5 is blent: the pure water of corresponding amount is added, stirs 10~20 minutes;
Bottling: S6 waits 5~bottling after ten minutes after the completion of stirring.
Wherein, in S1 prepared Chinese ink material include following parts by weight substance: 70 parts of high-carbon black pigment, water soluble acrylic acid rouge cream 5.5 parts of liquid, 5 parts of surfactant, 6.6 parts of dimethylolpropionic acid, 3.8 parts of environment-friendly water-based rosin resin, 3.3 parts of gelatine, blast 4.6 parts of agent, 2.2 parts of water softener, 2.4 parts of edible essence, 0.44 part of aqueous defoamer;550 parts of the pure water being added in S5.
Embodiment 4
Preliminary working: prepared Chinese ink material is poured into smokeless environment-friendly vertical counter-combustion boiler high temperature and pressure 10~20 minutes by S1;
S2, grinding: the material after taking out S1 processing pours into grinder, and fineness of grind to partial size is 85~350 nanometers;
S3, sunning: the materials'use drying equipment after taking out S2 processing is dried to 80% degree of drying;
Stirring: the material dried taking-up is poured into blender and stirred evenly by S4;
S5 is blent: the pure water of corresponding amount is added, stirs 10~20 minutes;
Bottling: S6 waits 5~bottling after ten minutes after the completion of stirring.
Prepared Chinese ink material includes the substance of following parts by weight in S1: 60 parts of high-carbon black pigment, water soluble acrylic acid fat liquor 5 Part, 4.5 parts of surfactant, 6 parts of dimethylolpropionic acid, 3.5 parts of environment-friendly water-based rosin resin, 3 parts of gelatine, 4.2 parts of brightener, 2 parts of water softener, 2.2 parts of edible essence, 0.4 part of aqueous defoamer;500 parts of the pure water being added in S5.
In embodiment 1 to 4, the food-grade carbon black F138 of high-carbon black pigment preferably Germany's Ou Lilong brand;Water soluble acrylic acid The product of the preferred Guangzhou Gongshi Chemical Manufacture of fat liquor;The preferred Jinan, Shandong Province Surfactant OP -10 of surfactant;Environment-protective water Property rosin resin be commercial product, preferably Guangzhou production product;The dedicated gelatine of prepared Chinese ink of the preferred Taian Shandong production of gelatine;Increase The product of bright dose of preferred Shandong Linyi production;The preferred Shanghai of edible essence is according to human relations board food-grade essence;Aqueous defoamer is preferred 1488 universal ink type auxiliary agent of TEGO FOAMEX;Various substances are commercial product.
In embodiment 1 to 4, traditional black master batch is replaced with high-carbon black pigment, as the source of prepared Chinese ink black, surface is living Property agent further function as the effect for exciting its black liveness, and water soluble acrylic acid fat liquor and gelatine are used to increase the viscous of prepared Chinese ink Consistency, and replace common borneol using edible essence, the penetrating odor of borneol and gelatine effect generation is avoided, is mentioned simultaneously The fragrance of prepared Chinese ink is risen;In addition, the anti-corrosion effect of environment-friendly water-based rosin resin is also used, after the promotion prepared Chinese ink use of brightener Vivid effect and use process in avoid generate bubble aqueous defoamer, in addition dimethylolpropionic acid increase carbon black exist As the dissolubility in the water of solvent;Various substance collective effects cooperate so that the prepared Chinese ink in the present invention has superelevation black Degree, and the property write, fluency improve on rice paper, the length of lines has also obtained increasing significantly, and deep or light dry and wet is easily controllable, It is suitble to use on various rice paper.
Experiment detection:
The prepared Chinese ink in certain commercially available brand prepared Chinese ink and the present invention in embodiment 1 to 4 is chosen as subjects, carries out following inspection It surveys:
1, odor test: two kinds of prepared Chinese ink are placed in the vessel, direct smelling.
2, Water Resistance Test is carried out using relevant regulations in QB/T2860-2007 standard.
3, color test is carried out using relevant regulations in QB/T2860-2007 standard.
4, brightness test, which is used, writes identical text in the newsprint of material and size of the same race, after it is spontaneously dried, Estimate brightness.
5, it carries out writing same font using same people using test, estimates writing effect.
6, rice paper test carries out writing identical text using several prices rice paper different with material, and effect is write in range estimation Fruit.
Concrete outcome is as follows:
It is compared by upper table it is found that the prepared Chinese ink in the present invention has superelevation blackness, and the property write, fluency mention on rice paper Height, and deep or light dry and wet is easily controllable, is suitble to use on various rice paper.
In addition, also having carried out the test of writing length, 100 milliliters of two kinds of prepared Chinese ink are taken, it is onesize identical by same person writing Text, it is found that after certain brand prepared Chinese ink is used up, the present invention in prepared Chinese ink there remains 68 milliliters, it is seen that the writing line of this prepared Chinese ink Length has also obtained increasing significantly.

Claims (6)

1. a kind of production method of superelevation blackness prepared Chinese ink, which comprises the following steps:
Preliminary working: prepared Chinese ink material is poured into smokeless environment-friendly vertical counter-combustion boiler high temperature and pressure 10~20 minutes by S1;
S2, grinding: the material after taking out S1 processing pours into grinder, and fineness of grind to partial size is 85~350 nanometers;
S3, sunning: the materials'use drying equipment after taking out S2 processing is dried to 80% degree of drying;
Stirring: the material dried taking-up is poured into blender and stirred evenly by S4;
S5 is blent: the pure water of corresponding amount is added, stirs 10~20 minutes;
Bottling: S6 waits 5~bottling after ten minutes after the completion of stirring.
2. the production method of superelevation blackness prepared Chinese ink according to claim 1, which is characterized in that bottling is manually or certainly in S6 Dynamic filling apparatus is bottled.
3. the production method of superelevation blackness prepared Chinese ink according to claim 1, which is characterized in that in S1 prepared Chinese ink material include with The substance of lower parts by weight: 50~70 parts of high-carbon black pigment, 4.5~5.5 parts of water soluble acrylic acid fat liquor, surfactant 4~5 Part, 5.4~6.6 parts of dimethylolpropionic acid, 3.2~3.8 parts of environment-friendly water-based rosin resin, 2.7~3.3 parts of gelatine, brightener 3.8 ~4.6 parts, 1.8~2.2 parts of water softener, 2~2.4 parts of edible essence, 0.36~0.44 part of aqueous defoamer;What is be added in S5 is pure 450~550 parts of water purification.
4. superelevation blackness prepared Chinese ink according to claim 2, which is characterized in that prepared Chinese ink material includes following parts by weight in S1 Substance: 50 parts of high-carbon black pigment, 4.5 parts of water soluble acrylic acid fat liquor, 4 parts of surfactant, 5.4 parts of dimethylolpropionic acid, 3.2 parts of environment-friendly water-based rosin resin, 2.7 parts of gelatine, 3.8 parts of brightener, 1.8 parts of water softener, 2 parts of edible essence, aqueous defoaming 0.36 part of agent;450 parts of the pure water being added in S5.
5. superelevation blackness prepared Chinese ink according to claim 2, which is characterized in that prepared Chinese ink material includes following parts by weight in S1 Substance: 70 parts of high-carbon black pigment, 5.5 parts of water soluble acrylic acid fat liquor, 5 parts of surfactant, 6.6 parts of dimethylolpropionic acid, 3.8 parts of environment-friendly water-based rosin resin, it is 3.3 parts of gelatine, 4.6 parts of brightener, 2.2 parts of water softener, 2.4 parts of edible essence, aqueous to disappear 0.44 part of infusion;550 parts of the pure water being added in S5.
6. superelevation blackness prepared Chinese ink according to claim 2, which is characterized in that prepared Chinese ink material includes following parts by weight in S1 Substance: 60 parts of high-carbon black pigment, 5 parts of water soluble acrylic acid fat liquor, 4.5 parts of surfactant, 6 parts of dimethylolpropionic acid, ring 3.5 parts of water-retaining property rosin resin, 3 parts of gelatine, 4.2 parts of brightener, 2 parts of water softener, 2.2 parts of edible essence, aqueous defoamer 0.4 Part;500 parts of the pure water being added in S5.
CN201811640699.2A 2018-12-29 2018-12-29 A kind of production method of superelevation blackness prepared Chinese ink Pending CN109504178A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115353768A (en) * 2022-08-24 2022-11-18 安徽省绩溪旭龙山庄四宝文化有限公司 Durable color-fast colorful logo and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1676555A (en) * 2004-03-31 2005-10-05 李联江 Water-soluble ink compositions, their manufacturing method and use
CN101180371A (en) * 2005-05-24 2008-05-14 东海碳素株式会社 Process for producing aqueous dispersion of carbon black
CN101798478A (en) * 2010-03-11 2010-08-11 齐成森 Leftover ink

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1676555A (en) * 2004-03-31 2005-10-05 李联江 Water-soluble ink compositions, their manufacturing method and use
CN101180371A (en) * 2005-05-24 2008-05-14 东海碳素株式会社 Process for producing aqueous dispersion of carbon black
CN101798478A (en) * 2010-03-11 2010-08-11 齐成森 Leftover ink

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115353768A (en) * 2022-08-24 2022-11-18 安徽省绩溪旭龙山庄四宝文化有限公司 Durable color-fast colorful logo and preparation method thereof

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Application publication date: 20190322

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