CN115259899A - Method for processing multicolor long afterglow luminescent glaze - Google Patents

Method for processing multicolor long afterglow luminescent glaze Download PDF

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Publication number
CN115259899A
CN115259899A CN202210877635.4A CN202210877635A CN115259899A CN 115259899 A CN115259899 A CN 115259899A CN 202210877635 A CN202210877635 A CN 202210877635A CN 115259899 A CN115259899 A CN 115259899A
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sintering
cavity
furnace body
cover plate
upper cover
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CN202210877635.4A
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CN115259899B (en
Inventor
邬俊明
余运龙
张利莺
吴捷春
何纲平
卢光前
卢复正
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Fujian Tianmeng Construction Co ltd
Fujian Jiangxia University
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Fujian Tianmeng Construction Co ltd
Fujian Jiangxia University
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Priority to CN202210877635.4A priority Critical patent/CN115259899B/en
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81Coating or impregnation
    • C04B41/85Coating or impregnation with inorganic materials
    • C04B41/86Glazes; Cold glazes
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C4/00Compositions for glass with special properties
    • C03C4/12Compositions for glass with special properties for luminescent glass; for fluorescent glass
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/50Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
    • C04B41/5022Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B17/00Furnaces of a kind not covered by any preceding group
    • F27B17/0016Chamber type furnaces
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D1/00Casings; Linings; Walls; Roofs
    • F27D1/18Door frames; Doors, lids, removable covers
    • F27D1/1808Removable covers
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D5/00Supports, screens, or the like for the charge within the furnace
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D99/00Subject matter not provided for in other groups of this subclass
    • F27D99/0001Heating elements or systems
    • F27D99/0033Heating elements or systems using burners

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Structural Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Furnace Charging Or Discharging (AREA)

Abstract

The invention discloses a processing method of a multicolor long afterglow luminescent glaze, which relates to the field of sintering devices and comprises a sintering furnace body, wherein a heating cavity and a sintering cavity are arranged in the sintering furnace body, the heating cavity is positioned at the bottom of the sintering cavity, a metal frame layer is arranged in the middle of the heating cavity, and the metal frame layer divides the heating cavity into an upper cavity and a lower cavity from top to bottom, the invention utilizes a sintering mode that a structural member to be sintered is completely coated by a filler, so that the purpose of sintering a molded glaze structural member which is uniformly sintered is realized, and the technical breakthrough is stronger, and the sintering mode that the structural member to be sintered is completely coated by the filler is utilized, so that the outer surface of the structural member to be sintered is uniformly doped with blue long afterglow phosphor powder, yellow phosphor powder and albite, and the molded glaze structural member can keep a long afterglow luminescent effect, and especially under a bright condition, the molded glaze structural member is more beautiful and bright.

Description

Method for processing multicolor long afterglow luminescent glaze
Technical Field
The invention relates to the technical field of luminescent glaze, in particular to a method for processing multicolor long-afterglow luminescent glaze.
Background
The sintering device is a process test instrument used in the technical fields of material science and metallurgical engineering. In the prior art, a sintering device is adopted in the method for manufacturing the glaze, the sintering device is difficult to ensure that the glaze on the whole surface of the structural part is uniformly sintered during sintering, the structural part is usually required to be placed on a screen plate for sintering, and the molding of the glaze at the bottom of the structural part is inconsistent with the molding of the glaze on the outer surface above the structural part after the molding of the glaze, so that the bottom of the structural part is difficult to keep the same aesthetic property as the exterior above the structural part, therefore, the method for processing the multicolor long-afterglow luminous glaze is invented.
Disclosure of Invention
The invention aims to provide a processing method of a multicolor long afterglow luminescent glaze, wherein a sintering mode that a structural part to be sintered is completely coated by a filling material is utilized, so that the purpose of sintering a molded glaze structural part which is completely and beautifully transparent and uniformly sintered is realized, and the technical breakthrough is stronger, and the sintering mode that the structural part to be sintered is completely coated by the filling material ensures that the external surface of the structural part to be sintered is uniformly doped with blue long afterglow powder, yellow fluorescent powder and sodium feldspar according to the weight ratio of 2 to 4, so that the integral molded glaze structural part can keep a long afterglow luminescent effect, and particularly under a bright condition, the integral molded glaze structural part is more beautiful and bright.
In order to achieve the purpose, the invention provides the following technical scheme:
the invention discloses a method for processing multicolor long afterglow luminous glaze, which comprises the following processing steps:
s1: preparing a material, namely preparing a filler, wherein the filler is a mixture of blue long afterglow powder, yellow fluorescent powder and albite according to a weight ratio of 2;
s2: laying dressing, namely loading the filler into a dressing box through a loading hopper of a processing device, starting a suction pump, conveying the filler to the bottom of a sintering cavity through a main pipeline, a lower concentration box and a first auxiliary pipe in sequence, and laying the dressing layer with the thickness of 5-8 cm;
s3: loading a structural part to be sintered, adsorbing and fixing the structural part to be sintered below a sucker, covering an upper cover plate, placing the structural part to be sintered on the surface of a dressing layer, and continuously filling filler into the sintering cavity through a suction pump so that the sintering cavity is filled with the filler and the structural part to be sintered is completely coated;
s4: and (3) sintering, namely adding fuel into the combustion chamber, sintering at 1210-1220 ℃ for 45-55min, sintering the structural part to be sintered, and forming a molded glaze structural part with a transparent whole outer surface of the sintered structural part to be sintered.
The processing device comprises a sintering furnace body, wherein a heating cavity and a sintering cavity are arranged in the sintering furnace body, the heating cavity is positioned at the bottom of the sintering cavity, a metal frame layer is arranged in the middle of the heating cavity, the metal frame layer divides the heating cavity into an upper chamber and a lower chamber from top to bottom, a second hole is formed in the inner wall of the upper end of the sintering cavity, a first hole is formed in the inner wall of the lower end of the sintering cavity, multiple groups of second holes are arranged in the second hole and the first hole, the multiple groups of second holes are distributed side by side, the multiple groups of first holes are distributed side by side, a dressing box for supplying filler into the sintering cavity is arranged on one side of the sintering furnace body, multiple groups of second auxiliary pipes and first auxiliary pipes are fixedly arranged on one side of the sintering furnace body, the second auxiliary pipes are connected with the corresponding second holes, the first auxiliary pipes are connected with the corresponding first holes, the end parts of the multiple groups of second auxiliary pipes are communicated with one group of upper concentration box, the multiple groups of first auxiliary pipes are communicated with one group of lower concentration box, the lower concentration box is connected with the upper concentration box through a suction pump, and one end of the main pipe is communicated with the interior of the dressing box;
the sintering furnace body is of a rectangular box structure, an opening is formed in the upper portion of a sintering cavity in the upper end of the sintering furnace body, an upper cover plate is arranged at the opening position, a lifting moving assembly is arranged on the upper cover plate, and a suction fixing assembly used for sucking and fixing a structural part to be processed is further arranged on the upper cover plate.
Preferably, the lifting and moving assembly comprises a second pushing unit and a first pushing unit, a side support is fixedly welded on one side of the sintering furnace body, one end of the second pushing unit is fixedly installed at the upper end of the side support, the other end of the second pushing unit is fixedly installed on the T-shaped connecting plate, the upper end of the first pushing unit is fixedly installed between the bottom of the T-shaped connecting plate, a negative pressure concentration box is fixedly installed at the lower end of the first pushing unit, the first pushing unit is distributed along the height direction of the sintering furnace body, and the second pushing unit is distributed along the width direction of the sintering furnace body.
The sintering mode that the filling material is used for completely coating the structural part to be sintered achieves the purpose of sintering the molded glaze structural part which is transparent and beautiful on the whole outer surface and is uniformly sintered, and has stronger technical breakthrough, and the sintering mode that the filling material is used for completely coating the structural part to be sintered enables the outer surface of the structural part to be sintered to be uniformly doped with blue long afterglow powder, yellow fluorescent powder and albite to be mixed according to the weight ratio of 2 to 4 in the sintering process, so that the integral molded glaze structural part can keep a long afterglow luminous effect, and particularly under the bright condition, the integral molded glaze structural part is more beautiful and bright.
Preferably, it produces the unit to inhale solid subassembly and includes second connecting pipe, first connecting pipe, sucking disc, negative pressure, the negative pressure produces the unit and fixes the upper surface one end at the upper cover plate, the negative pressure produces the unit and communicates in the one end bottom of the concentrated case of negative pressure, the concentrated case of negative pressure sets up in the top of upper cover plate, the multiunit is installed to the sucking disc in the bottom of upper cover plate, the upper end and the first connecting pipe intercommunication of sucking disc, the top of upper cover plate is extended to first connecting pipe, communicate between first connecting pipe and the second connecting pipe, the second connecting pipe communicates in the bottom of the concentrated case of negative pressure, fixed mounting is connected between first connecting pipe and the second connecting pipe.
Wherein, first promotion unit and second promotion unit all can use devices such as electric putter or cylinder, and first promotion unit can promote the upper cover plate and go up and down, makes things convenient for the upper cover plate to open or close the top opening in sintering chamber, and second promotion unit can promote the upper cover plate and remove along the width direction of sintering furnace body, and the convenience will treat that sintering structure adsorbs to fix in the bottom of sucking disc.
It needs to be noted that, the sucking disc uses the stainless steel sucking disc, its high temperature resistant is effectual, can not damage when the sintering, can use for a long time, and negative pressure produces devices such as unit use negative pressure sucking pump, negative pressure produces the unit and provides negative pressure suction for the sucking disc, make things convenient for the sucking disc to treat the sintering structure and inhale admittedly, wherein, sucking disc detachable connects on the upper cover plate, the convenience is according to treating the difference of sintering structure and changing the sucking disc of suitable shape, and the shape of sucking disc changes into current common technique, it treats the sintering structure to aim at the fixed of absorption that makes the sucking disc can be stable, do not describe here any more.
Preferably, the upper end of the dressing box is provided with a feeding hopper for adding filler into the dressing box.
The filler in the dressing box can be added through the position of the feeding hopper, and the filler can be mixed with blue long afterglow powder, yellow fluorescent powder and albite according to the weight ratio of (2).
Preferably, one side of the sintering furnace body is provided with an ash removal groove, an ash removal groove sealing door is sealed in the ash removal groove, and the ash removal groove corresponds to one side of the lower cavity.
The combustion chamber can use materials such as coal to supply heat, the fuel is combusted in the upper cavity above the combustion chamber, residues after the fuel is combusted can drop in the lower cavity, and ash in the lower cavity can be cleaned and discharged when the ash cleaning groove sealing door in the ash cleaning groove is opened, so that the use is convenient.
Preferably, one end of the sintering furnace body is provided with an inlet, the other end of the sintering furnace body is provided with an outlet, and the inlet and the outlet are respectively communicated with the inside and the outside of the upper cavity.
In the device, the inlet is used for fuel to enter, and the outlet is used for wind power to discharge, and the specific combustion process and technique are not repeated herein and are the prior common technology.
When fuel burns and burns through the surface of the metal frame layer, ash falls through gaps among the multiple groups of metal plates, and the ash refers to ash formed after the fuel burns.
Preferably, the metal frame layer includes the metal sheet of multiunit equidistance distribution, the metal sheet is fixed at the both ends inner wall in burning chamber, the metal sheet is curve platelike structure, forms the clearance between the multiunit metal sheet, have multiunit peak section and millet section on the metal sheet, multiunit peak section and multiunit millet section are adjacent to be distributed.
The fuel can use blocky fuel, the blocky fuel is easy to stay when being guided by the surface of the metal plate, the blocky fuel is convenient to fully burn and drop ash, and the fuel is reasonable to use and superior to the prior art.
Preferably, the length and the width of the upper cover plate are respectively greater than the length and the width of the sintering furnace body, a sealing ring is fixedly arranged at the bottom of the upper cover plate, and the sealing ring is sealed at the edge of the upper end of the sintering furnace body, which is clamped on the upper cover plate.
In the device, when the upper cover plate block was in sintering furnace body top, the sealing washer was sealed in the junction of sintering furnace body and upper cover plate, was convenient for realize the sealing connection between the structure.
Preferably, the width of the gap is smaller than the width of the metal plate.
The invention has the technical effects and advantages that:
1. the invention relates to a processing method of a multicolor long afterglow luminescent glaze, wherein a processing device adopted in the processing method comprises a sintering furnace body, a heating cavity and a sintering cavity are arranged in the sintering furnace body, the heating cavity is positioned at the bottom of the sintering cavity, a metal frame layer is arranged in the middle of the heating cavity, the metal frame layer divides the heating cavity into an upper cavity and a lower cavity from top to bottom, the inner wall of the upper end of the sintering cavity is provided with a second hole, and the inner wall of the lower end of the sintering cavity is provided with a first hole;
2. according to the processing method of the multicolor long afterglow luminescent glaze, the first pushing unit can push the upper cover plate to lift, so that the upper cover plate can open or close the upper opening of the sintering cavity conveniently, and the second pushing unit can push the upper cover plate to move along the width direction of the sintering furnace body, so that a structural part to be sintered can be conveniently adsorbed and fixed at the bottom of the sucking disc;
3. according to the processing method of the multicolor long afterglow luminous glaze, the sucker is a stainless steel sucker which has good high temperature resistance effect, can not be damaged during sintering and can be used for a long time, the negative pressure generating unit can use a negative pressure suction pump and other devices, the negative pressure generating unit provides negative pressure suction force for the sucker, and the sucker can conveniently suck and fix a structural part to be sintered;
4. according to the processing method of the multicolor long afterglow luminescent glaze, the filling material in the dressing box can be added through the position of the feeding hopper, and the filling material can be mixed by blue long afterglow powder, yellow fluorescent powder and albite according to the weight ratio of 2;
5. according to the processing method of the multicolor long afterglow luminescent glaze, materials such as coal and the like can be used in the combustion cavity to supply heat, the fuel is combusted in the upper cavity above the combustion cavity, residues after the fuel is combusted can fall into the lower cavity, ash in the lower cavity can be cleaned and discharged when an ash cleaning groove sealing door in an ash cleaning groove is opened, and the use is convenient;
6. according to the method for processing the multicolor long-afterglow luminous glaze, the fuel can be blocky fuel, the blocky fuel is easy to stay when being guided by the surface of the metal plate, is convenient for full combustion and ash falling, is reasonable to use and is superior to the prior art;
7. according to the method for processing the multicolor long afterglow luminescent glaze, when the upper cover plate is clamped above the sintering furnace body, the sealing ring is sealed at the joint of the sintering furnace body and the upper cover plate, so that the sealing connection between the structures is conveniently realized.
Drawings
FIG. 1 is a schematic view of the structure of the present invention.
FIG. 2 is a schematic diagram of the front side structure of the present invention.
Fig. 3 is a schematic diagram of the rear side structure of the present invention.
FIG. 4 is a schematic view of the internal structure of the present invention.
FIG. 5 is a schematic view of the filling material of the present invention.
FIG. 6 is an enlarged view of the structure at A in FIG. 3 according to the present invention.
In the figure: the device comprises a sintering furnace body 1, an inlet 2, an outlet 3, an upper cover plate 4, a suction cup 5, a first connecting pipe 6, a second connecting pipe 7, a negative pressure concentration box 8, a first pushing unit 9, a T-shaped connecting plate 10, a second pushing unit 11, a side support 12, a negative pressure generating unit 13, a loading hopper 14, a dressing box 15, an ash cleaning groove 16, an ash cleaning groove sealing door 17, an upper concentration box 18, a suction pump 19, a main pipeline 20, a lower concentration box 21, a first auxiliary pipe 22, a second auxiliary pipe 23, a first hole 25, a second hole 26, a lower chamber 27, an upper chamber 28, a metal frame layer 29, a sealing ring 30, a filling material 31, a valley section 32, a peak section 33, a metal plate 34 and a gap 35.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example one
The invention provides a processing device as shown in figures 1-6, which comprises a sintering furnace body 1, wherein a heating cavity and a sintering cavity are arranged in the sintering furnace body 1, the heating cavity is positioned at the bottom of the sintering cavity, a metal frame layer 29 is arranged in the middle of the heating cavity, the metal frame layer 29 divides the heating cavity into an upper chamber 28 and a lower chamber 27 from top to bottom, a second hole 26 is arranged on the inner wall of the upper end of the sintering cavity, a first hole 25 is arranged on the inner wall of the lower end of the sintering cavity, a plurality of groups of second holes 26 are arranged in the second hole 26 and the first hole 25, the plurality of groups of second holes 26 are distributed side by side, a dressing box 15 for supplying filler 31 into the sintering cavity is arranged on one side of the sintering furnace body 1, a plurality of groups of second auxiliary pipes 23 and first auxiliary pipes 22 are fixedly arranged on one side of the sintering furnace body 1, the second auxiliary pipes 23 are connected with the corresponding second holes 26, the first auxiliary pipes 22 are connected with the corresponding first holes 25, the ends of the plurality of second auxiliary pipes 23 are communicated with a group of upper concentration box 18, a plurality of first auxiliary pipes 22 are communicated with a group of lower concentration box 21, and a main pipe 20 connected with the upper concentration box 18 through a suction pump 20;
the sintering furnace body 1 is a rectangular box structure, the upper part of a sintering cavity at the upper end of the sintering furnace body 1 is provided with an opening, an upper cover plate 4 is arranged at the opening position, a lifting moving assembly is arranged on the upper cover plate 4, and a suction fixing assembly for sucking a structural part to be processed is further arranged on the upper cover plate 4.
The lifting moving assembly comprises a second pushing unit 11, a first pushing unit 9, a side support 12 is fixedly welded on one side of the sintering furnace body 1, one end of the second pushing unit 11 is fixedly installed at the upper end of the side support 12, the other end of the second pushing unit is fixedly installed on a T-shaped connecting plate 10, the upper end of the first pushing unit 9 and the bottom of the T-shaped connecting plate 10 are fixedly installed, a negative pressure concentration box 8 is fixedly installed at the lower end of the first pushing unit 9, the first pushing unit 9 is distributed along the height direction of the sintering furnace body 1, and the second pushing unit 11 is distributed along the width direction of the sintering furnace body 1.
According to the invention, the sintering mode that the filling material 31 is used for completely coating the structural part to be sintered is utilized, so that the purpose of sintering the molded glaze structural part which is transparent and beautiful on the whole outer surface and is uniformly sintered is realized, and a stronger technical breakthrough is achieved, and the sintering mode that the filling material 31 is used for completely coating the structural part to be sintered is utilized, so that the blue long afterglow powder, the yellow fluorescent powder and the albite are uniformly doped on the outer surface of the structural part to be sintered in the sintering process according to the weight ratio of 2 to 4, so that the integral molded glaze structural part can keep a long afterglow luminous effect, and especially under a bright condition, the integral molded glaze structural part is more beautiful and bright.
Inhale solid subassembly and include second connecting pipe 7, first connecting pipe 6, sucking disc 5, negative pressure produces unit 13 and fixes the upper surface one end at upper cover plate 4, negative pressure produces unit 13 and communicates in the one end bottom of the concentrated case 8 of negative pressure, the concentrated case 8 of negative pressure sets up in the top of upper cover plate 4, the multiunit is installed in the bottom at upper cover plate 4 to sucking disc 5, the upper end and the first connecting pipe 6 intercommunication of sucking disc 5, first connecting pipe 6 extends to the top of upper cover plate 4, communicate between first connecting pipe 6 and the second connecting pipe 7, second connecting pipe 7 communicates in the bottom of the concentrated case 8 of negative pressure, fixed mounting is connected between first connecting pipe 6 and the second connecting pipe 7.
Wherein, first promotion unit 9 and second promotion unit 11 all can use devices such as electric putter or cylinder, and first promotion unit 9 can promote the lift of upper cover plate 4, makes things convenient for upper cover plate 4 to open or close the top opening in sintering chamber, and second promotion unit 11 can promote upper cover plate 4 and remove along the width direction of sintering furnace body 1, and the convenience will treat that the absorption of sintered structure is fixed in the bottom of sucking disc 5.
It should be noted that, sucking disc 5 uses the stainless steel sucking disc, its high temperature resistant is effectual, can not damage when the sintering, can use for a long time, and negative pressure produces unit 13 and can use devices such as negative pressure sucking pump, negative pressure produces unit 13 and provides negative pressure suction for sucking disc 5, make things convenient for sucking disc 5 to treat the sintering structure and inhale admittedly, wherein, sucking disc 5 detachable connects on upper cover plate 4, the convenience is according to treating the difference of sintering structure and changing sucking disc 5 of suitable shape, and sucking disc 5's shape changes into current common technique, it treats the sintering structure to aim at making the fixed of absorption that sucking disc 5 can be stable, do not describe here any more.
The upper end of the dressing case 15 is provided with a hopper 14 for adding the filler 31 to the dressing case 15.
The filling material 31 in the dressing box 15 can be added through the position of the feeding hopper 14, and the filling material 31 can be made of other materials which can increase the brightness of the structural member to be sintered, such as glass fiber particles and the like, besides blue long afterglow powder, yellow fluorescent powder and albite which are mixed according to the weight ratio of 2.
An ash cleaning groove 16 is arranged on one side of the sintering furnace body 1, an ash cleaning groove sealing door 17 is sealed in the ash cleaning groove 16, and the ash cleaning groove 16 corresponds to one side of the lower chamber 27.
The combustion chamber can use materials such as coal to supply heat, fuel is combusted in the upper chamber 28 above the combustion chamber, residues after the fuel is combusted can fall into the lower chamber 27, ash in the lower chamber 27 can be cleaned and discharged when the ash cleaning groove sealing door 17 in the ash cleaning groove 16 is opened, and the use is convenient.
One end of the sintering furnace body 1 is provided with an inlet 2, the other end is provided with an outlet 3, and the inlet 2 and the outlet 3 are respectively communicated with the inside and the outside of the upper cavity 28.
In the device, the position of the inlet 2 is used for feeding fuel, and the position of the outlet 3 is used for discharging wind power.
When the fuel burns through the surface of the metal frame layer 29, ash, which is ash formed by the burning of the fuel, falls through the gaps 35 between the plurality of groups of metal plates 34.
The metal frame layer 29 comprises a plurality of groups of metal plates 34 distributed at equal intervals, the metal plates 34 are fixed on the inner walls of two ends of the combustion chamber, the metal plates 34 are in a curved plate-shaped structure, gaps 35 are formed among the plurality of groups of metal plates 34, a plurality of groups of peak sections 33 and valley sections 32 are arranged on the metal plates 34, and the plurality of groups of peak sections 33 and the plurality of groups of valley sections 32 are distributed adjacently.
The fuel can be blocky fuel, the blocky fuel is easy to stay when being guided by the surface of the metal plate 34, the blocky fuel is convenient to fully burn and drop ash, and the fuel is reasonable to use and superior to the prior art.
The length and width of the upper cover plate 4 are respectively greater than the length and width of the sintering furnace body 1, a sealing ring 30 is fixedly arranged at the bottom of the upper cover plate 4, and the sealing ring 30 is sealed at the edge of the upper cover plate 4 clamped at the upper end of the sintering furnace body 1.
In the device, when the upper cover plate 4 is clamped above the sintering furnace body 1, the sealing ring 30 is sealed at the joint of the sintering furnace body 1 and the upper cover plate 4, so that the sealing connection between the structures is conveniently realized.
The width of the gap 35 is smaller than the width of the metal plate 34.
The invention discloses a method for processing multicolor long afterglow luminous glaze, which comprises the following processing steps:
s1: preparing materials, namely preparing a filler 31, wherein the filler 31 is prepared by mixing blue long afterglow powder, yellow fluorescent powder and albite according to a weight ratio of 2;
s2: laying a dressing, namely filling the filler 31 into a dressing box 15 through a charging hopper 14, starting a suction pump 19, conveying the filler 31 to the bottom of a sintering cavity through a main pipeline 20, a lower concentration box 21 and a first auxiliary pipeline 22 in sequence, and laying the dressing layer with the thickness of 5cm to form a dressing layer, wherein the dressing layer with the thickness of 5cm can be used for sintering a structural member to be sintered with light weight, so that the phenomenon that the structural member to be sintered sinks to the bottom of the sintering cavity is avoided;
s3: loading a structural part to be sintered, adsorbing and fixing the structural part to be sintered below a sucker 5, covering an upper cover plate 4, placing the structural part to be sintered on the surface of a dressing layer, and continuously filling filler 31 into the sintering cavity through a suction pump 19 so that the sintering cavity is filled with the filler 31 and the structural part to be sintered is completely coated;
s4: and (3) sintering, namely adding fuel into the combustion chamber, wherein the sintering temperature is 1210-1220 ℃, sintering the structural part to be sintered, and forming a molded glaze structural part with a transparent whole outer surface on the sintered structural part to be sintered.
Example two
The invention provides a processing device as shown in figures 1-6, which comprises a sintering furnace body 1, wherein a heating cavity and a sintering cavity are arranged in the sintering furnace body 1, the heating cavity is positioned at the bottom of the sintering cavity, a metal frame layer 29 is arranged in the middle of the heating cavity, the metal frame layer 29 divides the heating cavity into an upper chamber 28 and a lower chamber 27 from top to bottom, a second hole 26 is arranged on the inner wall of the upper end of the sintering cavity, a first hole 25 is arranged on the inner wall of the lower end of the sintering cavity, a plurality of groups of second holes 26 are arranged in the second hole 26 and the first hole 25, the plurality of groups of second holes 26 are distributed side by side, the plurality of groups of first holes 25 are distributed side by side, a dressing box 15 for supplying filler 31 into the sintering cavity is arranged on one side of the sintering furnace body 1, a plurality of second auxiliary pipes 23 and first auxiliary pipes 22 are fixedly arranged on one side of the sintering furnace body 1, the second auxiliary pipes 23 are connected with the corresponding second holes 26, the first auxiliary pipes 22 are connected with the corresponding first holes 25, the ends of the plurality of second auxiliary pipes 23 are communicated on a group of upper concentration box 18, the main pipes 22 are communicated with a group of lower concentration box 21, the lower concentration box 21 and the upper concentration box 18 are connected with a main pipe 20, and a main pipe 15 is communicated with the main pipe 15 through a suction box 19;
the sintering furnace body 1 is a rectangular box structure, the upper part of a sintering cavity at the upper end of the sintering furnace body 1 is provided with an opening, an upper cover plate 4 is arranged at the opening position, a lifting moving assembly is arranged on the upper cover plate 4, and a suction fixing assembly for sucking a structural part to be processed is further arranged on the upper cover plate 4.
The lifting moving assembly comprises a second pushing unit 11, a first pushing unit 9, a side support 12 is fixedly welded on one side of the sintering furnace body 1, one end of the second pushing unit 11 is fixedly installed at the upper end of the side support 12, the other end of the second pushing unit is fixedly installed on a T-shaped connecting plate 10, the upper end of the first pushing unit 9 and the bottom of the T-shaped connecting plate 10 are fixedly installed, a negative pressure concentration box 8 is fixedly installed at the lower end of the first pushing unit 9, the first pushing unit 9 is distributed along the height direction of the sintering furnace body 1, and the second pushing unit 11 is distributed along the width direction of the sintering furnace body 1.
According to the invention, the sintering mode that the filling material 31 is used for completely coating the structural member to be sintered realizes the purpose of sintering the molded glaze structural member which is bright and beautiful on the whole outer surface and is uniformly sintered, and has a strong technical breakthrough, and the sintering mode that the filling material 31 is used for completely coating the structural member to be sintered ensures that the blue long afterglow powder, the yellow fluorescent powder and the albite are uniformly doped on the outer surface of the structural member to be sintered in the sintering process and are mixed according to the weight ratio of 2 to 4, so that the integral molded glaze structural member can keep a long afterglow luminous effect, and especially under a bright condition, the integral molded glaze structural member is beautiful and bright.
Inhale solid subassembly and include second connecting pipe 7, first connecting pipe 6, sucking disc 5, negative pressure produces unit 13 and fixes the upper surface one end at upper cover plate 4, negative pressure produces unit 13 and communicates in the one end bottom of the concentrated case 8 of negative pressure, the concentrated case 8 of negative pressure sets up in the top of upper cover plate 4, sucking disc 5 installs the multiunit in the bottom of upper cover plate 4, sucking disc 5's upper end and first connecting pipe 6 intercommunication, first connecting pipe 6 extends to the top of upper cover plate 4, communicate between first connecting pipe 6 and the second connecting pipe 7, second connecting pipe 7 communicates in the bottom of the concentrated case 8 of negative pressure, fixed mounting is connected between first connecting pipe 6 and the second connecting pipe 7.
Wherein, first promotion unit 9 and second promotion unit 11 all can use devices such as electric putter or cylinder, and first promotion unit 9 can promote the lift of upper cover plate 4, makes things convenient for upper cover plate 4 to open or close the top opening in sintering chamber, and second promotion unit 11 can promote upper cover plate 4 and remove along the width direction of sintering furnace body 1, and the convenience will treat that the absorption of sintered structure is fixed in the bottom of sucking disc 5.
It should be noted that, sucking disc 5 uses the stainless steel sucking disc, its high temperature resistant is effectual, can not damage when the sintering, can use for a long time, and negative pressure produces unit 13 and can use devices such as negative pressure sucking pump, negative pressure produces unit 13 and provides negative pressure suction for sucking disc 5, make things convenient for sucking disc 5 to treat the sintering structure and inhale admittedly, wherein, sucking disc 5 detachable connects on upper cover plate 4, the convenience is according to treating the difference of sintering structure and change the sucking disc 5 of suitable shape, and sucking disc 5's shape changes into current common technique, it treats the sintering structure to aim at making the fixed of absorption that sucking disc 5 can be stable, do not describe here any more.
The upper end of the dressing case 15 is provided with a hopper 14 for adding the filler 31 to the dressing case 15.
The filling material 31 in the dressing box 15 can be added through the position of the feeding hopper 14, and the filling material 31 can be mixed with blue long afterglow powder, yellow fluorescent powder and albite according to the weight ratio of 2 to 4, and can also be made of other materials capable of increasing the brightness of the structural member to be sintered, such as glass fiber particles and the like.
An ash cleaning groove 16 is arranged on one side of the sintering furnace body 1, an ash cleaning groove sealing door 17 is sealed in the ash cleaning groove 16, and the ash cleaning groove 16 corresponds to one side of the lower chamber 27.
The combustion chamber can use materials such as coal to supply heat, fuel is combusted in the upper chamber 28 above the combustion chamber, residues after the fuel is combusted can fall into the lower chamber 27, ash in the lower chamber 27 can be cleaned and discharged when the ash cleaning groove sealing door 17 in the ash cleaning groove 16 is opened, and the use is convenient.
One end of the sintering furnace body 1 is provided with an inlet 2, the other end is provided with an outlet 3, and the inlet 2 and the outlet 3 are respectively communicated with the inside and the outside of the upper chamber 28.
In the device, the position of the inlet 2 is used for feeding fuel, and the position of the outlet 3 is used for discharging wind power.
When the fuel burns through the surface of the metal frame layer 29, ash, which is ash formed by the burning of the fuel, falls through the gaps 35 between the plurality of groups of metal plates 34.
The metal frame layer 29 comprises a plurality of groups of metal plates 34 distributed at equal intervals, the metal plates 34 are fixed on the inner walls of two ends of the combustion chamber, the metal plates 34 are in a curved plate-shaped structure, gaps 35 are formed among the plurality of groups of metal plates 34, a plurality of groups of peak sections 33 and valley sections 32 are arranged on the metal plates 34, and the plurality of groups of peak sections 33 and the plurality of groups of valley sections 32 are distributed adjacently.
The fuel can be blocky fuel, the blocky fuel is easy to stay when being guided by the surface of the metal plate 34, the blocky fuel is convenient to fully burn and drop ash, and the fuel is reasonable to use and superior to the prior art.
The length and the width of the upper cover plate 4 are respectively greater than the length and the width of the sintering furnace body 1, a sealing ring 30 is fixedly arranged at the bottom of the upper cover plate 4, and the sealing ring 30 is sealed at the edge of the upper end position of the upper cover plate 4 clamped on the sintering furnace body 1.
In the device, when the upper cover plate 4 is clamped above the sintering furnace body 1, the sealing ring 30 is sealed at the joint of the sintering furnace body 1 and the upper cover plate 4, so that the sealing connection between the structures is conveniently realized.
The width of the gap 35 is smaller than the width of the metal plate 34.
The working principle is as follows: according to the invention, the sintering mode that the filling material 31 is used for completely coating the structural member to be sintered realizes the purpose of sintering the molded glaze structural member which is bright and beautiful on the whole outer surface and is uniformly sintered, and has a strong technical breakthrough, and the sintering mode that the filling material 31 is used for completely coating the structural member to be sintered ensures that the blue long afterglow powder, the yellow fluorescent powder and the albite are uniformly doped on the outer surface of the structural member to be sintered in the sintering process and are mixed according to the weight ratio of 2 to 4, so that the integral molded glaze structural member can keep a long afterglow luminous effect, and especially under a bright condition, the integral molded glaze structural member is beautiful and bright.
Inhale solid subassembly and include second connecting pipe 7, first connecting pipe 6, sucking disc 5, negative pressure produces unit 13 and fixes the upper surface one end at upper cover plate 4, negative pressure produces unit 13 and communicates in the one end bottom of the concentrated case 8 of negative pressure, the concentrated case 8 of negative pressure sets up in the top of upper cover plate 4, sucking disc 5 installs the multiunit in the bottom of upper cover plate 4, sucking disc 5's upper end and first connecting pipe 6 intercommunication, first connecting pipe 6 extends to the top of upper cover plate 4, communicate between first connecting pipe 6 and the second connecting pipe 7, second connecting pipe 7 communicates in the bottom of the concentrated case 8 of negative pressure, fixed mounting is connected between first connecting pipe 6 and the second connecting pipe 7.
First promotion unit 9 and second promotion unit 11 all can use devices such as electric putter or cylinder, and first promotion unit 9 can promote the lift of upper cover plate 4, makes things convenient for upper cover plate 4 to open or close the top opening in sintering chamber, and second promotion unit 11 can promote upper cover plate 4 and remove along the width direction of sintering furnace body 1, and the convenience will treat that the sintering structure adsorbs to be fixed in the bottom of sucking disc 5. Sucking disc 5 uses stainless steel sucking disc, its high temperature resistant is effectual, can not damage when the sintering, can use for a long time, and negative pressure produces unit 13 and can use devices such as negative pressure sucking pump, negative pressure produces unit 13 and provides negative pressure suction for sucking disc 5, make things convenient for sucking disc 5 to treat the sintered structure and inhale admittedly, wherein, sucking disc 5 detachable is connected on upper cover plate 4, the convenience is according to treating the difference of sintered structure and changing the sucking disc 5 of suitable shape, and sucking disc 5's shape changes into current common technique, it fixes the sintered structure of treating to aim at making the absorption that sucking disc 5 can be stable, do not do this and give unnecessary detail.
The filling material 31 in the dressing box 15 can be added through the position of the feeding hopper 14, and the filling material 31 can be made of other materials which can increase the brightness of the structural member to be sintered, such as glass fiber particles and the like, besides the blue long afterglow powder, the yellow fluorescent powder and the albite are mixed according to the weight ratio of 2.
The combustion chamber can use materials such as coal to supply heat, fuel is combusted in the upper chamber 28 above the combustion chamber, residues after the fuel is combusted can fall into the lower chamber 27, ash in the lower chamber 27 can be cleaned and discharged when the ash cleaning groove sealing door 17 in the ash cleaning groove 16 is opened, and the use is convenient.
The position of the inlet 2 is used for fuel to enter, and the position of the outlet 3 is used for wind power to discharge, and the specific combustion process and technique are not described herein again and are the prior common technology.
When fuel burns through the surface of the metal frame layer 29, ash, which is ash formed after the fuel burns, falls through the gaps 35 between the groups of metal plates 34.
The fuel can use blocky fuel, the blocky fuel is easy to stay when being guided by the surface of the metal plate 34, the blocky fuel is convenient for full combustion and ash falling, and the fuel is reasonable in use and superior to the prior art.
When the upper cover plate 4 is clamped above the sintering furnace body 1, the sealing ring 30 is sealed at the joint of the sintering furnace body 1 and the upper cover plate 4, so that the sealing connection between the structures is conveniently realized.

Claims (10)

1. A method for processing multicolor long afterglow luminous glaze is characterized by comprising the following processing steps:
s1: preparing materials, namely preparing a filler (31), wherein the filler (31) is prepared by mixing blue long afterglow powder, yellow fluorescent powder and albite according to a weight ratio of (2);
s2: laying dressing, namely filling the filler (31) into a dressing box (15) through a feeding hopper (14) of a processing device, starting a suction pump (19), conveying the filler (31) to the bottom of a sintering cavity through a main pipeline (20), a lower concentration box (21) and a first auxiliary pipeline (22) in sequence, and laying the filler to the thickness of 5cm-8cm to form a dressing layer;
s3: loading a structural part to be sintered, adsorbing and fixing the structural part to be sintered below a sucker (5), then covering an upper cover plate (4), placing the structural part to be sintered on the surface of a dressing layer, and then continuously filling filler (31) into the sintering cavity through a suction pump (19) so that the sintering cavity is filled with the filler (31) and the structural part to be sintered is completely coated;
s4: and (3) sintering, namely adding fuel into the combustion cavity, sintering the structural part to be sintered at 1210-1220 ℃ for 45-55min, and forming a molded glaze structural part with a transparent whole outer surface of the sintered structural part to be sintered.
2. The method for processing the multi-color long-afterglow luminescent glaze according to claim 1, wherein the processing device comprises a sintering furnace body (1), a heating cavity and a sintering cavity are arranged in the sintering furnace body (1), the heating cavity is positioned at the bottom of the sintering cavity, a metal frame layer (29) is arranged in the middle of the heating cavity, the metal frame layer (29) partitions the heating cavity into an upper chamber (28) and a lower chamber (27), a second hole (26) is formed in the inner wall of the upper end of the sintering cavity, a first hole (25) is formed in the inner wall of the lower end of the sintering cavity, a plurality of groups of second holes (26) are distributed side by side, a plurality of groups of first holes (25) are distributed side by side, a filling material box (15) for supplying filling material (31) into the sintering cavity is arranged on one side of the sintering furnace body (1), a plurality of second auxiliary pipes (23) and first auxiliary pipes (22) are fixedly arranged on one side of the sintering furnace body (1), the second auxiliary pipes (23) are connected with the corresponding second holes (26), the first auxiliary pipes (22) are connected with the first auxiliary pipes (23), the corresponding groups of the upper auxiliary pipes (21), and the upper auxiliary pipes (21) are communicated with the upper auxiliary pipes (18), one end of the main pipeline (20) is communicated with the interior of the dressing box (15) through a suction pump (19);
the sintering furnace body (1) is of a rectangular box structure, an opening is formed in the upper portion of a sintering cavity in the upper end of the sintering furnace body (1), an upper cover plate (4) is arranged at the opening position, a lifting moving assembly is arranged on the upper cover plate (4), and a suction fixing assembly used for sucking a structural part to be processed is further arranged on the upper cover plate (4).
3. The method for processing multicolor long-afterglow luminescent glaze according to claim 2, wherein the method comprises the following steps: the lifting and moving assembly comprises a second pushing unit (11) and a first pushing unit (9), a side support (12) is fixedly welded on one side of the sintering furnace body (1), one end of the second pushing unit (11) is fixedly installed at the upper end of the side support (12), the other end of the second pushing unit is fixedly installed on a T-shaped connecting plate (10), the upper end of the first pushing unit (9) is fixedly installed at the bottom of the T-shaped connecting plate (10), a negative pressure concentration box (8) is fixedly installed at the lower end of the first pushing unit (9), the first pushing unit (9) is distributed along the height direction of the sintering furnace body (1), and the second pushing unit (11) is distributed along the width direction of the sintering furnace body (1).
4. The method for processing multicolor long-afterglow luminescent glaze according to claim 2, wherein the method comprises the following steps: inhale solid subassembly and include second connecting pipe (7), first connecting pipe (6), sucking disc (5), negative pressure and produce unit (13), the negative pressure produces unit (13) and fixes the upper surface one end at upper cover plate (4), negative pressure produces unit (13) and communicates in the one end bottom of negative pressure concentrated case (8), negative pressure concentrated case (8) set up in the top of upper cover plate (4), the multiunit is installed in the bottom of upper cover plate (4) in sucking disc (5), the upper end and first connecting pipe (6) intercommunication of sucking disc (5), and first connecting pipe (6) extend to the top of upper cover plate (4), communicate between first connecting pipe (6) and second connecting pipe (7), second connecting pipe (7) communicate in the bottom of negative pressure concentrated case (8), fixed mounting is connected between first connecting pipe (6) and second connecting pipe (7).
5. The method for processing multicolor long afterglow luminescent glaze according to claim 4, wherein: the upper end of the dressing box (15) is provided with a loading hopper (14) for adding filler (31) into the dressing box (15).
6. The method for processing a multicolor long-afterglow luminescent glaze material as claimed in claim 4, wherein the method comprises the following steps: one side of the sintering furnace body (1) is provided with an ash removal groove (16), an ash removal groove sealing door (17) is sealed in the ash removal groove (16), and the ash removal groove (16) corresponds to one side of a lower cavity (27).
7. The method for processing a multicolor long-afterglow luminescent glaze material as claimed in claim 4, wherein the method comprises the following steps: one end of the sintering furnace body (1) is provided with an inlet (2), the other end of the sintering furnace body is provided with an outlet (3), and the inlet (2) and the outlet (3) are respectively communicated with the inside and the outside of the upper cavity (28).
8. The method for processing a multicolor long-afterglow luminescent glaze material as claimed in claim 7, wherein the method comprises the following steps: the metal frame layer (29) includes metal sheet (34) that the multiunit equidistance distributes, the both ends inner wall at combustion chamber is fixed in metal sheet (34), metal sheet (34) are curve platelike structure, form clearance (35) between multiunit metal sheet (34), have multiunit peak section (33) and valley section (32) on metal sheet (34), multiunit peak section (33) and multiunit valley section (32) adjacent distribution.
9. The method for processing multicolor long afterglow luminescent glaze according to claim 8, wherein: the length and width of the upper cover plate (4) are respectively greater than that of the sintering furnace body (1), a sealing ring (30) is fixedly arranged at the bottom of the upper cover plate (4), and the sealing ring (30) is sealed at the edge of the upper end of the upper cover plate (4) clamped at the sintering furnace body (1).
10. The method for processing multicolor long afterglow luminescent glaze according to claim 9, wherein: the width of the gap (35) is smaller than the width of the metal plate (34).
CN202210877635.4A 2022-07-25 2022-07-25 Method for processing multicolor long afterglow luminescent glaze Active CN115259899B (en)

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CN215038596U (en) * 2021-02-03 2021-12-07 福建省漳州建华陶瓷有限公司 Ceramic tile glaze spraying improves system
CN215702654U (en) * 2021-02-22 2022-02-01 唐山鼎鸿实业有限公司 Sealed glaze spraying machine for processing environment-friendly bone china tableware
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CN1613962A (en) * 2004-09-09 2005-05-11 董昇 Heat-resistant waterproof high-brightness luminous powder with long persistence and preparation thereof
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