CN115142190A - Preparation method of spring wrapping cloth - Google Patents
Preparation method of spring wrapping cloth Download PDFInfo
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- CN115142190A CN115142190A CN202210782926.5A CN202210782926A CN115142190A CN 115142190 A CN115142190 A CN 115142190A CN 202210782926 A CN202210782926 A CN 202210782926A CN 115142190 A CN115142190 A CN 115142190A
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- preparation
- spring
- wrapping cloth
- spring wrapping
- short fiber
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- 239000004744 fabric Substances 0.000 title claims abstract description 62
- 238000002360 preparation method Methods 0.000 title claims abstract description 33
- 239000000835 fiber Substances 0.000 claims abstract description 57
- 239000004743 Polypropylene Substances 0.000 claims abstract description 56
- -1 polypropylene Polymers 0.000 claims abstract description 44
- 229920001155 polypropylene Polymers 0.000 claims abstract description 44
- 238000009960 carding Methods 0.000 claims abstract description 23
- 239000003607 modifier Substances 0.000 claims abstract description 21
- 239000000203 mixture Substances 0.000 claims abstract description 18
- 230000002787 reinforcement Effects 0.000 claims abstract description 18
- 238000001125 extrusion Methods 0.000 claims abstract description 17
- 229910021536 Zeolite Inorganic materials 0.000 claims abstract description 16
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000000843 powder Substances 0.000 claims abstract description 16
- 239000010457 zeolite Substances 0.000 claims abstract description 16
- 239000000155 melt Substances 0.000 claims abstract description 15
- 238000012986 modification Methods 0.000 claims description 17
- 230000004048 modification Effects 0.000 claims description 17
- 238000002156 mixing Methods 0.000 claims description 16
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 claims description 15
- 238000005520 cutting process Methods 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- 238000000498 ball milling Methods 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 11
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims description 10
- 229920000742 Cotton Polymers 0.000 claims description 10
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims description 10
- 239000000783 alginic acid Substances 0.000 claims description 10
- 235000010443 alginic acid Nutrition 0.000 claims description 10
- 229920000615 alginic acid Polymers 0.000 claims description 10
- 229960001126 alginic acid Drugs 0.000 claims description 10
- 150000004781 alginic acids Chemical class 0.000 claims description 10
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 10
- 239000002245 particle Substances 0.000 claims description 10
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 claims description 10
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims description 10
- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 claims description 10
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 5
- IMQLKJBTEOYOSI-GPIVLXJGSA-N Inositol-hexakisphosphate Chemical compound OP(O)(=O)O[C@H]1[C@H](OP(O)(O)=O)[C@@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@H](OP(O)(O)=O)[C@@H]1OP(O)(O)=O IMQLKJBTEOYOSI-GPIVLXJGSA-N 0.000 claims description 5
- IMQLKJBTEOYOSI-UHFFFAOYSA-N Phytic acid Natural products OP(O)(=O)OC1C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C(OP(O)(O)=O)C1OP(O)(O)=O IMQLKJBTEOYOSI-UHFFFAOYSA-N 0.000 claims description 5
- 239000002202 Polyethylene glycol Substances 0.000 claims description 5
- 239000001110 calcium chloride Substances 0.000 claims description 5
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 5
- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 5
- 229940068041 phytic acid Drugs 0.000 claims description 5
- 235000002949 phytic acid Nutrition 0.000 claims description 5
- 239000000467 phytic acid Substances 0.000 claims description 5
- 229920001223 polyethylene glycol Polymers 0.000 claims description 5
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims description 5
- 229920000053 polysorbate 80 Polymers 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 4
- 230000008014 freezing Effects 0.000 claims description 3
- 238000007710 freezing Methods 0.000 claims description 3
- 238000012856 packing Methods 0.000 claims description 2
- 238000004080 punching Methods 0.000 claims 6
- 230000032683 aging Effects 0.000 abstract description 6
- 238000005260 corrosion Methods 0.000 abstract description 5
- 230000007797 corrosion Effects 0.000 abstract description 5
- 239000004745 nonwoven fabric Substances 0.000 abstract description 5
- 238000004140 cleaning Methods 0.000 abstract description 4
- 230000000052 comparative effect Effects 0.000 description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 238000002791 soaking Methods 0.000 description 5
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- 238000005098 hot rolling Methods 0.000 description 4
- 239000007864 aqueous solution Substances 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/4282—Addition polymers
- D04H1/4291—Olefin series
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/08—Melt spinning methods
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/44—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds as major constituent with other polymers or low-molecular-weight compounds
- D01F6/46—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds as major constituent with other polymers or low-molecular-weight compounds of polyolefins
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01G—PRELIMINARY TREATMENT OF FIBRES, e.g. FOR SPINNING
- D01G1/00—Severing continuous filaments or long fibres, e.g. stapling
- D01G1/02—Severing continuous filaments or long fibres, e.g. stapling to form staple fibres not delivered in strand form
- D01G1/04—Severing continuous filaments or long fibres, e.g. stapling to form staple fibres not delivered in strand form by cutting
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/44—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling
- D04H1/46—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
- D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
- D06M11/155—Halides of elements of Groups 2 or 12 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/165—Ethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/282—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
- D06M13/292—Mono-, di- or triesters of phosphoric or phosphorous acids; Salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/18—Synthetic fibres consisting of macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/20—Polyalkenes, polymers or copolymers of compounds with alkenyl groups bonded to aromatic groups
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/66—Disintegrating fibre-containing textile articles to obtain fibres for re-use
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Mechanical Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Springs (AREA)
- Nonwoven Fabrics (AREA)
Abstract
The invention discloses a preparation method of spring wrapping cloth, belonging to the technical field of non-woven fabrics, and the preparation method comprises the steps of melt extrusion, drafting, preparation of modified polypropylene short fibers, opening and cleaning, carding, lapping, needling reinforcement and post treatment; the melt extrusion is to dry and mix the PP slices, the modifier and the nano zeolite powder, and introduce the mixture into a screw extruder for melt extrusion to obtain a melt; the preparation method provided by the invention can improve the ageing resistance of the spring wrapping cloth and can also improve the mechanical property and corrosion resistance of the spring wrapping cloth.
Description
Technical Field
The invention relates to the technical field of non-woven fabrics, in particular to a preparation method of spring wrapping cloth.
Background
The raw material of the spring wrapping cloth is generally 100% polypropylene nonwoven fabric, but the use of 100% polypropylene nonwoven fabric has the following problems: with the increase of the price of the current global bulk commodity, the cost of the raw material polypropylene is increased; the polypropylene fiber is derived from petroleum byproducts, belongs to non-renewable resources and is not beneficial to developing the sustainable development concept of the current industry; the 100% pure PP polypropylene non-woven fabric is easy to age and short in service life.
In order to solve the problems and achieve resource recycling, the most common method at present is to mix other aging-resistant fibers in the preparation of the spring wrapping cloth, but after the other fibers are mixed, although the aging resistance can be improved and the service life can be prolonged, the mechanical property and the corrosion resistance of the spring wrapping cloth can be reduced, and at present, no method capable of improving the aging resistance and the mechanical property and the corrosion resistance of the spring wrapping cloth exists.
Disclosure of Invention
Aiming at the problems, the invention provides the preparation method of the spring wrapping cloth, which can improve the ageing resistance of the spring wrapping cloth and can also improve the mechanical property and the corrosion resistance of the spring wrapping cloth.
In order to solve the technical problems, the technical scheme adopted by the invention is as follows:
a preparation method of spring wrapping cloth comprises the steps of melt extrusion, drafting, modified polypropylene short fiber preparation, opening, carding, lapping, needling reinforcement and post-treatment.
The melt extrusion is to dry and mix the PP slices, the modifier and the nano zeolite powder, and to introduce the mixture into a screw extruder for melt extrusion to obtain a melt;
the temperatures of five heating zones of the screw extruder are respectively set to be 200-210 ℃, 210-220 ℃, 220-230 ℃, 230-240 ℃ and 240-250 ℃;
the particle size of the nano zeolite powder is 300-350nm;
wherein the weight ratio of the PP slices to the modifier to the nano zeolite powder is 45-48;
the preparation method of the modifier comprises the following steps: mixing zinc stearate, sodium dodecyl benzene sulfonate, water white hydrogenated rosin, alginic acid and nano boron nitride, then placing the mixture into a ball mill for ball milling, controlling the ball-material ratio during ball milling to be 10-15, the rotating speed to be 300-350rpm, the time to be 30-40min, after the ball milling is finished, placing the mixture at the temperature of-40 ℃ to-35 ℃ for freezing treatment for 45-50min, and then recovering the mixture to room temperature to obtain a modifier;
the particle size of the nano boron nitride is 200-300nm;
wherein the weight ratio of zinc stearate, sodium dodecyl benzene sulfonate, water white hydrogenated rosin, alginic acid and nano boron nitride is (5-7).
The step of drafting, wherein the polypropylene filament is obtained after the melt is drafted;
the preparation method comprises the following steps of (1) soaking polypropylene filaments in a surface modification solution for 45-50min at 40-45 ℃, and cutting the fibers into 75-90mm by a cutting machine to obtain modified polypropylene staple fibers;
wherein the mass ratio of the polypropylene filament to the surface modification liquid is 2;
the surface modification liquid comprises the following components in parts by weight: 80-85 parts of deionized water, 6-8 parts of polyethylene glycol 400,2-4 parts of phytic acid, 1-3 parts of calcium chloride and 0.5-1 part of tween 80;
the fineness of the modified polypropylene short fiber is 2.5-3D.
And (3) opening, namely mixing the modified polypropylene short fiber with 2.5D regenerated PET short fiber with the length of 51-64mm according to the weight ratio of 45-50 to 55, then grabbing cotton, opening and mixing to obtain the opened short fiber.
The carding step, the opened short fibers are introduced into a carding machine for carding, and the fiber feeding amount of the carding machine is controlled to be 30-40g/m 2 The linear speed is 50-55%, and the carded short fiber is obtained.
And (3) lapping, namely, lapping the carded short fibers in a lapping machine to obtain a cotton net, and controlling the number of lapping layers to be 5-6.
And (3) the needling reinforcement, namely introducing the cotton net into a needling machine for needling reinforcement, controlling the working width of the needling machine to be 4-5m, the needle density to be 4000-5000 pieces/m, the needling frequency to be 600-900 times/min and the production speed to be 16-22m/min, and tentering and hot rolling the needling reinforcement to obtain the primary spring wrapping cloth.
And the post-treatment is to carry out micro-current treatment on the primary spring wrapping cloth, control the micro-current in the micro-current treatment to be 15-20uA and the time to be 50-55min, and cut according to the requirement after the micro-current treatment is finished to obtain the spring wrapping cloth.
Compared with the prior art, the invention has the beneficial effects that:
(1) The preparation method of the spring wrapping cloth can improve the mechanical property of the spring wrapping cloth, and the prepared spring wrapping cloth has the breaking strength-MD of 43.5-44.9Lbf, the breaking strength-CD of 46.8-47.8Lbf, the breaking elongation-MD of 60.6-61.8%, the breaking elongation-CD of 72.2-73.9%, the tearing strength-MD of 20.8-22.5Lbf and the tearing strength-CD of 18.4-19.5Lbf;
(2) The preparation method of the spring wrapping cloth can improve the aging resistance of the spring wrapping cloth, and after the prepared spring wrapping cloth is placed at 30-35 ℃ and irradiated under an ultraviolet lamp for 3 months, the breaking strength-MD is 43.2-44.2Lbf, the breaking strength-CD is 46.5-47.5Lbf, the breaking elongation-MD is 60.3-61.6%, the breaking elongation-CD is 71.8-73.5%, the tearing strength-MD is 20.6-22.3Lbf, and the tearing strength-CD is 18.0-19.1Lbf;
(3) The preparation method of the spring coated cloth can improve the corrosion resistance of the spring coated cloth, and after the prepared spring coated cloth is soaked in a hydrochloric acid aqueous solution with the mass fraction of 5% for 1 month, the breaking strength-MD is 43.1-44.5Lbf, the breaking strength-CD is 46.5-47.6Lbf, the breaking elongation-MD is 60.2-61.4%, the breaking elongation-CD is 72.0-73.5%, the tearing strength-MD is 20.4-22.1Lbf, and the tearing strength-CD is 18.1-19.2Lbf; after the prepared spring pack cloth is soaked in a sodium hydroxide aqueous solution with the mass fraction of 5% for 1 month, the breaking strength-MD is 43.1-44.4Lbf, the breaking strength-CD is 46.2-47.2Lbf, the breaking elongation-MD is 60.2-61.3%, the breaking elongation-CD is 71.7-73.2%, the tearing strength-MD is 20.2-22.0Lbf, and the tearing strength-CD is 18.0-18.9Lbf.
Detailed Description
In order to more clearly understand the technical features, objects, and effects of the present invention, specific embodiments of the present invention will now be described.
Example 1
A preparation method of spring wrapping cloth specifically comprises the following steps:
1. melt extrusion: drying and mixing PP slices, a modifier and nano zeolite powder, and introducing the mixture into a screw extruder for melt extrusion to obtain a melt;
the temperatures of five heating areas of the screw extruder are respectively set to be 200 ℃, 210 ℃, 220 ℃, 230 ℃ and 240 ℃;
the particle size of the nano zeolite powder is 300nm;
wherein the weight ratio of the PP slices to the modifier to the nano zeolite powder is 45;
the preparation method of the modifier comprises the following steps: mixing zinc stearate, sodium dodecyl benzene sulfonate, water white hydrogenated rosin, alginic acid and nano boron nitride, then placing the mixture into a ball mill for ball milling, controlling the ball-material ratio during ball milling to be 10;
the particle size of the nano boron nitride is 200nm;
wherein the weight ratio of zinc stearate, sodium dodecyl benzene sulfonate, water white hydrogenated rosin, alginic acid and nano boron nitride is (5).
2. Drafting: drawing the melt to obtain polypropylene filaments;
3. preparing modified polypropylene short fibers: soaking the polypropylene filaments in the surface modification solution at 40 ℃ for 45min, and cutting the fibers into 75mm by a cutting machine to obtain modified polypropylene short fibers;
wherein the mass ratio of the polypropylene short fibers to the surface modification liquid is 2;
the surface modification liquid comprises the following components in parts by weight: 80 parts of deionized water, 6 parts of polyethylene glycol 400,2 parts of phytic acid, 1 part of calcium chloride and 0.5 part of tween 80;
the fineness of the modified polypropylene short fiber is 2.5D.
4. Opening and cleaning: and (2) mixing the modified polypropylene short fiber with a 2.5D PET short fiber with the length of 51mm according to the weight ratio of 50.
5. Carding: the short fibers after opening are led into a carding machine for carding, and the fiber feeding amount of the carding machine is controlled to be 30g/m 2 The linear velocity was 50%, and carded staple fibers were obtained.
6. Lapping: and (3) introducing the carded short fibers into a lapping machine for lapping to obtain a cotton net, and controlling the number of lapping layers to be 5.
7. And (3) needling reinforcement: and (2) introducing the cotton net into a needle machine for needling reinforcement, controlling the working width of the needle machine in the process to be 4m, the needle density to be 4000 pieces/m, the needling frequency to be 600 times/min, and the production speed to be 16m/min, and tentering and hot rolling the needling reinforcement to obtain the primary spring wrapping cloth.
8. And (3) post-treatment: and (3) carrying out micro-current treatment on the primary spring wrapping cloth, controlling the micro-current to be 15uA in the micro-current treatment, and cutting according to the requirement after the micro-current treatment is finished to obtain the spring wrapping cloth.
The gram weight of the spring wrapping cloth prepared in this example was 74g/m 2 。
Example 2
A preparation method of spring wrapping cloth specifically comprises the following steps:
1. melt extrusion: drying and mixing PP slices, a modifier and nano zeolite powder, and introducing the mixture into a screw extruder for melt extrusion to obtain a melt;
the temperatures of five heating zones of the screw extruder are respectively set to be 205 ℃, 215 ℃, 225 ℃, 235 ℃ and 245 ℃;
the particle size of the nano zeolite powder is 320nm;
wherein, the weight ratio of the PP slices, the modifier and the nano zeolite powder is 47;
the preparation method of the modifier comprises the following steps: mixing zinc stearate, sodium dodecyl benzene sulfonate, water white hydrogenated rosin, alginic acid and nano boron nitride, then placing the mixture into a ball mill for ball milling, controlling the ball-material ratio during ball milling to be 12, the rotating speed to be 320rpm, the time to be 35min, after the ball milling is finished, placing the mixture at-37 ℃ for freezing treatment for 47min, and then recovering to room temperature to obtain a modifier;
the particle size of the nano boron nitride is 250nm;
wherein the weight ratio of zinc stearate, sodium dodecyl benzene sulfonate, water white hydrogenated rosin, alginic acid and nano boron nitride is 6.5.
2. Drafting: drawing the melt to obtain polypropylene filaments;
3. preparing modified polypropylene short fibers: soaking the polypropylene filaments in the surface modification solution at 42 ℃ for 47min, and cutting the fibers into 80mm by a cutting machine to obtain modified polypropylene short fibers;
wherein the mass ratio of the polypropylene filament to the surface modification liquid is 2;
the surface modification liquid comprises the following components in parts by weight: 82 parts of deionized water, 7 parts of polyethylene glycol 400,3 parts of phytic acid, 2 parts of calcium chloride and 0.7 part of tween 80;
the fineness of the modified polypropylene short fiber is 2.7D.
4. Opening and cleaning: and (3) mixing the modified polypropylene short fiber with 2.5D PET short fiber with the length of 60mm according to the weight ratio of 48.
5. Carding: introducing the opened short fibers into a carding machine for carding, and controlling the fiber feeding amount of the carding machine to be 35g/m 2 The linear velocity was 52%, and carded staple was obtained.
6. Lapping: and (3) introducing the carded short fibers into a lapping machine for lapping to obtain a cotton net, and controlling the number of lapping layers to be 5.
7. And (3) needling reinforcement: the cotton net is introduced into a needle machine for needling reinforcement, the working width in the needle machine process is controlled to be 4.5m, the needling density is 4500 pieces/m, the needling frequency is 800 times/min, the production speed is 20m/min, and the primary spring wrapping cloth is obtained after the needling reinforcement and the tentering hot rolling.
8. And (3) post-treatment: and (3) carrying out micro-current treatment on the primary spring wrapping cloth, controlling the micro-current to be 17uA in the micro-current treatment, and cutting according to the requirement after the micro-current treatment is finished to obtain the spring wrapping cloth.
Spring prepared in this exampleThe gram weight of the wrapping cloth is 75g/m 2 。
Example 3
A preparation method of spring wrapping cloth specifically comprises the following steps:
1. melt extrusion: drying and mixing PP slices, a modifier and nano zeolite powder, and introducing the mixture into a screw extruder for melt extrusion to obtain a melt;
the temperatures of five heating zones of the screw extruder are respectively set to 210 ℃, 220 ℃, 230 ℃, 240 ℃ and 250 ℃;
the particle size of the nano zeolite powder is 350nm;
wherein the weight ratio of the PP slices to the modifier to the nano zeolite powder is 48;
the preparation method of the modifier comprises the following steps: mixing zinc stearate, sodium dodecyl benzene sulfonate, water white hydrogenated rosin, alginic acid and nano boron nitride, then placing the mixture into a ball mill for ball milling, controlling the ball-material ratio during ball milling to be 15;
the particle size of the nano boron nitride is 300nm;
wherein the weight ratio of zinc stearate, sodium dodecyl benzene sulfonate, water white hydrogenated rosin, alginic acid and nano boron nitride is 7.
2. Drafting: drawing the melt to obtain polypropylene filaments;
3. preparing modified polypropylene short fibers: soaking the polypropylene filaments in the surface modification solution at 45 ℃ for 50min, and cutting the fibers into 90mm by a cutting machine to obtain modified polypropylene short fibers;
wherein the mass ratio of the polypropylene filament to the surface modification liquid is 2;
the surface modification liquid comprises the following components in parts by weight: 85 parts of deionized water, 8 parts of polyethylene glycol 400,4 parts of phytic acid, 3 parts of calcium chloride and 1 part of tween 80;
the fineness of the modified polypropylene short fiber is 3D.
4. Opening and cleaning: and (2) mixing the modified polypropylene short fiber with 2.5D PET short fiber with the length of 64mm according to a weight ratio of 45.
5. Carding: introducing the opened short fibers into a carding machine for carding, and controlling the fiber feeding amount of the carding machine to be 40g/m 2 The linear velocity was 55%, and carded staple fibers were obtained.
6. Lapping: and (3) introducing the carded short fibers into a lapping machine for lapping to obtain a cotton net, and controlling the number of lapping layers to be 6.
7. And (3) needling reinforcement: and (2) introducing the cotton net into a needle machine for needling reinforcement, controlling the working width of the needle machine in the process to be 5m, the needle density to be 5000 pieces/m, the needling frequency to be 900 times/min and the production speed to be 22m/min, and tentering and hot rolling the needling reinforcement to obtain the primary spring wrapping cloth.
8. And (3) post-treatment: and (3) carrying out micro-current treatment on the primary spring wrapping cloth, controlling the micro-current in the micro-current treatment to be 20uA and the time to be 55min, and cutting according to the requirement after the micro-current treatment is finished to obtain the spring wrapping cloth.
The gram weight of the spring coating cloth prepared in the embodiment is 74.5g/m 2 。
Comparative example 1
The same preparation method of spring packing cloth as that of the embodiment 1 is different in that: the addition of the modifier was omitted in the melt extrusion step of step 1.
The grammage of the spring wrapping cloth prepared in this example was 72g/m 2 。
Comparative example 2
The same preparation method of spring wrapping cloth as that of the embodiment 1 is different in that: and 3, in the step of preparing the modified polypropylene short fiber, the step of soaking the polypropylene filament in the surface modification solution is omitted, namely, the polypropylene filament is directly cut into 75mm by a cutting machine to obtain the modified polypropylene short fiber.
The grammage of the spring wrapping cloth prepared in this example was 75.5g/m 2 。
Comparative example 3
The same preparation method of spring wrapping cloth as that of the embodiment 1 is different in that: and (3) omitting the post-treatment step of the step 8, namely directly cutting the primary spring wrapping cloth obtained in the step 7 by needling according to the requirement to obtain the spring wrapping cloth.
The gram weight of the spring wrapping cloth prepared in this example was 73g/m 2 。
The mechanical properties of the spring wraps prepared in examples 1 to 3 and comparative examples 1 to 3 were measured, and the results were as follows:
the spring bags prepared in the examples 1 to 3 and the comparative examples 1 to 3 are placed at 30 to 35 ℃, irradiated for 3 months by an ultraviolet lamp, the power of the ultraviolet lamp is controlled to be 80W, the wavelength is 300nm, and the mechanical property is tested after the irradiation is finished, wherein the test results are as follows:
the spring bags prepared in examples 1 to 3 and comparative examples 1 to 3 were placed in a 5% hydrochloric acid aqueous solution by mass and soaked for 1 month, and the mechanical properties were tested, and the test results were as follows:
the spring packs prepared in examples 1 to 3 and comparative examples 1 to 3 were placed in a 5% by mass aqueous sodium hydroxide solution and soaked for 1 month, and mechanical properties were measured, and the results were as follows:
all percentages used in the present invention are mass percentages unless otherwise indicated.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (10)
1. A preparation method of spring wrapping cloth is characterized by comprising the steps of melt extrusion, drafting, modified polypropylene short fiber preparation, opening, carding, lapping, needling reinforcement and post-treatment;
and (3) opening, namely mixing the modified polypropylene short fiber with 2.5D regenerated PET short fiber with the length of 51-64mm according to the weight ratio of 45-50 to 55, then grabbing cotton, opening and mixing to obtain the opened short fiber.
2. The preparation method of the spring coated cloth according to claim 1, wherein the melt extrusion is carried out by drying and mixing PP slices, the modifier and the nano zeolite powder, and introducing the mixture into a screw extruder for melt extrusion to obtain a melt;
the preparation method of the modifier comprises the following steps: mixing zinc stearate, sodium dodecyl benzene sulfonate, water white hydrogenated rosin, alginic acid and nano boron nitride, then placing the mixture into a ball mill for ball milling, controlling the ball-material ratio during ball milling to be 10-15, the rotating speed to be 300-350rpm, the time to be 30-40min, after the ball milling is finished, placing the mixture at the temperature of-40 ℃ to-35 ℃ for freezing treatment for 45-50min, and then recovering the temperature to room temperature to obtain the modifier.
3. The method for preparing spring packing cloth according to claim 2, wherein the temperatures of five heating zones of the screw extruder are set to 200 to 210 ℃, 210 to 220 ℃, 220 to 230 ℃, 230 to 240 ℃, and 240 to 250 ℃ respectively;
the particle size of the nano boron nitride is 200-300nm.
4. The preparation method of the spring coated cloth according to claim 1, wherein in the melt extrusion, the weight ratio of the PP slices, the modifier and the nano zeolite powder is 45-48;
the particle size of the nano zeolite powder is 300-350nm.
5. The preparation method of the spring coated cloth according to claim 1, wherein in the preparation of the modifier, the weight ratio of zinc stearate, sodium dodecyl benzene sulfonate, water white hydrogenated rosin, alginic acid and nano boron nitride is (5-7).
6. The method for preparing spring wrapping cloth according to claim 1, wherein the modified polypropylene short fiber is prepared by immersing polypropylene filaments in a surface modification solution at 40-45 ℃ for 45-50min, and cutting the fiber into 75-90mm with a cutter;
wherein the mass ratio of the polypropylene filament to the surface modification liquid is 2.
7. The method for preparing spring wrapping cloth according to claim 6, wherein the composition of the surface modification liquid comprises, in parts by weight: 80-85 parts of deionized water, 6-8 parts of polyethylene glycol 400,2-4 parts of phytic acid, 1-3 parts of calcium chloride and 0.5-1 part of tween 80;
the fineness of the modified polypropylene short fiber is 2.5-3D.
8. The method for preparing spring clothing according to claim 1, wherein the carding step comprises carding the opened staple fibers in a carding machine, and controlling the fiber feeding amount of the carding machine to be 30-40g/m 2 The linear speed is 50-55%, and the carded short fiber is obtained.
9. The method for preparing spring wrapping cloth according to claim 1, wherein the needle punching reinforcement is carried out by introducing the web into a needle punching machine for needle punching reinforcement, the working width in the process of the needle punching machine is controlled to be 4-5m, the needle density is 4000-5000 pieces/m, the needle punching frequency is 600-900 times/min, the production speed is 16-22m/min, and the needle punching reinforcement is tentered and hot rolled to the primary spring wrapping cloth.
10. The preparation method of the spring wrapping cloth according to claim 1, characterized in that the post-treatment is carried out by carrying out micro-current treatment on the primary spring wrapping cloth, wherein the micro-current in the micro-current treatment is controlled to be 15-20uA and the time is controlled to be 50-55min, and the spring wrapping cloth is obtained by cutting according to the requirement after the micro-current treatment is finished.
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Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3956783A (en) * | 1974-10-21 | 1976-05-18 | Phillips Petroleum Company | Mattress |
| CN1473975A (en) * | 2003-07-19 | 2004-02-11 | 仪征市恒丰无纺材料有限公司 | Environment protection type needle punched non-woven fabric |
| CN105696350A (en) * | 2016-03-28 | 2016-06-22 | 西南大学 | Method for preparing functional cotton fabric by complexing phytic acid through divalent calcium ions |
| CN110184667A (en) * | 2019-07-05 | 2019-08-30 | 常州兴烯石墨烯科技有限公司 | A kind of modified white graphite allyl synthetic fibre composite fibre and preparation method thereof |
| CN112726022A (en) * | 2021-01-07 | 2021-04-30 | 肇庆天乙非织造材料有限公司 | Preparation method of polypropylene-polyethylene composite non-woven fabric |
| CN112981701A (en) * | 2021-03-31 | 2021-06-18 | 肇庆浚荣非织造材料有限公司 | Multilayer melt-blown non-woven fabric and preparation method thereof |
| CN113026205A (en) * | 2021-03-31 | 2021-06-25 | 肇庆浚荣非织造材料有限公司 | Anti-yellowing melt-blown fabric and preparation method thereof |
| CN113265769A (en) * | 2021-05-10 | 2021-08-17 | 东营俊富净化科技有限公司 | High-quality electric cotton non-woven fabric material and preparation method thereof |
-
2022
- 2022-07-05 CN CN202210782926.5A patent/CN115142190B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3956783A (en) * | 1974-10-21 | 1976-05-18 | Phillips Petroleum Company | Mattress |
| CN1473975A (en) * | 2003-07-19 | 2004-02-11 | 仪征市恒丰无纺材料有限公司 | Environment protection type needle punched non-woven fabric |
| CN105696350A (en) * | 2016-03-28 | 2016-06-22 | 西南大学 | Method for preparing functional cotton fabric by complexing phytic acid through divalent calcium ions |
| CN110184667A (en) * | 2019-07-05 | 2019-08-30 | 常州兴烯石墨烯科技有限公司 | A kind of modified white graphite allyl synthetic fibre composite fibre and preparation method thereof |
| CN112726022A (en) * | 2021-01-07 | 2021-04-30 | 肇庆天乙非织造材料有限公司 | Preparation method of polypropylene-polyethylene composite non-woven fabric |
| CN112981701A (en) * | 2021-03-31 | 2021-06-18 | 肇庆浚荣非织造材料有限公司 | Multilayer melt-blown non-woven fabric and preparation method thereof |
| CN113026205A (en) * | 2021-03-31 | 2021-06-25 | 肇庆浚荣非织造材料有限公司 | Anti-yellowing melt-blown fabric and preparation method thereof |
| CN113265769A (en) * | 2021-05-10 | 2021-08-17 | 东营俊富净化科技有限公司 | High-quality electric cotton non-woven fabric material and preparation method thereof |
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