CN115120516A

CN115120516A - Rose toner and preparation method thereof

Info

Publication number: CN115120516A
Application number: CN202210999157.4A
Authority: CN
Inventors: 谢谦; 魏小香; 肖有兵; 杨艺明
Original assignee: Xiamen Haima Cosmetics Co ltd
Current assignee: Xiamen Haima Cosmetics Co ltd
Priority date: 2022-08-19
Filing date: 2022-08-19
Publication date: 2022-09-30

Abstract

The application relates to the field of natural plant skin care products, in particular to rose toner and a preparation method thereof. The rose toner comprises the following components in percentage by mass: 0.5-1.0% of tremella polysaccharide, 0.8-2.0% of vitamin B5, 85-90% of rose water, 0-0.2% of EDTA disodium, 3-6% of humectant and 5-8% of adjuvant; the preparation method comprises the following steps: mixing flos Rosae Rugosae water, vitamin B5, Tremella polysaccharide, EDTA disodium, and humectant, and stirring to obtain phase A; stirring the auxiliary agent until the auxiliary agent is dispersed to obtain a phase B; then the phase B is stirred and mixed with the phase A, and the product is obtained after filtration. This application has the advantage that improves the moisturizing effect of toner.

Description

Rose toner and preparation method thereof

Technical Field

The application relates to the field of natural plant skin care products, in particular to rose toner and a preparation method thereof.

Background

Toner is also known as firming lotion, smoothing lotion, toner, and the like. The human face skin is an acidic environment, the skin lipid film on the surface layer can continuously and dynamically adjust the acidity of the skin, and the toner can further help to adjust the pH value of the face to maintain a stable condition. In addition, tap water for daily washing of human faces has a large amount of hypochlorite ions, which are strongly oxidizing, remaining therein due to sterilization. Although the skin has the self-repairing and restoring functions, the ions still have certain harm to the face for a long time, so that the toner is needed to assist secondary cleaning and reduce the harm of the ions to the skin.

With the improvement of environmental awareness, the trend of 'simple skin care' is to simply and easily use necessary skin care products on the face without much daunting and fussy skin care. Therefore, in hot summer, some consumers only use the toner to replenish water after cleaning the face, so as to keep the face fresh. However, the toner on the market only has a water replenishing effect, the water locking effect depends on subsequent milk and cream, and the face of the consumer is abnormally dry after the consumer only applies the toner for a while. Thus, improvements are still needed.

Disclosure of Invention

In order to improve the moisturizing effect of the toner, the application provides the rose toner and the preparation method thereof.

In a first aspect, the application provides a rose toner, which adopts the following technical scheme:

the rose toner comprises the following components in percentage by mass: 0.5-1.0% of tremella polysaccharide and 0.8-2.0% of vitamin B ₅ 85-90% of rose water, 0-0.2% of EDTA disodium, 3-6% of humectant and 5-8% of adjuvant.

The rose water is rose hydrosol and is a distillation stock solution formed by distilling and extracting rose petals through natural plants. It is composed of small molecules, has strong permeability and can directly reach the bottom layer of the muscle. The product is mild and non-irritating, and has light and pleasant fragrance when used in the field of skin care products. In the technical scheme provided by the application, the rose hydrosol is used for replacing water, the characteristics of small molecules of the rose hydrosol are well utilized, and the overall skin absorbability of the toner is improved, so that the water replenishing effect is enhanced, and the skin barrier repairing and free radical removing capacity is improved.

Spraying astringent lotion on skin surface, and performing ring beating with warm finger abdomen to obtain vitamin B ₅ Under the common cooperation of the rose water, the two small molecular substances are matched together and quickly permeate into the stratum corneum along flapping, so that the rose water replenishing mask has a good water replenishing effect. Simultaneously, the combination of the two is beneficial to further improving the vitamin B ₅ The effect of promoting the hydration of the horny layer on the skin further enhances the water replenishing effect.

Then adding Tremella polysaccharide and vitamin B ₅ The tremella polysaccharide is dissolved in the rose water and swells to form a space network structure due to the fact that the tremella polysaccharide contains a large number of hydroxyl groups and carboxyl groups. The water-soluble substances in the rose water are firmly held, so that water molecules of the rose water are locked, various substances (such as phenethyl alcohol and citronellol) in the rose water are firmly held, and the active ingredients in the toner are not easy to lose and dissipate. The toner provided by the application can be preserved for a long time even if no preservative is additionally added. And moreover, due to the formation of the space network structure, after the toner is sprayed and beaten on the face, the toner can be quickly replenished with water, and meanwhile, the formed space network structure forms a protective film on the surface of the skin to further play a role in water locking, so that the evaporation of water is slowed down, and the face can be kept and locked for a long time.

Preferably, the tremella polysaccharide and the vitamin B ₅ The mass ratio of (1): (1.2-1.5).

By adopting the technical scheme, the tremella polysaccharide and the vitamin B are further limited ₅ The use proportion of rose water is put into, and the space network structure that makes the formation is more stable, is favorable to promoting the lock water effect.

Preferably, the auxiliary agent comprises one or more of propylene glycol, p-hydroxyacetophenone, 1, 2-hexanediol, 1, 2-pentanediol and 1, 6-hexanediol.

By adopting the technical scheme, the auxiliary agent can properly select some raw materials with the moisturizing effect, and can further improve the moisturizing effect and provide a larger amount of instant moisturizing amount for the skin on the original basis.

Preferably, the auxiliary agent is formed by mixing propylene glycol, p-hydroxyacetophenone and 1, 2-hexanediol; according to the mass fraction, the dosage of the propylene glycol accounts for 4-6% of the total toner, the dosage of the p-hydroxyacetophenone accounts for 0.2-0.7% of the total toner, and the dosage of the 1, 2-hexanediol accounts for 0.2-0.7% of the total toner.

By adopting the technical scheme, under the specific use proportion of the propylene glycol, the p-hydroxyacetophenone and the 1, 2-hexanediol, the antibacterial and antiseptic toner has good antibacterial and antiseptic effects in the toner. Compared with the products in the same industry, the raw materials are mixed in proportion, so that the whole dosage is low, the antibacterial activity is good, the antibacterial agent is not influenced by temperature, pH and the like, and the antibacterial agent is stable, and the product can be stored for a longer time; and the special auxiliary agent is not easy to irritate the skin, and can play a certain moisturizing effect, thereby achieving multiple purposes.

In a second aspect, the application provides a preparation method of rose toner, which adopts the following technical scheme:

a preparation method of rose toner comprises the following steps:

mixing flos Rosae Rugosae water and vitamin B ₅ Mixing and stirring tremella polysaccharide, EDTA disodium and a humectant to obtain a phase A;

stirring the auxiliary agent until the auxiliary agent is dispersed to obtain a phase B;

then the phase B is stirred and mixed with the phase A, and the product is obtained after filtration.

By adopting the technical scheme, in the process of preparing the toner, temperature rise is not needed, the requirement on equipment is low, energy consumption and production difficulty are reduced, and the toner has good economic value and is suitable for popularization and application in the industry.

Preferably, when the auxiliary agent is propylene glycol, p-hydroxyacetophenone and 1, 2-hexanediol, the propylene glycol and the 1, 2-hexanediol are mixed, and then the p-hydroxyacetophenone is added and stirred uniformly.

By adopting the technical scheme, the propylene glycol and the 1, 2-hexanediol are dissolved and stirred in advance, and then the powdery p-hydroxyacetophenone is added into the propylene glycol and the 1, 2-hexanediol for dispersion and dissolution, so that the three have a good mixing effect, are uniformly dispersed in a system and are distributed in a toner system, and a more comprehensive antibacterial and antiseptic effect is achieved.

Preferably, the phase A is prepared by first adding vitamin B ₅ Adding into rose water, stirring, adding Tremella polysaccharide, stirring, adding disodium EDTA and humectant, and stirring.

By adopting the technical scheme, firstly, the rose water is used for dissolving vitamin B ₅ Dispersing, mixing with Tremella polysaccharide, and mixing with flos Rosae Rugosae water and vitamin B ₅ Firmly grasping, and not easy to disperse the materials, thereby having good water replenishing and locking effects.

Preferably, the rotation speed of mixing and stirring is set at 450-650r/min when preparing the phase A.

By adopting the technical scheme, the rotating speed is adjusted to be within a specific range, and the rose water and the vitamin B are mixed when the rose water and the vitamin B rotate at high speed ₅ The tremella polysaccharide is fully mixed, and a certain amount of heat is provided, so that the movement of molecules is accelerated, and the grasping effect is enhanced; thereby further improving the water replenishing and locking effects of the toner.

In summary, the present application has the following beneficial effects:

1. spraying astringent lotion on skin surface, and performing ring beating to obtain vitamin B solution ₅ Under the common cooperation of rose water, the two small molecular substances are matched together and quickly permeate into the stratum corneum along with beating, so that the rose water replenishing mask has a good water replenishing effect. Simultaneously, the combination of the two is beneficial to further improving the vitamin B ₅ The effect of promoting the hydration of the horny layer on the skin further enhances the water replenishing effect.

2. The white fungus polysaccharide and the vitamin B ₅ The combination of rose water and tremellaBecause the sugar contains a large number of hydroxyl and carboxyl, the sugar is dissolved in rose water and swells to form a spatial network structure. The water-soluble substances in the rose water are firmly held, so that water molecules of the rose water are locked, various substances (such as phenethyl alcohol and citronellol) in the rose water are firmly held, and the active ingredients in the toner are not easy to lose and dissipate. The toner provided by the application can be preserved for a long time even if no preservative is additionally added. And moreover, due to the formation of the space network structure, after the toner is sprayed and beaten on the face, the toner can be quickly replenished with water, and meanwhile, the formed space network structure forms a protective film on the surface of the skin to further play a role in water locking, so that the evaporation of water is slowed down, and the face can be kept and locked for a long time.

3. Under the specific use proportion of the propylene glycol, the p-hydroxyacetophenone and the 1, 2-hexanediol, the antibacterial and antiseptic toner has good antibacterial and antiseptic effects in the toner. Compared with the products in the same industry, the raw materials are mixed in proportion, so that the whole dosage is low, the antibacterial activity is good, the antibacterial agent is not influenced by temperature, pH and the like, and the antibacterial agent is stable, and the product can be stored for a longer time; and the special matched auxiliary agent is not easy to irritate the skin, and can play a certain moisturizing effect, thereby achieving multiple purposes.

Detailed Description

The present application will be described in further detail with reference to examples.

The raw materials used in the following examples and comparative examples are all commercially available products.

Examples

Example 1

The rose toner comprises the following components: tremella polysaccharide and vitamin B ₅ Rose (rosaugosa) flower water, disodium EDTA, a humectant and an auxiliary agent.

The humectant is glycerol; the auxiliary agent is formed by mixing propylene glycol, p-hydroxyacetophenone and 1, 2-hexanediol.

The specific amounts of each raw material are detailed in table 1.

The application also provides a preparation method of the rose toner, which comprises the following steps:

adding rose water into the reaction kettle, adjusting the rotating speed of the reaction kettle to 550r/min, and adding vitamin B ₅ Adding into rose water, and stirring. Keeping the rotating speed, adding the tremella polysaccharide into the reaction kettle, and stirring uniformly. And then adding the EDTA disodium and the humectant into the reaction kettle, and stirring the mixture uniformly to obtain a phase A.

Adding propylene glycol and 1, 2-hexanediol into the reaction kettle, adjusting the rotating speed to 550r/min, stirring until the mixture is uniform, then adding p-hydroxyacetophenone into the reaction kettle, adjusting the rotating speed to 600r/min, and stirring until the mixture is uniformly dispersed to obtain a phase B.

And putting the phase A and the phase B into a reaction kettle, and stirring and mixing the phase A and the phase B to be uniform under the condition of the rotating speed of 600 r/min. Stopping stirring, standing to room temperature, filtering with 1200 mesh filter cloth, and taking out of the pot to obtain the product.

Example 2

A rose toner is different from the rose toner in example 1 in that hyaluronic acid is selected as the humectant. The used amount of each raw material is different, and the details are shown in table 1.

The preparation method of the rose toner is different from the preparation method of the example 1 in that the rotating speed of a reaction kettle is 450 r/min.

Example 3

The rose toner is different from the rose toner in example 1 in that betaine is selected as the humectant. The used amount of each raw material is different, and the details are shown in table 1.

The preparation method of the rose toner is different from the preparation method of the example 1 in that the rotating speed of a reaction kettle is 650 r/min.

Example 4

The rose toner is different from the rose toner in example 1 in that tremella polysaccharide and vitamin B ₅ The mass ratio of the rose water is 1: 1.2, namely the usage amount of the tremella polysaccharide is 0.8kg, and the vitamin B ₅ The amount of (3) used was 0.96kg, and the amount of rose water used was 87.14 kg.

Example 5

A rose toner is different from the rose toner in example 1 in that tremella polysaccharide and vitamin B ₅ Mass ratio of rose waterIs 1: 2.5, namely the usage amount of the tremella polysaccharide is 0.8kg, and the vitamin B ₅ The amount of rose water used was 2kg, and the amount of rose water used was 86.1 kg.

The specific amounts of the respective starting materials in examples 3 to 5 are summarized in Table 1.

TABLE 1

Example 6

A rose toner is different from that of example 1 in that the adjuvant is 1, 6-hexanediol.

Example 7

The rose toner is different from the rose toner in example 1 in that the auxiliary agents are propylene glycol, p-hydroxyacetophenone and 1, 2-hexanediol. The using amount of the propylene glycol is 0.5kg, the using amount of the p-hydroxyacetophenone is 4kg, and the using amount of the 1, 2-hexanediol is 1.5 kg.

Example 8

A preparation method of rose toner is different from that of the example 1 in that,

regulating rotation speed to 550r/min, mixing flos Rosae Rugosae water and vitamin B ₅ The tremella polysaccharide, the EDTA disodium and the humectant are directly added into a reaction kettle, and the mixture is mixed and stirred uniformly to obtain phase A.

Regulating the rotating speed to 550r/min, directly putting propylene glycol, 1, 2-hexanediol and p-hydroxyacetophenone into a reaction kettle, and stirring until the mixture is dispersed to obtain a phase B.

The rest of the processing is the same.

Example 9

The preparation method of the rose toner is different from the preparation method of the example 1 in that the rotating speed of a reaction kettle is 75 r/min.

Comparative example

Comparative example 1

A rose toner is different from the rose toner in example 1 in that tremella polysaccharide is replaced by aloe juice with equal mass.

Comparative example 2

A rose toner is different from the one in example 1,mixing vitamin B ₅ Replacing with equal mass of vitamin E.

Comparative example 3

The rose toner is different from the rose toner in example 1 in that the rose water is replaced by deionized water with equal mass.

Comparative example 4

The rose toner is different from the rose toner in example 1 in that the rose toner is replaced by equal-quality peppermint hydrolat.

Comparative example 5

A rose toner is different from the rose toner in example 1 in that the usage amount of tremella polysaccharide is 4kg, and vitamin B is added ₅ The usage amount of (1) is 0.2kg, and the usage amount of the rose water is 84.7 kg.

Performance test

1. Moisture retention property: 30 volunteers with healthy human skin were selected to participate in the test, and two volunteers were assigned to use the corresponding products of examples 1-9 and comparative examples 1-5, respectively, and the blank sample. Before detection, the face was cleaned with commercial facial cleanser and rested for 15 min. Then the product was evenly sprayed on the face of the volunteer and then the finger bellies were used to draw circles evenly on the face for 1 min.

After face cleaning, spraying for 5min and spraying for 4h, the water content of the skin at the forehead of the volunteer is detected by a water content detector.

The blank sample was deionized water.

2. Preservation Property: the products of examples 1 to 9, comparative examples 1 to 5 and the blank control were filled in 100ml clear glass bottles, the caps were opened, and the bottles were placed at 40 ℃ and 75 to 80% relative humidity, and the onset of rancidity was observed on the next day.

Rancidity index: the product is rancid and emits unpleasant odor.

Normal indexes are as follows: the product is not abnormal, clear and transparent, and has pure fragrance.

The results of the above tests 1-2 are detailed in Table 2.

TABLE 2

According to the comparison of the detection data of the example 1 and the comparative examples 1-4 in the table 2, the toner of the example 1 can rapidly replenish water to the face of a volunteer after being sprayed for 5 min; after 4h of spraying, higher skin moisture content can be maintained, which shows that the toner of example 1 has good water locking effect. The toner of comparative examples 1 to 4 supplemented a small amount of water in a short time on the face of the volunteer, which is far less than the effect of example 1; the fact that the level of water content of the volunteer's face fell back to the face after 4 hours of spraying indicated that the toner of comparative examples 1-4 had poor water-holding capacity. The contents are stated in the white fungus polysaccharide and vitamin B ₅ The effect of the toner on the facial skin is greatly improved by the cooperation of the rose water, and the toner has good water replenishing and locking effects, and the three raw materials are lack of one. Comparing the detection data of the example 1 and the comparative examples 1-2 and 4, it can be seen that the combination of the three is beneficial to the dispersion of the raw materials in the system, and the storage life is prolonged to a certain extent. In comparative example 3, which contains less active ingredient and is mostly water, rancidity is less sensitive than the remaining comparative examples.

According to the comparison of the detection data of the example 1 and the comparative example 5, the tremella polysaccharide and the vitamin B ₅ The rose water needs to be matched in a specific proportion, and good water replenishing and locking effects can be achieved.

According to the comparison of the detection data of the embodiments 1 and 4 and the detection data of the embodiment 5, after the toner of the embodiments 1 and 4 acts on the face of a volunteer, the water content of the face is effectively improved in a short time, and the toner can well play a water locking effect on the face for a long time. When Tremella polysaccharide and vitamin B are changed ₅ The blending ratio (example 5) of (a) has good water replenishing and locking effects, but is not as remarkable as those of examples 1 and 4.

As can be seen from comparison of the test data of example 1 with those of examples 6 and 7, the skin moisture content of the toner of example 1 after 5min of spraying and 4h of spraying was higher than those of examples 6 and 7, and the rancidity time of the toner of example 1 was also later than those of examples 6 and 7. The specific selection and proportion of the auxiliary agent (example 1) is shown to act in the toner, which is beneficial to prolonging the storage time of the toner. Besides, the water replenishing and locking aspects are improved to a certain extent.

As can be seen from comparison of the test data of example 1 with those of examples 8 and 9, the toner of example 1 has better performance in terms of water replenishing, water locking and storage than those of examples 8 and 9. The better dispersion effect is achieved among various raw materials under the specific stirring sequence and the stirring rotating speed, so that the better matching effect is achieved, and the moisture retention and preservation performance of the toner is improved.

The present embodiment is only for explaining the present application, and it is not limited to the present application, and those skilled in the art can make modifications of the present embodiment without inventive contribution as needed after reading the present specification, but all of them are protected by patent law within the scope of the claims of the present application.

Claims

1. The rose toner is characterized by comprising the following components in percentage by mass: 0.5-1.0% of tremella polysaccharide, 0.8-2.0% of vitamin B5, 85-90% of rose water, 0-0.2% of EDTA disodium, 3-6% of humectant and 5-8% of adjuvant.

2. The rose toner of claim 1, wherein: the mass ratio of the tremella polysaccharide to the vitamin B5 is 1: (1.2-1.5).

3. The rose toner of claim 1, wherein: the auxiliary agent comprises one or more of propylene glycol, p-hydroxyacetophenone, 1, 2-hexanediol, 1, 2-pentanediol and 1, 6-hexanediol.

4. The rose toner of claim 1, wherein: the auxiliary agent is formed by mixing propylene glycol, p-hydroxyacetophenone and 1, 2-hexanediol; according to the mass fraction, the dosage of the propylene glycol accounts for 4-6% of the total toner, the dosage of the p-hydroxyacetophenone accounts for 0.2-0.7% of the total toner, and the dosage of the 1, 2-hexanediol accounts for 0.2-0.7% of the total toner.

5. A preparation method of the rose toner according to any one of claims 1 to 4, which is characterized by comprising the following steps:

mixing flos Rosae Rugosae water, vitamin B5, Tremella polysaccharide, EDTA disodium, and humectant, and stirring to obtain phase A;

6. The method for preparing the rose toner according to claim 5, wherein the method comprises the following steps: when the auxiliary agent is propylene glycol, p-hydroxyacetophenone and 1, 2-hexanediol, the propylene glycol and the 1, 2-hexanediol are mixed, and then the p-hydroxyacetophenone is added and stirred uniformly.

7. The method for preparing the rose toner according to claim 5, wherein the method comprises the following steps: when the phase A is prepared, firstly, the vitamin B5 is put into rose water and stirred uniformly, then the tremella polysaccharide is added and stirred uniformly, and the EDTA disodium and the humectant are added and stirred uniformly.

8. The method for preparing the rose toner according to claim 5, wherein the method comprises the following steps: when the phase A is prepared, the rotation speed of mixing and stirring is set at 450-650 r/min.