CN115093130A - 一种多功能镜面复合处理方法 - Google Patents
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- 238000003672 processing method Methods 0.000 title claims abstract description 13
- 239000002131 composite material Substances 0.000 title claims abstract description 9
- 239000011521 glass Substances 0.000 claims abstract description 79
- 238000005406 washing Methods 0.000 claims abstract description 35
- 239000000758 substrate Substances 0.000 claims abstract description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000007888 film coating Substances 0.000 claims abstract description 24
- 238000009501 film coating Methods 0.000 claims abstract description 24
- 239000002253 acid Substances 0.000 claims abstract description 15
- 238000004544 sputter deposition Methods 0.000 claims abstract description 13
- 238000005498 polishing Methods 0.000 claims abstract description 12
- 238000005530 etching Methods 0.000 claims abstract description 11
- 238000001035 drying Methods 0.000 claims abstract description 6
- 238000007688 edging Methods 0.000 claims abstract description 6
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- 238000009713 electroplating Methods 0.000 claims description 25
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 20
- 238000005554 pickling Methods 0.000 claims description 11
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 10
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 10
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 10
- 229910052786 argon Inorganic materials 0.000 claims description 10
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 10
- 239000007789 gas Substances 0.000 claims description 10
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- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 5
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 5
- 230000002378 acidificating effect Effects 0.000 claims description 5
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 5
- 239000011248 coating agent Substances 0.000 claims description 5
- 238000000576 coating method Methods 0.000 claims description 5
- 229910003460 diamond Inorganic materials 0.000 claims description 5
- 239000010432 diamond Substances 0.000 claims description 5
- 229910017604 nitric acid Inorganic materials 0.000 claims description 5
- 229910052710 silicon Inorganic materials 0.000 claims description 5
- 239000010703 silicon Substances 0.000 claims description 5
- 229910001220 stainless steel Inorganic materials 0.000 claims description 5
- 239000010935 stainless steel Substances 0.000 claims description 5
- 238000005496 tempering Methods 0.000 claims description 5
- 229910052719 titanium Inorganic materials 0.000 claims description 5
- 239000010936 titanium Substances 0.000 claims description 5
- 150000001875 compounds Chemical class 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 4
- 238000000034 method Methods 0.000 description 5
- 230000002035 prolonged effect Effects 0.000 description 3
- 230000004313 glare Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000005357 flat glass Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
- C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
- C03C17/40—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal all coatings being metal coatings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B11/00—Cleaning flexible or delicate articles by methods or apparatus specially adapted thereto
- B08B11/04—Cleaning flexible or delicate articles by methods or apparatus specially adapted thereto specially adapted for plate glass, e.g. prior to manufacture of windshields
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C15/00—Surface treatment of glass, not in the form of fibres or filaments, by etching
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
- C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
- C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
- C03C17/3615—Coatings of the type glass/metal/other inorganic layers, at least one layer being non-metallic
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
- C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
- C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
- C03C17/3642—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer the multilayer coating containing a metal layer
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
- C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
- C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
- C03C17/3649—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer made of metals other than silver
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
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- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
- C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
- C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
- C03C17/3657—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer the multilayer coating having optical properties
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- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
- C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
- C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
- C03C17/3657—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer the multilayer coating having optical properties
- C03C17/3663—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer the multilayer coating having optical properties specially adapted for use as mirrors
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- C03C23/00—Other surface treatment of glass not in the form of fibres or filaments
- C03C23/0075—Cleaning of glass
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/10—Deposition methods
- C03C2218/15—Deposition methods from the vapour phase
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Abstract
本发明公开了一种多功能镜面复合处理方法,包括体如下步骤:S1:对玻璃依次进行切割、磨边处理,然后将处理后的玻璃单面贴膜S2:通过蒙砂粉溶液针对玻璃基材未贴膜一面进行蚀刻,然后将蚀刻完成的玻璃基材放置到抛光机上进行表面抛光处理;S3:将S2得到的玻璃基材依次进行酸洗和进行水洗并干燥;S4:将步骤S3得到的玻璃基底送入镀膜箱体,进行双层镀膜。首选通过蚀刻使玻璃表面形成凹凸不平表面,造成光线漫反射,从而达到防眩光的目的。通利用溅射的方式对处理后的玻璃表明进行双层镀膜,使得玻璃表面具有更加顺滑的触感,同时起到对玻璃表面防护的作用,以及减低玻璃的防眩光效果。
Description
技术领域
本发明涉及涉及镜面复合技术领域,更具体地说,涉及一种多功能镜面复合处理方法。
背景技术
玻璃本体,尤其是普通平板玻璃本体具有的性能有限,应用受到限制。因此,常需要对玻璃进行深加工处理,以改善和提高其性能。而在各种玻璃深加工技术中,玻璃表面镀膜是一种常用的方法,通过镀不同的膜,可以改善玻璃的光学、热学、电学、化学和力学等性能。玻璃镜面用处很多,为了使镜面反射更加清楚或者透光效果更好,常要求镜面光滑,但是光滑的镜面使其在光线下存在炫光反射。因此在保证镜面与膜复合后具有较高性能的同时,又要降低其炫光反射是亟待解决的技术问题。
发明内容
本发明的目的在于提供一种多功能镜面复合处理方法,用以解决上述背景技术中存在的技术问题。
本发明技术方案提供一种多功能镜面复合处理方法,包括体如下步骤:
S1:对玻璃依次进行切割、磨边处理,然后将处理后的玻璃单面贴膜,贴膜面下静置10-15min,得到玻璃基材;
S2:通过蒙砂粉溶液针对玻璃基材未贴膜一面进行蚀刻,使玻璃基材表面形成粗糙的蒙砂面,然后将蚀刻完成的玻璃基材放置到抛光机上进行表面抛光处理;
S3:将S2得到的玻璃基材放入酸洗池中酸洗3-5min,然后用清水冲去玻璃表面残留的酸性物质,通过金刚毛刷清洗设备进行水洗并干燥;
S4:将步骤S3得到的玻璃基底送入镀膜箱体,进行双层镀膜,开启一号电流和一号电压,向所述镀膜箱体中注入氩气和氧气工作气体,溅射不锈钢靶材,形成第一膜层;开启二号电流和二号电压,向所述镀膜箱体中注入氩气和氧气工作气体,溅射钛靶材形成第二膜层。
在一个优选地实施例中,所使用的酸洗有7-8个蚀刻位,且平均速度在6-8m/min,而在温度较低时,需要加长时间;
在一个优选地实施例中,酸洗用到的酸为硫酸、盐酸、磷酸和硝酸中的一种或多种。
在一个优选地实施例中,S3中水洗过程为:将所述钢化处理的玻璃依次进行第一次毛刷刷洗、一级纯水冲洗、第二次毛刷刷洗、二级纯水冲洗和三级离子水冲洗。
在一个优选地实施例中,S4中镀膜箱体中安装4-6个硅靶,第一膜层电镀条件为:真空环境下,一号电压为350-360V,一号电流为60-70A,电镀温度35-45℃,电镀时间5-10min;第二膜层电镀条件为:真空环境下,二号电压为370-380V,二号电流为70-80A,电镀温度40-45℃,电镀时间8-15min。
本发明技术方案的有益效果是:
通过单边贴膜对玻璃进行防护,以防处理过程中对无需处理的一面造成损坏。首选通过蚀刻使玻璃表面形成凹凸不平表面,造成光线漫反射,从而达到防眩光的目的。通利用溅射的方式对处理后的玻璃表明进行双层镀膜,使得玻璃表面具有更加顺滑的触感,同时起到对玻璃表面防护的作用,以及减低玻璃的防眩光效果。
具体实施方式
下面结合具体实施方式对本发明作进一步详细的说明。本发明的实施例是为了示例和描述方便起见而给出的,而并不是无遗漏的或者将本发明限于所公开的形式。很多修改和变化对于本领域的普通技术人员而言是显而易见的。选择和描述实施例是为了更好说明本发明的原理和实际应用,并且使本领域的普通技术人员能够理解本发明从而设计适于特定用途的带有各种修改的各种实施例。
实施例1
本发明技术方案提供一种多功能镜面复合处理方法,包括体如下步骤:S1:对玻璃依次进行切割、磨边处理,然后将处理后的玻璃单面贴膜,贴膜面下静置10min,得到玻璃基材;S2:通过蒙砂粉溶液针对玻璃基材未贴膜一面进行蚀刻,使玻璃基材表面形成粗糙的蒙砂面,然后将蚀刻完成的玻璃基材放置到抛光机上进行表面抛光处理;S3:将S2得到的玻璃基材放入酸洗池中酸洗3min,然后用清水冲去玻璃表面残留的酸性物质,通过金刚毛刷清洗设备进行水洗并干燥;S4:将步骤S3得到的玻璃基底送入镀膜箱体,进行双层镀膜,开启一号电流和一号电压,向所述镀膜箱体中注入氩气和氧气工作气体,溅射不锈钢靶材,形成第一膜层;开启二号电流和二号电压,向所述镀膜箱体中注入氩气和氧气工作气体,溅射钛靶材形成第二膜层。
所使用的酸洗有7个蚀刻位,且平均速度在6m/min,而在温度较低时,需要加长时间;酸洗用到的酸为硫酸、盐酸、磷酸和硝酸中的一种或多种。
S3中水洗过程为:将所述钢化处理的玻璃依次进行第一次毛刷刷洗、一级纯水冲洗、第二次毛刷刷洗、二级纯水冲洗和三级离子水冲洗。
S4中镀膜箱体中安装4个硅靶,第一膜层电镀条件为:真空环境下,一号电压为350V,一号电流为60A,电镀温度35℃,电镀时间5min;第二膜层电镀条件为:真空环境下,二号电压为370V,二号电流为70A,电镀温度40℃,电镀时间8min。
实施例2
本发明技术方案提供一种多功能镜面复合处理方法,包括体如下步骤:
S1:对玻璃依次进行切割、磨边处理,然后将处理后的玻璃单面贴膜,贴膜面下静置15min,得到玻璃基材;S2:通过蒙砂粉溶液针对玻璃基材未贴膜一面进行蚀刻,使玻璃基材表面形成粗糙的蒙砂面,然后将蚀刻完成的玻璃基材放置到抛光机上进行表面抛光处理;S3:将S2得到的玻璃基材放入酸洗池中酸洗5min,然后用清水冲去玻璃表面残留的酸性物质,通过金刚毛刷清洗设备进行水洗并干燥;S4:将步骤S3得到的玻璃基底送入镀膜箱体,进行双层镀膜,开启一号电流和一号电压,向所述镀膜箱体中注入氩气和氧气工作气体,溅射不锈钢靶材,形成第一膜层;开启二号电流和二号电压,向所述镀膜箱体中注入氩气和氧气工作气体,溅射钛靶材形成第二膜层。
所使用的酸洗有8个蚀刻位,且平均速度在8m/min,而在温度较低时,需要加长时间;酸洗用到的酸为硫酸、盐酸、磷酸和硝酸中的一种或多种。
S3中水洗过程为:将所述钢化处理的玻璃依次进行第一次毛刷刷洗、一级纯水冲洗、第二次毛刷刷洗、二级纯水冲洗和三级离子水冲洗。
S4中镀膜箱体中安装6个硅靶,第一膜层电镀条件为:真空环境下,一号电压为360V,一号电流为70A,电镀温度45℃,电镀时间10min;第二膜层电镀条件为:真空环境下,二号电压为380V,二号电流为80A,电镀温度45℃,电镀时间15min。
实施例3
本发明技术方案提供一种多功能镜面复合处理方法,包括体如下步骤:
S1:对玻璃依次进行切割、磨边处理,然后将处理后的玻璃单面贴膜,贴膜面下静置12min,得到玻璃基材;
S2:通过蒙砂粉溶液针对玻璃基材未贴膜一面进行蚀刻,使玻璃基材表面形成粗糙的蒙砂面,然后将蚀刻完成的玻璃基材放置到抛光机上进行表面抛光处理;
S3:将S2得到的玻璃基材放入酸洗池中酸洗4min,然后用清水冲去玻璃表面残留的酸性物质,通过金刚毛刷清洗设备进行水洗并干燥;
S4:将步骤S3得到的玻璃基底送入镀膜箱体,进行双层镀膜,开启一号电流和一号电压,向所述镀膜箱体中注入氩气和氧气工作气体,溅射不锈钢靶材,形成第一膜层;开启二号电流和二号电压,向所述镀膜箱体中注入氩气和氧气工作气体,溅射钛靶材形成第二膜层。
所使用的酸洗有8个蚀刻位,且平均速度在7m/min,而在温度较低时,需要加长时间;酸洗用到的酸为硫酸、盐酸、磷酸和硝酸中的一种或多种。
S3中水洗过程为:将所述钢化处理的玻璃依次进行第一次毛刷刷洗、一级纯水冲洗、第二次毛刷刷洗、二级纯水冲洗和三级离子水冲洗。
S4中镀膜箱体中安装6个硅靶,第一膜层电镀条件为:真空环境下,一号电压为355V,一号电流为65A,电镀温度38℃,电镀时间8min;第二膜层电镀条件为:真空环境下,二号电压为375V,二号电流为75A,电镀温度42℃,电镀时间10min。
通过单边贴膜对玻璃进行防护,以防处理过程中对无需处理的一面造成损坏。首选通过蚀刻使玻璃表面形成凹凸不平表面,造成光线漫反射,从而达到防眩光的目的。通利用溅射的方式对处理后的玻璃表明进行双层镀膜,使得玻璃表面具有更加顺滑的触感,同时起到对玻璃表面防护的作用,以及减低玻璃的防眩光效果。
显然,所描述的实施例仅仅是本发明的一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域及相关领域的普通技术人员在没有作出创造性劳动的前提下所获得的所有其他实施例,都应属于本发明保护的范围。本发明中未具体描述和解释说明的结构、装置以及操作方法,如无特别说明和限定,均按照本领域的常规手段进行实施。
Claims (5)
1.一种多功能镜面复合处理方法,其特征在于,包括体如下步骤:
S1:对玻璃依次进行切割、磨边处理,然后将处理后的玻璃单面贴膜,贴膜面下静置10-15min,得到玻璃基材;
S2:通过蒙砂粉溶液针对玻璃基材未贴膜一面进行蚀刻,使玻璃基材表面形成粗糙的蒙砂面,然后将蚀刻完成的玻璃基材放置到抛光机上进行表面抛光处理;
S3:将S2得到的玻璃基材放入酸洗池中酸洗3-5min,然后用清水冲去玻璃表面残留的酸性物质,通过金刚毛刷清洗设备进行水洗并干燥;
S4:将步骤S3得到的玻璃基底送入镀膜箱体,进行双层镀膜,开启一号电流和一号电压,向所述镀膜箱体中注入氩气和氧气工作气体,溅射不锈钢靶材,形成第一膜层;开启二号电流和二号电压,向所述镀膜箱体中注入氩气和氧气工作气体,溅射钛靶材形成第二膜层。
2.根据权利要求1所述的一种多功能镜面复合处理方法,其特征在于,所使用的酸洗有7-8个蚀刻位,且平均速度在6-8m/min,而在温度较低时,需要加长时间。
3.根据权利要求1所述的一种多功能镜面复合处理方法,其特征在于,酸洗用到的酸为硫酸、盐酸、磷酸和硝酸中的一种或多种。
4.根据权利要求1所述的一种多功能镜面复合处理方法,其特征在于,S3中水洗过程为:将所述钢化处理的玻璃依次进行第一次毛刷刷洗、一级纯水冲洗、第二次毛刷刷洗、二级纯水冲洗和三级离子水冲洗。
5.根据权利要求1所述的一种多功能镜面复合处理方法,其特征在于,S4中镀膜箱体中安装4-6个硅靶,第一膜层电镀条件为:真空环境下,一号电压为350-360V,一号电流为60-70A,电镀温度35-45℃,电镀时间5-10min;第二膜层电镀条件为:真空环境下,二号电压为370-380V,二号电流为70-80A,电镀温度40-45℃,电镀时间8-15min。
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CN114538787A (zh) * | 2022-01-11 | 2022-05-27 | 无锡市科虹标牌有限公司 | 玻璃正面蚀刻电镀方法 |
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