CN115006293A - Formula and preparation method of traditional Chinese medicine leg and foot membrane externally applied to safflower oleosomes - Google Patents
Formula and preparation method of traditional Chinese medicine leg and foot membrane externally applied to safflower oleosomes Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
- A61K36/286—Carthamus (distaff thistle)
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/906—Zingiberaceae (Ginger family)
- A61K36/9068—Zingiber, e.g. garden ginger
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/14—Liposomes; Vesicles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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Abstract
The invention discloses a formula and a preparation method of an externally-applied safflower oleosome traditional Chinese medicine leg-foot membrane, and relates to the technical field of foot membrane production. The feed is prepared from the following raw materials in parts by weight: the component A comprises 86 +/-1 wt% of the component B, 16 +/-1 wt% of the component B, 0.5 +/-0.1 wt% of the component C, 1.5 +/-0.1 wt% of the component D and 2.4 +/-0.1 wt% of the component E; the component D comprises plant sterilization and mite removal stock solution accounting for 0.05 +/-0.01 wt% of the total raw materials, ginger essential oil accounting for 0.3 +/-0.1 wt%, essence accounting for 0.5 +/-0.1 wt%, ligusticum wallichii oil accounting for 0.2 +/-0.1 wt% and safflower oleosome accounting for 0.25 +/-0.1 wt%. Compared with most of the existing foot membranes, the foot membrane of the invention is added with the plant sterilization mite-killing stock solution, the ginger essential oil, the essence, the ligusticum oil and the safflower oleosome, and has good skin moistening effect, can moisten the skin of a user, can improve the skin quality and maintain the skin effect, thereby utilizing the natural extracts as main skin moistening materials and reducing the probability of anaphylactic reaction.
Description
Technical Field
The invention relates to the technical field of foot membrane production, in particular to a formula and a preparation method of an externally-applied safflower oleosome traditional Chinese medicine leg and foot membrane.
Background
Along with the improvement of the living standard of people, maintenance products and cosmetics are more and more popular with people, the acceptance of the facial mask, the eye mask and the foot mask for maintaining the cotton face, the eyes and the feet is also obviously improved, and the degree of importance of people on the foot mask is slightly lower compared with the facial mask and the eye mask.
The main cost of foot mask products on the market at present is synthetic, although the foot mask products have the capability of moistening and moisturizing skin, the skin types of different people are different, the probability of anaphylactic reaction caused by the synthetic is higher, the probability of anaphylactic reaction caused by natural extracts is lower, and related foot mask formulas and production processes are lacked at the present stage.
Disclosure of Invention
The invention aims to provide a formula of an externally-applied safflower oleosome traditional Chinese medicine leg-foot membrane and a preparation method thereof, and aims to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme: a formula of a traditional Chinese medicine leg and foot membrane for external application of safflower oleosomes is prepared from the following raw materials in parts by weight: the component A comprises 86 +/-1 wt% of the component B, 16 +/-1 wt% of the component B, 0.5 +/-0.1 wt% of the component C, 1.5 +/-0.1 wt% of the component D and 2.4 +/-0.1 wt% of the component E;
the component A comprises deionized water accounting for 69 +/-1 weight percent of the total raw materials and carbomer U10 accounting for 4 +/-1 weight percent;
the component B comprises emulsifier GP200 accounting for 1 plus or minus 0.1wt percent of the total raw materials and emulsifier 165 accounting for 3 plus or minus 0.1wt percent of the total raw materials;
the component C comprises preservative 9010 accounting for 0.6 +/-0.1 wt% of the total raw materials;
the component D comprises plant sterilization and mite removal stock solution accounting for 0.05 +/-0.01 wt% of the total raw materials, ginger essential oil accounting for 0.3 +/-0.1 wt%, essence accounting for 0.5 +/-0.1 wt%, ligusticum wallichii oil accounting for 0.2 +/-0.1 wt% and safflower oleosome accounting for 0.25 +/-0.1 wt%;
the component E comprises arginine accounting for 0.4 plus or minus 0.1 wt% of the total raw materials.
Further, the component A also comprises glycerol accounting for 6 +/-0.1 wt% of the total raw materials, allantoin accounting for 0.3 +/-0.1 wt%, butanediol accounting for 6.5 +/-0.1 wt% of the total raw materials and EDTA-2Na accounting for 0.15 +/-0.1 wt%.
Further, the component B also comprises 8 plus or minus 0.1 wt% of DUB85, 2 plus or minus 0.1 wt% of mixed alcohol and 2 plus or minus 0.1 wt% of DC200/100 based on the total raw material.
Still further, the component E further comprises deionized water in an amount of 2. + -. 0.1 wt% based on the total amount of the raw materials.
A preparation method of an externally-applied safflower oleosome traditional Chinese medicine leg-foot membrane uses a formula of the externally-applied safflower oleosome traditional Chinese medicine leg-foot membrane, and the preparation method comprises the following steps:
the method comprises the following steps: adding the component A into a water phase pot for dissolving, and adding into an emulsifying pot after dissolving;
step two: adding the component B into an oil phase pot for dissolving, and adding into the emulsifying pot obtained in the first step after the dissolving is finished;
step three: homogenizing at high speed for a period of time;
step four: cooling the emulsifying pot for the first stage, and then adding the component C and homogenizing;
step five: cooling the interval of the emulsifying pot in the second stage, and then adding the component D;
step six: premixing the component E, adding the cooked rice containing the component E into an emulsifying pot, and adjusting the pH value;
step seven: and cooling the emulsifying pot in the third stage, and discharging after the quality inspection is qualified.
Further, the water phase pot in the first step and the oil phase pot in the second step need to be stirred and heated to 75-80 ℃ when being dissolved.
Furthermore, the vacuum degree of the materials in the first step and the second step when the materials are added into the emulsifying pot from the water phase pot and the oil phase pot is controlled between 0.03MPa and 0.04 MPa.
Furthermore, the heat preservation temperature of the emulsifying pot in the third step is 75-80 ℃, and the high-speed homogenizing mode is stirring at 50rpm for 5 minutes.
Furthermore, the first stage cooling reduces the temperature of the emulsifying pot to 60-65 ℃, the second stage cooling reduces the temperature of the emulsifying pot to 35-42 ℃, and the third stage cooling reduces the temperature of the emulsifying pot to 30 ℃.
Further, in the sixth step, the pH value inside the emulsifying pot is adjusted to 5.2-6.0.
Compared with the prior art, the invention has the beneficial effects that:
according to the formula and the preparation method of the externally-applied traditional Chinese medicine leg-foot membrane containing the safflower oleosomes, the plant sterilization and mite removal stock solution, the ginger essential oil, the essence, the ligusticum wallichii oil and the safflower oleosomes are added into the formula of the foot membrane, and compared with most of existing foot membranes, the foot membrane is all natural extracts, has a good skin moistening effect, can moisten the skin of a user, and can improve the skin quality and maintain the skin, so that the natural extracts are used as main skin moistening materials, and the probability of occurrence of anaphylactic reaction can be reduced.
Meanwhile, according to the formula targeted design production process, the raw materials with the water phase property and the raw materials with the oil phase property are mixed and emulsified, the lubricating raw materials and the auxiliary materials are mixed according to enough components, and the safflower oleosome and other extracts are added under the condition that the effect of the natural extract of the component D is not broken, so that the activity of the natural components in the package can be effectively packaged, and the using effect of the package is ensured.
In addition, the ligusticum wallichii, the ginger essential oil and the safflower are all used for promoting local circulation, so that the skin feel can be heated, the metabolism is promoted, the moisture is moistened and preserved, the repair and the relief are realized, and the effect on dermatophytosis is also realized.
Drawings
FIG. 1 is a schematic diagram of the process flow structure of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
For ease of understanding, the following references to english-name materials are first explained:
EDTA-2Na is disodium ethylenediamine tetraacetate with chemical formula C 10 H 14 N 2 Na 2 O 8 Molecular weight 336.206, it has six coordinating atoms, and the complex formed is called chelate.
The DUB85 standard Chinese name is cetearyl alcohol ethyl caproic acid vinegar, called seabird feather oil, has excellent waterproof performance, good air permeability and spreadability, and is moist and not sticky.
DC200/100 standard Chinese name: Dimethicone.
The invention provides a technical scheme that: a formula of a traditional Chinese medicine leg and foot membrane for external application of safflower oleosomes is prepared from the following raw materials in parts by weight: the component A comprises 86 +/-1 wt% of the component B, 16 +/-1 wt% of the component B, 0.5 +/-0.1 wt% of the component C, 1.5 +/-0.1 wt% of the component D and 2.4 +/-0.1 wt% of the component E;
the component A comprises deionized water accounting for 69 +/-1 weight percent of the total raw materials, carbomer U10 accounting for 4 +/-1 weight percent of the total raw materials, glycerol accounting for 6 +/-0.1 weight percent of the total raw materials, allantoin accounting for 0.3 +/-0.1 weight percent of the total raw materials, butanediol accounting for 6.5 +/-0.1 weight percent of the total raw materials and EDTA-2Na accounting for 0.15 +/-0.1 weight percent of the total raw materials;
the component B comprises 1 plus or minus 0.1 wt% of emulsifier GP200 and 3 plus or minus 0.1 wt% of emulsifier 165, 8 plus or minus 0.1 wt% of DUB85, 2 plus or minus 0.1 wt% of mixed alcohol and 2 plus or minus 0.1 wt% of DC 200/100;
the component C comprises preservative 9010 accounting for 0.6 +/-0.1 wt% of the total raw materials;
the component D comprises plant sterilization and mite removal stock solution accounting for 0.05 +/-0.01 wt% of the total raw materials, ginger essential oil accounting for 0.3 +/-0.1 wt%, essence accounting for 0.5 +/-0.1 wt%, ligusticum wallichii oil accounting for 0.2 +/-0.1 wt% and safflower oleosome accounting for 0.25 +/-0.1 wt%;
the component E comprises arginine accounting for 0.4 plus or minus 0.1 wt% of the total raw materials and deionized water accounting for 2 plus or minus 0.1 wt%.
As shown in figure 1, a preparation method of an externally applied safflower oleosome traditional Chinese medicine leg and foot membrane is adopted, and a formula of the externally applied safflower oleosome traditional Chinese medicine leg and foot membrane is used, and the preparation method comprises the following steps:
the method comprises the following steps: adding the component A into a water phase pot for dissolving, and adding into an emulsifying pot after dissolving;
step two: adding the component B into an oil phase pot for dissolving, and adding into the emulsifying pot obtained in the first step after the dissolving is finished;
the water phase pot in the first step and the oil phase pot in the second step need to be stirred and heated to 75-80 ℃ when being dissolved, and the vacuum degree of materials added into the emulsifying pot from the water phase pot and the oil phase pot is controlled between 0.03MPa-0 and 04MPa
Step three: homogenizing at high speed for a period of time;
step four: cooling the emulsifying pot at the first stage, adding the component C, and homogenizing, wherein the temperature of the emulsifying pot is kept at 75-80 ℃, and the high-speed homogenizing mode is stirring at 50rpm for 5 minutes;
step five: cooling the interval of the emulsifying pot in the second stage, and then adding the component D;
step six: premixing the component E, adding the cooked rice containing the component E into an emulsifying pot, and adjusting the pH value to 5.2-6.0;
step seven: and cooling the emulsifying pot in the third stage, and discharging after the quality inspection is qualified.
It is noted that the first stage cooling reduces the temperature of the emulsifying pot to 60-65 ℃, the second stage cooling reduces the temperature of the emulsifying pot to 35-42 ℃, and the third stage cooling reduces the temperature of the emulsifying pot to 30 ℃ to produce a finished product with a viscosity of 200 cst-100 cst, thereby improving the moistening and protecting effects on the skin.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (10)
1. A formula of a traditional Chinese medicine leg and foot membrane externally applied to safflower oleosomes is characterized in that: the feed is prepared from the following raw materials in parts by weight: the component A comprises 86 +/-1 wt% of the component B, 16 +/-1 wt% of the component B, 0.5 +/-0.1 wt% of the component C, 1.5 +/-0.1 wt% of the component D and 2.4 +/-0.1 wt% of the component E;
the component A comprises deionized water accounting for 69 +/-1 weight percent of the total raw materials and carbomer U10 accounting for 4 +/-1 weight percent;
the component B comprises emulsifier GP200 accounting for 1 plus or minus 0.1wt percent of the total raw materials and emulsifier 165 accounting for 3 plus or minus 0.1wt percent of the total raw materials;
the component C comprises preservative 9010 accounting for 0.6 +/-0.1 wt% of the total raw materials;
the component D comprises plant sterilization and mite removal stock solution accounting for 0.05 +/-0.01 wt% of the total raw materials, ginger essential oil accounting for 0.3 +/-0.1 wt%, essence accounting for 0.5 +/-0.1 wt%, ligusticum wallichii oil accounting for 0.2 +/-0.1 wt% and safflower oleosome accounting for 0.25 +/-0.1 wt%;
the component E comprises arginine accounting for 0.4 plus or minus 0.1 wt% of the total raw materials.
2. The externally applied safflower oleosome traditional Chinese medicine leg and foot membrane formula according to claim 1, which is characterized in that: the component A also comprises glycerol accounting for 6 +/-0.1 wt% of the total raw materials, allantoin accounting for 0.3 +/-0.1 wt%, butanediol accounting for 6.5 +/-0.1 wt% of the total raw materials and EDTA-2Na accounting for 0.15 +/-0.1 wt%.
3. The externally applied safflower oleosome traditional Chinese medicine leg and foot membrane formula according to claim 1, which is characterized in that: the component B also comprises 8 +/-0.1 wt% of DUB85, 2 +/-0.1 wt% of mixed alcohol and 2 +/-0.1 wt% of DC200/100 based on the total raw material.
4. The externally applied safflower oleosome traditional Chinese medicine leg and foot membrane formula according to claim 1, which is characterized in that: the component E also comprises deionized water accounting for 2 +/-0.1 wt% of the total raw materials.
5. A preparation method of an externally-applied safflower oleosome traditional Chinese medicine leg-foot membrane uses any one of the formulas of claims 1 to 4, and is characterized in that: the preparation method comprises the following steps:
the method comprises the following steps: adding the component A into a water phase pot for dissolving, and adding into an emulsifying pot after dissolving;
step two: adding the component B into an oil phase pot for dissolving, and adding into the emulsifying pot obtained in the first step after the dissolving is finished;
step three: homogenizing at high speed for a period of time;
step four: cooling the emulsifying pot for the first stage, and then adding the component C and homogenizing;
step five: cooling the interval of the emulsifying pot in the second stage, and then adding the component D;
step six: premixing the component E, adding the cooked rice containing the component E into an emulsifying pot, and adjusting the pH value;
step seven: and cooling the emulsifying pot in the third stage, and discharging after the quality inspection is qualified.
6. The preparation method of the externally applied safflower oleosome traditional Chinese medicine leg and foot membrane as claimed in claim 5, which is characterized in that: and the water phase pot in the first step and the oil phase pot in the second step need to be stirred and heated to 75-80 ℃ when being dissolved.
7. The preparation method of the externally applied safflower oleosome traditional Chinese medicine leg and foot membrane as claimed in claim 5, which is characterized in that: and in the first step and the second step, the vacuum degree of the materials added into the emulsifying pot from the water phase pot and the oil phase pot is controlled between 0.03MPa and 0.04 MPa.
8. The preparation method of the externally applied safflower oleosome traditional Chinese medicine leg and foot membrane as claimed in claim 5, which is characterized in that: the heat preservation temperature of the emulsifying pot in the third step is 75-80 ℃, and the high-speed homogenization mode is stirring at 50rpm for 5 minutes.
9. The preparation method of the externally applied safflower oleosome traditional Chinese medicine leg and foot membrane as claimed in claim 5, which is characterized in that: the first stage cooling enables the temperature of the emulsifying pot to be reduced to 60-65 ℃, the second stage cooling enables the temperature of the emulsifying pot to be reduced to 35-42 ℃, and the third stage cooling enables the temperature of the emulsifying pot to be reduced to 30 ℃.
10. The preparation method of the externally applied safflower oleosome traditional Chinese medicine leg and foot membrane as claimed in claim 5, which is characterized in that: and in the sixth step, the pH value in the emulsifying pot is adjusted to 5.2-6.0.
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Citations (5)
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CN102026662A (en) * | 2008-04-11 | 2011-04-20 | 赛姆生物系统遗传公司 | Stabilized oleosome preparations and methods of making them |
CN103142962A (en) * | 2013-03-20 | 2013-06-12 | 集粹坊科贸(北京)有限责任公司 | Foot protection composition, foot mask and preparation method of foot protection composition |
CN107126410A (en) * | 2017-05-17 | 2017-09-05 | 广州真润生物科技有限公司 | A kind of brothers' film and preparation method thereof |
CN107384582A (en) * | 2017-09-06 | 2017-11-24 | 吉林农业大学 | A kind of extracting method of safflower oil bodies |
CN112294733A (en) * | 2020-10-27 | 2021-02-02 | 广州真润生物科技有限公司 | Foot mask with warming nursing effect and preparation method thereof |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN102026662A (en) * | 2008-04-11 | 2011-04-20 | 赛姆生物系统遗传公司 | Stabilized oleosome preparations and methods of making them |
CN103142962A (en) * | 2013-03-20 | 2013-06-12 | 集粹坊科贸(北京)有限责任公司 | Foot protection composition, foot mask and preparation method of foot protection composition |
CN107126410A (en) * | 2017-05-17 | 2017-09-05 | 广州真润生物科技有限公司 | A kind of brothers' film and preparation method thereof |
CN107384582A (en) * | 2017-09-06 | 2017-11-24 | 吉林农业大学 | A kind of extracting method of safflower oil bodies |
CN112294733A (en) * | 2020-10-27 | 2021-02-02 | 广州真润生物科技有限公司 | Foot mask with warming nursing effect and preparation method thereof |
Non-Patent Citations (1)
Title |
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ROYALAPOTHIC泊诗蔻: "\"「升级提醒」泊诗蔻经典配方全新升级,奢宠力UP\"", pages 1 - 5, Retrieved from the Internet <URL:https://baijiahao.baidu.com/s?id=1674166887607715689&wfr=spider&for=pc> * |
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