CN115005379A - Tonic tricholoma matsutake powder electuary and preparation method thereof - Google Patents
Tonic tricholoma matsutake powder electuary and preparation method thereof Download PDFInfo
- Publication number
- CN115005379A CN115005379A CN202210591581.5A CN202210591581A CN115005379A CN 115005379 A CN115005379 A CN 115005379A CN 202210591581 A CN202210591581 A CN 202210591581A CN 115005379 A CN115005379 A CN 115005379A
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- CN
- China
- Prior art keywords
- powder
- tricholoma matsutake
- nitrogen
- matsutake
- energy
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 241000121220 Tricholoma matsutake Species 0.000 title claims abstract description 140
- 239000000843 powder Substances 0.000 title claims abstract description 138
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 230000001256 tonic effect Effects 0.000 title description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 91
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 45
- 238000000227 grinding Methods 0.000 claims abstract description 23
- 239000002245 particle Substances 0.000 claims abstract description 23
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims abstract description 18
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- 230000001954 sterilising effect Effects 0.000 claims abstract description 16
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- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 36
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- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 26
- OVBPIULPVIDEAO-LBPRGKRZSA-N folic acid Chemical compound C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)N[C@@H](CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-LBPRGKRZSA-N 0.000 claims description 26
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- CADNYOZXMIKYPR-UHFFFAOYSA-B ferric pyrophosphate Chemical compound [Fe+3].[Fe+3].[Fe+3].[Fe+3].[O-]P([O-])(=O)OP([O-])([O-])=O.[O-]P([O-])(=O)OP([O-])([O-])=O.[O-]P([O-])(=O)OP([O-])([O-])=O CADNYOZXMIKYPR-UHFFFAOYSA-B 0.000 claims description 11
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- WBZFUFAFFUEMEI-UHFFFAOYSA-M Acesulfame k Chemical compound [K+].CC1=CC(=O)[N-]S(=O)(=O)O1 WBZFUFAFFUEMEI-UHFFFAOYSA-M 0.000 claims description 5
- 235000010358 acesulfame potassium Nutrition 0.000 claims description 5
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- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 4
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- YGCFIWIQZPHFLU-UHFFFAOYSA-N acesulfame Chemical compound CC1=CC(=O)NS(=O)(=O)O1 YGCFIWIQZPHFLU-UHFFFAOYSA-N 0.000 claims description 2
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- MKWYFZFMAMBPQK-UHFFFAOYSA-J sodium feredetate Chemical compound [Na+].[Fe+3].[O-]C(=O)CN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O MKWYFZFMAMBPQK-UHFFFAOYSA-J 0.000 claims 2
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L11/00—Pulses, i.e. fruits of leguminous plants, for production of food; Products from legumes; Preparation or treatment thereof
- A23L11/60—Drinks from legumes, e.g. lupine drinks
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3409—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of gases, e.g. fumigation; Compositions or apparatus therefor
- A23L3/3418—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of gases, e.g. fumigation; Compositions or apparatus therefor in a controlled atmosphere, e.g. partial vacuum, comprising only CO2, N2, O2 or H2O
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
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Abstract
An energy-extracting tricholoma matsutake powder electuary and a preparation method thereof belong to the field of fungus tricholoma matsutake deep processing, and particularly relate to a key production technology for preparing the energy-extracting tricholoma matsutake powder electuary by the technical processes of ultrasonic low-temperature sterilization, microwave freeze drying, low-temperature high-energy nano electuary grinding, low-temperature wet ball grinding and nitrogen mediated packaging. The technology can effectively maintain the good flavor of the tricholoma matsutake product, and the prepared tricholoma matsutake powder particles are small in particle size, easy to redissolve and easy to absorb. Meanwhile, the anti-fatigue and immunity-improving effects are achieved. Animal experiments prove that compared with a control group, the product can effectively increase the hypoxia tolerance of an organism and can also obviously reduce the content of serum urea nitrogen and blood lactic acid generated after the organism strenuous exercise. Obviously prolong the swimming time and the hypoxia tolerance time of the loaded mice.
Description
Technical Field
The invention relates to a novel functional electuary, which is prepared and developed by taking high-value fungus tricholoma matsutake as a main nutrient component and utilizing the rich nutrient value of the tricholoma matsutake, and can meet the current time background. The invention relates to a key production technology for preparing energy-extracting tricholoma matsutake powder medicinal granules by technical processes of ultrasonic low-temperature sterilization, microwave freeze drying, low-temperature high-energy nano medicinal granule grinding, low-temperature wet ball milling and nitrogen-mediated packaging.
Background
The functional beverage has health promotion effects of quenching thirst, regulating body function, and enhancing immunity. In the invention, the tricholoma matsutake is rich in nutrition and contains nutrient substances such as beneficial polysaccharide, protein peptide, amino acid, vitamin, mineral substance, trace elements and the like, and particularly, the tricholoma matsutake double-chain polysaccharide, tricholoma matsutake protein and other precious bioactive components have the effects of improving immunity and resisting fatigue. The rich flavor-developing nucleotide and amino acid also endow the tricholoma matsutake powder granules with fresh and sweet taste. Therefore, functional granules of the tricholoma matsutake powder granules are developed, and the energy extraction effect of the functional granules is mainly dependent on the immunity and the anti-fatigue activity of tricholoma matsutake polysaccharide and tricholoma matsutake protein. Functional granules have a short history, but combine the advantages of functional beverages and solid beverages, developing rapidly in terms of packaging, taste and function. The tricholoma matsutake powder granules can provide part of high-quality protein required by diet for human bodies, are purposefully developed and researched according to the nutritional requirement characteristics of different crowds, and have wide development space in the future along with the continuous improvement of products, the diversification of functions of functional granules and the diversification of audience groups.
The matsutake is a natural and precious wild edible and medicinal fungus, and has complete basic nutritional ingredients. Previous research shows that the main compounds in tricholoma matsutake are protein, carbohydrate and crude fiber, the contents of which respectively reach 20.3, 36.67 and 29.1 percent, the contents of crude fat and ash are respectively 5.04 and 8.89 percent, and the tricholoma matsutake further contains more than 10 mineral elements such as potassium, sodium, phosphorus, calcium, iron, copper, manganese, zinc and the like, as well as vitamins B1, B2, C, D and the like. On one hand, the tricholoma matsutake contains balanced nutrient components and is rich in polysaccharide, protein polypeptide, amino acid, vitamin, mineral substance, trace elements and the like; on the other hand, the fruit body of the mushroom also contains valuable bioactive components such as tricholoma matsutake double-chain polysaccharide, tricholoma matsutake alcohol and the like, and is highly appreciated and enjoyed the reputation of "king in bacteria". Modern medical research finds that tricholoma matsutake has various pharmacological effects and functional values, such as: anti-tumor, anti-mutation, anti-radiation, liver protection, antibacterial, gastrointestinal function promotion, antioxidant, antiaging, antifatigue, and immunoregulation effects. The energy-extracting effect of the tricholoma matsutake powder mainly depends on the immunity and the anti-fatigue activity of tricholoma matsutake polysaccharide and tricholoma matsutake protein. In the previous experiments, the extracted protein and polysaccharide have been proved to have the effects of resisting fatigue and improving immunity. The research result of the influence of the tricholoma matsutake polysaccharides on the content of serum urea nitrogen, blood lactic acid and liver glycogen of a mouse after exercise shows that the tricholoma matsutake polysaccharides not only can effectively increase the hypoxia tolerance of an organism, but also can obviously reduce the content of serum urea nitrogen and blood lactic acid generated after the organism strenuous exercise.
The current state analysis and development prospect research report of the solid beverage industry in 2022 + 2028 in China shows that the yield of various solid beverages is rapidly increased in China, wherein the yield accounts for more than half of all the beverages, and the solid beverage industry in all big cities in China is rapidly developed. The functional granules in the invention are prepared from plants and extracts thereof (except fruits, vegetables, tea and coffee) serving as main raw materials, and other food raw and auxiliary materials and food additives are added or not added into the main raw materials and the extracts, and then the solid beverage is prepared. The invention is characterized in that the content (mass fraction) of protein is not less than 0.5% according to the current regulation, and vitamin A acetate, cholecalciferol, cyanocobalamine, folic acid, maltodextrin, instant bean powder, full-cream milk powder, excipient carrier powder, thiamine hydrochloride, riboflavin, calcium carbonate and zinc oxide are added on the basis; the detection method of the protein in the tricholoma matsutake functional granule package needs to meet the requirements specified in GB 5009.5-2016; the addition amount of the food additive and the nutrition enhancer meets the regulations of GB 2760-.
Disclosure of Invention
The invention designs a preparation technology of tricholoma matsutake energy-increasing medicinal granules under microwave freeze drying and high-energy nanometer impact mill, innovatively adopts a core technology of microwave freeze drying, low-temperature high-energy nanometer impact mill, low-temperature wet ball milling, high-energy nanometer impact mill and nitrogen mediated packaging in the industrial field of solid beverages, has outstanding originality, effectively controls the color of tricholoma matsutake raw materials, reduces brown stain of tricholoma matsutake, and maintains the protein, fat, total sugar content and product flavor of the dried tricholoma matsutake. At low temperature, the Tricholoma matsutake can be pulverized to submicron level to obtain Tricholoma matsutake powder with small particle size, easy redissolution and absorption.
The technical scheme of the invention is as follows:
1. the electuary is characterized by being prepared from pine mushroom powder, instant soybean powder, whole milk powder, folic acid, vitamin A acetate, cholecalciferol, thiamine hydrochloride, riboflavin, cyanocobalamine, calcium carbonate, zinc oxide, ferric pyrophosphate, sodium iron ethylenediaminetetraacetate, vitamin C, citric acid, acesulfame potassium and maltodextrin through the steps of cleaning and crushing raw materials at low temperature, carrying out ultrasonic sterilization, carrying out microwave freeze drying, preparing pine mushroom powder, carrying out fine treatment on the pine mushroom powder, mixing the extracted pine mushroom powder electuary and packaging. The energy-extracting tricholoma matsutake powder electuary product is prepared, wherein the high-quality product rate is more than or equal to 99.99%, the nitrogen residual quantity is more than or equal to 98.00%, and the residual oxygen quantity is less than or equal to 0.3%; animal experiments prove that compared with a control group, the product can effectively increase the hypoxia tolerance of an organism and can also obviously reduce the content of serum urea nitrogen and blood lactic acid generated after the organism strenuous exercise. Obviously prolong the swimming time and the hypoxia tolerance time of the loaded mice;
2. a preparation method of the energy-increasing tricholoma matsutake powder electuary comprises the following steps:
1) the raw materials are cleaned and crushed at low temperature: the method is characterized in that the tricholoma matsutake accepted by raw materials is subjected to bubble cleaning in water at the temperature of 2-6 ℃ for 20-40 min, and no surface dirt or pollutants exist;
2) the ultrasonic sterilization comprises the following steps: carrying out ultrasonic sterilization on the processed tricholoma matsutake at the frequency of 10-40 kHz and the power of 1000-5000W and the processing temperature of 60-80 ℃;
3) the microwave freeze drying refers to that the sample sterilized by ultrasonic low temperature is subjected to microwave freeze drying to obtain a dried tricholoma matsutake product;
4) the preparation method of the tricholoma matsutake powder comprises the following steps: putting a dried tricholoma matsutake product into a low-temperature high-energy nano impact mill, and crushing the dried tricholoma matsutake for 5-10 h under the condition of 200-800 r/min to obtain tricholoma matsutake powder particles smaller than 1 mu m;
5) the fine processing of the tricholoma matsutake powder comprises the following steps: the method comprises the following steps of further crushing the pine mushroom powder particles, putting the pine mushroom powder particles into a low-temperature wet grinding machine, wherein the working temperature is 2-8 ℃, the grinding medium is 0.1-0.7 mm ZetaBeads (3-4 kg/l), the grinding speed is 2000-4000 rpm/min, the grinding pressure is 0.5-0.8 bar, the cycle time is 15-20 times/h, and the grinding solvent is pure water or ethanol to obtain pine mushroom fine powder with the particle size of less than 500 nm;
6) mixing and packaging the extract powder of tricholoma matsutake electuary: the preparation method comprises the steps of sequentially carrying out vibration screening treatment on fine matsutake powder, 0.0205-0.0369kg of vitamin A acetate, 0.0160-0.0360kg of cholecalciferol, 0.0040-0.0108kg of cyanocobalamine, 0.0060-0.0150kg of folic acid, 5.000-8.000kg of maltodextrin, 67.320-94.000kg of instant soybean powder, 1.000-36.000kg of whole milk powder, 1.625-14.789kg of excipient carrier powder, 0.0045-0.0094kg of thiamine hydrochloride, 0.0400-0.0078kg of riboflavin, 4.5000-6.000kg of calcium carbonate, 0.0299-0.0747kg of zinc oxide, 0.4000-0.5182kg of iron pyrophosphate, 0.1659-0.21549kg of sodium iron ethylenediaminetetraacetate, 2.000-4.000kg of vitamin C, 0.800-1.2000kg of citric acid and 0.600-0.720kg of zinc pyrophosphate under the mediation of nitrogen, and controlling the number of a vibration screen mesh to be 80-40 meshes. Mixing and packaging under nitrogen mediation in the whole process to obtain the extract tricholoma matsutake powder medicinal granules;
7) mixing the extract powder and the tricholoma matsutake powder into granules: 38.000-42.000kg of fine matsutake powder, 0.0205-0.0369kg of vitamin A acetate, 0.0160-0.0360kg of cholecalciferol, 0.0040-0.0108kg of cyanocobalamin, 0.0060-0.0150kg of folic acid and 5.000-8.000kg of maltodextrin are mixed for 10-15 minutes in a dark closed environment under the mediation of nitrogen to obtain the energy-increasing instant matsutake powder granules with primary protection. 67.320-94.000kg of instant soybean powder with protein content more than or equal to 32%, 1.000-36.000kg of whole milk powder with protein content more than or equal to 23%, 1.625-14.789kg of excipient carrier powder consisting of maltodextrin, 0.0045-0.0094kg of thiamine hydrochloride, 0.0400-0.0078kg of riboflavin, 4.5000-6.000kg of calcium carbonate, 0.0299-0.0747kg of zinc oxide, 0.4000-0.5182kg of ferric pyrophosphate, 0.1659-0.21549kg of ethylenediaminetetraacetic acid sodium 6 relatively stable nutrient enhancing factors are put into the compound granule powder for primary protection to be mixed in a nitrogen-mediated environment to obtain a second compound granule powder. Mixing 2.000-4.000kg of vitamin C, 0.800-1.2000kg of citric acid, 0.600-0.720kg of acesulfame potassium and the second compound granule powder under the nitrogen-mediated environment to obtain high-stability compound granules;
8) the package of the Tongjiang pine mushroom powder electuary comprises the following steps: performing full-automatic quantitative filling of strip bags or pillow bags at 20 +/-0.15 g/bag and hot-melt sealing under the mediation of nitrogen with the purity of 98.00-99.99%, the ventilation capacity of 400-2000L/h and the ventilation pressure of 0.4-1.5 MPa, wherein the hot-melt temperature is 125-250 ℃;
3. the Yineng tricholoma matsutake powder electuary is characterized by having the effects of small particle size, easy redissolution, easy absorption, immunity improvement and the like.
4. The energy-extracting tricholoma matsutake powder electuary is characterized in that tricholoma matsutake is subjected to ultrasonic sterilization, microwave freeze drying, preparation of tricholoma matsutake powder and fine treatment of the tricholoma matsutake powder to obtain fine tricholoma matsutake powder with the granularity of less than 500nm, and the fine tricholoma matsutake powder electuary is obtained by mixing with other auxiliary materials.
5. The energy-extracting tricholoma matsutake powder granules are characterized by being prepared by conducting nitrogen mediated protection on products with the nitrogen purity of 98.00-99.99%, the nitrogen ventilation capacity of 400-2000L/h and the nitrogen ventilation pressure of 0.4-1.5 MPa in the mixing and packaging processes.
The invention has the technical advantages that: the main aspects are as follows:
firstly, the core technology of the application patent focuses on the preparation technology of the functional granule package for improving the energy of the tricholoma matsutake, and the original originality of the plant protein solid beverage which takes the tricholoma matsutake as a main material and is added with a plurality of functional auxiliary materials is very outstanding in the solid beverage industry field.
Secondly, the core technology of the application is microwave freeze drying, and the technology can effectively keep the color and luster of the tricholoma matsutake and reduce the browning of the tricholoma matsutake. The protein, fat and total sugar content of the tricholoma matsutake energy-increasing medicinal granules can be effectively controlled, good flavor is kept, and technical support is provided for comprehensively improving the quality of tricholoma matsutake energy-increasing medicinal granule bags.
Thirdly, the core technology of the application patent is a high-energy nanometer impact mill, and the technology can crush the tricholoma matsutake into submicron level under the condition of low temperature, thereby preparing the tricholoma matsutake powder particles with small particle size, easy redissolution and easy absorption, and providing technical support for comprehensively improving the brewing quality of the tricholoma matsutake energy-increasing medicinal granules.
Fourth, the patent core technology of application has realized the efficiency of antifatigue promotion immunity, and animal experiments prove that compared with the control group, this product can effectively increase the ability of resisting anoxia of the organism, can also show and reduce serum urea nitrogen and blood lactic acid content that the organism produces after strenuous exercise. Obviously prolong the swimming time and the hypoxia tolerance time of the loaded mice.
Detailed Description
Example 1:
the Tricholoma matsutake accepted by raw materials is cleaned by air bubbles in water of 2 ℃ for 40min, and has no surface dirt and pollutants. Performing ultrasonic sterilization on the processed Tricholoma matsutake at a frequency of 30kHz and a power of 2000W and at a processing temperature of 80 ℃; carrying out microwave freeze drying on the sample subjected to ultrasonic low-temperature sterilization to obtain a dried tricholoma matsutake product; placing the dried Tricholoma matsutake product in a low-temperature high-energy nanometer impact mill, and pulverizing at 800r/min for 10 hr to obtain Tricholoma matsutake powder particles smaller than 1 μm; the pine mushroom powder particles are put into a low-temperature wet grinding machine, the working temperature is 6 ℃, the grinding medium is 0.3mm ZetaBeads (3.56kg/l), the grinding speed is 2000rpm/min, the grinding pressure is 0.6bar, the cycle time is 17 times/h, and the grinding solvent is ethanol, so that the pine mushroom fine powder with the particle size of less than 500nm is obtained. The nitrogen-mediated conditions comprise 98.99 percent of nitrogen purity, 3500L/h of nitrogen ventilation and 1.2MPa of nitrogen ventilation pressure. The tricholoma matsutake fine powder, vitamin A acetate, cholecalciferol, cyanocobalamine, folic acid, maltodextrin, instant soybean powder, whole milk powder, excipient carrier powder, thiamine hydrochloride, riboflavin, calcium carbonate, zinc oxide, ferric pyrophosphate, sodium iron ethylene diamine tetraacetate, vitamin C and citric acid are respectively and sequentially subjected to vibrating screen sieving treatment under the mediation of nitrogen, and the mesh number of a vibrating screen is controlled to be 80 meshes. 42.000kg of tricholoma matsutake fine powder, 0.0205kg of vitamin A acetate, 0.0360kg of cholecalciferol, 0.0040kg of cyanocobalamin, 0.0150kg of folic acid and 5.000kg of maltodextrin are mixed for 10 minutes in a dark closed environment under the mediation of nitrogen, and the energy-increasing instant tricholoma matsutake powder granules with primary protection are obtained. 67.320kg of instant bean powder, 5.000kg of whole milk powder and 1.625kg of maltodextrin, 0.0045kg of thiamine hydrochloride, 0.0400kg of riboflavin, 4.5000kg of calcium carbonate, 0.0299kg of zinc oxide, 0.4000kg of ferric pyrophosphate and 0.1659kg of 6 relatively stable nutrient enhancing factors of ethylene diamine tetraacetic acid are put into the primarily protected compound granule powder to be mixed, and then the second compound granule powder is obtained. 3.000kg of vitamin C, 1.2000kg of citric acid and 0.720kg of acesulfame are mixed with the second compound granule powder to obtain the high-stability compound granule. The full-automatic strip-shaped bag or pillow bag is quantitatively filled with 20 +/-0.15 g/bag and is sealed by hot melting under the mediation of nitrogen, and the hot melting temperature is 250 ℃. The extract can be made into powder. Animal experiments prove that compared with a control group, the product can effectively increase the hypoxia tolerance of an organism and can also obviously reduce the content of serum urea nitrogen and blood lactic acid generated after the organism strenuous exercise. Obviously prolong the swimming time and the hypoxia tolerance time of the loaded mice.
Example 2
The tricholoma matsutake accepted by raw materials is subjected to bubble cleaning in water at the temperature of 2-6 ℃ for 20min, and no surface dirt or pollutants exist. Carrying out ultrasonic sterilization on the processed tricholoma matsutake at the frequency of 10kHz and the power of 5000W and the processing temperature of 75 ℃; carrying out microwave freeze drying on the sample subjected to ultrasonic low-temperature sterilization to obtain a dried tricholoma matsutake product; placing the dried Tricholoma matsutake product in a low-temperature high-energy nanometer impact mill, and pulverizing at 400r/min for 7 hr to obtain Tricholoma matsutake powder particles smaller than 1 μm; placing the Tricholoma matsutake powder particles into a low-temperature wet grinding machine, wherein the working temperature is 8 ℃, the grinding medium is 0.6mm ZetaBeads (3kg/l), the grinding speed is 3000rpm/min, the grinding pressure is 0.7bar, the cycle time is 20 times/h, and the grinding solvent is pure water, so as to obtain the Tricholoma matsutake fine powder with the particle size of less than 500 nm. The nitrogen-mediated conditions were that the purity of nitrogen was 99.99%, the aeration rate of nitrogen was 1500L/h, and the aeration pressure of nitrogen was 0.9 MPa. The tricholoma matsutake fine powder, vitamin A acetate, cholecalciferol, cyanocobalamine, folic acid, maltodextrin, instant soybean powder, whole milk powder, excipient carrier powder, thiamine hydrochloride, riboflavin, calcium carbonate, zinc oxide, ferric pyrophosphate, sodium iron ethylene diamine tetraacetate, vitamin C and citric acid are respectively subjected to vibrating screen screening treatment under the mediation of nitrogen in sequence, and the mesh number of a vibrating screen is controlled to be 40-80 meshes. 38.000kg of tricholoma matsutake fine powder, 0.0369kg of vitamin A acetate, 0.0160kg of cholecalciferol, 0.0040kg of cyanocobalamine, 0.0060kg of folic acid and 7.000kg of maltodextrin are mixed for 15 minutes in a dark closed environment under the mediation of nitrogen, and the energy-increasing instant pine antler powder granules with primary protection are obtained. 70.000kg of instant soybean powder, 20.000kg of full-cream milk powder and 14.789kg of excipient carrier powder consisting of maltodextrin, and 0.0094kg of thiamine hydrochloride, 0.0478kg of riboflavin, 5.000kg of calcium carbonate, 0.0599kg of zinc oxide, 0.4082kg of ferric pyrophosphate and 0.1859kg of ethylene diamine tetraacetic acid iron sodium 6 relatively stable nutrient reinforcing factors are put into the primarily protected compound granule powder for mixing to obtain the second compound granule powder. 3.000kg of vitamin C, 1.000kg of citric acid and 0.700kg of acesulfame potassium are mixed with the second compound granule powder to obtain the high-stability compound granule. The full-automatic strip-shaped bag or pillow bag is quantitatively filled with 20 +/-0.15 g/bag and is sealed by hot melting under the mediation of nitrogen, and the hot melting temperature is 225 ℃. The extract can be made into powder. Animal experiments prove that compared with a control group, the product can effectively increase the anoxia resistance of an organism and can also obviously reduce the content of serum urea nitrogen and blood lactic acid generated after the organism strenuous exercise. Obviously prolong the swimming time and the hypoxia tolerance time of the loaded mice.
Example 3
The tricholoma matsutake subjected to raw material acceptance is subjected to bubble cleaning in water at the temperature of 2-6 ℃ for 30min, and no surface dirt or pollutants exist. Carrying out ultrasonic sterilization on the processed tricholoma matsutake at the frequency of 20kHz and the power of 4000W and the processing temperature of 60 ℃; carrying out microwave freeze drying on the sample subjected to ultrasonic low-temperature sterilization to obtain a dried tricholoma matsutake product; placing the dried Tricholoma matsutake product in a low-temperature high-energy nanometer impact mill, and pulverizing at 700r/min for 10 hr to obtain Tricholoma matsutake powder particles smaller than 1 μm; the pine mushroom powder particles are put into a low-temperature wet grinding machine, the working temperature is 2 ℃, the grinding medium is 0.1mm ZetaBeads (3.85kg/l), the grinding speed is 4000rpm/min, the grinding pressure is 0.8bar, the cycle time is 17 times/h, and the grinding solvent is pure water, so that the pine mushroom fine powder with the particle size of less than 500nm is obtained. The nitrogen-mediated conditions were 98.00% nitrogen purity, 1000L/h nitrogen aeration, and 1.2MPa nitrogen aeration pressure. The tricholoma matsutake fine powder, vitamin A acetate, cholecalciferol, cyanocobalamine, folic acid, maltodextrin, instant soybean powder, whole milk powder, excipient carrier powder, thiamine hydrochloride, riboflavin, calcium carbonate, zinc oxide, ferric pyrophosphate, sodium iron ethylene diamine tetraacetate, vitamin C and citric acid are respectively and sequentially subjected to vibrating screen sieving treatment under the mediation of nitrogen, and the mesh number of a vibrating screen is controlled to be 80 meshes. 42.000kg of tricholoma matsutake fine powder, 0.0369kg of vitamin A acetate, 0.0260kg of cholecalciferol, 0.0108kg of cyanocobalamine, 0.0150kg of folic acid and 5.000kg of maltodextrin are mixed for 10 minutes in a dark closed environment under the mediation of nitrogen, and the energy-increasing instant pine antler powder granules with primary protection are obtained. 94.000kg of instant bean powder, 1.000kg of full cream milk powder and 1.625kg of excipient powder consisting of maltodextrin and 0.0045kg of thiamine hydrochloride, 0.0400kg of riboflavin, 4.5000kg of calcium carbonate, 0.0299kg of zinc oxide, 0.4000kg of ferric pyrophosphate and 0.165kg of ethylene diamine tetraacetic acid iron sodium 6 relatively stable nutrient enhancing factors are put into the compound granule powder for primary protection to be mixed, and the second compound granule powder is obtained. 2.000kg of vitamin C, 0.800kg of citric acid and 0.600kg of acesulfame potassium are mixed with the second compound granule powder to obtain the high-stability compound granule. The full-automatic strip-shaped bag or pillow bag is quantitatively filled with 20 +/-0.15 g/bag and is sealed by hot melting under the mediation of nitrogen, and the hot melting temperature is 125 ℃. The extract can be made into powder. Animal experiments prove that compared with a control group, the product can effectively increase the hypoxia tolerance of an organism and can also obviously reduce the content of serum urea nitrogen and blood lactic acid generated after the organism strenuous exercise. Obviously prolong the swimming time and the hypoxia tolerance time of the loaded mice.
Claims (4)
1. A preparation method of energy-extracting tricholoma matsutake powder granules is characterized in that the energy-extracting tricholoma matsutake powder granules are prepared from the tricholoma matsutake powder, instant soybean powder, whole milk powder, folic acid, vitamin A acetate, cholecalciferol, thiamine hydrochloride, riboflavin, cyanocobalamine, calcium carbonate, zinc oxide, ferric pyrophosphate, sodium ferric ethylene diamine tetraacetate, vitamin C, citric acid, acesulfame and maltodextrin through the steps of cleaning and crushing raw materials at low temperature, carrying out ultrasonic sterilization, carrying out microwave freeze drying, preparing the tricholoma matsutake powder, carrying out fine treatment on the tricholoma matsutake powder, mixing and packaging the energy-extracting tricholoma matsutake powder granules, wherein the excellent product rate is more than or equal to 99.99%, the residual nitrogen gas content is more than or equal to 98.00%, and the residual oxygen content is less than or equal to 0.3%; the storage temperature is 37 +/-2 ℃, the relative humidity is 75 +/-5%, an accelerated test is carried out for 180 days under the condition of avoiding direct light, the product stability is good, the TBARS (tert-butyl ether-trimethyl ammonium chloride) rise is lower than 20%, animal experiments prove that the tricholoma matsutake can effectively increase the hypoxia resistance of an organism and can also obviously reduce the serum urea nitrogen and blood lactic acid content generated after the organism violently moves, and the tricholoma matsutake polysaccharide can obviously prolong the swimming time and the hypoxia resistance time of a loaded mouse;
1) the raw materials are cleaned and crushed at low temperature: the method is characterized in that the tricholoma matsutake accepted by raw materials is subjected to bubble cleaning in water at the temperature of 2-6 ℃ for 20-40 min, and no surface dirt or pollutants exist;
2) the ultrasonic sterilization is to perform ultrasonic sterilization on the processed tricholoma matsutake at the frequency of 10-40 kHz and the power of 1000-5000W and the processing temperature of 60-80 ℃;
3) the microwave freeze drying refers to that the sample sterilized by ultrasonic low temperature is subjected to microwave freeze drying to obtain a dried tricholoma matsutake product;
4) the preparation of the tricholoma matsutake powder is to put a dried tricholoma matsutake product into a low-temperature high-energy nano impact mill, and crush the dried tricholoma matsutake for 5-10 h under the condition of 200-800 r/min to obtain tricholoma matsutake powder particles smaller than 1 mu m;
5) the fine processing of the tricholoma matsutake powder refers to the process of further crushing the tricholoma matsutake powder particles, the tricholoma matsutake powder particles are placed in a low-temperature wet grinding machine, the working temperature is 2-8 ℃, the grinding medium is 0.1-0.7 mm ZetaBeads (3-4 kg/l), the grinding speed is 2000-4000 rpm/min, the grinding pressure is 0.5-0.8 bar, the cycle time is 15-20 times/h, and the grinding solvent is pure water or ethanol, so that the tricholoma matsutake fine powder with the particle size of less than 500nm is obtained;
6) mixing and packaging the medicinal granules of the energy-increasing tricholoma matsutake powder: the preparation method comprises the steps of sequentially carrying out vibration screening on fine matsutake powder, 0.0205-0.0369kg of vitamin A acetate, 0.0160-0.0360kg of cholecalciferol, 0.0040-0.0108kg of cyanocobalamine, 0.0060-0.0150kg of folic acid, 5.000-8.000kg of maltodextrin, 67.320-94.000kg of instant soybean powder, 1.000-36.000kg of whole milk powder, 1.625-14.789kg of excipient carrier powder, 0.0045-0.0094kg of thiamine hydrochloride, 0.0400-0.0078kg of riboflavin, 4.5000-6.000kg of calcium carbonate, 0.0299-0.0747kg of zinc oxide, 0.4000-0.5182kg of iron, 0.1659-0.21549kg of ferric sodium ethylene diamine tetraacetate, 2.000-4.000kg of vitamin C, 0.800-1.2000kg of citric acid and 0.600-0.720kg of the fine matsutake powder under the condition of nitrogen mediation, carrying out vibration screening on the fine matsutake powder under the condition of 80 meshes of a vibration screen mesh, and packaging the whole process under the condition of nitrogen mediation and the whole process of the mixed powder can be prepared into granules;
7) the mixing of the energy-increasing pine mushroom powder granules is to place 38.000-42.000kg of fine pine mushroom powder, 0.0205-0.0369kg of vitamin A acetate, 0.0160-0.0360kg of cholecalciferol, 0.0040-0.0108kg of cyanocobalamin, 0.0060-0.0150kg of folic acid and 5.000-8.000kg of maltodextrin in a dark closed environment under the mediation of nitrogen for mixing for 10-15 minutes to obtain the primarily protected energy-increasing instant pine mushroom powder granules; 67.320-94.000kg of instant soybean powder with protein content of more than or equal to 32 percent, 1.000-36.000kg of whole milk powder with protein content of more than or equal to 23 percent, 1.625-14.789kg of maltodextrin and shaped carrier powder consisting of 0.0045-0.0094kg of thiamine hydrochloride, 0.0400-0.0078kg of riboflavin, 4.5000-6.000kg of calcium carbonate, 0.0299-0.0747kg of zinc oxide, 0.4000-0.5182kg of ferric pyrophosphate, 0.1659-0.21549kg of ethylenediamine tetraacetic acid sodium 6 relatively stable nutrient strengthening factors are put into the compound granule powder protected in the initial step to be mixed under the nitrogen-mediated environment to obtain second compound granule powder; mixing 2.000-4.000kg of vitamin C, 0.800-1.2000kg of citric acid, 0.600-0.720kg of acesulfame potassium and the second compound granule powder under the nitrogen-mediated environment to obtain high-stability compound granules;
8) the package of the energy-extracting tricholoma matsutake powder granules is characterized in that full-automatic strip-shaped bags or pillow bags are quantitatively filled by 20 +/-0.15 g/bag and are subjected to hot melting sealing under the mediation of nitrogen with the purity of 98.00-99.99%, the ventilation capacity of 400-2000L/h and the ventilation pressure of 0.4-1.5 MPa, and the hot melting temperature is 125-250 ℃.
2. The preparation method of the tricholoma matsutake powder granules according to claim 1, which is characterized by comprising the following steps: the matsutake is processed by ultrasonic sterilization, microwave freeze drying, preparation of matsutake powder, and fine processing of matsutake powder to obtain fine matsutake powder with granularity less than 500nm, and is mixed with other adjuvants to obtain the LINENG powder granule.
3. The method for preparing the tricholoma matsutake powder granules as claimed in claim 1, wherein the nitrogen mediated protection is carried out during the mixing and packaging process with the nitrogen purity of 98.00-99.99%, the nitrogen ventilation amount of 400-2000L/h and the nitrogen ventilation pressure of 0.4-1.5 MPa.
4. A Tonic tricholoma matsutake powder granule prepared by the method of any one of claims 1 to 3.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103082273A (en) * | 2013-02-04 | 2013-05-08 | 云南茂昽实业有限责任公司 | Tricholoma matsutake dried product with nutrients and flavor fully preserved, and preparation method thereof |
| CN104431995A (en) * | 2015-01-14 | 2015-03-25 | 佟立君 | Preparation method of fresh tricholoma matsutake active material |
| CN112841315A (en) * | 2021-02-09 | 2021-05-28 | 赣州市全标生物科技有限公司 | Hypoallergenic ferrous-based fortified infant complementary food nutrition bag and preparation method thereof |
| CN112841319A (en) * | 2021-02-09 | 2021-05-28 | 赣州市全标生物科技有限公司 | Whole-process nitrogen-mediated infant complementary food nutrition bag and preparation method thereof |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103082273A (en) * | 2013-02-04 | 2013-05-08 | 云南茂昽实业有限责任公司 | Tricholoma matsutake dried product with nutrients and flavor fully preserved, and preparation method thereof |
| CN104431995A (en) * | 2015-01-14 | 2015-03-25 | 佟立君 | Preparation method of fresh tricholoma matsutake active material |
| CN112841315A (en) * | 2021-02-09 | 2021-05-28 | 赣州市全标生物科技有限公司 | Hypoallergenic ferrous-based fortified infant complementary food nutrition bag and preparation method thereof |
| CN112841319A (en) * | 2021-02-09 | 2021-05-28 | 赣州市全标生物科技有限公司 | Whole-process nitrogen-mediated infant complementary food nutrition bag and preparation method thereof |
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