CN114983860A - Freeze-dried ball for skin care and beauty and preparation method thereof - Google Patents
Freeze-dried ball for skin care and beauty and preparation method thereof Download PDFInfo
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- CN114983860A CN114983860A CN202210583748.3A CN202210583748A CN114983860A CN 114983860 A CN114983860 A CN 114983860A CN 202210583748 A CN202210583748 A CN 202210583748A CN 114983860 A CN114983860 A CN 114983860A
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- freeze
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- dried ball
- collagen solution
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0241—Containing particulates characterized by their shape and/or structure
- A61K8/025—Explicitly spheroidal or spherical shape
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
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- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to the technical field of beauty treatment, and discloses a freeze-dried ball for skin care and beauty treatment, which comprises the following raw materials in percentage by weight: 2-8% of mannitol, 10-15% of hydroxyethyl cellulose, 1-5% of hydrolyzed collagen, 8.5-11% of oligopeptide and 70-80% of distilled water. The freeze-dried ball for skin care and beauty and the preparation method thereof can efficiently extract the effective components in the skin care product, prevent the components from being inactivated, and freeze-dry the extracted components into the freeze-dried ball in vacuum, so that the structural stability of the product is maintained, the faster drying rate is ensured, the moisture is reduced, and the quality guarantee period is prolonged by tightly bottling the freeze-dried ball.
Description
Technical Field
The invention belongs to the technical field of beauty treatment, and particularly relates to a freeze-dried ball for skin care and beauty treatment and a preparation method thereof.
Background
With the pollution of modern environment and the higher and higher requirements of the public, the requirements on skin care products are more and more strict, and the existing skin care products on the market mostly mainly comprise essences and creams, so that the active substances in the skin care products can not play the most role, and compared with the traditional essence, the skin care products are more moist for achieving the aim of comprehensively improving the skin condition, and the production process of the skin care products needs to be changed.
In the skin care products in the prior art, essences are directly smeared on skin, the preparation method of the skin care products causes that some active ingredients which are easy to degrade and oxidize are difficult to store, and the using effect is influenced.
Disclosure of Invention
The invention aims to provide a freeze-dried ball for skin care and beauty and a manufacturing method thereof, which aim to solve the problems in the background technology.
In order to achieve the above purpose, the invention provides the following technical scheme: the freeze-dried ball for skin care and beauty comprises the following raw materials in percentage by weight: 2-8% of mannitol, 10-15% of hydroxyethyl cellulose, 1-5% of hydrolyzed collagen, 8.5-11% of oligopeptide and 70-80% of distilled water.
Preferably, the raw materials of the product comprise the following components in percentage by weight: 6% of mannitol, 13% of hydroxyethyl cellulose, 2% of hydrolyzed collagen, 10.5% of oligopeptide and 75% of water.
The application also provides a manufacturing method of the freeze-dried ball for skin care and beauty, which comprises the following specific steps:
s1, preparing a hydrolyzed collagen solution with the purity of 35-65% in advance, and adding a proper amount of acylating reagent into the hydrolyzed collagen solution to maintain the pH value of the hydrolyzed collagen solution at 6.8-7.2;
s2, after the reaction is finished, putting the solution into extraction equipment for extraction and purification to obtain collagen solution essence;
s3, adding distilled water into a heatable metal container in advance, placing the collagen solution into the heatable metal container, stirring and mixing the two uniformly, then sequentially adding mannitol, hydroxyethyl cellulose and oligopeptide into the interior, and stirring again to form low-concentration viscous colloid;
s4, sampling the colloid prepared in the S3 step for performance detection;
and S5, after the product is qualified, adding the colloid material into the mold, and then putting the mold into freeze-drying equipment for freezing-sublimation drying-desorption drying to prepare the freeze-dried ball.
Preferably, in the step S1, the hydrolyzed collagen solution is added with the acylating agent in a circular motion, and the material is added while stirring manually.
Preferably, the distilled water in the step S3 is heated in advance and controlled to be 28-33 ℃, and then the collagen solution and the distilled water are mixed by a mechanical device and stirred, and the rotating speed is 120r/min and the duration is 5/min; the viscosity number of the low-concentration viscous colloid is 2.64-2.80 mPas.
Preferably, the performance test in the step S4 includes a sensory stimulation test, a microorganism content test, a solubility test and a material activity test.
The invention has the following beneficial effects:
1. the freeze-dried ball for skin care and beauty and the preparation method thereof can efficiently extract the effective components in the skin care product, prevent the components from being inactivated, and freeze-dry the extracted components into the freeze-dried ball in vacuum, so that the structural stability of the product is maintained, the faster drying rate is ensured, the moisture is reduced, and the quality guarantee period is prolonged by tightly bottling the freeze-dried ball.
Drawings
FIG. 1 is an external view of a freeze-dried pellet product of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be obtained by a person skilled in the art without making any creative effort based on the embodiments in the present invention, belong to the protection scope of the present invention.
As shown in fig. 1, the embodiment of the invention provides a freeze-dried ball for skin care and beauty treatment, which comprises the following raw materials in percentage by weight: 2-8% of mannitol, 10-15% of hydroxyethyl cellulose, 1-5% of hydrolyzed collagen, 8.5-11% of oligopeptide and 70-80% of distilled water.
The product comprises the following raw materials in percentage by weight: 6% of mannitol, 13% of hydroxyethyl cellulose, 2% of hydrolyzed collagen, 10.5% of oligopeptide and 75% of water.
The invention also provides a preparation method of the freeze-dried ball for skin care and beauty, which comprises the following steps:
s1, preparing a hydrolyzed collagen solution with the purity of 35-65% in advance, and adding a proper amount of acylating reagent into the hydrolyzed collagen solution to maintain the pH value of the hydrolyzed collagen solution at 6.8-7.2;
s2, after the reaction is finished, putting the solution into extraction equipment for extraction and purification to obtain collagen solution essence;
s3, adding distilled water into a heatable metal container in advance, placing the collagen solution into the heatable metal container, stirring and mixing the two uniformly, then sequentially adding mannitol, hydroxyethyl cellulose and oligopeptide into the interior, and stirring again to form low-concentration viscous colloid;
s4, sampling the colloid prepared in the step S3 for performance detection;
s5, after the product is qualified, adding the colloid material into a mold, and then putting the mold into freeze-drying equipment for freezing-sublimation drying-desorption drying to prepare a freeze-dried ball;
hydrolyzed collagen, namely thick soluble collagen essence, is adopted to realize multi-dimension skin tightening, promote skin microcirculation, tighten and repair skin, and deeply moisten skin bottom to make skin bright, moist and elastic;
by the adoption of the technical scheme, the intensive repair function of the skin care product is played comprehensively, the dark and oxidized skin state is improved, the skin care product is converted into a solid state in an ultralow temperature environment by a refrigeration and drying technology, secondary freeze drying is performed, the moisture content is lower, the structure is stable, active repair substances are effectively stored, factor activity in the sterile powder is activated by the essence, and therefore light-age activity is injected into the skin, the skin becomes firmer, and the skin repair force is improved.
Wherein, in the step S1, the hydrolyzed collagen solution is added with the acylating agent in a circular motion mode, and the material is added and stirred manually in the process.
Wherein, the distilled water in the step S3 is heated in advance and controlled to be 28-33 ℃, and then the collagen solution and the distilled water are mixed by mechanical equipment for stirring, the rotating speed is 120r/min, and the duration is 5/min; the viscosity number of the low-concentration viscous colloid is 2.64-2.80 mPas.
Wherein the performance test in the step S4 comprises a sensory stimulation test, a microorganism content test, a solubility test and a material activity test;
for some cosmetic products of spreading type, because the cosmetic product needs to be directly spread on the skin, the cortex of each person is different, so as to avoid a series of maladaptive symptoms such as allergy, and the like, and the cosmetic product needs to be tested at present, such as searching for a targeted test of experimenters or a chemical equipment inspection, and the like.
The use method of the freeze-drying ball comprises the following steps:
placing the freeze-dried ball in the palm, pouring the toner into fingers to form a ring on the palm, so that the freeze-dried ball is melted in the toner and becomes high-concentration collagen water, the texture of the collagen water is very moist, when the collagen water is used, the user needs to remember not to massage the ring on the face, but to lightly pat and press the collagen water by hands until the collagen water is absorbed by the skin, because the concentration is higher, the skin can be easily rubbed with mud if the whole face is massaged and circled; after being absorbed, the skin care product is very fresh and not sticky at all, and the approximate steps are that the skin care product is used almost as much as the toner, the toner is mixed with the toner every day for use, and then the subsequent skin care products are added, so that the skin is obviously improved after one month.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. A freeze-dried ball for skin care and beauty is characterized in that: the product comprises the following raw materials in percentage by weight: 2-8% of mannitol, 10-15% of hydroxyethyl cellulose, 1-5% of hydrolyzed collagen, 8.5-11% of oligopeptide and 70-80% of distilled water.
2. The freeze-dried ball for skin care and beauty according to claim 1, wherein: the product comprises the following raw materials in percentage by weight: 6% of mannitol, 13% of hydroxyethyl cellulose, 2% of hydrolyzed collagen, 10.5% of oligopeptide and 75% of water.
3. A method for preparing freeze-dried balls for skin care and beauty is characterized by comprising the following steps:
s1, preparing a hydrolyzed collagen solution with the purity of 35-65% in advance, and adding a proper amount of acylating reagent into the hydrolyzed collagen solution to maintain the pH value of the hydrolyzed collagen solution at 6.8-7.2;
s2, after the reaction is finished, putting the solution into extraction equipment for extraction and purification to obtain collagen solution essence;
s3, adding distilled water into a heatable metal container in advance, placing the collagen solution into the heatable metal container, stirring and mixing the two uniformly, then sequentially adding mannitol, hydroxyethyl cellulose and oligopeptide into the interior, and stirring again to form low-concentration viscous colloid;
s4, sampling the colloid prepared in the step S3 for performance detection;
and S5, after the colloid material is qualified, adding the colloid material into a mold, and then putting the mold into a freeze-drying device for freezing-sublimation drying-desorption drying to prepare the freeze-dried ball.
4. The method for manufacturing the freeze-dried ball for skin care and beauty according to claim 3, wherein the freeze-dried ball for skin care and beauty comprises the following steps: in the step S1, the hydrolyzed collagen solution is added with the acylating agent in a circular motion, and the material is manually added while stirring.
5. The method for manufacturing the freeze-dried ball for skin care and beauty according to claim 3, wherein the freeze-dried ball for skin care and beauty comprises the following steps: in the step S3, distilled water is heated in advance to be controlled to be 28-33 ℃, and then the collagen solution and the distilled water are mixed by adopting mechanical equipment to stir, wherein the rotating speed is 120r/min, and the duration is 5/min; the viscosity number of the low-concentration viscous colloid is 2.64-2.80 mPas.
6. The method for manufacturing the skin-care beauty freeze-dried ball according to claim 3, characterized in that: the performance test in the step S4 comprises a sensory stimulation test, a microorganism content test, a solubility test and a material activity test.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210583748.3A CN114983860A (en) | 2022-05-25 | 2022-05-25 | Freeze-dried ball for skin care and beauty and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210583748.3A CN114983860A (en) | 2022-05-25 | 2022-05-25 | Freeze-dried ball for skin care and beauty and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN114983860A true CN114983860A (en) | 2022-09-02 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210583748.3A Pending CN114983860A (en) | 2022-05-25 | 2022-05-25 | Freeze-dried ball for skin care and beauty and preparation method thereof |
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| CN (1) | CN114983860A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105078783A (en) * | 2015-09-06 | 2015-11-25 | 无锡贝迪生物工程有限公司 | Instant collagen lyophilized ball and preparation method thereof |
| CN113576944A (en) * | 2021-08-09 | 2021-11-02 | 中山中研化妆品有限公司 | Freeze-dried ball and preparation method thereof and skin care product |
-
2022
- 2022-05-25 CN CN202210583748.3A patent/CN114983860A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105078783A (en) * | 2015-09-06 | 2015-11-25 | 无锡贝迪生物工程有限公司 | Instant collagen lyophilized ball and preparation method thereof |
| CN113576944A (en) * | 2021-08-09 | 2021-11-02 | 中山中研化妆品有限公司 | Freeze-dried ball and preparation method thereof and skin care product |
Non-Patent Citations (1)
| Title |
|---|
| 广州铭威生物科技有限公司: "朵润美冻干粉+溶酶液，备案编号：粤G妆网备字2020114090", Retrieved from the Internet <URL:https://hzpba.nmpa.gov.cn/gccx/chakanHis.html?prodId=20200617135334eoriy&gb=G> * |
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