CN114958477A - Treatment process for removing acid value of ganoderma lucidum spore oil - Google Patents
Treatment process for removing acid value of ganoderma lucidum spore oil Download PDFInfo
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- CN114958477A CN114958477A CN202210643376.9A CN202210643376A CN114958477A CN 114958477 A CN114958477 A CN 114958477A CN 202210643376 A CN202210643376 A CN 202210643376A CN 114958477 A CN114958477 A CN 114958477A
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- 240000008397 Ganoderma lucidum Species 0.000 title claims abstract description 131
- 235000001637 Ganoderma lucidum Nutrition 0.000 title claims abstract description 131
- 239000002253 acid Substances 0.000 title claims abstract description 38
- 238000000034 method Methods 0.000 title claims abstract description 26
- 238000003756 stirring Methods 0.000 claims abstract description 170
- 239000000843 powder Substances 0.000 claims abstract description 101
- 239000002245 particle Substances 0.000 claims abstract description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 30
- 238000000605 extraction Methods 0.000 claims abstract description 20
- 238000004519 manufacturing process Methods 0.000 claims abstract description 20
- 239000008213 purified water Substances 0.000 claims abstract description 19
- 239000002131 composite material Substances 0.000 claims abstract description 15
- 238000003815 supercritical carbon dioxide extraction Methods 0.000 claims abstract description 6
- 241000222336 Ganoderma Species 0.000 claims description 23
- 238000010438 heat treatment Methods 0.000 claims description 23
- 238000003860 storage Methods 0.000 claims description 21
- 239000000284 extract Substances 0.000 claims description 17
- 238000001816 cooling Methods 0.000 claims description 13
- 238000001035 drying Methods 0.000 claims description 12
- 238000007599 discharging Methods 0.000 claims description 11
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 10
- 239000011259 mixed solution Substances 0.000 claims description 9
- 238000004821 distillation Methods 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 7
- 230000001681 protective effect Effects 0.000 claims description 7
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 5
- 239000001569 carbon dioxide Substances 0.000 claims description 5
- 239000012530 fluid Substances 0.000 claims description 5
- 238000001704 evaporation Methods 0.000 claims description 4
- 238000011049 filling Methods 0.000 claims description 4
- 238000005469 granulation Methods 0.000 claims description 3
- 230000003179 granulation Effects 0.000 claims description 3
- 230000001007 puffing effect Effects 0.000 claims description 3
- 239000000523 sample Substances 0.000 claims description 3
- 239000000243 solution Substances 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 abstract description 5
- 239000002994 raw material Substances 0.000 abstract description 3
- 235000021049 nutrient content Nutrition 0.000 abstract description 2
- 239000000463 material Substances 0.000 description 20
- 230000000694 effects Effects 0.000 description 13
- 239000000203 mixture Substances 0.000 description 11
- 239000007788 liquid Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 238000004448 titration Methods 0.000 description 3
- 206010011224 Cough Diseases 0.000 description 2
- 206010003549 asthenia Diseases 0.000 description 2
- 208000006673 asthma Diseases 0.000 description 2
- 238000007664 blowing Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 208000037823 Cerebral ischemia/reperfusion injury Diseases 0.000 description 1
- 208000007443 Neurasthenia Diseases 0.000 description 1
- 206010033557 Palpitations Diseases 0.000 description 1
- 241000222341 Polyporaceae Species 0.000 description 1
- 208000013738 Sleep Initiation and Maintenance disease Diseases 0.000 description 1
- 208000012886 Vertigo Diseases 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000007908 dry granulation Methods 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000035784 germination Effects 0.000 description 1
- 206010022437 insomnia Diseases 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 150000004671 saturated fatty acids Chemical class 0.000 description 1
- 238000010257 thawing Methods 0.000 description 1
- 230000002936 tranquilizing effect Effects 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 231100000889 vertigo Toxicity 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
- C11B1/104—Production of fats or fatty oils from raw materials by extracting using super critical gases or vapours
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
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- Engineering & Computer Science (AREA)
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- Oil, Petroleum & Natural Gas (AREA)
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- Organic Chemistry (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
The invention provides a treatment process for removing acid value of ganoderma lucidum spore oil, belongs to the technical field of health-care product preparation, and is used for solving the technical problems of low oil yield and high acid value of the existing ganoderma lucidum spore oil. According to the treatment process for removing the acid value of the ganoderma lucidum spore oil, the wall breaking is carried out on the embrittled ganoderma lucidum spore powder through an ultrafine grinder, the wall-broken ganoderma lucidum spore powder with the wall breaking rate of more than or equal to 98% can be obtained, and therefore the oil yield of the ganoderma lucidum spore oil and the nutrient content of the ganoderma lucidum spore oil are improved; through the composite stirring device, the consumption of raw materials in the transfer process is reduced, so that the stirring is faster and more uniform, the production cost is reduced, and the production efficiency is improved; the proportion of the ganoderma lucidum spore powder and the purified water in the ganoderma lucidum spore particles is controlled by the composite stirring device, and when supercritical carbon dioxide extraction is carried out, the extraction efficiency is high, and the acid value of the ganoderma lucidum spore oil is effectively reduced.
Description
Technical Field
The invention belongs to the technical field of health-care product preparation, and relates to a treatment process for removing acid value of ganoderma lucidum spore oil.
Background
Ganoderma Lucidum is also called Linzhongling and Qiongzhen (scientific name: Ganoderma Lucidum Karst), and is the fruiting body of Ganoderma Lucidum of Polyporaceae. Has effects in invigorating qi, tranquilizing mind, relieving cough and asthma, and prolonging life. Can be used for treating vertigo, insomnia, palpitation, short breath, neurasthenia, and cough with asthma due to asthenia. Mainly distributed in Zhejiang, Heilongjiang, Jilin, Anhui, Jiangxi, Hunan, Guizhou, Guangdong, Fujian and other places in China;
the ganoderma lucidum spore oil is oily lipid extracted from wall-broken ganoderma lucidum spores by a supercritical carbon dioxide fluid extraction technology, integrates various active components of the ganoderma lucidum spores, is yellow transparent liquid, mainly contains saturated fatty acid, unsaturated fatty acid and the like, contains a small amount of ganoderma lucidum acid components, and has the effects of resisting cerebral ischemia/reperfusion injury and resisting oxidation and removing free radicals;
the prepared ganoderma lucidum spore oil has higher acid value index and lower oil yield in the existing ganoderma lucidum spore oil preparation process, and the stirring device used by the existing equipment has independent structure, no linkage effect, high unit power consumption and longer stirring working hours.
Through retrieval, for example, the chinese patent document discloses a preparation method of ganoderma lucidum spore oil [ application number: CN 201810114907.9; publication No.: CN108485794B, the preparation method takes ganoderma lucidum spore powder without wall breaking as raw material, ganoderma lucidum spore oil is obtained by extraction after germination, enzymolysis and ultrasonic freeze thawing, and the wall breaking rate reaches more than 96%. According to the invention, the ganoderma lucidum spore powder is germinated before wall breaking, and three freeze-thaw cycles are matched, so that the effective components in the ganoderma lucidum spore oil are maximally reserved, and the wall breaking rate and the oil yield of the ganoderma lucidum spore powder are improved.
Although the process can prepare the ganoderma lucidum spore oil extract, the prepared ganoderma lucidum spore oil has higher acid value and lower oil yield, and the stirring device has independent structure, no linkage effect, high unit power consumption and longer stirring working hours.
Based on the above, a treatment process for removing acid value of the ganoderma lucidum spore oil is designed, the prepared ganoderma lucidum spore oil has low acid value and high oil yield, and a composite stirring device is adopted for production, so that the production time is short; the unit power consumption is low.
Disclosure of Invention
The invention aims to solve the problems in the prior art, provides a treatment process for removing acid value of ganoderma lucidum spore oil, and the device aims to solve the technical problems that: how to reduce the acid value of the ganoderma lucidum spore oil, improve the oil yield and improve the production efficiency.
The purpose of the invention can be realized by the following technical scheme:
a treatment process for removing acid value of ganoderma spore oil comprises the following production process steps:
step one, embrittlement of ganoderma lucidum spore powder: placing Ganoderma spore powder in a vacuum puffing tank, setting embrittlement temperature at 97-102 deg.C, evacuating and drying for 0.8-1.1h, and evacuating and drying at 76-82 deg.C;
step two, breaking the wall of ganoderma lucidum spore powder: placing the embrittled ganoderma lucidum spore powder obtained in the step one in an ultrafine pulverizer to obtain wall-broken ganoderma lucidum spore powder with the wall-broken rate of more than or equal to 98%;
step three, stirring the ganoderma lucidum spore powder: mixing wall-broken ganoderma lucidum spore powder and purified water according to a weight ratio of 1: (0.3-0.6) introducing into a stirring device, stirring for 2-3min, and gradually heating to 30-34 deg.C while stirring to obtain a mixed solution;
step four, the ganoderma lucidum spore powder is agglomerated; according to the weight ratio of 1: (0.3-0.5) taking the mixed liquor obtained in the third step and the wall-broken ganoderma lucidum spore powder obtained in the second step, introducing the mixed liquor into a stirring device, gradually and continuously adding the wall-broken ganoderma lucidum spore powder into the mixed liquor, continuously stirring the mixed liquor, and gradually heating the mixed liquor to 45-48 ℃ under stirring to obtain ganoderma lucidum spore powder agglomerates;
step five, granulating the agglomerates: putting the conglomerate into a granulator for granulation, wherein the particle size is 10-11 meshes, and obtaining ganoderma lucidum spore powder particles;
step six, drying ganoderma lucidum spore powder particles: drying Ganoderma spore powder in a dryer at 82-88 deg.C for 5-6 hr; the moisture content of the dried spore powder particles is less than or equal to 5.4 percent;
step seven, cooling the ganoderma lucidum spore powder particles: putting the dried spore powder particles into a cooling machine for cooling, controlling the temperature of the cooled spore powder particles to be 48-53 ℃, and cooling for 0.7-1 h;
step eight, supercritical carbon dioxide extraction of ganoderma lucidum spore powder particles: and (2) filling qualified product particles into an extraction kettle, introducing supercritical carbon dioxide fluid, adjusting the pressure of the extraction kettle to 34-35MPa, controlling the temperature of the extraction kettle to 43-48 ℃, and controlling the extraction flow: 600-650Nm 3 Min, extracting for 80-100Min to obtain extract;
and step nine, distilling the extract under reduced pressure: according to the weight ratio of the extract to the purified water of 1: (7-10), pouring the extract into a distillation still, and completely evaporating purified water in the distillation still to obtain the ganoderma lucidum spore oil.
The stirring device used in the third step to the fourth step is a composite stirring device, the composite stirring device comprises a support frame and an electric cabinet, a stirring tank is fixed on the support frame, the stirring tank is composed of a cover body and a tank body, a plurality of support columns are fixed at the upper end of the stirring tank, a storage tank is fixed on the support columns, the side end of the stirring tank is connected with a water inlet pipe, a flow electromagnetic valve is installed on the water inlet pipe, the lower end of the stirring tank is provided with a discharge pipe, a first electric control valve is installed on the discharge pipe, a power mechanism and a discharging mechanism are arranged at the upper end of the stirring tank, a stirring mechanism and a heating mechanism are arranged inside the stirring tank, the lower end of the storage tank is connected with two connecting pipes, a second electric control valve is installed on the connecting pipes, the lower end of each connecting pipe is provided with a quantifying mechanism, one quantifying mechanism is located right above the discharging mechanism, the lower end of the other quantifying mechanism is connected with a guide pipe, and the lower end of the guide pipe is communicated with the inside of the stirring tank.
By adopting the structure, after the second electric control valve is opened, the wall-broken ganoderma lucidum spore powder enters the quantitative mechanism from the material storage tank, after the weight in the quantitative mechanism meets the preset amount, the second electric control valve is closed, then a certain amount of purified water is injected into the stirring tank through the water inlet pipe and the flow electromagnetic valve, then the power mechanism drives the stirring mechanism to stir, the heating mechanism gradually heats the mixture to 30-34 ℃, after the mixture is stirred for a certain time, the blanking mechanism slowly injects the wall-broken ganoderma lucidum spore powder into the stirring tank, the mixture is continuously stirred and gradually heats the mixture to 45-48 ℃, and after the mixture is fully stirred, the conglomerate is taken out from the discharge pipe.
Power unit installs driving motor including fixing the mounting bracket on the agitator tank lid on the mounting bracket, is fixed with drive gear on driving motor's the output shaft, and the agitator tank lid is middle to be rotated and to be provided with driven gear, and installs thrust bearing between driven gear and the agitator tank, and the through-hole has been seted up to driven gear's centre, is fixed with the return bend in the through-hole, and the return bend runs through the lid of agitator tank.
Structure more than adopting, driving motor passes through drive gear, driven gear and return bend and rotates for broken wall glossy ganoderma spore powder through the return bend whereabouts disperses more, improves stirring effect.
Unloading mechanism is including hopper and unloading pipe down, be fixed with a plurality of branches on the agitator tank, the hopper is fixed in the branch upper end down, the unloading pipe is fixed at the hopper lower extreme down, and unloading pipe is just to the upper end opening part of return bend, it violently manages to be fixed with in the middle of the unloading pipe, violently manage the side and be fixed with unloading push rod motor, violently the inside slip of pipe is provided with the carriage release lever, set up a plurality of equidistant distribution's recess on the carriage release lever, the recess is located the one end of carriage release lever, and the length of recess is half of carriage release lever length, be fixed with the center pin in the middle of the carriage release lever, the one end of center pin is fixed with turning gear, the other end rotates and is connected with the connecting block, the other end of connecting block and the output shaft fixed connection of unloading push rod motor, the driven gear upper surface is provided with round and turning gear assorted meshing tooth.
Structure more than adopting, when once stirring, the one end that the recess was not seted up to the carriage release lever can block down the whereabouts of broken wall glossy ganoderma spore powder in the hopper, during the stirring of second time, unloading push rod motor drives the carriage release lever and removes, make the one end that the recess was seted up to the carriage release lever be located hopper below down, and at this moment rotating gear and meshing tooth meshing, driven gear rotates this moment and can drive rotating gear and carriage release lever and rotate, along with the carriage release lever rotates, the recess is with broken wall glossy ganoderma spore powder area income unloading pipe lower extreme gradually, and inside getting into the agitator tank through the return bend, realize slow reinforced function, make broken wall glossy ganoderma spore powder disperse more, and the stirring effect is improved.
Rabbling mechanism includes puddler, first stirring leaf and second stirring leaf, and the lower extreme at the return bend is fixed to the puddler, and first stirring leaf is the heliciform and fixes the outside at the puddler, and second stirring leaf is the heliciform setting in the first stirring leaf outside, is fixed with a plurality of dead levers between second stirring leaf and the puddler, and first stirring leaf and second stirring leaf spiral opposite direction.
Structure more than adopting, first stirring leaf and second stirring leaf can carry out the equidirectional upset with the material in the agitator tank for the material mixes more evenly, improves stirring effect.
The quantifying mechanism comprises a shell fixed at the lower end of the connecting pipe, an upper end opening material storage barrel is arranged inside the shell, a plurality of fixing blocks distributed at equal intervals are fixed between the outer side of the material storage barrel and the inner wall of the shell, a material discharging push rod motor is fixed at the bottom of the material storage barrel, a push plate is fixed on an output shaft of the material discharging push rod motor, the upper surface of the push plate is a conical surface, a weight sensor is embedded at the bottom of the push plate, and a plurality of vibrating motors distributed at equal intervals are fixed on the lower surface of the push plate.
Structure more than adopting, broken wall glossy ganoderma spore powder gets into from the connecting pipe and deposits the feed cylinder in, has the weight of broken wall glossy ganoderma spore powder in the push pedal of weighing sensor detection, and after the weight reached set amount, closed the second automatically controlled valve, then blowing push rod motor is with the push pedal catch bar that makes progress to discharge broken wall glossy ganoderma spore powder all around, making broken wall glossy ganoderma spore powder discharge more thoroughly through vibrating motor.
Heating mechanism includes safety cover, heating wire and temperature sensor, and the safety cover is fixed on the agitator tank inner wall, and the heating wire is around establishing between safety cover and agitator tank lateral wall, and the agitator tank outside is provided with the power supply and connects, and temperature sensor fixes in the agitator tank upper end, and temperature sensor's probe is located inside the agitator tank.
Structure more than adopting, heats the agitator tank through the electric heat silk, and rethread temperature sensor monitors the temperature, guarantees that the temperature is stable.
Compared with the prior art, the treatment process for removing the acid value of the ganoderma lucidum spore oil has the following advantages:
1. the wall-broken ganoderma lucidum spore powder after embrittlement is broken through an ultrafine pulverizer, so that the wall-broken ganoderma lucidum spore powder with the wall-broken rate of more than or equal to 98% can be obtained, and the oil yield of ganoderma lucidum spore oil and the nutrient content of the ganoderma lucidum spore oil are improved.
2. Through compound agitating unit, reduced the consumption that the transportation raw and other materials produced in the production process for the stirring is more quick and even, has not only reduced manufacturing cost, but also has improved production efficiency.
3. The proportion of the ganoderma lucidum spore powder and the purified water in the ganoderma lucidum spore particles is controlled by the composite stirring device, and when supercritical carbon dioxide extraction is carried out, the extraction efficiency is high, and the acid value of the ganoderma lucidum spore oil is effectively reduced.
Drawings
FIG. 1 is a flow chart of the process for preparing ganoderma lucidum spore oil according to the invention;
FIG. 2 is a schematic perspective view of the composite stirring apparatus of the present invention;
FIG. 3 is a schematic view of a partial plan view of the composite stirring apparatus of the present invention;
FIG. 4 is a schematic structural view of the power mechanism and the blanking mechanism of the present invention;
FIG. 5 is a schematic structural view of a blanking mechanism according to the present invention;
FIG. 6 is a schematic view of a partial structure of the blanking mechanism of the present invention;
FIG. 7 is a schematic sectional view of the dosing mechanism of the present invention;
FIG. 8 is a schematic sectional view of the agitation tank of the present invention;
in the figure: 1. a support frame; 2. an electric cabinet; 3. a stirring tank; 4. a support pillar; 5. a material storage tank; 6. a water inlet pipe; 7. a flow rate solenoid valve; 8. a discharge pipe; 9. a first electrically controlled valve; 10. a power mechanism; 1001. a mounting frame; 1002. a drive motor; 1003. a drive gear; 1004. a driven gear; 1005. a thrust bearing; 1006. bending the pipe; 11. a blanking mechanism; 1101. a strut; 1102. feeding a hopper; 1103. a discharging pipe; 1104. a transverse tube; 1105. a travel bar; 1106. a groove; 1107. a central shaft; 1108. a rotating gear; 1109. meshing teeth; 1110. a blanking push rod motor; 1111. connecting blocks; 12. a stirring mechanism; 1201. a stirring rod; 1202. a first stirring blade; 1203. a second stirring blade; 13. a connecting pipe; 14. a second electrically controlled valve; 15. a dosing mechanism; 1501. a housing; 1502. a material storage barrel; 1503. a fixed block; 1504. a discharging push rod motor; 1505. pushing the plate; 1506. a weight sensor; 1507. a vibration motor; 16. a guide tube; 17. a heating mechanism; 1701. a protective cover; 1702. an electric heating wire; 1703. a power supply connector; 1704. a temperature sensor.
Detailed Description
The technical solution of the present patent will be described in further detail with reference to the following embodiments.
Reference will now be made in detail to embodiments of the present patent, examples of which are illustrated in the accompanying drawings, wherein like or similar reference numerals refer to the same or similar elements or elements having the same or similar function throughout. The embodiments described below with reference to the drawings are illustrative only for the purpose of explaining the present patent and are not to be construed as limiting the present patent.
In the description of this patent, it is to be understood that the terms "center," "upper," "lower," "front," "rear," "left," "right," "vertical," "horizontal," "top," "bottom," "inner," "outer," and the like are used in the orientations and positional relationships indicated in the drawings for the convenience of describing the patent and for the simplicity of description, and are not intended to indicate or imply that the referenced devices or elements must have a particular orientation, be constructed and operated in a particular orientation, and are not to be considered limiting of the patent.
In the description of this patent, it is noted that unless otherwise specifically stated or limited, the terms "mounted," "connected," and "disposed" are to be construed broadly and can include, for example, fixedly connected, disposed, detachably connected, disposed, or integrally connected and disposed. The specific meaning of the above terms in this patent may be understood by those of ordinary skill in the art as appropriate.
The first embodiment is as follows:
referring to fig. 1-8, the present embodiment provides a treatment process for removing acid value of ganoderma lucidum spore oil, and the production process comprises the following steps:
step one, embrittlement of ganoderma lucidum spore powder: placing Ganoderma spore powder in a vacuum puffing tank, setting the embrittlement temperature at 100 deg.C, evacuating and drying for 1 hr, evacuating and drying at 80 deg.C;
step two, breaking the wall of ganoderma lucidum spore powder: placing the embrittled ganoderma lucidum spore powder obtained in the step one in an ultrafine pulverizer to obtain wall-broken ganoderma lucidum spore powder with the wall-broken rate of more than or equal to 98%;
step three, stirring the ganoderma lucidum spore powder: mixing wall-broken ganoderma lucidum spore powder and purified water according to a weight ratio of 1: 0.5 introducing into a stirring device, stirring for 2min, and gradually heating to 32 deg.C while stirring to obtain mixed solution;
step four, the ganoderma lucidum spore powder is coalesced; according to the weight ratio of 1: 0.4 taking the mixed solution obtained in the third step and the wall-broken ganoderma lucidum spore powder obtained in the second step, introducing the mixed solution into a stirring device, gradually and continuously adding the wall-broken ganoderma lucidum spore powder into the mixed solution, continuously stirring the mixed solution during mixing, and gradually heating the mixed solution to 46 ℃ during stirring to obtain ganoderma lucidum spore powder agglomerates;
step five, granulating the agglomerates: putting the conglomerate into a granulator for granulation, wherein the particle size is 10-11 meshes, and obtaining ganoderma lucidum spore powder particles;
step six, drying ganoderma lucidum spore powder particles: drying Ganoderma spore powder in a dryer at 85 deg.C for 5 hr; the moisture content of the dried spore powder particles is less than or equal to 5.4 percent;
step seven, cooling ganoderma lucidum spore powder particles: putting the dried spore powder particles into a cooling machine for cooling, controlling the temperature after cooling to be 50 ℃, and cooling for 0.7 h;
step eight, supercritical carbon dioxide extraction of ganoderma lucidum spore powder particles: and (3) filling qualified product particles into an extraction kettle, introducing supercritical carbon dioxide fluid, adjusting the pressure of the extraction kettle to 34-35MPa, controlling the temperature of the extraction kettle to be 45 ℃, and extracting the flow: 620Nm 3 Min, extracting for 90Min to obtain extract liquid;
and step nine, distilling the extract under reduced pressure: according to the weight ratio of the extract to the purified water of 1: 10, pouring the extract into a distillation kettle, and completely evaporating purified water in the distillation kettle to obtain the ganoderma lucidum spore oil.
The stirring device used in the third step and the fourth step is a composite stirring device, the composite stirring device comprises a support frame 1 and an electric cabinet 2, a stirring tank 3 is fixed on the support frame 1, the stirring tank 3 consists of a cover body and a tank body, a plurality of support columns 4 are fixed at the upper end of the stirring tank 3, a material storage tank 5 is fixed on the support columns 4, a water inlet pipe 6 is connected with the side end of the stirring tank 3, a flow electromagnetic valve 7 is installed on the water inlet pipe 6, a discharge pipe 8 is arranged at the lower end of the stirring tank 3, a first electric control valve 9 is installed on the discharge pipe 8, a power mechanism 10 and a blanking mechanism 11 are arranged at the upper end of the stirring tank 3, a stirring mechanism 12 and a heating mechanism 17 are arranged in the stirring tank 3, two connecting pipes 13 are connected at the lower end of the material storage tank 5, a second electric control valve 14 is installed on the connecting pipe 13, a quantifying mechanism 15 is arranged at the lower end of the connecting pipe 13, and one quantifying mechanism 15 is positioned right above the blanking mechanism 11, the lower end of the other quantitative mechanism 15 is connected with a guide pipe 16, and the lower end of the guide pipe 16 is communicated with the interior of the stirring tank 3; after the second electric control valve 14 is opened, the wall-broken ganoderma lucidum spore powder enters the quantitative mechanism 15 from the material storage tank 5, after the weight in the quantitative mechanism 15 meets the preset amount, the second electric control valve 14 is closed, then a certain amount of purified water is injected into the stirring tank 3 through the water inlet pipe 6 and the flow electromagnetic valve 7, then the power mechanism 10 drives the stirring mechanism 12 to stir, the heating mechanism 17 gradually heats the mixture to 32 ℃, after the mixture is stirred for a certain time, the blanking mechanism 11 slowly injects the wall-broken ganoderma lucidum spore powder into the stirring tank 3, the mixture is continuously stirred and gradually heats the mixture to 46 ℃, and after the mixture is fully stirred, the conglomerate is taken out from the discharge pipe 8.
The power mechanism 10 comprises a mounting rack 1001 fixed on the cover body of the stirring tank 3, a driving motor 1002 is mounted on the mounting rack 1001, a driving gear 1003 is fixed on an output shaft of the driving motor 1002, a driven gear 1004 is rotatably arranged in the middle of the cover body of the stirring tank 3, a thrust bearing 1005 is mounted between the driven gear 1004 and the stirring tank 3, a through hole is formed in the middle of the driven gear 1004, a bent pipe 1006 is fixed in the through hole, and the bent pipe 1006 penetrates through the cover body of the stirring tank 3; driving motor 1002 rotates through drive gear 1003, driven gear 1004 and return bend 1006 for broken wall ganoderma lucidum spore powder through the return bend 1006 whereabouts disperses more, improves the stirring effect.
The blanking mechanism 11 comprises a blanking hopper 1102 and a blanking pipe 1103, a plurality of supporting rods 1101 are fixed on the stirring tank 3, the blanking hopper 1102 is fixed at the upper ends of the supporting rods 1101, the blanking pipe 1103 is fixed at the lower end of the blanking hopper 1102, the blanking pipe 1103 faces the opening at the upper end of the bent pipe 1006, the transverse pipe 1104 is fixed in the middle of the blanking pipe 1103, the blanking push rod motor 1110 is fixed at the side end of the transverse pipe 1104, the moving rod 1105 is arranged in the transverse pipe 1104 in a sliding manner, a plurality of grooves 1106 distributed at equal intervals are arranged on the moving rod 1105, the grooves 1106 are positioned at one end of the moving rod 1105, the length of the groove 1106 is half of that of the moving rod 1105, a central shaft 1107 is fixed in the middle of the moving rod 1105, one end of the central shaft 1107 is fixed with a rotating gear 1108, the other end of the central shaft 1107 is rotatably connected with a connecting block 1111, the other end of the connecting block 1111 is fixedly connected with an output shaft of a blanking push rod motor 1110, and the upper surface of the driven gear 1004 is provided with a circle of meshing teeth 1109 matched with the rotating gear 1108; when the stirring of once, the one end that recess 1106 was not seted up to carriage release lever 1105 can block down the whereabouts of broken wall glossy ganoderma spore powder in the hopper 1102, during the stirring of second time, unloading push rod motor 1110 drives carriage release lever 1105 and removes, make the one end that recess 1106 was seted up to carriage release lever 1105 be located hopper 1102 below down, and rotating gear 1108 and meshing tooth 1109 meshing this moment, driven gear 1004 rotates this moment and can drive rotating gear 1108 and carriage release lever 1105 and rotate, along with carriage release lever 1105 rotates, recess 1106 takes broken wall glossy ganoderma spore powder into unloading pipe 1103 lower extreme gradually, and it is inside to get into agitator tank 3 through return bend 1006, realize slow reinforced function, make broken wall glossy ganoderma spore powder disperse more, improve the stirring effect.
The stirring mechanism 12 comprises a stirring rod 1201, a first stirring blade 1202 and a second stirring blade 1203, the stirring rod 1201 is fixed at the lower end of the bent pipe 1006, the first stirring blade 1202 is fixed at the outer side of the stirring rod 1201 in a spiral shape, the second stirring blade 1203 is arranged at the outer side of the first stirring blade 1202 in a spiral shape, a plurality of fixing rods are fixed between the second stirring blade 1203 and the stirring rod 1201, and the spiral directions of the first stirring blade 1202 and the second stirring blade 1203 are opposite; first stirring leaf 1202 and second stirring leaf 1203 can carry out not equidirectional upset with the interior material of agitator tank 3 for the material mixes more evenly, improves stirring effect.
The quantitative mechanism 15 comprises a shell 1501 fixed at the lower end of the connecting pipe 13, a storage cylinder 1502 with an opening at the upper end is arranged in the shell 1501, a plurality of fixing blocks 1503 which are distributed at equal intervals are fixed between the outer side of the storage cylinder 1502 and the inner wall of the shell 1501, a discharging push rod motor 1504 is fixed at the bottom of the storage cylinder 1502, a push plate 1505 is fixed on an output shaft of the discharging push rod motor 1504, the upper surface of the push plate 1505 is a conical surface, a weight sensor 1506 is embedded at the bottom of the push plate 1505, and a plurality of vibrating motors 1507 which are distributed at equal intervals are fixed on the lower surface of the push plate 1505; broken wall ganoderma lucidum spore powder gets into storage cylinder 1502 from connecting pipe 13 in, has weight sensor 1506 to detect the weight of broken wall ganoderma lucidum spore powder on push pedal 1505, and after the weight reached the set amount, close second automatically controlled valve 14, then blowing push rod motor 1504 pushes up the push pedal 1505 push rod to discharge broken wall ganoderma lucidum spore powder all around, make broken wall ganoderma lucidum spore powder discharge more thoroughly through vibrating motor 1507.
The heating mechanism 17 comprises a protective cover 1701, a heating wire 1702 and a temperature sensor 1704, wherein the protective cover 1701 is fixed on the inner wall of the stirring tank 3, the heating wire 1702 is wound between the protective cover 1701 and the side wall of the stirring tank 3, a power supply connector 1703 is arranged on the outer side of the stirring tank 3, the temperature sensor 1704 is fixed at the upper end of the stirring tank 3, and a probe of the temperature sensor 1704 is positioned in the stirring tank 3; agitator tank 3 is heated through heating wire 1702, and the temperature is monitored through temperature sensor 1704, guarantees that the temperature is stable.
The fixing modes are all the most common fixing connection modes in the field, such as welding, bolt connection, interference fit and the like; the above electrical components, such as the driving motor 1002, the first electrical control valve 9, the second electrical control valve 14, the weight sensor 1506, the vibration motor 1507, the blanking push rod motor 1110, the blanking push rod motor 1504, the temperature sensor 1704, etc., are all prior art products, and can be directly purchased and used in the market, and the detailed principle is not repeated.
After the second electric control valve 14 is opened, the wall-broken ganoderma lucidum spore powder enters the storage cylinder 1502 from the connecting pipe 13, the weight of the wall-broken ganoderma lucidum spore powder on the push plate 1505 is detected by the weight sensor 1506, after the weight reaches a set amount, the second electric control valve 14 is closed, then the discharge push rod motor 1504 pushes the push plate 1505 upwards to push the rod, the wall-broken ganoderma lucidum spore powder is discharged to the periphery, the wall-broken ganoderma lucidum spore powder is more thoroughly discharged by the vibration motor 1507, then a certain amount of purified water is injected into the stirring tank 3 through the water inlet pipe 6 and the flow electromagnetic valve 7, then the driving motor 1002 is driven to drive the stirring rod 1201 to stir, the first stirring blade 1202 and the second stirring blade 1203 can overturn the materials in the stirring tank 3 in different directions, the materials are more uniformly mixed, the stirring effect is improved, the heating wires 1702 are gradually heated to 32 ℃, after stirring for a certain time, the blanking push rod 1110 drives the moving rod 1105 to move, make the movable rod 1105 offer the one end of recess 1106 and be located hopper 1102 below down, and rotating gear 1108 and meshing tooth 1109 meshing this moment, driven gear 1004 rotates this moment and can drive rotating gear 1108 and movable rod 1105 and rotate, along with movable rod 1105 rotates, recess 1106 takes broken wall ganoderma lucidum spore powder into unloading pipe 1103 lower extreme gradually, and get into agitator tank 3 inside through return bend 1006, continue the stirring, and heat to 46 ℃ gradually, after the intensive mixing, the conglomerate is taken out from discharging pipe 8.
The composite stirring device can continuously stir twice, does not need to transport materials, cannot cause heat loss, can reduce power consumption, has the advantages of uniform blanking and rapid stirring, stable temperature and good stirring effect, not only saves the time spent in the stirring process, but also can ensure stable mixing, uniformly stir and mix and improve the mixing efficiency.
Example two:
compared with the first embodiment, the second embodiment adopts the same processing steps as the first embodiment, except that:
in the second embodiment, the existing stirring equipment is adopted for production, two times of stirring are separately carried out, linkage is lacked, the temperature and the time cannot be stably controlled, and when materials are transported between two times of stirring, the heat and the water are seriously lost, the stirring effect is poor, the oil yield is reduced, the working hours are prolonged, and the prepared ganoderma lucidum spores have higher acid value.
Example three:
the third embodiment is different from the first embodiment in that:
the third embodiment adopts the existing process and the existing equipment to produce:
firstly, breaking the wall of ganoderma lucidum spore powder by using a wall breaking machine to obtain the ganoderma lucidum spore powder with the wall breaking rate of more than or equal to 80%;
step two, performing dry granulation on the wall-broken ganoderma lucidum spore powder by using a granulator to obtain ganoderma lucidum spore powder particles with the particle size of 13-14 meshes;
step three, filling ganoderma lucidum spore powder particles and ganoderma lucidum spore powder particles into an extraction kettle, introducing supercritical carbon dioxide fluid, adjusting the pressure of the extraction kettle to 34-35MPa, adjusting the temperature of the extraction kettle to 45 ℃, and extracting at a flow rate: 600-650Nm 3 Min, extracting for 120Min to obtain extract liquid;
step four, according to the weight ratio of the extract to the purified water of 1: 10, pouring the extract into a distillation kettle, and completely evaporating purified water in the distillation kettle to obtain the ganoderma lucidum spore oil.
Example four:
example four compared with example one, example four and example one used the same process steps and production equipment, except that:
the weight ratio of the wall-broken ganoderma lucidum spore powder to the purified water in the third step is 1: 0.3.
the weight ratio of the mixed liquid to the wall-broken ganoderma lucidum spore powder in the fourth step is 1: 0.5.
the ganoderma lucidum spore oil extracts prepared in the first to fourth examples were subjected to comparative experiments: wherein the comparison standard is as follows: production efficiency (production amount per unit time) and power consumption per unit and properties of ganoderma lucidum spore oil extract: oil yield, acid value, peroxide value.
The experimental table is as follows (table 1):
TABLE 1
Through the embodiment that table 1 can be clear, adopt compound agitating unit can effectively reduce the electric quantity consumption to promote production efficiency.
EXAMPLE one table for testing acid value of Ganoderma spore oil (Table 2)
| Weight (g) | Titration volume (ml) | Acid value (mg/g) |
| 5.2136 | 2.13 | 2.54 |
| 5.2506 | 2.18 | 2.59 |
| 5.2314 | 2.16 | 2.62 |
| 5.1996 | 2.09 | 2.55 |
TABLE 2 acid value test Table for Ganoderma spore oil of example two (TABLE 3)
| Weight (g) | Titration volume (ml) | Acid value (mg/g) |
| 5.2366 | 2.14 | 2.76 |
| 5.2031 | 2.20 | 2.96 |
| 5.4001 | 2.23 | 2.79 |
| 5.2396 | 2.19 | 2.82 |
TABLE 3 acid value test Table for Ganoderma spore oil of example III (TABLE 4)
| Weight (g) | Titration volume (ml) | Acid value (mg/g) |
| 5.0136 | 2.15 | 5.21 |
| 5.2154 | 2.08 | 6.92 |
| 5.2309 | 2.30 | 5.47 |
| 5.3006 | 2.11 | 4.92 |
TABLE 4 acid value test Table for Ganoderma spore oil of example four (TABLE 5)
TABLE 5 comparison of Ganoderma spore oil data prepared in examples one to four (Table 6)
| Group of | Time of extraction | Acid value | Wall breaking rate | Oil yield |
| Example one | 90min | ≤2.65 | ≥98％ | ≥31％ |
| Example two | 100min | ≤3.00 | ≥98％ | ≥26％ |
| EXAMPLE III | 120min | ≥4.50 | ≥80％ | ≤22％ |
| Example four | 90min | ≤2.80 | ≥98％ | ≥28％ |
TABLE 6
Comparing tables 2 to 6, the acid value of the extracted ganoderma lucidum spore oil is obviously reduced and the oil yield is obviously improved by the process of the invention.
By adopting the process, the acid value of the ganoderma lucidum spore oil can be effectively reduced, the product quality and the oil yield of the collar spore oil are improved, the consumption of raw materials transferred in the production process is reduced through the composite stirring device, the stirring is quicker and more uniform, the production cost is reduced, the production efficiency is also improved, and meanwhile, the composite stirring device can better control the proportion of ganoderma lucidum spore powder and purified water in ganoderma lucidum spore particles, so that the extraction efficiency is high when the ganoderma lucidum spore particles are subjected to supercritical carbon dioxide extraction.
Although the preferred embodiments of the present patent have been described in detail, the present patent is not limited to the above embodiments, and various changes can be made without departing from the spirit of the present patent within the knowledge of those skilled in the art.
Claims (9)
1. A treatment process for removing acid value of ganoderma lucidum spore oil is characterized by comprising the following production process steps:
step one, embrittlement of ganoderma lucidum spore powder: placing Ganoderma spore powder in a vacuum puffing tank, setting embrittlement temperature at 97-102 deg.C, evacuating and drying for 0.8-1.1h, and evacuating and drying at 76-82 deg.C;
step two, breaking the wall of ganoderma lucidum spore powder: placing the embrittled ganoderma lucidum spore powder obtained in the step one in an ultrafine pulverizer to obtain wall-broken ganoderma lucidum spore powder with the wall-broken rate of more than or equal to 98%;
step three, stirring the ganoderma lucidum spore powder: mixing wall-broken ganoderma lucidum spore powder and purified water according to a weight ratio of 1: (0.3-0.6) introducing into a stirring device, stirring for 2-3min, and gradually heating to 30-34 deg.C while stirring to obtain a mixed solution;
step four, the ganoderma lucidum spore powder is coalesced; according to the weight ratio of 1: (0.3-0.5) taking the mixed liquor obtained in the third step and the wall-broken ganoderma lucidum spore powder obtained in the second step, introducing the mixed liquor into a stirring device, gradually and continuously adding the wall-broken ganoderma lucidum spore powder into the mixed liquor, continuously stirring the mixed liquor, and gradually heating the mixed liquor to 45-48 ℃ under stirring to obtain ganoderma lucidum spore powder agglomerates;
step five, granulating the agglomerates: putting the conglomerate into a granulator for granulation, wherein the particle size is 10-11 meshes, and obtaining ganoderma lucidum spore powder particles;
step six, drying ganoderma lucidum spore powder particles: drying Ganoderma spore powder in a dryer at 82-88 deg.C for 5-6 hr; the moisture content of the dried spore powder particles is less than or equal to 5.4 percent;
step seven, cooling ganoderma lucidum spore powder particles: putting the dried spore powder particles into a cooling machine for cooling, controlling the temperature of the cooled spore powder particles to be 48-53 ℃, and cooling for 0.7-1 h;
step eight, supercritical carbon dioxide extraction of ganoderma lucidum spore powder particles: and (2) filling qualified product particles into an extraction kettle, introducing supercritical carbon dioxide fluid, adjusting the pressure of the extraction kettle to 34-35MPa, controlling the temperature of the extraction kettle to 43-48 ℃, and controlling the extraction flow: 600-650Nm 3 Min, extracting for 80-100Min to obtain extractive solution;
and step nine, distilling the extract under reduced pressure: according to the weight ratio of the extract to the purified water of 1: (7-10), pouring the extract into a distillation still, and completely evaporating purified water in the distillation still to obtain the ganoderma lucidum spore oil.
2. The treatment process for removing acid value of ganoderma lucidum spore oil as claimed in claim 1, wherein the weight ratio of the wall-broken ganoderma lucidum spore powder to the purified water in the third step is 1: 0.5.
3. the treatment process for removing acid value of ganoderma lucidum spore oil according to claim 1, wherein the weight ratio of the mixed solution and the wall-broken ganoderma lucidum spore powder in the fourth step is 1: 0.4.
4. the treatment process for removing acid value of ganoderma lucidum spore oil according to any one of claims 1 to 3, wherein the stirring device used in the third step to the fourth step is a composite stirring device, the composite stirring device comprises a support frame (1) and an electric cabinet (2), a stirring tank (3) is fixed on the support frame (1), the stirring tank (3) consists of a cover body and a tank body, a plurality of support columns (4) are fixed at the upper end of the stirring tank (3), a storage tank (5) is fixed on each support column (4), a water inlet pipe (6) is connected to the side end of the stirring tank (3), a flow electromagnetic valve (7) is installed on the water inlet pipe (6), a discharge pipe (8) is arranged at the lower end of the stirring tank (3), a first electric control valve (9) is installed on the discharge pipe (8), a power mechanism (10) and a blanking mechanism (11) are arranged at the upper end of the stirring tank (3), stirring mechanism (12) and heating mechanism (17) are equipped with in agitator tank (3), the lower extreme of storage tank (5) is connected with two connecting pipes (13), install second automatically controlled valve (14) on connecting pipe (13), the lower extreme of connecting pipe (13) is equipped with dosing mechanism (15), dosing mechanism (15) are located unloading mechanism (11) directly over, the lower extreme of another dosing mechanism (15) is connected with stand pipe (16), and stand pipe (16) lower extreme and agitator tank (3) inside intercommunication.
5. The treatment process for removing acid value of ganoderma lucidum spore oil according to claim 4, wherein the power mechanism (10) comprises a mounting frame (1001) fixed on a cover body of the stirring tank (3), a driving motor (1002) is mounted on the mounting frame (1001), a driving gear (1003) is fixed on an output shaft of the driving motor (1002), a driven gear (1004) is rotatably arranged in the middle of the cover body of the stirring tank (3), a thrust bearing (1005) is mounted between the driven gear (1004) and the stirring tank (3), a through hole is formed in the middle of the driven gear (1004), a bent pipe (1006) is fixed in the through hole, and the bent pipe (1006) penetrates through the cover body of the stirring tank (3).
6. The treatment process for treating the deacidification value of the ganoderma lucidum spore oil according to claim 5, wherein the blanking mechanism (11) comprises a blanking hopper (1102) and a blanking pipe (1103), a plurality of supporting rods (1101) are fixed on the stirring tank (3), the blanking hopper (1102) is fixed at the upper ends of the supporting rods (1101), the blanking pipe (1103) is fixed at the lower end of the blanking hopper (1102), the blanking pipe (1103) is opposite to the opening at the upper end of the bent pipe (1006), a transverse pipe (1104) is fixed in the middle of the blanking pipe (1103), a blanking push rod motor (1110) is fixed at the side end of the transverse pipe (1104), a moving rod (1105) is arranged in the transverse pipe (1104) in a sliding manner, a plurality of grooves (1106) which are distributed at equal intervals are formed in the moving rod (1105), the grooves (1106) are positioned at one end of the moving rod (1105), the length of the grooves (1106) is half of the length of the moving rod (1105), a central shaft (1107) is fixed in the middle of the moving rod (1105), one end of the central shaft (1107) is fixed with a rotating gear (1108), the other end of the central shaft is rotatably connected with a connecting block (1111), the other end of the connecting block (1111) is fixedly connected with an output shaft of the blanking push rod motor (1110), and the upper surface of the driven gear (1004) is provided with a circle of meshing teeth (1109) matched with the rotating gear (1108).
7. The treatment process for removing acid value of ganoderma lucidum spore oil according to claim 5, wherein the stirring mechanism (12) comprises a stirring rod (1201), a first stirring blade (1202) and a second stirring blade (1203), the stirring rod (1201) is fixed at the lower end of the bent pipe (1006), the first stirring blade (1202) is fixed at the outer side of the stirring rod (1201) in a spiral shape, the second stirring blade (1203) is arranged at the outer side of the first stirring blade (1202) in a spiral shape, a plurality of fixing rods are fixed between the second stirring blade (1203) and the stirring rod (1201), and the spiral directions of the first stirring blade (1202) and the second stirring blade (1203) are opposite.
8. The treatment process for removing acid value of ganoderma lucidum spore oil according to claim 4, wherein the quantifying mechanism (15) comprises a shell (1501) fixed at the lower end of the connecting pipe (13), a storage barrel (1502) with an opening at the upper end is arranged in the shell (1501), a plurality of fixing blocks (1503) which are distributed at equal intervals are fixed between the outer side of the storage barrel (1502) and the inner wall of the shell (1501), a discharging push rod motor (1504) is fixed at the bottom of the storage barrel (1502), a push plate (1505) is fixed on an output shaft of the discharging push rod motor (1504), the upper surface of the push plate (1505) is a conical surface, a weight sensor (1506) is embedded at the bottom of the push plate (1505), and a plurality of vibrating motors (1507) which are distributed at equal intervals are fixed on the lower surface of the push plate (1505).
9. The treatment process for removing acid value of ganoderma lucidum spore oil according to claim 4, wherein the heating mechanism (17) comprises a protective cover (1701), a heating wire (1702) and a temperature sensor (1704), the protective cover (1701) is fixed on the inner wall of the stirring tank (3), the heating wire (1702) is wound between the protective cover (1701) and the side wall of the stirring tank (3), a power supply connector (1703) is arranged on the outer side of the stirring tank (3), the temperature sensor (1704) is fixed at the upper end of the stirring tank (3), and a probe of the temperature sensor (1704) is positioned inside the stirring tank (3).
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