CN114903800A - Three-layer hair care composition and preparation method thereof - Google Patents
Three-layer hair care composition and preparation method thereof Download PDFInfo
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- CN114903800A CN114903800A CN202110833021.1A CN202110833021A CN114903800A CN 114903800 A CN114903800 A CN 114903800A CN 202110833021 A CN202110833021 A CN 202110833021A CN 114903800 A CN114903800 A CN 114903800A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/03—Liquid compositions with two or more distinct layers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
Abstract
The invention belongs to the technical field of A61K8/34 cosmetics, and particularly relates to a three-layer hair care composition and a preparation method thereof. A three-layer hair care composition comprises an upper layer liquid, a middle layer liquid and a lower layer liquid; the preparation raw material of the upper layer liquid comprises polysiloxane; the preparation raw material of the middle layer liquid comprises a hydroxyl-containing compound; the preparation raw materials of the lower layer liquid comprise ester substances and/or modified polysiloxane. According to different raw material dosage ratios, the hair care composition can deeply nourish and repair damaged hair, the hair is soft and moist after the hair care composition is used, smooth and easy to comb, and the problems of frizzy hair, furcation, dry hair and the like can be immediately and obviously relieved; the high temperature can be isolated, the hot air damage such as high-temperature blowing and scalding and electric roll modeling can be effectively relieved, static electricity is prevented, hair explosion is avoided, and the light damage caused by strong sunlight irradiation can be reduced; and the hair cream is light in texture, easy to absorb, free of greasy and heavy feeling, and free of hand washing, and the hair is not sticky after use.
Description
Technical Field
The invention belongs to the technical field of A61K8/34 cosmetics, and particularly relates to a three-layer hair care composition and a preparation method thereof.
Background
With the improvement of living standard and consumption level of people, consumers also begin to pay more attention to the appearance or mental satisfaction of the consumers, so that perm, hair dyeing, hair care and the like become some more concerned aspects of modern people.
However, with the occurrence of activities such as perming and dyeing, the hair quality of people is damaged to a certain extent, so that the requirements of perming and dyeing of consumers are met, and meanwhile, the maintenance and the moistening of the hair are ensured, and the problem which needs to be solved urgently at the present stage is also solved.
The Chinese patent with patent publication number CN110812252A discloses a three-layer hair care composition and a preparation method and application thereof, in the disclosed patent, the combination of plant base oil, siloxane and polyalcohol is adopted to ensure that the prepared hair care composition has rancidity resistance, and the hair flexibility and scalp moistening are improved, but 0.01-2% of inorganic salt is added into the preparation raw materials disclosed by the disclosed patent, so that the viscosity and thickening effect of the system can be improved, the sticky effect can be caused when the hair care composition is used on the hair surface, the sticky feeling on the hair surface or the hand is caused when the hair care composition is used, and the popularity is reduced.
In order to further improve the excellent hair care effect of the hair care composition and better experience of use, the formula and effect of the hair care composition still need to be further optimized, and the hair care composition still remains a challenge in the current research stage.
Disclosure of Invention
In order to solve the above technical problems, the present invention provides in a first aspect a three-layer hair care composition comprising an upper layer liquid, a middle layer liquid and a lower layer liquid;
the preparation raw material of the upper layer liquid comprises polysiloxane;
the preparation raw material of the middle layer liquid comprises a hydroxyl-containing compound;
the preparation raw materials of the lower layer liquid comprise ester substances and/or modified polysiloxane.
In some preferred embodiments, the upper layer liquid is 2-70%, the lower layer liquid is 2-70%, and the middle layer liquid makes up the balance to 100% by weight.
In some preferred embodiments, the polysiloxane comprises at least one of polydimethylsiloxane, aminosiloxane, cyclotetrasiloxane, cyclopentadimethylsiloxane, and cyclohexasiloxane.
In some preferred embodiments, the polysiloxane has a kinematic viscosity of 1 to 1000000 cst.
In some preferred embodiments, the polysiloxane is selected from at least one polydimethylsiloxane having a kinematic viscosity of 1.5cst, 5cst, 10cst, 350cst, 60000cst, 10000000 cst.
Further preferably, the polysiloxane is selected from polydimethylsiloxane having a kinematic viscosity of 60000cst and 10000000 cst.
More preferably, the weight ratio of the polydimethylsiloxane with the kinematic viscosity of 60000cst and 10000000cst is 1: (0.5-3).
Polydimethylsiloxane, available from wacker chemical (china) ltd.
In some preferred embodiments, the raw material for preparing the upper layer liquid comprises polydimethylsiloxane with the kinematic viscosity of 60000cst and 10000000cst, cyclopentadecylmethicone and cyclohexasiloxane.
In some preferred embodiments, the starting material for the preparation of the upper liquid further comprises dimethiconol.
Dimethiconol, available from wacker chemical (china) ltd.
In some preferred embodiments, the hydroxyl containing compound comprises at least one of water, 1, 3-propanediol, glycerol, 1, 3-butanediol, pentanediol, hexanediol, dipropylene glycol, polyglycerol, and polyethylene glycol.
In some preferred embodiments, the degree of polymerization of the polyglycerol is from 3 to 10.
In some preferred embodiments, the polyethylene glycol has a degree of polymerization of 4 to 32.
In some preferred embodiments, the polyethylene glycol is selected from at least one of polyethylene glycol-4, polyethylene glycol-10, and polyethylene glycol 32.
Wherein "polyethylene glycol-4" represents polyethylene glycol with a degree of polymerization of 4.
More preferably, the degree of polymerization of the polyglycerol is 10.
The polyglycerin having a polymerization degree of 10 is represented as polyglycerin-10, and the polyglycerin having a polymerization degree of 3 is represented as polyglycerin-3.
More preferably, the raw materials for preparing the middle layer liquid are water, 1, 3-propanediol and polyglycerol-10.
In some preferred embodiments, the preparation feedstock further comprises a conditioning agent and a pigment.
In some preferred embodiments, the raw materials for making the middle layer liquid further include a conditioning agent; the conditioning agent is at least one of polyquaternium-11, polyquaternium-28, polyquaternium-55 and polyquaternium-69.
Further preferably, the conditioning agent is polyquaternium-55 and polyquaternium-69.
More preferably, the weight ratio of the polyquaternium-55 to the polyquaternium-69 is 1: 1.
in some preferred embodiments, the raw materials for the preparation of the middle layer liquid are water, 1, 3-propanediol, polyglycerol-10, polyquaternium-55 and polyquaternium-69.
In some preferred embodiments, the raw materials for preparing the lower layer liquid comprise one or more compounds selected from sucrose acetate isobutyrate, tributyl acetylcitrate, bis-diethoxydiethylene glycol cyclohexane 1,4-dicarboxylate, diethoxyethyl succinate, dimethyldiphenyl polydimethylsiloxane, trimethylpentaphenyl trisiloxane, tetramethyltetraphenyl trisiloxane and trimethylsiloxyphenyl polydimethylsiloxane.
Further preferably, the raw materials for preparing the lower layer liquid comprise sucrose acetate isobutyrate, bis-diethoxy diethylene glycol cyclohexane 1,4-dicarboxylate, diethoxyethyl succinate and dimethyl diphenyl polydimethylsiloxane.
Bis-diethoxydiethylene glycol cyclohexane 1,4-dicarboxylate, english name: BIS-ETHOXYDIGLYCOL cycloxetane 1, 4-DICARBOXYLATE.
In the experimental process, the applicant is researched and found through a large number of creative experiments, in the system, when the sucrose acetate isobutyrate, bis-diethoxydiethylene glycol cyclohexane 1,4-dicarboxylate, diethoxyethyl succinate and dimethyl diphenyl polydimethylsiloxane are used as lower layer liquid and can be coated on the uppermost layer of hands for the surface of hair in a spreading mode during use, the lower layer liquid acts on the hair firstly, then a protective film is formed on the surface of the hair, when the system is used for hot air and the like such as high-temperature blowing and ironing, electric roll modeling and the like, the active hydroxyl, carboxyl, ester, silanol and other structures exist in the system, the active hydroxyl, carboxyl, ester, silanol and other structures absorb heat due to decomposition when the system is used for high-temperature action, the damage to the hair due to high temperature is reduced, the phenomenon that the hair is damaged excessively and 'hair explosion' is avoided, and the light damage caused by strong sunlight irradiation can also be reduced.
In some preferred embodiments, the upper layer liquid and the lower layer liquid further comprise 0.0001 wt% of oil-soluble pigment.
In some preferred embodiments, the middle layer liquid further comprises 0.0001-0.0005 wt% of water-soluble pigment.
It should be noted that the water-soluble pigments and the oil-soluble pigments described in the present application are all common raw materials in the art, and are not limited at all.
In a second aspect, the present invention provides a process for the preparation of a three-layer hair care composition comprising the steps of:
mixing the above materials at 20-35 deg.C, stirring, and standing.
Has the advantages that: the hair care composition provided by the invention has the following advantages:
the invention selects three hair care raw materials which are not mutually soluble and contain at least one polysiloxane, at least one hydroxyl compound (water or at least one polyalcohol) and at least one grease or modified polysiloxane with special solubility, and the three raw materials are compounded to effectively combine the smoothness of silicone oil, the moisture retention of a water-alcohol system and the brightening property of special grease, so that the problems of damaged, rough, dry and dull hair and the like can be solved simultaneously after single use. Meanwhile, after the cationic conditioning polymer is added into the hydroxyl-containing compound, the hairdressing effects such as frizziness resistance, hair styling and the like can be further provided. According to the different proportion of the raw materials, the hair care composition can deeply nourish and repair damaged hair, the hair is soft and moist after the hair care composition is used, smooth and easy to comb, and the problems of frizziness, furcation, withering and the like can be immediately and obviously relieved; the high temperature can be isolated, the hot air damage such as high-temperature blowing and ironing, electric roll modeling and the like can be effectively relieved, static electricity is prevented, hair explosion in a frightened manner is avoided, and the light damage caused by strong sunlight irradiation can be reduced; and the hair cream is light in texture, easy to absorb, free of greasy and heavy feeling, and free of hand washing, and the hair is not sticky after use.
Detailed Description
Example 1
A three-layer hair care composition comprises an upper layer liquid, a middle layer liquid and a lower layer liquid;
the preparation raw materials of the upper layer liquid comprise the following components in percentage by weight:
20% of polydimethylsiloxane with the kinematic viscosity of 1.5cst, 20% of polydimethylsiloxane with the kinematic viscosity of 60000cst and 0.0001% of oil-soluble pigment;
the preparation raw materials of the lower layer comprise the following components in percentage by weight:
20% sucrose acetate isobutyrate, 10% tributyl acetyl citrate, 10% dimethyl diphenyl polydimethylsiloxane, 0.0001% oil-soluble pigment;
the preparation raw materials of the middle-layer liquid comprise the following components in percentage by weight:
2% of 1, 3-propylene glycol, 2% of glycerol, 2% of 1, 3-butanediol, 2% of pentanediol, 2% of polyglycerol-3, 0.0001% of water-soluble pigment and the balance of water to 100%.
Polydimethylsiloxane, available from wacker chemical (china) ltd; polyglycerol-3, available from KCI Limited, korea;
a process for preparing a three-layer hair care composition comprising the steps of:
mixing the above materials at 28 deg.C, stirring, and standing.
Example 2
A three-layer hair care composition comprises an upper layer liquid, a middle layer liquid and a lower layer liquid;
the preparation raw materials of the upper layer liquid comprise the following components in percentage by weight:
10% of polydimethylsiloxane with a kinematic viscosity of 5cst, 10% of polydimethylsiloxane with a kinematic viscosity of 10cst, 10% of polydimethylsiloxane with a kinematic viscosity of 350cst, 10% of polydimethylsiloxane with a kinematic viscosity of 10000000cst and 0.0001% of oil-soluble pigment;
the preparation raw materials of the lower layer comprise the following components in percentage by weight:
10% bis-diethoxydiethylene glycol cyclohexane 1,4-dicarboxylate, 10% diethoxyethyl succinate, 10% dimethyldiphenyl polydimethylsiloxane, 5% tetramethyltetraphenyl trisiloxane, 10% trimethylsiloxyphenyl polydimethylsiloxane, 0.0001% oil-soluble pigment;
the preparation raw materials of the middle-layer liquid comprise the following components in percentage by weight:
3% of hexanediol, 3% of dipropylene glycol, 4% of polyglycerol-10, 10% of polyethylene glycol-4, 5% of polyethylene glycol-10, 3% of polyethylene glycol-32, 0.0001% of water-soluble pigment and the balance of water to 100%.
Polydimethylsiloxane, available from wacker chemical (china) ltd; polyglycerol-10, available from KCI Limited, korea; polyethylene glycol-4, polyethylene glycol-10, polyethylene glycol-32, available from Haoist (Hallstar) Inc.
A method of making a three-layer hair care composition comprising the steps of:
mixing the above materials at 28 deg.C, stirring, and standing.
Example 3
A three-layer hair care composition comprises an upper layer liquid, a middle layer liquid and a lower layer liquid;
the preparation raw materials of the upper layer liquid comprise the following components in percentage by weight:
15% of polydimethylsiloxane with the kinematic viscosity of 10000000cst, 5% of dimethiconol, 20% of cyclotetrapolydimethylsiloxane and 0.0001% of oil-soluble pigment;
the preparation raw materials of the lower layer comprise the following components in percentage by weight:
sucrose acetate isobutyrate 5%, tributyl acetyl citrate 4%, bis-diethoxy diethylene glycol cyclohexane 1,4-dicarboxylate 4%, diethoxyethyl succinate 5%, trimethylpentaphenyl trisiloxane 20%, oil-soluble pigments 0.0001%;
the preparation raw materials of the middle-layer liquid comprise the following components in percentage by weight:
5% of glycerol, 5% of 1, 3-butanediol, 5% of hexanediol, 1% of polyquaternium-28, 0.00002% of water-soluble pigment and the balance of water to 100%.
Polydimethylsiloxane, available from wacker chemical (china) ltd.
A process for preparing a three-layer hair care composition comprising the steps of:
mixing the above materials at 28 deg.C, stirring, and standing.
Example 4
A three-layer hair care composition comprises an upper layer liquid, a middle layer liquid and a lower layer liquid;
the preparation raw materials of the upper layer liquid comprise the following components in percentage by weight:
5% of polydimethylsiloxane with the kinematic viscosity of 60000cst, 5% of polydimethylsiloxane with the kinematic viscosity of 10000000cst, 15% of cyclopentadimethylsiloxane, 15% of cyclohexasiloxane and 0.0001% of oil-soluble pigment;
the preparation raw materials of the lower layer comprise the following components in percentage by weight:
10% sucrose acetate isobutyrate, 5% bis-diethoxydiol cyclohexane 1,4-dicarboxylate, 2% diethoxyethyl succinate, 6% dimethyldiphenyl polydimethylsiloxane, 0.0001% oil-soluble pigment;
the preparation raw materials of the middle layer liquid comprise the following components in percentage by weight:
10% of 1, 3-propylene glycol, 10% of polyglycerol-10, 0.0003% of water-soluble pigment and the balance of water to 100%.
Polydimethylsiloxane, available from wacker chemical (china) ltd; polyglycerol-10, available from KCI Limited, korea.
A process for preparing a three-layer hair care composition comprising the steps of:
mixing the above materials at 28 deg.C, stirring, and standing.
Example 5
A three-layer hair care composition is the same as that in example 4, and is different from example 4 in that the preparation raw materials of a middle-layer liquid further comprise 1% of polyquaternium-55 and 1% of polyquaternium-69, and the balance of water is up to 100%.
Example 6
A three-layer hair care composition according to the same embodiment as that of example 5, except that:
the weight percentage of the polydimethylsiloxane with the kinematic viscosity of 60000cst in the preparation raw material of the upper layer liquid is 10 percent;
the balance of raw material water for preparing the middle layer liquid is supplemented to 100 percent.
Example 7
A three-layer hair care composition according to the same embodiment as that of example 5, except that:
the weight percentage of the cyclopenta dimethyl siloxane in the upper layer liquid preparation raw material is 10 percent;
the weight percentage of 1, 3 propylene glycol in the middle layer liquid preparation raw material is 15%, and the balance of water is supplemented to 100%.
Example 8
A three-layer hair care composition according to the same embodiment as that of example 5, except that:
the weight percentage of dimethyl diphenyl polydimethylsiloxane in the lower layer liquid preparation raw material is 11%;
the balance of the raw material water for preparing the middle layer liquid is 100 percent.
Performance test
1. Hair smoothness test:
the dry hair friction, i.e., hair smoothness, of the hair is measured by the instrument DIASTRON. The damaged hair bundle is fixed on a flat plate end to end, a cylindrical rubber probe slides back and forth over the hair bundle at the speed of 150mm/min, the surface friction force J of the hair can be directly read, and the lower the numerical value, the better the smoothness of the hair is.
2. Hair softness test:
tress softness was measured by the INSTRON & SLT module. In the test process, the hair bundle to be tested is pulled up at the speed of 1000mm/min, and the total energy of the hair stripped from the sleeve in the SLT component is recorded through the sensor. During the experiment, the total energy (Equiescence and Erotation) of the hair peeled from the sleeve is measured under 2 states of the sleeve being static and the sleeve freely rotating respectively, the Erotation represents the softness of the hair, the unit is gf.mm, and the smaller the value, the softer the hair.
3. Hair gloss test:
30 healthy women aged 18-40 years were recruited. The hair care compositions prepared in examples 1-8 were applied to the hair in sequence, and each example was tested for 1 week before evaluation and scoring of the gloss of the hair after application, with a score of 0-10: 0 pole difference; 10 is excellent.
The results of the performance tests are reported in table 1 below.
Table 1:
| experiment of | Hair surface friction force J | Softness/gf.mm of hair | Hair shine score |
| Example 1 | 0.029 | 2380 | 6 |
| Example 2 | 0.031 | 2530 | 6 |
| Example 3 | 0.026 | 2120 | 6 |
| Example 4 | 0.024 | 2250 | 7 |
| Example 5 | 0.019 | 2040 | 8 |
| Example 6 | 0.015 | 1970 | 8 |
| Example 7 | 0.021 | 2100 | 8 |
| Example 8 | 0.018 | 1990 | 9 |
The subjects were also tested for safety prior to testing, 8 examples were tested for safety, and the results: the number of reaction stages of all subjects is 0, and no adverse reaction and no allergy occur when the three-layer hair care composition is used. The product of the invention is safe to use and is suitable for any skin.
Claims (10)
1. A three-layer hair care composition comprising an upper liquid layer, a middle liquid layer and a lower liquid layer;
the preparation raw material of the upper layer liquid comprises polysiloxane;
the preparation raw material of the middle layer liquid comprises a hydroxyl-containing compound;
the preparation raw materials of the lower layer liquid comprise ester substances and/or modified polysiloxane.
2. The triple layer hair care composition of claim 1, wherein the upper layer liquid is 2-70 wt%, the lower layer liquid is 2-70 wt%, and the middle layer liquid makes up the balance to 100 wt%.
3. A three-layer hair care composition according to claim 1 or 2, wherein said silicone comprises at least one member selected from the group consisting of polydimethylsiloxane, aminosilicone, cyclotetrasilylene, cyclopentadimethylsiloxane and cyclohexasiloxane.
4. A triple layer hair care composition according to claim 3 wherein the silicone has a kinematic viscosity of from 1 to 1000000 cst.
5. A triple layer hair care composition according to claim 1 or 2 wherein said hydroxyl containing compound comprises at least one of water, 1, 3-propanediol, glycerol, 1, 3-butanediol, pentanediol, hexanediol, dipropylene glycol, polyglycerol, and polyethylene glycol.
6. A triple layer hair care composition according to claim 5, wherein said polyglycerol has a degree of polymerization of from 3 to 10.
7. A triple layer hair care composition according to claim 5, wherein said polyethylene glycol has a degree of polymerization ranging from 4 to 32.
8. A three-layer hair care composition according to claim 1, wherein said lower layer liquid is prepared from a composition comprising one or more of sucrose acetate isobutyrate, tributyl acetyl citrate, bis-diethoxydiol cyclohexane 1,4-dicarboxylate, diethoxyethyl succinate, dimethyldiphenyl polydimethylsiloxane, trimethylpentaphenyl trisiloxane, tetramethyltetraphenyl trisiloxane, trimethylsiloxyphenyl polydimethylsiloxane.
9. A triple layer hair care composition according to claim 1 wherein the raw materials further comprise conditioning agents and pigments.
10. A process for the preparation of a triple layer hair care composition according to any one of claims 1 to 9 comprising the steps of:
mixing the above materials at 20-35 deg.C, stirring, and standing.
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102058493A (en) * | 2009-05-12 | 2011-05-18 | 赢创德固赛(中国)投资有限公司 | Cosmetic composition |
| CN104619306A (en) * | 2012-07-25 | 2015-05-13 | Elc管理有限责任公司 | Three-layered hair conditioning composition and consumer product |
| CN107929103A (en) * | 2017-12-18 | 2018-04-20 | 珠海伊斯佳科技股份有限公司 | A kind of three layers of hair/scalp care spraying |
| CN110812252A (en) * | 2019-12-06 | 2020-02-21 | 广州环亚化妆品科技有限公司 | Three-layer hair care composition and preparation method and application thereof |
| CN110934752A (en) * | 2019-12-05 | 2020-03-31 | 广州立白企业集团有限公司 | Hair care essence composition and preparation method thereof |
-
2021
- 2021-07-22 CN CN202110833021.1A patent/CN114903800A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102058493A (en) * | 2009-05-12 | 2011-05-18 | 赢创德固赛(中国)投资有限公司 | Cosmetic composition |
| CN104619306A (en) * | 2012-07-25 | 2015-05-13 | Elc管理有限责任公司 | Three-layered hair conditioning composition and consumer product |
| CN107929103A (en) * | 2017-12-18 | 2018-04-20 | 珠海伊斯佳科技股份有限公司 | A kind of three layers of hair/scalp care spraying |
| CN110934752A (en) * | 2019-12-05 | 2020-03-31 | 广州立白企业集团有限公司 | Hair care essence composition and preparation method thereof |
| CN110812252A (en) * | 2019-12-06 | 2020-02-21 | 广州环亚化妆品科技有限公司 | Three-layer hair care composition and preparation method and application thereof |
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