CN114887545A - Preparation method of natural refreshing flower and fruit flavor essence - Google Patents
Preparation method of natural refreshing flower and fruit flavor essence Download PDFInfo
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- CN114887545A CN114887545A CN202210479963.9A CN202210479963A CN114887545A CN 114887545 A CN114887545 A CN 114887545A CN 202210479963 A CN202210479963 A CN 202210479963A CN 114887545 A CN114887545 A CN 114887545A
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- flower
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- mixing
- fruit flavor
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- 239000008369 fruit flavor Substances 0.000 title claims abstract description 42
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 239000002994 raw material Substances 0.000 claims abstract description 63
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 claims abstract description 26
- VAMXMNNIEUEQDV-UHFFFAOYSA-N methyl anthranilate Chemical compound COC(=O)C1=CC=CC=C1N VAMXMNNIEUEQDV-UHFFFAOYSA-N 0.000 claims abstract description 25
- 239000003205 fragrance Substances 0.000 claims abstract description 21
- QUKGYYKBILRGFE-UHFFFAOYSA-N benzyl acetate Chemical compound CC(=O)OCC1=CC=CC=C1 QUKGYYKBILRGFE-UHFFFAOYSA-N 0.000 claims abstract description 18
- PPXUHEORWJQRHJ-UHFFFAOYSA-N ethyl isovalerate Chemical compound CCOC(=O)CC(C)C PPXUHEORWJQRHJ-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000005792 Geraniol Substances 0.000 claims abstract description 13
- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 claims abstract description 13
- 229940113087 geraniol Drugs 0.000 claims abstract description 13
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 12
- 229940102398 methyl anthranilate Drugs 0.000 claims abstract description 11
- HNAGHMKIPMKKBB-UHFFFAOYSA-N 1-benzylpyrrolidine-3-carboxamide Chemical compound C1C(C(=O)N)CCN1CC1=CC=CC=C1 HNAGHMKIPMKKBB-UHFFFAOYSA-N 0.000 claims abstract description 9
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 claims abstract description 9
- XMLSXPIVAXONDL-PLNGDYQASA-N Jasmone Chemical compound CC\C=C/CC1=C(C)CCC1=O XMLSXPIVAXONDL-PLNGDYQASA-N 0.000 claims abstract description 9
- 229940007550 benzyl acetate Drugs 0.000 claims abstract description 9
- OBNCKNCVKJNDBV-UHFFFAOYSA-N butanoic acid ethyl ester Natural products CCCC(=O)OCC OBNCKNCVKJNDBV-UHFFFAOYSA-N 0.000 claims abstract description 9
- IVLCENBZDYVJPA-ARJAWSKDSA-N cis-Jasmone Natural products C\C=C/CC1=C(C)CCC1=O IVLCENBZDYVJPA-ARJAWSKDSA-N 0.000 claims abstract description 9
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 claims abstract description 9
- -1 methyl hexyl Chemical group 0.000 claims abstract description 9
- XMLSXPIVAXONDL-UHFFFAOYSA-N trans-jasmone Natural products CCC=CCC1=C(C)CCC1=O XMLSXPIVAXONDL-UHFFFAOYSA-N 0.000 claims abstract description 9
- GUUHFMWKWLOQMM-UHFFFAOYSA-N alpha-n-hexylcinnamic aldehyde Natural products CCCCCCC(C=O)=CC1=CC=CC=C1 GUUHFMWKWLOQMM-UHFFFAOYSA-N 0.000 claims abstract description 8
- HUAZGNHGCJGYNP-UHFFFAOYSA-N propyl butyrate Chemical compound CCCOC(=O)CCC HUAZGNHGCJGYNP-UHFFFAOYSA-N 0.000 claims abstract description 5
- 238000002156 mixing Methods 0.000 claims description 67
- 238000003756 stirring Methods 0.000 claims description 28
- 239000003795 chemical substances by application Substances 0.000 claims description 18
- 244000014047 Polianthes tuberosa Species 0.000 claims description 17
- 235000016067 Polianthes tuberosa Nutrition 0.000 claims description 17
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims description 16
- 238000004821 distillation Methods 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- ZCTQGTTXIYCGGC-UHFFFAOYSA-N Benzyl salicylate Chemical compound OC1=CC=CC=C1C(=O)OCC1=CC=CC=C1 ZCTQGTTXIYCGGC-UHFFFAOYSA-N 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 12
- QPJVMBTYPHYUOC-UHFFFAOYSA-N methyl benzoate Chemical compound COC(=O)C1=CC=CC=C1 QPJVMBTYPHYUOC-UHFFFAOYSA-N 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 11
- 235000010254 Jasminum officinale Nutrition 0.000 claims description 10
- 239000000463 material Substances 0.000 claims description 10
- 238000000926 separation method Methods 0.000 claims description 9
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims description 8
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims description 8
- HCRBXQFHJMCTLF-ZCFIWIBFSA-N ethyl (2r)-2-methylbutanoate Chemical compound CCOC(=O)[C@H](C)CC HCRBXQFHJMCTLF-ZCFIWIBFSA-N 0.000 claims description 8
- 239000000834 fixative Substances 0.000 claims description 8
- 229930007744 linalool Natural products 0.000 claims description 8
- 239000007788 liquid Substances 0.000 claims description 8
- 239000003607 modifier Substances 0.000 claims description 8
- SIKJAQJRHWYJAI-UHFFFAOYSA-N Indole Chemical compound C1=CC=C2NC=CC2=C1 SIKJAQJRHWYJAI-UHFFFAOYSA-N 0.000 claims description 7
- 230000001276 controlling effect Effects 0.000 claims description 7
- 238000001914 filtration Methods 0.000 claims description 7
- 239000011259 mixed solution Substances 0.000 claims description 7
- 230000001105 regulatory effect Effects 0.000 claims description 7
- OALYTRUKMRCXNH-UHFFFAOYSA-N 5-pentyloxolan-2-one Chemical compound CCCCCC1CCC(=O)O1 OALYTRUKMRCXNH-UHFFFAOYSA-N 0.000 claims description 6
- PHXATPHONSXBIL-UHFFFAOYSA-N xi-gamma-Undecalactone Chemical compound CCCCCCCC1CCC(=O)O1 PHXATPHONSXBIL-UHFFFAOYSA-N 0.000 claims description 6
- 240000007436 Cananga odorata Species 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 5
- 239000004615 ingredient Substances 0.000 claims description 5
- 229940095102 methyl benzoate Drugs 0.000 claims description 5
- 150000004702 methyl esters Chemical class 0.000 claims description 5
- 239000000243 solution Substances 0.000 claims description 5
- 239000001813 ethyl (2R)-2-methylbutanoate Substances 0.000 claims description 4
- 229940090910 ethyl 2-methylbutyrate Drugs 0.000 claims description 4
- KVWWIYGFBYDJQC-MNOVXSKESA-N methyl 2-[(1r,2s)-3-oxo-2-pentylcyclopentyl]acetate Chemical compound CCCCC[C@H]1[C@@H](CC(=O)OC)CCC1=O KVWWIYGFBYDJQC-MNOVXSKESA-N 0.000 claims description 4
- 239000002562 thickening agent Substances 0.000 claims description 4
- PZOUSPYUWWUPPK-UHFFFAOYSA-N indole Natural products CC1=CC=CC2=C1C=CN2 PZOUSPYUWWUPPK-UHFFFAOYSA-N 0.000 claims description 3
- RKJUIXBNRJVNHR-UHFFFAOYSA-N indolenine Natural products C1=CC=C2CC=NC2=C1 RKJUIXBNRJVNHR-UHFFFAOYSA-N 0.000 claims description 3
- ZNJFBWYDHIGLCU-HWKXXFMVSA-N jasmonic acid Chemical compound CC\C=C/C[C@@H]1[C@@H](CC(O)=O)CCC1=O ZNJFBWYDHIGLCU-HWKXXFMVSA-N 0.000 claims description 3
- 238000007789 sealing Methods 0.000 claims description 3
- 240000005385 Jasminum sambac Species 0.000 claims 2
- 230000001681 protective effect Effects 0.000 claims 2
- 235000009508 confectionery Nutrition 0.000 abstract description 3
- 230000000694 effects Effects 0.000 description 9
- 241000207840 Jasminum Species 0.000 description 8
- 239000000203 mixture Substances 0.000 description 6
- 238000007599 discharging Methods 0.000 description 5
- 239000012535 impurity Substances 0.000 description 5
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 4
- 235000017491 Bambusa tulda Nutrition 0.000 description 4
- 241001330002 Bambuseae Species 0.000 description 4
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 4
- 239000011425 bamboo Substances 0.000 description 4
- 230000002045 lasting effect Effects 0.000 description 4
- 239000002304 perfume Substances 0.000 description 4
- 238000000746 purification Methods 0.000 description 4
- XPPALVZZCMPTIV-ARJAWSKDSA-N Jasmine lactone Chemical compound CC\C=C/CC1CCCC(=O)O1 XPPALVZZCMPTIV-ARJAWSKDSA-N 0.000 description 3
- XPPALVZZCMPTIV-UHFFFAOYSA-N Jasmine lactone Natural products CCC=CCC1CCCC(=O)O1 XPPALVZZCMPTIV-UHFFFAOYSA-N 0.000 description 3
- 230000009471 action Effects 0.000 description 3
- 239000002537 cosmetic Substances 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 230000008859 change Effects 0.000 description 2
- 230000008602 contraction Effects 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 239000013040 bath agent Substances 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229940117916 cinnamic aldehyde Drugs 0.000 description 1
- KJPRLNWUNMBNBZ-UHFFFAOYSA-N cinnamic aldehyde Natural products O=CC=CC1=CC=CC=C1 KJPRLNWUNMBNBZ-UHFFFAOYSA-N 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000001877 deodorizing effect Effects 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 239000003676 hair preparation Substances 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- XCZTYYQNVNLGKI-UZAOFVRNSA-N methyl tuberonate Chemical group COC(=O)C[C@H]1CCC(=O)[C@H]1C\C=C/CCO XCZTYYQNVNLGKI-UZAOFVRNSA-N 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Images
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/80—Forming a predetermined ratio of the substances to be mixed
- B01F35/88—Forming a predetermined ratio of the substances to be mixed by feeding the materials batchwise
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
- B01F23/80—After-treatment of the mixture
- B01F23/808—Filtering the mixture
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F35/93—Heating or cooling systems arranged inside the receptacle
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
- C11B9/0019—Aliphatic compounds containing oxygen as the only heteroatom carbocylic acids; Salts or esters thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/0034—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0042—Essential oils; Perfumes compounds containing condensed hydrocarbon rings
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F2035/99—Heating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
- B01F2101/21—Mixing of ingredients for cosmetic or perfume compositions
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention relates to the technical field of essence preparation, and discloses a preparation method of natural refreshing flower and fruit flavor essence, which comprises the following steps: s1: preparing raw materials, wherein the raw materials comprise 1.5-3 parts of ethyl butyrate, 1.5-3 parts of butyl acetate, 0.5-0.7 part of 2-methyl ethyl butyrate, 0.2-0.8 part of ethyl isovalerate, 0.4-0.8 part of benzyl acetate, 0.4-0.8 part of methyl hexyl cinnamaldehyde, 0.2-0.6 part of cis-jasmone, 0.3-0.7 part of methyl anthranilate and 0.1-0.6 part of geraniol. The invention ensures the purity of the flower and fruit flavor essence, improves the quality of the fresh flower and fruit flavor essence, increases the fragrance of the essence, ensures that the essence has the sour and sweet fragrance of fruits, has rich levels, prolongs the fragrance time of the essence, and can make the fragrance of the essence fresh for a long time.
Description
Technical Field
The invention relates to the technical field of essence preparation, in particular to a preparation method of natural refreshing flower and fruit flavor essence.
Background
The daily chemical essence is essence for perfuming and flavoring perfume, cosmetics, cleaning products and industrial products, is mainly applied to perfume, cologne, toilet water, beauty cosmetics, skin care cosmetics, perfumed soap, bath agents, detergents, hair cosmetics, aromatic curative effect agents, indoor aromatizers, deodorizing agents and insecticides, at present, the demand of daily chemical products is not limited to the functions of the daily chemical products, the smell of the products is more interesting, the essence is properly selected, the products can be more favored by consumers, the common perfume raw materials have independent smell, and different fragrances are generated through the matching of different perfume raw materials.
At present, most of the essence used in the prior art is artificially synthesized, the essence has sharp aroma, the aroma is diffused quickly, the effect of lasting aroma cannot be achieved, and the requirement of people cannot be met.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides a preparation method of natural refreshing flower and fruit flavor, which mainly solves the problems that the flavor has sharp aroma, the aroma is quickly emitted, and the effect of lasting aroma cannot be achieved.
(II) technical scheme
In order to achieve the purpose, the invention provides the following technical scheme:
a preparation method of natural refreshing flower and fruit flavor essence comprises the following steps:
s1: preparing raw materials, wherein the raw materials comprise 1.5-3 parts of ethyl butyrate, 1.5-3 parts of butyl acetate, 0.5-0.7 part of 2-methyl ethyl butyrate, 0.2-0.8 part of ethyl isovalerate, 0.4-0.8 part of benzyl acetate, 0.4-0.8 part of methyl hexyl cinnamaldehyde, 0.2-0.6 part of cis-jasmone, 0.3-0.7 part of methyl anthranilate, 0.1-0.6 part of geraniol, 0.2-0.5 part of linalool, 0.2-0.5 part of high cis-dihydrojasmonate, 0.9-1.3 parts of tuberose absolute oil, 0.9-1.3 part of jasmine absolute oil, 0.9-1.3 part of ylang oil, 0.9-1.3 part of orange flower oil, 50-60 parts of water, 25-35 parts of a blending agent, 7-15 parts of a fragrance fixative and 12-22 parts of a modifier;
s2: stirring and mixing, namely putting prepared ethyl butyrate, butyl acetate, ethyl 2-methylbutyrate, ethyl isovalerate, benzyl acetate, methyl hexyl cinnamaldehyde, cis-jasmone, methyl anthranilate, geraniol, linalool, high cis-methyl dihydrojasmonate, tuberose absolute oil, jasmine absolute oil, ylang-ylang oil, orange flower oil and water into stirring equipment for stirring and mixing;
s3: heating and mixing, namely adding the blending agent, the fixative and the thickening agent into stirring equipment according to the formula, then stirring and mixing again, heating the raw materials during mixing, and controlling the heating temperature to be between 60 and 80 ℃;
s4: solid-liquid separation, namely standing the mixed solution for 5-10 minutes, and separating out precipitated residues;
s5: distilling and extracting, namely putting the separated solution into a distillation flask for high-temperature distillation, controlling the temperature during distillation at 120 ℃ and the pressure at normal pressure, and controlling the time at 3-4 hours to obtain the primary flower and fruit flavor essence, wherein when the plant raw materials are placed in boiling water, essence oil containing fragrance escapes along with water vapor, and when the steam is condensed into water, the oil floats on the water surface, and then the oil and the water can be collected;
s6: curing, namely standing the prepared essence for 2-3 days to cure to obtain the flower and fruit flavor essence;
s7: purifying, and circularly filtering the cured flower and fruit flavor essence for 2-5 times to obtain the natural refreshing flower and fruit flavor essence.
Furthermore, the S1 blending agent is preferably methyl tuberonate 3-7 parts, jasmonate 3-7 parts, indole 2-10 parts, methyl anthranilate 2-10 parts, the fixative is preferably methyl benzoate 0.6-2 parts, benzyl salicylate 0.1-2 parts, the modifier is peach aldehyde 0.4-0.6 part, coconut aldehyde 0.4-0.7 part, geraniol 0.1-0.3 part.
Further, in S2, the mixing device is started, the raw materials are stirred and mixed at a low speed, the raw materials need to be fed in batches according to the properties of the raw materials, the feeding time does not exceed 5-8 minutes, the batch feeding interval time is 0.7-1.5 minutes, and the raw materials need to be mixed at a high speed for 5-10 minutes after the feeding is completed.
Further, in S4, the solid-liquid separation apparatus includes a filter screen and a filter rack, and the filter screen is preferably 1000 mesh.
The invention also provides a mixing preparation device of the natural refreshing flower and fruit flavor essence, which comprises a shell, wherein the top end of the shell is fixedly connected with a motor, one end of an output shaft of the motor is fixedly connected with a connecting shaft, one end of the connecting shaft is positioned in the shell, one side of the circumference of the connecting shaft is fixedly connected with a plurality of stirring frames, the inner walls of multiple sides of the shell are fixedly connected with a material guide cylinder and a supporting plate, the supporting plate is fixedly connected with the material guide cylinder, the upper surface of the supporting plate is fixedly connected with a heater, the inner walls of multiple sides of the shell are fixedly connected with a supporting frame, the upper surface of the supporting frame is fixedly connected with a filter screen, the bottom of the supporting plate is movably connected with an adjusting plate, the upper surface of the supporting plate is provided with a plurality of discharging ports, the inner wall of one side of the shell is movably connected with an electric push rod, and one end of the electric push rod is movably connected with the bottom of the adjusting plate.
Further: the upper surface fixed connection of backup pad has the heat conduction protection casing, and the heater is located the heat conduction protection casing.
Further: the inner walls of the two sides of the shell are fixedly connected with inclined plates.
Further: one side of the shell is hermetically inserted with a discharge pipe, and one end of the discharge pipe is sleeved with a filter mantle.
Further: one side of the shell is movably connected with a side plate, one side of the shell is movably connected with a cover plate, one side of the cover plate is hermetically inserted with a feeding cylinder, and one end of the feeding cylinder is fixedly connected with a sealing plate.
(III) advantageous effects
Compared with the prior art, the invention provides a preparation method of natural refreshing flower and fruit flavor essence, which has the following beneficial effects:
1. according to the invention, the mixed solution is fully filtered by the filter screen in the earlier stage, so that the influence of impurities on the distillation of the fresh flower and fruit flavor essence is prevented, the purity of the flower and fruit flavor essence is ensured, and the quality of the fresh flower and fruit flavor essence is improved.
2. According to the invention, peach aldehyde, coconut aldehyde, tuberose acid methyl ester and jasmine lactone are used to highlight the fruit fragrance of tuberose, methyl benzoate, benzyl salicylate, tuberose absolute, jasmine absolute, ylang-ylang oil and orange flower oil are used to increase the fragrance of the essence, and the essence has the sour and sweet fragrance of fruits, is abundant in hierarchy, prolongs the fragrance time of the essence, and can make the fragrance of the essence lasting and fresh.
3. According to the invention, through the batch feeding method, raw materials with different properties can enter the shell in batches, so that the change of the properties of the raw materials caused by overlong mixing time of part of the raw materials is effectively reduced, and the preparation effect of the fresh flower and fruit flavor essence in the later period is ensured.
4. According to the invention, by using the heater, the raw materials can be heated when the heater is needed, and the raw materials can be fully mixed at a proper temperature, so that the mixing effect of the raw materials is improved.
Drawings
Fig. 1 is a schematic left side perspective view of a mixing preparation device of a natural refreshing flower and fruit-flavored essence provided by the present invention;
FIG. 2 is a schematic cross-sectional view of a mixing and preparing apparatus for natural refreshing flower and fruit-flavored essence according to the present invention;
FIG. 3 is a schematic diagram of a separation structure with a partial cross-sectional view of a mixing and preparing apparatus for natural fresh flower and fruit-flavored essence according to the present invention;
FIG. 4 is a schematic diagram of a right side perspective view of a mixing and preparing apparatus for natural fresh flower and fruit-flavored essence according to the present invention;
fig. 5 is a schematic flow structure diagram of a preparation method of the natural refreshing flower and fruit flavored essence provided by the invention.
In the figure: 1. a housing; 2. a motor; 3. a connecting shaft; 4. a stirring frame; 5. a support plate; 6. a material guide cylinder; 7. an adjusting plate; 8. an electric push rod; 9. a support frame; 10. a filter screen; 11. a feeding port; 12. a heater; 13. a heat-conducting shield; 14. a sloping plate; 15. a discharge pipe; 16. a filter housing; 17. a side plate; 18. a cover plate; 19. a feeding cylinder; 20. and (7) sealing the plate.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
Referring to fig. 1 to 5, a method for preparing natural refreshing flower and fruit flavored essence comprises the following steps:
s1: preparing raw materials, wherein the raw materials comprise 2 parts of ethyl butyrate, 2 parts of butyl acetate, 0.5 part of 2-methyl ethyl butyrate, 0.6 part of ethyl isovalerate, 0.5 part of benzyl acetate, 0.6 part of methyl-hexyl cinnamaldehyde, 0.4 part of cis-jasmone, 0.5 part of methyl anthranilate, 0.3 part of geraniol, 0.2 part of linalool, 0.3 part of high-cis methyl dihydrojasmonate, 1.2 parts of tuberose absolute oil, 1.2 parts of jasmine absolute oil, 0.9 part of ylang oil, 0.9 part of orange flower oil, 55 parts of water, 30 parts of a blending agent, 9 parts of a fragrance fixative and 18 parts of a modifier;
s2: stirring and mixing, namely putting prepared ethyl butyrate, butyl acetate, ethyl 2-methylbutyrate, ethyl isovalerate, benzyl acetate, methyl hexyl cinnamaldehyde, cis-jasmone, methyl anthranilate, geraniol, linalool, high cis-methyl dihydrojasmonate, tuberose absolute oil, jasmine absolute oil, ylang-ylang oil, orange flower oil and water into stirring equipment for stirring and mixing;
s3: heating and mixing, namely adding the blending agent, the fixative and the thickening agent into stirring equipment according to the formula, then stirring and mixing again, heating the raw materials during mixing, and controlling the heating temperature to be 65 ℃;
s4: solid-liquid separation, namely standing the mixed solution for 8 minutes, and separating out precipitated residues;
s5: distilling and extracting, namely putting the separated solution into a distillation flask for high-temperature distillation, wherein the temperature during distillation is controlled at 115 ℃, the pressure is normal pressure, and the time is controlled at 3.5 hours, so as to obtain the primary flower and fruit flavor essence;
s6: curing, namely standing the prepared essence for 2 days to cure to obtain the flower and fruit flavor essence;
s7: purifying, namely performing 3 times of circulating filtration on the cured flower and fruit flavor essence to obtain natural fresh flower and fruit flavor essence, preferably performing full filtration in the purification process to prevent impurities from influencing the purity of purification,
in the invention, the blending agent in S1 is preferably 5 parts of tuberose acid methyl ester, 5 parts of jasmine lactone, 7 parts of indole, 7 parts of anthranilic acid methyl ester, the fragrance fixing agent is preferably 1.2 parts of benzoic acid methyl ester, 1.3 parts of salicylic acid benzyl ester, the modifier is peach aldehyde 0.4 part, coconut aldehyde 0.4 part and geraniol 0.1 part, the fruit fragrance of tuberose is highlighted by using peach aldehyde, coconut aldehyde, tuberose acid methyl ester and jasmine lactone, the methyl benzoate, benzyl salicylate, tuberose absolute oil, jasmine absolute oil, ylang oil and orange flower oil are used to increase the fragrance of the essence, the fragrance of the fruit is sour and sweet, the hierarchy is rich, the time of the fragrance is prolonged, the fragrance of the essence can be kept lasting and fresh, in S2, a mixing device is started, low-speed stirring mixing is firstly carried out, raw material ingredients are fed in batches according to the properties of the fruit, the raw materials with different properties can be fed into the shell in batches by the batch feeding method design, effectively reduced the change of the raw materials nature that partial raw materials leads to because of the mix time overlength, the preparation effect of the fresh flower fruit flavor essence in later stage has been ensured, feed time is no longer than 6 minutes, batch feed interval time is 1.2 minutes, batch feed interval time overlength can cause the rise of temperature, mix the production influence to the raw materials, after the feeding is accomplished, need carry out high-speed mixing 7 minutes, high-speed mixed purpose, can make the misce bene, include filter screen and filter stand when carrying out solid-liquid separation in S4, carry out abundant filtration to mixed solution via the filter screen, prevent impurity influence the distillation of flower fruit flavor essence, the purity of flower fruit flavor essence has been guaranteed, the filter screen is preferably 1000 meshes.
The invention also provides a mixing preparation device of the natural refreshing flower and fruit flavor essence, which comprises a shell 1, wherein the top end of the shell 1 is fixed with a motor 2 through a bolt, one end of an output shaft of the motor 2 is fixed with a connecting shaft 3 through a bolt, one end of the connecting shaft 3 is positioned in the shell 1, one side of the circumference of the connecting shaft 3 is fixed with a plurality of stirring frames 4 through bolts, the inner walls of the multiple sides of the shell 1 are fixed with a material guide cylinder 6 and a supporting plate 5 through bolts, the supporting plate 5 is fixedly connected with the material guide cylinder 6, the upper surface of the supporting plate 5 is fixed with a heater 12 through bolts, the raw materials can be heated when the heater 12 is needed by the raw materials through the addition of the heater 12, the sufficient mixing of the raw materials can be ensured at a proper temperature, the mixing effect of the raw materials is improved, the supporting frames 9 are fixed on the inner walls of the multiple sides of the shell 1 through bolts, the upper surface of carriage 9 is fixed with filter screen 10 through the bolt, the bottom of backup pad 5 is rotated and is connected with regulating plate 7, and the upper surface of backup pad 5 has seted up a plurality of feed openings 11, one side inner wall of casing 1 is rotated and is connected with electric putter 8, and electric putter 8's one end is rotated with the bottom of regulating plate 7 and is connected, because electric putter 8's both ends are the movable mode, consequently for regulating plate 7 is opened downwards to the unloading of mixture.
The upper surface of backup pad 5 is fixed with heat conduction protection casing 13 through the bolt, heater 12 is located heat conduction protection casing 13, the design of heat conduction protection casing 13, so as to protect heater 12, the both sides inner wall of casing 1 has swash plate 14 through the bolt fastening, one side seal of casing 1 is pegged graft and is had discharging pipe 15, filter mantle 16 has been cup jointed to the one end of discharging pipe 15, one side of casing 1 is rotated and is connected with curb plate 17, one side of casing 1 is rotated and is connected with apron 18, one side seal of apron 18 is pegged graft and is had a feeding section of thick bamboo 19, the one end of a feeding section of thick bamboo 19 is passed through the bolt fastening and is had closing plate 20.
The working principle of the embodiment is as follows: when in use, the motor 2 is started to mix the raw materials at a low speed, then the raw materials are put into the shell 1 in batches through the feeding cylinder 19, after all the raw materials are put into the mixer, high-speed mixing is started to enable the raw materials to be mixed more uniformly, the heater 12 is started to heat and mix the raw materials at the same time, after the mixing is finished, the electric push rod 8 is started, the adjusting plate 7 is pulled by the contraction of the electric push rod 8, because both ends of the electric push rod 8 are in a movable mode, the adjusting plate 7 is opened downwards, so that the raw material in the shell 1 is discharged through the feed opening 11, and the inclined plate 14 guides the raw material, so that the raw material is intensively dropped on the filter screen 10, the mixed raw material is filtered by the filter screen 10, falls to the bottom of the housing 1 and is discharged through the discharge pipe 15, and is filtered by the filter mantle 16.
Example 2
Referring to fig. 1-5, a preparation method of a natural refreshing flower and fruit flavored essence comprises the following steps:
s1: preparing raw materials, wherein the raw materials comprise 2.5 parts of ethyl butyrate, 2.8 parts of butyl acetate, 0.6 part of 2-methyl ethyl butyrate, 0.8 part of ethyl isovalerate, 0.8 part of benzyl acetate, 0.7 part of methyl hexyl cinnamaldehyde, 0.6 part of cis-jasmone, 0.7 part of methyl anthranilate, 0.5 part of geraniol, 0.4 part of linalool, 0.5 part of high-cis methyl dihydrojasmonate, 1.3 parts of tuberose absolute oil, 1.3 parts of jasmine absolute oil, 1.2 parts of ylang oil, 1.3 parts of orange flower oil, 60 parts of water, 35 parts of a blending agent, 13 parts of a fixing agent and 20 parts of a modifier;
s2: stirring and mixing, namely putting prepared ethyl butyrate, butyl acetate, ethyl 2-methylbutyrate, ethyl isovalerate, benzyl acetate, methyl hexyl cinnamaldehyde, cis-jasmone, methyl anthranilate, geraniol, linalool, high cis-methyl dihydrojasmonate, tuberose absolute oil, jasmine absolute oil, ylang-ylang oil, orange flower oil and water into stirring equipment for stirring and mixing;
s3: heating and mixing, namely adding the blending agent, the fixative and the thickening agent into stirring equipment according to the formula, then stirring and mixing again, heating the raw materials during mixing, and controlling the heating temperature to be 75 ℃;
s4: solid-liquid separation, namely standing the mixed solution for 10 minutes, and separating out precipitated residues;
s5: distilling and extracting, namely putting the separated solution into a distillation flask for high-temperature distillation, wherein the temperature during distillation is controlled at 120 ℃, the pressure is normal pressure, and the time is controlled at 4 hours, so as to obtain the primary flower and fruit flavor essence;
s6: curing, namely standing the prepared essence for 3 days to cure to obtain the flower and fruit flavor essence;
s7: purifying, namely performing 5 times of circulating filtration on the cured flower and fruit flavor essence to obtain natural fresh flower and fruit flavor essence, preferably performing full filtration in the purification process to prevent impurities from influencing the purity of purification,
in the invention, the blending agent in S1 is preferably 7 parts of tuberose acid methyl ester, 7 parts of jasmonate, 9 parts of indole, 8 parts of anthranilate methyl ester, the fragrance fixing agent is preferably 1.5 parts of methyl benzoate, 1.5 parts of benzyl salicylate, the modifier is peach aldehyde 0.6 part, coconut aldehyde 0.7 part and geraniol 0.3 part, in S2, a mixing device is started, low-speed stirring and mixing are firstly carried out, raw material ingredients need to be fed in batches according to the properties of the raw material ingredients, the feeding time does not exceed 8 minutes, the feeding interval time in batches is 1.5 minutes, the temperature is increased due to overlong feeding interval time in batches, the raw material mixing is influenced, after the feeding is finished, high-speed mixing is required for 10 minutes, the purpose of high-speed mixing is realized, the mixing is uniform, a filter screen and a filter rack are included in S4 during solid-liquid separation, the mixed solution is fully filtered through the filter screen, and the distillation of floral and fruity flavor is prevented from being influenced by impurities, the purity of the flower and fruit flavor essence is ensured, and the filter screen is preferably 1000 meshes.
The invention also provides a mixing preparation device of the natural refreshing flower and fruit flavor essence, which comprises a shell 1, wherein the top end of the shell 1 is fixed with a motor 2 through a bolt, one end of an output shaft of the motor 2 is fixed with a connecting shaft 3 through a bolt, one end of the connecting shaft 3 is positioned in the shell 1, one side of the circumference of the connecting shaft 3 is fixed with a plurality of stirring frames 4 through bolts, the inner walls of the multiple sides of the shell 1 are fixed with a material guide cylinder 6 and a supporting plate 5 through bolts, the supporting plate 5 is fixedly connected with the material guide cylinder 6, the upper surface of the supporting plate 5 is fixed with a heater 12 through bolts, the raw materials can be heated when the heater 12 is needed by the raw materials through the addition of the heater 12, the sufficient mixing of the raw materials can be ensured at a proper temperature, the mixing effect of the raw materials is improved, the supporting frames 9 are fixed on the inner walls of the multiple sides of the shell 1 through bolts, the upper surface of carriage 9 is fixed with filter screen 10 through the bolt, the bottom of backup pad 5 is rotated and is connected with regulating plate 7, and the upper surface of backup pad 5 has seted up a plurality of feed openings 11, one side inner wall of casing 1 is rotated and is connected with electric putter 8, and electric putter 8's one end is rotated with the bottom of regulating plate 7 and is connected, because electric putter 8's both ends are the movable mode, consequently for regulating plate 7 is opened downwards, so that the unloading of mixture.
The upper surface of backup pad 5 is fixed with heat conduction protection casing 13 through the bolt, heater 12 is located heat conduction protection casing 13, the design of heat conduction protection casing 13, so as to protect heater 12, the both sides inner wall of casing 1 has swash plate 14 through the bolt fastening, one side seal of casing 1 is pegged graft and is had discharging pipe 15, filter mantle 16 has been cup jointed to the one end of discharging pipe 15, one side of casing 1 is rotated and is connected with curb plate 17, one side of casing 1 is rotated and is connected with apron 18, one side seal of apron 18 is pegged graft and is had a feeding section of thick bamboo 19, the one end of a feeding section of thick bamboo 19 is passed through the bolt fastening and is had closing plate 20.
The working principle of the embodiment is as follows: when in use, the motor 2 is started to mix the raw materials at a low speed, then the raw materials are put into the shell 1 in batches through the feeding cylinder 19, after all the raw materials are put into the mixer, high-speed mixing is started to enable the raw materials to be mixed more uniformly, the heater 12 is started to heat and mix the raw materials at the same time, after the mixing is finished, the electric push rod 8 is started, the adjusting plate 7 is pulled by the contraction of the electric push rod 8, because both ends of the electric push rod 8 are in a movable mode, the adjusting plate 7 is opened downwards, so that the raw material in the shell 1 is discharged through the feed opening 11, and the inclined plate 14 guides the raw material, so that the raw material is intensively dropped on the filter screen 10, the mixed raw material is filtered by the filter screen 10, falls to the bottom of the housing 1 and is discharged through the discharge pipe 15, and is filtered by the filter mantle 16.
The electrical components presented in the document are all electrically connected with an external master controller and 220V mains, and the master controller can be a conventional known device controlled by a computer or the like.
In the description herein, it is to be noted that, unless expressly stated or limited otherwise, the terms "connected" and "connected" are to be construed broadly, e.g., as meaning either a fixed connection, a removable connection, or an integral connection; the connection may be mechanical or electrical, and may be direct or indirect via an intermediate. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.
In the description herein, it is noted that relational terms such as first and second, and the like, are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (9)
1. A preparation method of natural refreshing flower and fruit flavor essence is characterized by comprising the following steps: the method comprises the following steps:
s1: preparing raw materials, wherein the raw materials comprise 1.5-3 parts of ethyl butyrate, 1.5-3 parts of butyl acetate, 0.5-0.7 part of 2-methyl ethyl butyrate, 0.2-0.8 part of ethyl isovalerate, 0.4-0.8 part of benzyl acetate, 0.4-0.8 part of methyl hexyl cinnamaldehyde, 0.2-0.6 part of cis-jasmone, 0.3-0.7 part of methyl anthranilate, 0.1-0.6 part of geraniol, 0.2-0.5 part of linalool, 0.2-0.5 part of high cis-dihydrojasmonate, 0.9-1.3 parts of tuberose absolute oil, 0.9-1.3 part of jasmine absolute oil, 0.9-1.3 part of ylang oil, 0.9-1.3 part of orange flower oil, 50-60 parts of water, 25-35 parts of a blending agent, 7-15 parts of a fragrance fixative and 12-22 parts of a modifier;
s2: stirring and mixing, namely putting prepared ethyl butyrate, butyl acetate, ethyl 2-methylbutyrate, ethyl isovalerate, benzyl acetate, methyl hexyl cinnamaldehyde, cis-jasmone, methyl anthranilate, geraniol, linalool, high cis-methyl dihydrojasmonate, tuberose absolute oil, jasmine absolute oil, ylang-ylang oil, orange flower oil and water into stirring equipment for stirring and mixing;
s3: heating and mixing, namely adding the blending agent, the fixative and the thickening agent into stirring equipment according to the formula, then stirring and mixing again, heating the raw materials during mixing, and controlling the heating temperature to be between 60 and 80 ℃;
s4: solid-liquid separation, namely standing the mixed solution for 5-10 minutes, and separating out precipitated residues;
s5: distilling and extracting, namely putting the separated solution into a distillation flask for high-temperature distillation, controlling the temperature at 100-120 ℃, the pressure at normal pressure and the time at 3-4 hours during distillation to obtain the primary flower and fruit flavor essence;
s6: curing, namely standing the prepared essence for 2-3 days to cure to obtain the flower and fruit flavor essence;
s7: purifying, and circularly filtering the cured flower and fruit flavor essence for 2-5 times to obtain the natural refreshing flower and fruit flavor essence.
2. The method for preparing natural refreshing flower and fruit flavored essence according to claim 1, which is characterized in that: the blending agent in the S1 is preferably 3-7 parts of tuberose acid methyl ester, 3-7 parts of jasmonate, 2-10 parts of indole, 2-10 parts of methyl anthranilate, the fixing agent is preferably 0.6-2 parts of methyl benzoate, 0.1-2 parts of benzyl salicylate, the modifier is 0.4-0.6 part of peach aldehyde, 0.4-0.7 part of coconut aldehyde and 0.1-0.3 part of geraniol.
3. The method for preparing natural refreshing flower and fruit flavored essence according to claim 1, which is characterized in that: in the step S2, the material mixing device is started, low-speed stirring and mixing are firstly carried out, raw material ingredients need to be fed in batches according to the properties of the raw material ingredients, the feeding time does not exceed 5-8 minutes, the batch feeding interval time is 0.7-1.5 minutes, and high-speed mixing needs to be carried out for 5-10 minutes after the feeding is finished.
4. The method for preparing natural refreshing flower and fruit flavored essence according to claim 1, which is characterized in that: in the step S4, the solid-liquid separation step includes a filter screen and a filter holder, and the filter screen is preferably 1000 mesh.
5. The mixing preparation device of the natural refreshing flower and fruit flavor essence comprises a shell (1) and is characterized in that a motor (2) is fixedly connected to the top end of the shell (1), a connecting shaft (3) is fixedly connected to one end of an output shaft of the motor (2), one end of the connecting shaft (3) is located in the shell (1), a plurality of stirring frames (4) are fixedly connected to one side of the circumference of the connecting shaft (3), a material guide cylinder (6) and a supporting plate (5) are fixedly connected to the inner wall of the multiple sides of the shell (1), the supporting plate (5) is fixedly connected with the material guide cylinder (6), a heater (12) is fixedly connected to the upper surface of the supporting plate (5), a supporting frame (9) is fixedly connected to the inner wall of the multiple sides of the shell (1), a filter screen (10) is fixedly connected to the upper surface of the supporting frame (9), and an adjusting plate (7) is movably connected to the bottom of the supporting plate (5), and a plurality of feed openings (11) have been seted up to the upper surface of backup pad (5), one side inner wall swing joint electric putter (8) of casing (1), the bottom swing joint of one end and regulating plate (7) of electric putter (8).
6. The mixing and preparing device of natural refreshing flower and fruit flavor according to claim 5, characterized in that: the upper surface of the supporting plate (5) is fixedly connected with a heat-conducting protective cover (13), and the heater (12) is positioned in the heat-conducting protective cover (13).
7. The mixing and preparing device of natural refreshing flower and fruit flavor according to claim 6, characterized in that: the inner walls of two sides of the shell (1) are fixedly connected with inclined plates (14).
8. The mixing and preparing device of natural refreshing flower and fruit flavor according to claim 7, characterized in that: a discharge pipe (15) is connected to one side of the shell (1) in a sealed and inserting mode, and a filter cover (16) is sleeved at one end of the discharge pipe (15).
9. The mixing and preparing device of natural refreshing flower and fruit flavor according to claim 8, characterized in that: one side of the shell (1) is movably connected with a side plate (17), one side of the shell (1) is movably connected with a cover plate (18), one side of the cover plate (18) is hermetically inserted with a feeding cylinder (19), and one end of the feeding cylinder (19) is fixedly connected with a sealing plate (20).
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