CN114848521A - 宠物专用免洗清洁剂及其制备方法 - Google Patents
宠物专用免洗清洁剂及其制备方法 Download PDFInfo
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- CN114848521A CN114848521A CN202210446719.2A CN202210446719A CN114848521A CN 114848521 A CN114848521 A CN 114848521A CN 202210446719 A CN202210446719 A CN 202210446719A CN 114848521 A CN114848521 A CN 114848521A
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Abstract
本发明涉及一种宠物专用免洗清洁剂,其包含:5‑10wt%的椰子油酰胺丙基甜菜碱(CAB);0.5‑1.5wt%的椰油基葡糖苷;1‑5wt%的椰油酰两性基二乙酸二钠;5‑10wt%的椰油酰甲基牛磺酸牛磺酸钠;0.001‑0.1wt%的枯草菌脂肽钠;1‑5wt%的椰油基‑葡糖苷酒石酸酯钠;0.5‑1.5wt%癸基葡糖苷;0.5‑1.5wt%月桂基葡糖苷;0.1‑1wt%的角鲨烷;0.1‑0.5wt%的精氨酸;0.05‑0.1wt%的肉豆蔻酰胺丙基PG‑二甲基氯化铵磷酸酯;0.01‑0.05wt%的丁香提取物;0.01‑0.05wt%的山鸡椒果油;0.01‑0.05wt%的欧百里香提取物;0.01‑0.05wt%的苦参提取物;余量为水。本发明还涉及上述宠物专用免洗清洁剂的制备方法。
Description
技术领域
本发明属于宠物护理品用配制品技术领域,尤其涉及一种宠物专用免洗清洁剂及其制备方法。
背景技术
目前饲养猫、狗类宠物家庭的日渐增多,宠物与人的生活日趋密切,其健康状况也日益受到宠物饲养主的重视。猫、狗类宠物由于其毛发较多且较长,皮毛上容易沾染携带多种致病菌,毛发内部容易滋生寄生虫,宠物的皮肤也经常遭受皮肤疾病(如皮炎、瘙痒等)的困扰,这不仅会对宠物带来生活中的不利也会给宠物的饲养者带来健康威胁,所以定期对宠物进行清洗显得十分必要。而市场上的宠物清洁产品存在以下技术问题:
1.宠物清洁产品容易对宠物产生一定的刺激性,间接导致与宠物接触的饲养者产生过敏红肿等不良反应;
2.现有的宠物清洁产品大多为沐浴露等液态状物质,都是需要水才能完成清洗过程,而有些宠物对于水有应激反应,导致使用宠物清洁产品清洗宠物的过程不顺利,目前针对宠物开发的免水洗清洁产品较少;
3.市场上已出现的免水洗清洁产品(如免洗干粉、免洗泡沫、免洗沐浴露等)其清洁效果不够理想,在使用之后会在宠物的毛发上产生残留物,而宠物存在的舔舐毛发的行为,因此残留物对于宠物的健康带来潜在的风险;
4.现有的宠物清洁产品大多不具备清洁以外的功效,例如杀菌、护理、促进伤口愈合等。
发明内容
针对现有技术中存在的技术问题,本发明旨在提供一种宠物专用免洗清洁剂,该宠物专用免洗清洁剂对与猫、狗类宠物温和无刺激,并且清洁后在宠物的毛发上产生的微量残留物无毒并且无刺激性。使用该宠物专用免洗清洁剂清洁对宠物清洁后能使得宠物的毛柔顺、光泽,同时能该宠物专用免洗清洁剂具有快速清洁毛发和皮肤、无需水洗、促进伤口愈合、保湿修复皮肤、温和刺激性低、消炎抗菌的效果,从而改善宠物的皮肤状态。
一方面,本发明提供一种宠物专用免洗清洁剂,包含:
5-10wt%的椰子油酰胺丙基甜菜碱(CAB);
0.5-1.5wt%的椰油基葡糖苷;
1-5wt%的椰油酰两性基二乙酸二钠;
5-10wt%的椰油酰甲基牛磺酸牛磺酸钠;
0.001-0.1wt%的枯草菌脂肽钠;
1-5wt%的椰油基-葡糖苷酒石酸酯钠;
0.5-1.5wt%癸基葡糖苷;
0.5-1.5wt%月桂基葡糖苷;
0.1-1wt%的角鲨烷;
0.1-0.5wt%的精氨酸;
0.05-0.1wt%的肉豆蔻酰胺丙基PG-二甲基氯化铵磷酸酯;
0.01-0.05wt%的丁香提取物;
0.01-0.05wt%的山鸡椒果油;
0.01-0.05wt%的欧百里香提取物;
0.01-0.05wt%的苦参提取物;
余量为水。
所述宠物专用免洗清洁剂采用水作为主溶剂。
所述宠物专用免洗清洁剂中,椰子油酰胺丙基甜菜碱(CAB)、椰油基葡糖苷、椰油酰两性基二乙酸二钠、椰油酰甲基牛磺酸牛磺酸钠、枯草菌脂肽钠、椰油基-葡糖苷酒石酸酯钠、癸基葡糖苷和月桂基葡糖苷均为温和型的表面活性剂,从而进一步减少宠物专用免洗清洁剂对于宠物的刺激性。上述表面活性剂的组合具有快速清洁宠物的毛发和皮肤的作用,同时加强宠物专用免洗清洁剂体系中各组分的稳定性,且上述述表面活性剂的组合使用安全性高不存在毒性和致癌性,不会对宠物造成伤害。椰子油酰胺丙基甜菜碱(CAB)、椰油基葡糖苷、椰油酰两性基二乙酸二钠、椰油酰甲基牛磺酸牛磺酸钠的组合使得所述宠物专用免洗清洁剂清洁宠物后宠物的毛达到柔顺不打结粘连的效果,枯草菌脂肽钠、椰油基-葡糖苷酒石酸酯钠、癸基葡糖苷和月桂基葡糖苷的组合使得所述宠物专用免洗清洁剂清洁宠物后宠物的毛有光泽。癸基葡糖苷和月桂基葡糖苷的组合使得丁香提取物、山鸡椒果油、欧百里香提取物、苦参根提取物的组合在所述宠物专用免洗清洁剂体系中稳定均匀分散。枯草菌脂肽钠能有效减少宠物专用免洗清洁剂在宠物的毛发上产生的残留物。
所述宠物专用免洗清洁剂中,肉豆蔻酰胺丙基PG-二甲基氯化铵磷酸酯为阳离子调理剂,角鲨烷为油脂,肉豆蔻酰胺丙基PG-二甲基氯化铵磷酸酯和角鲨烷的组合使得宠物专用免洗清洁剂对于宠物皮肤具有保湿功效。
所述宠物专用免洗清洁剂中,精氨酸、丁香提取物、山鸡椒果油、欧百里香提取物、苦参提取物的组合能够使得宠物专用免洗清洁剂对于宠物皮肤具有修复调理、促进伤口愈合、镇定止痛和有效杀菌抗炎的功效。山鸡椒果油是由山鸡椒提取而来,山鸡椒果油具有清香气味,可视作香精香料、气味抑制剂,并且山鸡椒果油具有消肿止痛的作用。苦参提取物是从豆科苦参属的植物苦参中提取的一种生物碱,包括苦参碱、氧化苦参碱、羟基苦参碱、安那吉碱等。其原材根部质坚韧,断面粗纤维性,黄白色,气微,味极苦。苦参性寒,有清热燥湿,杀虫的功效。苦参提取物能够杀虫止痒,对皮肤瘙痒有很好的缓解作用,能够平衡油脂分泌,疏通并收敛毛孔,清除皮肤内毒素杂质。丁香提取物和欧百里香提取物均可视为安全、可接触粘膜的广谱高效杀菌剂,并可抑制产品氧化。丁香提取物和欧百里香提取物的组合无特殊气味、无刺激、安全性高,作用温和,并且具有高效抗菌消炎,迅速舒缓发炎,红肿的作用。
本发明提供一种宠物专用免洗清洁剂为水溶剂型,从低温-5℃至高温50℃范围内都呈现稳定均匀状态,使用时将宠物专用免洗清洁剂揉搓涂抹在宠物需要清洗的皮肤毛发上,轻轻按摩产生丰富的泡沫,至泡沫渗透清洁好后用湿巾或者毛巾或者纸巾将未消泡的残留轻轻拭去。使用宠物专用免洗清洁剂能有效清洁宠物毛发并且祛除异味、消炎抗菌。
另一方面,本发明提供了所述宠物专用免洗清洁剂的制备方法,具体包括以下步骤:
步骤一,将丁香提取物、山鸡椒果油、欧百里香提取物、苦参根提取物与癸基葡糖苷和月桂基葡糖苷混合均匀,得到混合物A;
步骤二,用水溶解均匀混合物A,得到混合物B,备用;
步骤三,用水溶解肉豆蔻酰胺丙基PG-二甲基氯化铵磷酸酯,得到混合物C,备用;
步骤四,将椰油基葡糖苷、角鲨烷、枯草菌脂肽钠、椰油基-葡糖苷酒石酸酯钠、椰子油酰胺丙基甜菜碱(CAB)混合均匀得到混合物D,备用;
步骤五,用水溶解精氨酸得到混合物E,备用;
步骤六,将椰油酰两性基二乙酸二钠和椰油酰甲基牛磺酸牛磺酸钠加入水中中,搅拌均匀得到混合物F;
步骤七,将混合物B、混合物C、混合物D加入至混合物F中,搅拌均匀得到混合物G;
步骤八,将混合物E加入混合物G中,搅拌均匀得到混合物H;
步骤九,检测混合物H的理化指标,合格后出料灌装得到所述宠物专用免洗清洁剂。
与现有技术相比,本发明的技术方案至少存在以下有益效果:
1.本发明提供的宠物专用免洗清洁剂使用的表面活性剂组合能够有效的起到清洁的作用同时对于清洁后可能造成的在毛发上的残留对于宠物不会产生伤害和刺激,且表面活性剂的组合使宠物专用免洗清洁剂处于稳定状态;
2.本发明提供的宠物专用免洗清洁剂对于宠物温和无刺激,并且在清洁效果之外还能对宠物皮肤起到保湿修复、消炎镇静、杀菌抗炎、促进伤口愈合的效果;
3.本发明提供的宠物专用免洗清洁剂对于宠物的皮肤具有调理功效,清洁宠物后能使得宠物的毛柔顺、光泽。
具体实施方式
应当理解,此处所描述的具体实施例仅仅用以解释本发明,并不用于限定本发明。
以下通过具体实施方式进一步描述本发明,但本发明不仅仅限于以下实施例。在本发明的范围内或者在不脱离本发明的内容、精神和范围内,对本发明进行适当改进、替换功效相同的组分,对于本领域技术人员来说是显而易见的,它们都被视为包括在本发明的范围之内。
若无特殊说明,本发明所用的组分均采用常规市售商品。
实施例1-3提供的宠物专用免洗清洁剂的具体组分配比如表1所示。
实施例1-3提供的宠物专用免洗清洁剂均采用如下制备方法进行制备:
步骤一,将丁香提取物、山鸡椒果油、欧百里香提取物、苦参根提取物与癸基葡糖苷和月桂基葡糖苷混合均匀,得到混合物A;
步骤二,用水溶解均匀混合物A,得到混合物B,备用;
步骤三,用水溶解肉豆蔻酰胺丙基PG-二甲基氯化铵磷酸酯,得到混合物C,备用;
步骤四,将椰油基葡糖苷、角鲨烷、枯草菌脂肽钠、椰油基-葡糖苷酒石酸酯钠、椰子油酰胺丙基甜菜碱(CAB)混合均匀得到混合物D,备用;
步骤五,用水溶解精氨酸得到混合物E,备用;
步骤六,将椰油酰两性基二乙酸二钠和椰油酰甲基牛磺酸牛磺酸钠加入水中中,搅拌均匀得到混合物F;
步骤七,将混合物B、混合物C、混合物D加入至混合物F中,搅拌均匀得到混合物G;
步骤八,将混合物E加入混合物G中,搅拌均匀得到混合物H;
步骤九,检测混合物H的理化指标,合格后出料灌装得到所述宠物专用免洗清洁剂。
对比例1-8提供的宠物专用免洗清洁剂的具体组分配比如表2所示。
表1
表2
对实施例1-3提供的宠物专用免洗清洁剂、对比例1-8提供的宠物专用免洗清洁剂进行如下测试试验:
一、清洁效果及安全性评价
1.实验品:实施例1-3样品、对比例1-8样品。
2.受试宠物数量:选取宠物幼犬80只,随机分为8组,每组10只。
3.实验方法:分别使用实施例1-3样品以及对比例1-8样品,每周对宠物幼犬进行1次清洗,连续1个月后,对使用后宠物毛发光泽,清洁后持续效果等情况观察并进行统计分析。若毛色光泽度好、精神好为效果显著;毛色光泽度良好、精神良好为有效;其它则为无效。1个月后观察,宠物使用后的精神健康状态。
观察数据记录如表3和表4所示,其中表3为实施例1-3提供的宠物专用免洗清洁剂的测试结果,表4为对比例1-8提供的宠物专用免洗清洁剂的测试结果。
由表表3和表4的试验观察数据中可以得知,本发明实施例1-3提供的宠物专用免洗清洁剂相比于对比例1-8提供的宠物专用免洗清洁剂能够有效的保持宠物毛发的清洁,且具有持久的保持清洁无异味作用。1个月后对宠物的使用情况观察均没有发现受试宠物狗有感冒发烧、刺激瘙痒、过敏红肿等异常症状,说明本发明提供的提供的宠物专用免洗清洁剂使用安全。
表3
表4
二、促进伤口愈合评价试验
1.实验材料:实施例1-3样品、对比例1-8样品、空白液。
2.实验方法:用成年雄性白鼠45只,体重200±10g,随机分为9个手术组,每组5只,均在乙醚麻醉下剃毛,并于背中线左侧0.5cm处,作6.0cm长的皮肤切口,深达肌层表面,然后缝合,9个手术组分别在外部擦拭对应的实施例1-3样品、对比例1-8样品以及空白液,连续10天,术后第5天进行拆线。第10天在乙醚麻醉下,取切口皮肤,用10%福尔马林固定,常规石蜡包埋,切片5μm,H.E染色,观察伤口愈合的组织形态学变化。
3.伤口愈合的肉眼观察结果
以肉眼观察可知,使用实施例1-3提供的宠物专用免洗清洁剂清洁伤口在伤后的第8天即可减轻伤口周围红斑,10天后白鼠伤口创面面积减小,伤口收缩速度快,对于伤口均具有明显促进愈合的效果。空白液组白鼠伤口周围红斑,水肿症状明显,伤口愈合速度最缓慢,创面面积相比实施例1-3以及对比例1-8大。相较于实施例1-3以及对比例1-6,对比例7-8对应的白鼠的伤口愈合速度缓慢,且在愈合过程伤口周围出现明显的红斑症状。
由试验现象可以得知,实施例1-3提供的宠物专用免洗清洁剂具有促进伤口愈合的作用以及对受伤皮肤具有修复消炎镇定的效果。若所述宠物专用免洗清洁剂缺少癸基葡糖苷或月桂基葡糖苷,会显著影响宠物专用免洗清洁剂的促进伤口愈合以及修复消炎镇定的效果,猜测原因为缺少癸基葡糖苷或月桂基葡糖苷会引起丁香提取物、山鸡椒果油、欧百里香提取物、苦参提取物的组合的析出,使得宠物专用免洗清洁剂的促进伤口愈合的作用以及修复消炎镇定的作用减弱。
三、稳定性测试试验
1.实验材料:实施例1-3样品、对比例1-8样品、空白液。
2.实验方法:
(1)将样品置于-5℃的环境温度下储存,在-5℃储存试验进行4周,储存过程每周取样,对样品的理化性能指标以及清洁效果进行相关的实验测试;
(2)将样品置于50℃的环境温度下储存,50℃储存试验进行8周,储存过程每2周取样,对样品的理化性能指标以及清洁效果进行相关的实验测试;
(3)将样品置于50℃的室温(约为28℃)下储存,室温储存试验进行1年,储存过程每季度取样,对样品的理化性能指标以及清洁效果进行相关的实验测试。
3.试验结果记录
在-5℃进行4周的储存试验,在存储过程每周进行取样,对样品的相态,气味,清洁效果进行测试。实施例1-3样品各项测试结果均无异常,料液保持稳定均匀不分层。对比例1-6样品在第2周时物料体系不稳定开始有晶体析出,对比例7-8样品在第1周时物料体系不稳定开始有晶体析出。由此可知该温度条件下本发明实施例1-3提供的宠物专用免洗清洁剂具有稳定性强的特点,即表面活性剂的组合使用增强了本发明体系的稳定性。
在50℃进行8周的储存试验,在存储过程每2周进行取样,对样品的相态,气味,清洁效果进行测试。实施例1-3样品的测试结果均与初始状态相同,且物料组分稳定未出现分层。对比例7-8样品在第1周时开始出现分层的现象。在第4周对比例1-4样品以及对比例6样品均出现分层。在第7周对比例5样品出现分层并且气味出现异常。以上结果表明在50℃的存储过程中本发明实施例1-3提供的宠物专用免洗清洁剂能够有效保持稳定性。
在常温下进行1年的储存试验,在存储过程每季度进行取样,对样品的相态,气味,清洁效果进行测试。实施例1-3样品在相态,气味上均无明显变化,物料均匀无分层现象,且经过1年的长期储存依旧能够达到初始的清洁效果。对比例7-8样品在第1周时开始出现分层的现象,在第2季度对比例1-6样品样品均出现分层,并且气味出现异常。由此可以得出在长期常温保存条件下本发明实施例1-3提供的宠物专用免洗清洁剂的体系稳定,物料组分均匀不分层,同时能够达到有效清洁的目的。
在不同的温度条件对本发明进行稳定性的测试,从测试的结果可以判断,本发明提供的宠物专用免洗清洁剂通过表面活性剂的组合使用增强了体系的稳定性同时具有持久清洁的作用。
从以上试验可以得出本项发明技术中各项组分之间的协同作用能够产生清洁毛发和皮肤、无需水洗、促进伤口愈合、保湿修复皮肤、有效抑菌消炎镇定的功效,且不会对宠物和饲养者产生的刺激性,表面活性剂的组合使用增强了宠物专用免洗清洁剂体系的稳定性。
以上所述实施例的各技术特征可以进行任意的组合,为使描述简洁,未对上述实施例中的各个技术特征所有可能的组合都进行描述,然而,只要这些技术特征的组合不存在矛盾,都应当认为是本说明书记载的范围。
以上所述实施例仅表达了本发明的几种实施方式,其描述较为具体和详细,但并不能因此而理解为对发明专利范围的限制。应当指出的是,对于本领域的普通技术人员来说,在不脱离本发明构思的前提下,还可以做出若干变形和改进,这些都属于本发明的保护范围。因此,本发明专利的保护范围应以所附权利要求为准。
Claims (2)
1.一种宠物专用免洗清洁剂,其特征在于,包含:
5-10wt%的椰子油酰胺丙基甜菜碱;
0.5-1.5wt%的椰油基葡糖苷;
1-5wt%的椰油酰两性基二乙酸二钠;
5-10wt%的椰油酰甲基牛磺酸牛磺酸钠;
0.001-0.1wt%的枯草菌脂肽钠;
1-5wt%的椰油基-葡糖苷酒石酸酯钠;
0.5-1.5wt%癸基葡糖苷;
0.5-1.5wt%月桂基葡糖苷;
0.1-1wt%的角鲨烷;
0.1-0.5wt%的精氨酸;
0.05-0.1wt%的肉豆蔻酰胺丙基PG-二甲基氯化铵磷酸酯;
0.01-0.05wt%的丁香提取物;
0.01-0.05wt%的山鸡椒果油;
0.01-0.05wt%的欧百里香提取物;
0.01-0.05wt%的苦参提取物;
余量为水。
2.制备权利要求1所述的宠物专用免洗清洁剂的方法,其特征在于,包括如下步骤:
步骤一,将丁香提取物、山鸡椒果油、欧百里香提取物、苦参根提取物与癸基葡糖苷和月桂基葡糖苷混合均匀,得到混合物A;
步骤二,用水溶解均匀混合物A,得到混合物B,备用;
步骤三,用水溶解肉豆蔻酰胺丙基PG-二甲基氯化铵磷酸酯,得到混合物C,备用;
步骤四,将椰油基葡糖苷、角鲨烷、枯草菌脂肽钠、椰油基-葡糖苷酒石酸酯钠、椰子油酰胺丙基甜菜碱混合均匀得到混合物D,备用;
步骤五,用水溶解精氨酸得到混合物E,备用;
步骤六,将椰油酰两性基二乙酸二钠和椰油酰甲基牛磺酸牛磺酸钠加入水中中,搅拌均匀得到混合物F;
步骤七,将混合物B、混合物C、混合物D加入至混合物F中,搅拌均匀得到混合物G;
步骤八,将混合物E加入混合物G中,搅拌均匀得到混合物H;
步骤九,检测混合物H的理化指标,合格后出料灌装得到所述宠物专用免洗清洁剂。
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