CN114796028A - Hair care essence oil - Google Patents
Hair care essence oil Download PDFInfo
- Publication number
- CN114796028A CN114796028A CN202210662825.4A CN202210662825A CN114796028A CN 114796028 A CN114796028 A CN 114796028A CN 202210662825 A CN202210662825 A CN 202210662825A CN 114796028 A CN114796028 A CN 114796028A
- Authority
- CN
- China
- Prior art keywords
- oil
- parts
- hair care
- camellia seed
- stirring
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
- A61K8/892—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a hydroxy group, e.g. dimethiconol
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a hair care essence oil, which relates to the field of daily chemicals and comprises the following components: cyclopentadimethylsiloxane, camellia seed oil, dimethiconol, corn germ oil, argan oil, squalane, blumea oil, rice germ oil, oregano flower oil, hinoki oil, and tocopheryl acetate; the preparation method comprises the following steps: (1) mixing cyclopentadimethylsiloxane and dimethiconol, stirring and heating; (2) adding camellia seed oil and stirring; (3) adding corn germ oil, stirring and cooling; (4) sequentially adding argan oil, hinoki oil, rice germ oil, squalane, oleum folium Artemisiae Argyi, oil of origanum vulgare flower, and tocopherol acetate, and stirring to obtain the final product. Compared with the prior art, the hair care essential oil disclosed by the invention can effectively solve the problem that hair is easy to break.
Description
Technical Field
The invention relates to the field of daily chemicals, in particular to a preparation method and application of hair care essential oil.
Background
In daily life, people often wash hair with shampoo, oil on the surface of the hair can be washed off while dirt is washed off, hair scales on the surface of the hair are damaged, the friction force between the hair is increased, the hair is easy to tangle and difficult to comb, static electricity is particularly easy to generate, the hair is easy to brush, and the luster is poor. The damage to the hair during perming and dyeing is more serious, and the hair is exposed in the external environment, is easily irradiated by ultraviolet rays and is more easily damaged. The hair is fragile and easy to break under the influence of various internal and external factors. Therefore, the existing hair care essential oil has room for further improvement in solving the problem of hair breakage.
Disclosure of Invention
Aiming at the defects of the prior art, the technical problem solved by the invention is how to further prevent the hair from being easily broken.
In order to solve the technical problems, the invention adopts the technical scheme that the hair care essential oil comprises the following components in parts by mass:
50-75 parts of cyclopentasiloxane;
15-30 parts of camellia seed oil;
5-10 parts of dimethiconol;
3-8 parts of corn germ oil;
5-8 parts of argan oil;
2-6 parts of plant squalane;
1-3 parts of blumea oil;
1-3 parts of rice germ oil;
1-3 parts of winter oregano flower oil;
1-8 parts of hinoki oil;
1-5 parts of tocopherol acetate;
the preparation method comprises the following steps:
(1) mixing cyclopentadimethylsiloxane and dimethiconol, stirring uniformly, and heating to 70 ℃;
(2) adding camellia seed oil, keeping the temperature, and stirring for 5min at the rotation speed of 300 rpm;
(3) adding corn germ oil, stirring for 10min at 300rpm, and cooling to 50-55 deg.C;
(4) sequentially adding argan oil, hinoki oil, rice germ oil, squalane, oleum folium Artemisiae Argyi, origanum vulgare flower oil, and tocopherol acetate, and stirring at 300rpm for 15min to obtain the final product.
The camellia seed oil is customized camellia seed oil or camellia seed oil containing hair care factors.
The preparation method of the camellia seed oil containing the hair care factors comprises the following steps:
(1) smashing coffee and sour bean fruits in a mass ratio of 1:3 into powder of 100 meshes and 150 meshes, treating for 30min at the temperature of 120 ℃ and the pressure of 0.2MPa, and drying for 2h at the temperature of 60 ℃ for later use.
(2) Weighing the mixed raw materials, mixing the mixed raw materials with an ethanol solution according to the mass ratio of 1:35, and extracting for 2 hours at 50 ℃;
(3) adding the customized camellia oil according to the mass ratio of 1:30, and extracting for 2h at the temperature of 45 ℃;
(4) cooling to 35 ℃, filtering at 80 meshes, and then concentrating under reduced pressure at 50 ℃ until the ethanol solvent is completely removed;
(5) cooling to 35 deg.C, fine-filtering with filter plate with aperture of 8um to clarify to obtain camellia seed oil containing hair care factor.
The preparation method of the customized camellia oil comprises the following steps:
(1) crushing camellia seed kernels obtained after husking camellia seeds to 200 meshes and 300 meshes, adding water, heating to 90 ℃, stirring for 30min, and filtering and then performing centrifugal treatment on filter residues for dehydration;
(2) mixing camellia seed kernel filter residue and an enzymolysis liquid solution according to a mass ratio of 2:5, heating to 38 ℃, preserving heat, sealing and placing for 35 minutes, then heating to 52 ℃, preserving heat, sealing and placing for 1 hour, and then cooling to room temperature;
(3) taking out the enzymolyzed semen Camelliae Japonicae, filtering to obtain residue, oven drying at 48 deg.C, placing under 1.9MPa, and making into slurry;
(4) putting the obtained slurry into a pressure tank, vacuumizing, filling argon, setting the pressure to be 2.5Pa for 5 minutes, carrying out homogenizing shearing at 10000rpm, then centrifuging, separating an oil layer, removing residues, taking an emulsion layer, adding modified carboxymethyl cellulose powder with the mass of 0.5 per thousand of that of the emulsion layer, placing the emulsion layer into microwave equipment, treating for 2 minutes in 350MHz microwave frequency and 350W power, placing the emulsion layer into 10000rpm, carrying out homogenizing shearing, centrifuging and layering, and combining oil layers to obtain crude oil slurry;
(5) adding the crude oil slurry into a supercritical CO2 device, setting the initial pressure at 3MPa, increasing the pressure at 0.5MPa per minute, and maintaining the pressure at 12MPa for 30min for extraction to obtain the customized camellia seed oil.
In the step (2), the enzymolysis solution is prepared by mixing a citric acid solution with a mass concentration of 45% and soybean protein powder according to a mass ratio of 1:0.8 to prepare a soybean protein solution, heating to 95 ℃, keeping the temperature for 15min, cooling the swollen soybean protein solution to 20 ℃, adding cellulase, protease and water into the soybean protein solution, and carrying out enzymolysis;
the soybean protein solution is prepared by adding 3000U of cellulase, 2000U of protease and 400mL of water into every gram of soybean protein solution and mixing.
Compared with the prior art, the hair care essential oil disclosed by the invention can effectively solve the problem that hair is easy to break.
Detailed Description
The following examples and experiments are provided to further illustrate the embodiments of the present invention, but are not intended to limit the present invention.
Example 1:
the hair care essential oil comprises the following components in parts by mass:
65 parts of cyclopenta dimethyl silicone polymer;
customizing 20 parts of camellia seed oil;
5 parts of dimethiconol;
3 parts of corn germ oil;
5 parts of Arcago glycerin;
6 parts of plant squalane;
1 part of blumea oil;
1 part of rice germ oil;
1 part of winter oregano flower oil;
5 parts of hinoki oil;
2 parts of tocopherol acetate;
the preparation method comprises the following steps:
(1) mixing cyclopentadimethylsiloxane and dimethiconol, stirring uniformly, and heating to 70 ℃;
(2) adding the customized camellia seed oil, preserving heat, and stirring for 5min at the rotating speed of 300 rpm;
(3) adding corn germ oil, stirring for 10min at 300rpm, and cooling to 50-55 deg.C;
(4) sequentially adding argan oil, hinoki oil, rice germ oil, squalane, oleum folium Artemisiae Argyi, origanum vulgare flower oil, and tocopherol acetate, and stirring at 300rpm for 15min to obtain the final product.
The preparation method of the customized camellia seed oil comprises the following steps:
(1) crushing camellia seed kernels obtained after husking camellia seeds to 200 meshes and 300 meshes, adding water, heating to 90 ℃, stirring for 30min, and filtering and then performing centrifugal treatment on filter residues for dehydration;
(2) mixing camellia seed kernel filter residue and an enzymolysis liquid solution according to a mass ratio of 2:5, heating to 38 ℃, preserving heat, sealing and placing for 35 minutes, then heating to 52 ℃, preserving heat, sealing and placing for 1 hour, and then cooling to room temperature;
(3) taking out the enzymolyzed semen Camelliae Japonicae, filtering to obtain residue, oven drying at 48 deg.C, placing under 1.9MPa, and making into slurry;
(4) putting the obtained slurry into a pressure tank, vacuumizing, filling argon, setting the pressure to be 2.5Pa for 5 minutes, carrying out homogenizing shearing at 10000rpm, then centrifuging, separating an oil layer, removing residues, taking an emulsion layer, adding modified carboxymethyl cellulose powder with the mass of 0.5 per thousand of that of the emulsion layer, placing the emulsion layer into microwave equipment, treating for 2 minutes in 350MHz microwave frequency and 350W power, placing the emulsion layer into 10000rpm, carrying out homogenizing shearing, centrifuging and layering, and combining oil layers to obtain crude oil slurry;
(5) adding the crude oil slurry into a supercritical CO2 device, setting the initial pressure at 3MPa, increasing the pressure at 0.5MPa per minute, and maintaining the pressure at 12MPa for 30min for extraction to obtain the customized camellia seed oil.
In the step (2), mixing citric acid solution with the mass concentration of 45% and soybean protein powder according to the mass ratio of 1:0.8 to prepare soybean protein solution, heating to 95 ℃, keeping the temperature for 15min, cooling the swollen soybean protein solution to 20 ℃, adding cellulase, protease and water into the soybean protein solution, and carrying out enzymolysis to obtain enzymolysis solution;
the soybean protein solution is prepared by adding 3000U of cellulase, 2000U of protease and 400mL of water into every gram of soybean protein solution and mixing.
Example 2
The hair care essential oil comprises the following components in parts by mass: 65 parts of cyclopentacalydimethylsiloxane, 20 parts of camellia seed oil containing hair care factors, 5 parts of dimethiconol, 3 parts of corn germ oil, 5 parts of argan oil, 6 parts of squalane, 1 part of blumea oil, 1 part of rice germ oil, 1 part of origanum vulgare flower oil, 5 parts of hinoki oil and 2 parts of tocopherol acetate; the preparation method comprises the following steps:
(1) mixing cyclopentadimethylsiloxane and dimethiconol, stirring uniformly, and heating to 70 ℃;
(2) adding camellia seed oil containing hair care factor, keeping the temperature, and stirring for 5min at the rotation speed of 300 rpm;
(3) adding corn germ oil, stirring for 10min at 300rpm, and cooling to 50-55 deg.C;
(4) sequentially adding argan oil, hinoki oil, rice germ oil, squalane, oleum folium Artemisiae Argyi, origanum vulgare flower oil, and tocopherol acetate, and stirring at 300rpm for 15min to obtain the final product.
The preparation method of the camellia seed oil containing the hair care factors comprises the following steps:
(1) smashing coffee and sour bean fruits in a mass ratio of 1:3 into powder of 100 meshes and 150 meshes, treating for 30min at the temperature of 120 ℃ and the pressure of 0.2MPa, and drying for 2h at the temperature of 60 ℃ for later use.
(2) Weighing the mixed raw materials, mixing the mixed raw materials with an ethanol solution according to the mass ratio of 1:35, and extracting for 2 hours at 50 ℃;
(3) adding the customized camellia oil according to the mass ratio of 1:30, and extracting for 2h at the temperature of 45 ℃;
(4) cooling to 35 ℃, filtering at 80 meshes, and then concentrating under reduced pressure at 50 ℃ until the ethanol solvent is completely removed;
(5) cooling to 35 deg.C, fine-filtering with filter plate with aperture of 8um to clarify to obtain camellia seed oil containing hair care factor.
Example 3
The hair care essence oil comprises the following components in parts by mass:
50 parts of cyclopenta dimethyl silicone polymer;
customizing 30 parts of camellia seed oil;
5 parts of dimethiconol;
8 parts of corn germ oil;
5 parts of argan oil;
6 parts of plant squalane;
1 part of blumea oil;
3 parts of rice germ oil;
1 part of winter oregano flower oil;
8 parts of hinoki oil;
1 part of tocopherol acetate;
example 4
The hair care essence oil comprises the following components in parts by mass:
65 parts of cyclopenta dimethyl silicone polymer;
customizing 25 parts of camellia seed oil;
8 parts of dimethiconol;
5 parts of corn germ oil;
6 parts of argan oil;
4 parts of plant squalane;
2 parts of blumea oil;
2 parts of rice germ oil;
2 parts of winter oregano flower oil;
5 parts of hinoki oil;
3 parts of tocopherol acetate;
example 5
The hair care essence oil comprises the following components in parts by mass:
75 parts of cyclopentasiloxane;
customizing 15 parts of camellia seed oil;
10 parts of dimethiconol;
3 parts of corn germ oil;
8 parts of argan oil;
2 parts of plant squalane;
3 parts of blumea oil;
1 part of rice germ oil;
3 parts of winter oregano flower oil;
1 part of hinoki oil;
5 parts of tocopherol acetate;
the preparation method of the hair care essential oil according to the embodiments 3 to 5 comprises the following steps:
(1) mixing cyclopentadimethylsiloxane and dimethiconol, stirring uniformly, and heating to 70 ℃;
(2) adding camellia seed oil, keeping the temperature, and stirring for 5min at the rotation speed of 300 rpm;
(3) adding corn germ oil, stirring for 10min at 300rpm, and cooling to 50-55 deg.C;
(4) sequentially adding argan oil, hinoki oil, rice germ oil, squalane, oleum folium Artemisiae Argyi, origanum vulgare flower oil, and tocopherol acetate, and stirring at 300rpm for 15min to obtain the final product.
The camellia seed oil in the hair care essential oil of the above embodiments 3 to 5 can be customized camellia seed oil or camellia seed oil containing hair care factor.
When the camellia seed oil in the hair care essential oil is the customized camellia seed oil, the preparation method comprises the following steps:
(1) crushing camellia seed kernels obtained after husking camellia seeds to 200 meshes and 300 meshes, adding water, heating to 90 ℃, stirring for 30min, and filtering and then performing centrifugal treatment on filter residues for dehydration;
(2) mixing camellia seed kernel filter residue and an enzymolysis liquid solution according to a mass ratio of 2:5, heating to 38 ℃, preserving heat, sealing and placing for 35 minutes, then heating to 52 ℃, preserving heat, sealing and placing for 1 hour, and then cooling to room temperature;
(3) taking out the enzymolyzed semen Camelliae Japonicae, filtering to obtain residue, oven drying at 48 deg.C, placing under 1.9MPa, and making into slurry;
(4) putting the obtained slurry into a pressure tank, vacuumizing, filling argon, setting the pressure to be 2.5Pa for 5 minutes, carrying out homogenizing shearing at 10000rpm, then centrifuging, separating an oil layer, removing residues, taking an emulsion layer, adding modified carboxymethyl cellulose powder with the mass of 0.5 per thousand of that of the emulsion layer, placing the emulsion layer into microwave equipment, treating for 2 minutes in 350MHz microwave frequency and 350W power, placing the emulsion layer into 10000rpm, carrying out homogenizing shearing, centrifuging and layering, and combining oil layers to obtain crude oil slurry;
(5) adding the crude oil slurry into a supercritical CO2 device, setting the initial pressure at 3MPa, increasing the pressure at 0.5MPa per minute, and maintaining the pressure at 12MPa for 30min for extraction to obtain the customized camellia seed oil.
In the step (2), mixing citric acid solution with the mass concentration of 45% and soybean protein powder according to the mass ratio of 1:0.8 to prepare soybean protein solution, heating to 95 ℃, keeping the temperature for 15min, cooling the swollen soybean protein solution to 20 ℃, adding cellulase, protease and water into the soybean protein solution, and carrying out enzymolysis to obtain enzymolysis solution;
the soybean protein solution is prepared by adding 3000U of cellulase, 2000U of protease and 400mL of water into every gram of soybean protein solution and mixing.
When the camellia seed oil in the hair care essential oil of the embodiments 3 to 5 is the camellia seed oil containing the hair care factor, the preparation method comprises the following steps:
(1) smashing coffee and sour bean fruits in a mass ratio of 1:3 into powder of 100 meshes and 150 meshes, treating for 30min at the temperature of 120 ℃ and the pressure of 0.2MPa, and drying for 2h at the temperature of 60 ℃ for later use.
(2) Weighing the mixed raw materials, mixing the mixed raw materials with an ethanol solution according to the mass ratio of 1:35, and extracting for 2 hours at 50 ℃;
(3) adding the customized camellia oil according to the mass ratio of 1:30, and extracting for 2h at the temperature of 45 ℃;
(4) cooling to 35 ℃, filtering at 80 meshes, and then concentrating under reduced pressure at 50 ℃ until the ethanol solvent is completely removed;
(5) cooling to 35 deg.C, fine-filtering with filter plate with aperture of 8um to clarify to obtain camellia seed oil containing hair care factor.
Comparative example 1
A hair care essential oil, which is different from the hair care essential oil in example 1 in that the used camellia oil is the commercial camellia oil.
Comparative example 2
A hair care essential oil, which is different from that in example 2, camellia seed oil containing hair care factors is prepared by using commercially available camellia seed oil.
To better illustrate the beneficial effects of the hair care essential oils of the present invention, the following efficacy evaluation experiments were conducted:
(I) stability test
20g of each of the above examples and comparative examples are sealed in a sealed bottle, each sample is placed in an environment of-18 ℃ to 2 ℃ to 25 ℃ to 40 ℃ to 48 ℃ and is taken out after being placed for 3 months to observe whether the measured physicochemical indexes are normal or not, and the records are as follows:
(II) Hair breakage prevention test
Testing materials: black, flat hair strand in the original state, 15cm, 2.5g
Testing an instrument: hair breaking force tester
And (3) testing environment: the temperature is 21 ℃ plus or minus 1.0 ℃; humidity: 50% +/-10%
The test scheme is as follows:
(1) randomly taking 2 identical flat hair bundles (2.5 g, 15cm, healthy hair bundles) and balancing in a constant temperature and humidity environment for 24 hours;
(2) after the hair is cleaned, wiping excessive water, uniformly smearing 0.5g of essence oil sample on hair for each hair bundle, taking the hair for 8h, then cleaning with shampoo base material without adding functional components, washing with water flow for 30s, and repeating the operation more than once. The operation was performed 5 times in total. Placing the isolated hair at a temperature of 21 ℃ plus or minus 1.0 ℃; naturally airing for 24 hours in a constant temperature and humidity environment with the humidity of 50 +/-10%;
(3) after 24 hours, individual hair breaks were measured using a hair strand tester.
The test analysis method comprises the following steps:
and (3) performing significance test on data normal distribution by using SSPS software, if the data of the sample group Sig (on both sides) >0.01 is normal distribution, performing paired sample t test, and testing the standard alpha =0.05, otherwise, performing rank sum test, and analyzing the improvement percentage of comparison before and after treatment by using the test sample. The control group is the raw data before hair treatment.
Results of breaking force test descriptive statistics (Unit: N)
"ns" means P >0.05, "-" means 0.01. ltoreq. P < 0.05; "+" indicates 0.001. ltoreq. p < 0.01, and "+" indicates p < 0.001.
By analyzing the breaking force test result descriptive statistics, it can be derived:
example 1 is only adding the customized camellia seed oil prepared by the invention, the commercial camellia seed oil is used in the comparative example 1, the improvement rate of the anti-breaking effect of example 1 is improved from 13.52% to 29.60% compared with the improvement rate of the comparative example 1, and the improvement rate is remarkably improved;
example 2 is the hair care factor-containing camellia seed oil added with coffee and tamarind, compared with example 1, the anti-breaking effect is improved from 29.60% to 88.92% compared with example 1, and is improved significantly. Therefore, the camellia seed oil containing the hair care factors, which is added with the coffee and the tamarind fruit, has an obvious effect of improving the hair breakage prevention effect.
The improvement rate of the example 2 and the comparative example 2 is increased from 50.67% to 88.92%, and the effect shows that the hair-care factor-containing camellia seed oil prepared by the customized camellia seed oil has more remarkable hair-breakage prevention effect.
The embodiments of the present invention have been described in detail with reference to the examples, but the present invention is not limited to the described embodiments. It will be apparent to those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention.
Claims (6)
1. The hair care essence oil is characterized by comprising the following components in parts by mass:
50-75 parts of cyclopentasiloxane;
15-30 parts of camellia seed oil;
5-10 parts of dimethiconol;
3-8 parts of corn germ oil;
5-8 parts of argan oil;
2-6 parts of plant squalane;
1-3 parts of blumea oil;
1-3 parts of rice germ oil;
1-3 parts of winter oregano flower oil;
1-8 parts of hinoki oil;
1-5 parts of tocopherol acetate;
the preparation method comprises the following steps:
(1) mixing cyclopentadimethylsiloxane and dimethiconol, stirring uniformly, and heating to 70 ℃;
(2) adding camellia seed oil, keeping the temperature, and stirring for 5min at the rotation speed of 300 rpm;
(3) adding corn germ oil, stirring for 10min at 300rpm, and cooling to 50-55 deg.C;
(4) sequentially adding argan oil, hinoki oil, rice germ oil, squalane, oleum folium Artemisiae Argyi, origanum vulgare flower oil, and tocopherol acetate, and stirring at 300rpm for 15min to obtain the final product.
2. The hair care essence oil according to claim 1, wherein the camellia seed oil is customized camellia seed oil or camellia seed oil containing hair care factors.
3. The hair care essence oil according to claim 2, wherein the preparation method of the camellia oil containing the hair care factor comprises the following steps:
(1) smashing coffee and sour bean fruits in a mass ratio of 1:3 into powder of 100 meshes and 150 meshes, treating for 30min at the temperature of 120 ℃ and the pressure of 0.2MPa, and drying for 2h at the temperature of 60 ℃ for later use.
Weighing the mixed raw materials, mixing the mixed raw materials with an ethanol solution according to the mass ratio of 1:35, and extracting for 2 hours at 50 ℃;
(3) adding the customized camellia oil according to the mass ratio of 1:30, and extracting for 2h at the temperature of 45 ℃;
(4) cooling to 35 ℃, filtering at 80 meshes, and then concentrating under reduced pressure at 50 ℃ until the ethanol solvent is completely removed;
(5) cooling to 35 deg.C, fine-filtering with filter plate with aperture of 8um to clarify to obtain camellia seed oil containing hair care factor.
5. The hair care essence oil according to claim 3, wherein the customized camellia oil preparation method comprises the following steps:
(1) crushing camellia seed kernels obtained after husking camellia seeds to 200 meshes and 300 meshes, adding water, heating to 90 ℃, stirring for 30min, and filtering and then performing centrifugal treatment on filter residues for dehydration;
(2) mixing camellia seed kernel filter residue and an enzymolysis liquid solution according to a mass ratio of 2:5, heating to 38 ℃, preserving heat, sealing and placing for 35 minutes, then heating to 52 ℃, preserving heat, sealing and placing for 1 hour, and then cooling to room temperature;
(3) taking out the enzymolyzed semen Camelliae Japonicae, filtering to obtain residue, oven drying at 48 deg.C, placing under 1.9MPa, and exploding to obtain slurry;
(4) putting the obtained slurry into a pressure tank, vacuumizing, filling argon, setting the pressure to be 2.5Pa for 5 minutes, carrying out homogenizing shearing at 10000rpm, then centrifuging, separating an oil layer, removing residues, taking an emulsion layer, adding modified carboxymethyl cellulose powder with the mass of 0.5 per thousand of that of the emulsion layer, placing the emulsion layer into microwave equipment, treating for 2 minutes in 350MHz microwave frequency and 350W power, placing the emulsion layer into 10000rpm, carrying out homogenizing shearing, centrifuging and layering, and combining oil layers to obtain crude oil slurry;
(5) adding the crude oil slurry into a supercritical CO2 device, setting the initial pressure at 3MPa, increasing the pressure at 0.5MPa per minute, and maintaining the pressure at 12MPa for 30min for extraction to obtain the customized camellia seed oil.
6. The hair care essence oil according to claim 4, wherein in the step (2), the enzymatic hydrolysate is prepared by mixing a citric acid solution with a mass concentration of 45% and soy protein powder according to a mass ratio of 1:0.8 to prepare a soy protein solution, heating to 95 ℃, keeping the temperature for 15min, cooling the swollen soy protein solution to 20 ℃, and adding cellulase, protease and water into the soy protein solution for enzymolysis;
the hair care essence oil according to claim 5, wherein the soy protein solution is prepared by adding 3000U of cellulase, 2000U of protease and 400mL of water into every gram of soy protein solution and mixing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210662825.4A CN114796028A (en) | 2022-06-13 | 2022-06-13 | Hair care essence oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210662825.4A CN114796028A (en) | 2022-06-13 | 2022-06-13 | Hair care essence oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN114796028A true CN114796028A (en) | 2022-07-29 |
Family
ID=82521475
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210662825.4A Pending CN114796028A (en) | 2022-06-13 | 2022-06-13 | Hair care essence oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN114796028A (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101484131A (en) * | 2006-07-03 | 2009-07-15 | 株式会社资生堂 | Cosmetic hair preparation |
| JP2014015418A (en) * | 2012-07-09 | 2014-01-30 | Kracie Home Products Ltd | Hair cosmetic |
| KR20150109232A (en) * | 2014-03-19 | 2015-10-01 | 초임계연구소 주식회사 | Process for Manufacturing Camellia seed Oil of High Oxidative Stability and Low Color with Supercritical Fluid |
| CN110923053A (en) * | 2019-11-09 | 2020-03-27 | 贵州石阡佛顶山野生油茶油业有限公司 | Method for extracting tea oil with high freezing resistance |
| CN111374920A (en) * | 2020-04-26 | 2020-07-07 | 刘科勇 | Pure natural hair washing, hair care, moisturizing and repairing composition and preparation method thereof |
| CN111529435A (en) * | 2020-05-20 | 2020-08-14 | 无限极（中国）有限公司 | Hair care essential oil |
-
2022
- 2022-06-13 CN CN202210662825.4A patent/CN114796028A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101484131A (en) * | 2006-07-03 | 2009-07-15 | 株式会社资生堂 | Cosmetic hair preparation |
| JP2014015418A (en) * | 2012-07-09 | 2014-01-30 | Kracie Home Products Ltd | Hair cosmetic |
| KR20150109232A (en) * | 2014-03-19 | 2015-10-01 | 초임계연구소 주식회사 | Process for Manufacturing Camellia seed Oil of High Oxidative Stability and Low Color with Supercritical Fluid |
| CN110923053A (en) * | 2019-11-09 | 2020-03-27 | 贵州石阡佛顶山野生油茶油业有限公司 | Method for extracting tea oil with high freezing resistance |
| CN111374920A (en) * | 2020-04-26 | 2020-07-07 | 刘科勇 | Pure natural hair washing, hair care, moisturizing and repairing composition and preparation method thereof |
| CN111529435A (en) * | 2020-05-20 | 2020-08-14 | 无限极（中国）有限公司 | Hair care essential oil |
Non-Patent Citations (6)
| Title |
|---|
| 99健康网: "咖啡除了提神还有这功效", pages 6, Retrieved from the Internet <URL:https://ys.99.com.cn/qtyy/690963.htm> * |
| UFAVLIFE熙梵尼: "聚二甲基硅氧烷醇在护肤化妆品中的功效与作用", pages 2 - 3, Retrieved from the Internet <URL:https://www.kqmmm.com/cosmetic/202361.html> * |
| 吴景勉;田俊;赵丹;谷志静;王昌涛;: "植物"精油"的护发功效解析", 香料香精化妆品, no. 5, pages 64 - 68 * |
| 周泉诚, 吴谋成: "超临界CO_2萃取技术在油脂工业中的应用", 中国油脂, vol. 28, no. 3, pages 17 - 20 * |
| 欧莱雅: "卡诗菁纯亮泽经典香氛护发油 国妆网备进字（沪）2019000149", pages 1, Retrieved from the Internet <URL:https://hzpba.nmpa.gov.cn/jkcx/chakanjk.html?prodId=1087753688241405952&gb=J> * |
| 王姝畅;吴亚妮;: "山茶油在化妆品应用中的功效研究", 香料香精化妆品, no. 1, pages 67 - 71 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104413207B (en) | A kind of highland barley chrysanthemum teabag drink and preparation method thereof | |
| CN102266111B (en) | Husk and kernel separating method for fresh fruits of synsepalum dulcificum | |
| CN106109530A (en) | A kind of Folium Isatidis fresh squeezing spray-dried granules decoction pieces and preparation technology thereof | |
| CN109105822A (en) | A kind of processing method of konjaku powder | |
| WO2020257825A1 (en) | Natural composite materials derived from seaweed and methods of making the same | |
| CN105670815B (en) | A kind of tea seed cleanser and its preparation process | |
| CN103907993B (en) | A kind of sweet corn health beverage and preparation method thereof | |
| CN114796028A (en) | Hair care essence oil | |
| WO2017047191A1 (en) | Polyisoprene production method | |
| CN108403574A (en) | A kind of preparation method based on purple rice extracting solution whitening moisturizing face masque | |
| CN107773479A (en) | A kind of agalloch eaglewood stoste | |
| CN115957275A (en) | Traditional Chinese medicine eye drop for eye care and preparation method thereof | |
| CN110711160A (en) | Plant formula with effects of lifting, tightening and resisting wrinkles and application thereof | |
| CN110893158A (en) | Composition with scalp care function and preparation method thereof | |
| JPH11255657A (en) | Agent for proliferating fibroblast and skin preparation used for external use and containing the same | |
| CN108379178A (en) | A kind of plant extracts topical composition and preparation method thereof with antiallergic sense | |
| CN108283289A (en) | Instant powder product rich in purpurin | |
| CN114920856A (en) | Method for preparing high-whiteness konjac glucomannan from fine bulbil konjac powder | |
| CN1650737A (en) | Preparation method of hairgvein agrimony poly saccharide gum | |
| CN106986902A (en) | Improve the process for purification of GM1 finished product purity | |
| CN108684895A (en) | Threeleaf akebia tea bag composition and preparation method thereof | |
| CN109172643A (en) | A kind of Shuanhuanglian injection and its preparation process | |
| CN109528888A (en) | A kind of arisaema cum bile purification medicine materical crude slice and preparation method thereof | |
| TWI734589B (en) | Method for preparing passion fruit flower extract and passion fruit flower extract | |
| CN108617903A (en) | Barley young leaf green juice and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |