CN114618658A - Grinding dispersion machine for graphene preparation and cleaning method thereof - Google Patents
Grinding dispersion machine for graphene preparation and cleaning method thereof Download PDFInfo
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- CN114618658A CN114618658A CN202210283578.7A CN202210283578A CN114618658A CN 114618658 A CN114618658 A CN 114618658A CN 202210283578 A CN202210283578 A CN 202210283578A CN 114618658 A CN114618658 A CN 114618658A
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- 238000000227 grinding Methods 0.000 title claims abstract description 132
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 56
- 229910021389 graphene Inorganic materials 0.000 title claims abstract description 50
- 239000006185 dispersion Substances 0.000 title claims abstract description 39
- 238000002360 preparation method Methods 0.000 title claims abstract description 22
- 238000000034 method Methods 0.000 title claims description 15
- 238000004140 cleaning Methods 0.000 title claims description 9
- 238000002156 mixing Methods 0.000 claims abstract description 68
- 238000007789 sealing Methods 0.000 claims abstract description 32
- 239000000463 material Substances 0.000 claims abstract description 15
- 239000002270 dispersing agent Substances 0.000 claims abstract description 9
- 229910002804 graphite Inorganic materials 0.000 claims abstract description 7
- 239000010439 graphite Substances 0.000 claims abstract description 7
- 239000007788 liquid Substances 0.000 claims description 23
- 238000012545 processing Methods 0.000 claims description 3
- 239000010865 sewage Substances 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- -1 graphite alkene Chemical class 0.000 claims 1
- 239000011325 microbead Substances 0.000 abstract description 15
- 239000011550 stock solution Substances 0.000 abstract description 9
- 239000002994 raw material Substances 0.000 abstract description 7
- 239000000243 solution Substances 0.000 abstract description 4
- 238000007599 discharging Methods 0.000 abstract 2
- 238000003756 stirring Methods 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000001125 extrusion Methods 0.000 description 3
- 238000010248 power generation Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 230000000149 penetrating effect Effects 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 238000013508 migration Methods 0.000 description 1
- 230000005012 migration Effects 0.000 description 1
- 230000036651 mood Effects 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000011882 ultra-fine particle Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C19/00—Other disintegrating devices or methods
- B02C19/0056—Other disintegrating devices or methods specially adapted for specific materials not otherwise provided for
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C23/00—Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C23/00—Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
- B02C23/18—Adding fluid, other than for crushing or disintegrating by fluid energy
- B02C23/36—Adding fluid, other than for crushing or disintegrating by fluid energy the crushing or disintegrating zone being submerged in liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B15/00—Preventing escape of dirt or fumes from the area where they are produced; Collecting or removing dirt or fumes from that area
- B08B15/02—Preventing escape of dirt or fumes from the area where they are produced; Collecting or removing dirt or fumes from that area using chambers or hoods covering the area
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
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- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Mechanical Engineering (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The invention relates to the technical field of graphite preparation, in particular to a grinding dispersion machine for graphene preparation, which comprises a dispersion machine main body, wherein a dispersing agent discharging pipe is fixedly connected to one side of the dispersion machine main body, a grinding barrel bin is fixedly connected to one end of one side of the dispersion machine main body, a discharging port is formed in one end of one side of the grinding barrel bin, and an anti-splashing mechanism is hinged to one end of one side of the grinding barrel bin through a hinged shaft. According to the invention, when the microbeads are stirred by the rotary material conveying sheet, the collision friction force formed among the microbeads is quickly contacted with the graphene stock solution sucked in the mixing bin, so that the grinding efficiency of the graphene stock solution is increased, the surface of the grinding barrel bin is covered by the cover plate, so that the sealing property in the grinding barrel bin is increased during operation, and the problem that the raw material solution stored in the grinding barrel bin can splash outwards and drop to cause certain material loss due to high-speed rotation of the inner stator and rotor and the auxiliary grinding mechanism during use is avoided.
Description
Technical Field
The invention relates to the technical field of graphite preparation, in particular to a grinding dispersion machine for graphene preparation and a cleaning method thereof.
Background
Graphene is the thinnest and the hardest nanomaterial in the world at present, and is the material with the smallest resistivity in the world. Because of its extremely low resistivity and fast electron migration, it is expected to be used to develop a new generation of thinner and faster conductive electronic components or transistors, and since graphene is a transparent and good conductor in nature, and is also suitable for manufacturing transparent touch screens, optical panels, and even solar cells, more and more manufacturers are beginning to research and produce graphene;
in the existing production and preparation process of graphene, a graphite grinding disperser is often needed to be used, so that graphene slurry forms turbulence at the high linear speed of equipment, the graphene slurry is continuously impacted, crushed, ground, dispersed and homogenized in gaps between a stator and a rotor, and a certain proper dispersing agent is added as an auxiliary agent, so that ultrafine particles are obtained. The working efficiency is seriously influenced, the grinding of the stator and the rotor has certain limitation, if a large amount of graphene mixed liquid is contained in the grinding cylinder wall, the grinding and stirring are carried out by the independent stator and rotor, and more graphene mixed liquid cannot be stirred, so that the stirring and grinding speed is reduced, and the production efficiency of machinery is influenced;
in the existing patent solution, CN107204735A is an energy-saving graphene dispersing machine, which includes a base, a sampler, a dispersing barrel, and a photovoltaic power generation device, where the photovoltaic power generation device includes a photovoltaic panel, a retraction mechanism, a folding mechanism and an adjustment mechanism, the retraction mechanism includes a support plate, a sliding plate and a driving component, the folding mechanism includes a fixed block, a folding rod, a second motor, a driving wheel and a connecting rope, and the adjustment mechanism includes a rotating shaft, a third motor, a driving wheel, a driven wheel, a belt and an adjusting rod, and when the machine does not work, the energy-saving graphene dispersing machine can take out the photovoltaic power generation device, place the machine in the sun, convert solar energy into electric energy, so as to maintain the high-speed operation of the machine during operation, reduce energy consumption of factories and industrial production cost, but the design needs to separately set the photovoltaic panel, so that it only simply relies on increasing input power, the rate-increasing effect is not significant enough and the cost is high.
Disclosure of Invention
The invention aims to provide a grinding dispersion machine for graphene preparation and a cleaning method thereof, and aims to solve the problems that in the prior art, certain defects still exist in practical use, mechanical grinding of a stator and a rotor can cause certain damage after being used for a long time, an operator needs to replace the stator and the rotor regularly, the operator wastes time and labor when replacing the stator and the rotor, and the stirring and grinding speed is reduced by grinding and stirring the stator and the rotor independently when a large amount of graphene mixed liquid is contained in the wall of a grinding cylinder.
In order to achieve the purpose, the invention provides the following technical scheme: a grinding dispersion machine for graphene preparation and a cleaning method thereof comprise a dispersion machine main body, wherein a dispersant blanking pipe is fixedly connected to one side of the dispersion machine main body, a grinding barrel bin is fixedly connected to one end of one side of the dispersion machine main body, a discharge port is formed in one end of one side of the grinding barrel bin, a rotary rod is arranged inside the discharge port, one end of the rotary rod is connected with the output end of the dispersion machine main body, a stator and a rotor are sleeved on the surface of the rotary rod, an auxiliary grinding mechanism is fixedly connected to the other end of the rotary rod and comprises a mixing bin, a fixing ring is arranged at one end of the mixing bin, a touch block is arranged on one side inside the fixing ring, a first connecting rod is fixedly connected to one end of the touch block, one end of the first connecting rod penetrates through the mixing bin to extend into the mixing bin, a first conical gear is sleeved on the surface of one end of the first connecting rod, a second interlocking rod is arranged in the mixing bin, two ends of the second interlocking rod are connected with the inner wall of the mixing bin through embedded bearings, a second bevel gear is sleeved on the surface of one end of the second interlocking rod and meshed with the first bevel gear, a piston pipeline is arranged in the middle of the surface of one end of the mixing bin, a fixed pipeline is arranged at one end of the piston pipeline, the periphery of the fixed pipeline is connected with the inner wall of the grinding barrel bin through a support frame, a moving block is arranged in the fixed pipeline, a pull rod is fixedly connected to one end of the moving block, one end of the pull rod penetrates through the piston pipeline and extends into the piston pipeline, a piston part is fixedly connected to one end of the pull rod, a liquid inlet is arranged at one side of the mixing bin, a first fixing part is fixedly connected to the inner wall of the liquid inlet, and a first sealing plate is arranged at one side of the first fixing part, the utility model discloses a grinding barrel, including grinding barrel storehouse, fixed connection, mixing bin, fixed connection, the surface cover of first mounting is equipped with first spring, the one end of first spring is connected with the fixed surface of first mounting, the other end of first spring is connected with first closing plate, the liquid outlet has been seted up to the opposite side of mixing the storehouse, fixedly connected with second mounting on the inner wall of liquid outlet, one side of second mounting is provided with the second and seals, the surface cover of second mounting is equipped with the second spring part, and the one end of second spring part and the sealed one end fixed connection of second, the other end of second spring part and the fixed surface of second mounting are connected, the inside in mixing the storehouse evenly is provided with the microballon, the one end of grinding barrel storehouse one side is through articulated to have the outer mechanism that spatters of preventing.
Preferably, the surface of the second linkage rod is uniformly sleeved with a rotary material conveying sheet, and the rotary material conveying sheet is spiral.
Preferably, the inner wall of the fixing ring is uniformly and fixedly connected with tooth blocks, and the surface of the contact block is uniformly and fixedly connected with tooth blocks.
Preferably, the surface of the piston piece is glued with a sealing gasket, and the surface of the sealing gasket is attached to the inner wall of the piston pipeline.
Preferably, a plug is fixedly connected to one side of the first sealing plate and one side of the second sealing plate, and a rubber pad is glued to the surface of the plug.
Preferably, the anti-splashing mechanism comprises a cover plate, a fixing plate is arranged on one side of the cover plate, one end of the fixing plate is fixedly connected with one end of the grinding barrel bin, a slot is formed in one side, close to the fixing plate, of the cover plate, a screwing threaded rod is inserted into one side of the fixing plate in a penetrating mode, and a screwing block is fixedly connected to one side of the screwing threaded rod.
Preferably, one side of the screwing threaded rod is semicircular, the inner wall of one end of the slot is inclined, and a rubber pad is glued on the surface of one side of the screwing threaded rod.
Preferably, the surface of the screwing block is glued with a non-slip mat, and the surface of the non-slip mat is provided with non-slip lines.
Preferably, a sealing ring is glued at one end of the cover plate, and the surface of the sealing ring is attached to the surface of one end of the grinding barrel bin.
A cleaning method of a grinding dispersion machine for graphene preparation is characterized by comprising the following steps: the method comprises the following specific operation steps:
the method comprises the following steps: after the user finishes processing the graphite, continuously injecting moisture into the grinding barrel bin, and then starting the dispersion machine main body;
step two: after the dispersion machine main body is opened, the rotating rod, the stator and the rotor and the auxiliary grinding mechanism quickly rotate in the grinding barrel bin, and certain vortexes are continuously generated in the grinding barrel bin due to the rotation of the stator and the rotor, so that residual stains on the wall of the barrel can be effectively removed when the grinding barrel bin is machined;
step three: the rotary rod is when the rotation, constantly drive simultaneously and assist grinding mechanism and carry out the rotation in grinding the inside of barrel storehouse simultaneously, the movable block can be according to rotary rod rotation direction, drive the piston spare and make sliding motion in piston tube's inside fast, make the inside water source of grinding barrel storehouse can not end and flow to the inside of mixing the storehouse, cooperation second trace drives the rotation of rotatory defeated tablet in mixing the inside of storehouse, can accomplish simultaneously fast and accomplish the clearance back to the clearance of mixing the inside of storehouse, through the discharge gate, can outwards discharge to the inside sewage of grinding barrel storehouse fast.
Compared with the prior art, the invention has the beneficial effects that: according to the invention, when the microbeads are stirred by the rotary material conveying sheet, the collision friction force formed among the microbeads is quickly contacted with the graphene stock solution sucked in the mixing bin, so that the grinding efficiency of the graphene stock solution is increased, the surface of the grinding barrel bin is covered by the cover plate, the sealing property in the grinding barrel bin is increased during operation, and the problem that when the grinding barrel bin is used, the raw material solution stored in the grinding barrel bin can splash outwards due to high-speed rotation of the inner stator and rotor and the auxiliary grinding mechanism, so that certain material loss is caused is avoided;
1. by arranging the auxiliary grinding mechanism, when a user uses the device to prepare graphene, a certain pressure difference is quickly formed inside the mixing bin, and through the pressure formed inside the mixing bin, the graphene raw material which can be stirred in the grinding barrel bin can rapidly enter the mixing bin to contact with the microbeads, and the microbeads roll in the mixing bin, can fully contact with the graphene raw material, quickly contact with the graphene stock solution sucked in the mixing bin through the contact friction force formed between the microbeads when the microbeads are stirred by the rotary material conveying sheet to quickly grind the graphene stock solution, increase the grinding efficiency of the graphene stock solution, and match with a stator and a rotor, the high-speed autorotation grinding in the grinding barrel bin greatly enhances the production efficiency of the device on the graphene stock solution, is convenient for users to use, and greatly enhances the practical application of the device on graphene grinding dispersion;
2. through being provided with and preventing outer mechanism that spatters, the device is when using, the user can directly draw and draw the apron, make the apron do circular motion fast, until covering the surface that grinds the bucket storehouse, the user can be quick is twisted and is moved the piece of twisting, make it move the inside that the threaded rod got into the slot fast to twist, form certain decurrent extrusion to the apron and leave, can make the quick surface that covers in the grinding bucket storehouse of apron, when the increase operation, grind the inside leakproofness in bucket storehouse, the inside raw materials liquid of depositing in the grinding bucket storehouse that leads to because of its inside stator and rotor and supplementary grinding mechanism's high-speed rotation can outwards splash down when avoiding using, reduce the loss of material, avoid the material directly to drip around operational environment, cause the pollution to surrounding environment, the use mood of operating personnel is said in the influence, the user has strengthened the application range of device simultaneously.
Drawings
FIG. 1 is a schematic sectional elevation view of the structure of the present invention;
FIG. 2 is a schematic sectional view of the grinding barrel chamber in front view;
FIG. 3 is an enlarged view of the structure A in FIG. 2 according to the present invention;
FIG. 4 is an enlarged view of the structure of B in FIG. 2 according to the present invention;
FIG. 5 is an enlarged view of the structure C in FIG. 2 according to the present invention;
FIG. 6 is a schematic top sectional view of the grinding barrel compartment of the present invention;
FIG. 7 is a schematic side view of the structure of the present invention;
fig. 8 is a schematic front view of the structure of the present invention.
In the figure: 100. a disperser body; 200. a dispersant feeding pipe; 300. grinding the barrel bin; 400. a discharge port; 500. rotating the rod; 600. a stator and a rotor; 700. an auxiliary grinding mechanism; 710. a mixing bin; 711. a stationary ring; 712. a contact block; 713. a first linkage rod; 714. a first bevel gear; 715. a second linkage rod; 716. rotating the material conveying sheet; 717. a second bevel gear; 718. a piston conduit; 719. fixing the pipeline; 720. a moving block; 721. a pull rod; 722. a piston member; 723. a liquid inlet; 724. a first fixing member; 725. a first sealing plate; 726. a first spring; 727. a liquid outlet; 728. a second fixing member; 729. a second spring member; 730. a second sealing plate; 731. microbeads; 800. an anti-splatter mechanism; 810. a cover plate; 811. a slot; 812. a fixing plate; 813. screwing the threaded rod; 814. and (5) screwing the block.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-8, an embodiment of the present invention:
a grinding dispersion machine for graphene preparation and a cleaning method thereof comprise a dispersion machine main body 100, wherein one side of the dispersion machine main body 100 is fixedly connected with a dispersing agent blanking pipe 200, one end of one side of the dispersion machine main body 100 is fixedly connected with a grinding barrel bin 300, one end of one side of the grinding barrel bin 300 is provided with a discharge hole 400, the inside of the discharge hole 400 is provided with a rotating rod 500, one end of the rotating rod 500 is connected with the output end of the dispersion machine main body 100, the surface of the rotating rod 500 is sleeved with a stator 600, the other end of the rotating rod 500 is fixedly connected with an auxiliary grinding mechanism 700, the auxiliary grinding mechanism 700 comprises a mixing bin 710, one end of the mixing bin 710 is provided with a fixing ring 711, one side of the inside of the fixing ring 711 is provided with a contact block 712, one end of the contact block 712 is fixedly connected with a first connecting rod 713, one end of the first connecting rod 713 passes through the mixing bin 710 and extends to the inside of the mixing bin 710, a first conical gear 714 is sleeved on the surface of one end of a first linkage bar 713, a second linkage bar 715 is arranged inside the mixing bin 710, two ends of the second linkage bar 715 are connected with the inner wall of the mixing bin 710 through embedded bearings, a second conical gear 717 is sleeved on the surface of one end of the second linkage bar 715, the second conical gear 717 is meshed with the first conical gear 714, a piston pipeline 718 is arranged in the middle of the surface of one end of the mixing bin 710, a fixed pipeline 719 is arranged at one end of the piston pipeline 718, the periphery of the fixed pipeline 719 is connected with the inner wall of the grinding barrel bin 300 through a support frame, a moving block 720 is arranged inside the fixed pipeline 719, a pull rod 721 is fixedly connected to one end of the moving block 720, one end of the pull rod 721 penetrates through the piston pipeline 718 to extend into the piston pipeline 718, a piston member is fixedly connected to one end of the pull rod 721, a liquid inlet 723 is arranged on one side of the mixing bin 710, a first fixing member 724 is fixedly connected to the inner wall of the liquid inlet 723, a first sealing plate 725 is arranged on one side of the first fixing member 724, a first spring 726 is sleeved on the surface of the first fixing member 724, one end of the first spring 726 is fixedly connected to the surface of the first fixing member 724, the other end of the first spring 726 is connected to the first sealing plate 725, a liquid outlet 727 is arranged on the other side of the mixing bin 710, a second fixing member 728 is fixedly connected to the inner wall of the liquid outlet 727, a second seal 730 is arranged on one side of the second fixing member 728, a second spring member 729 is sleeved on the surface of the second fixing member 728, one end of the second spring part 729 is fixedly connected with one end of the second seal 730, the other end of the second spring part 729 is fixedly connected with the surface of the second fixing part 728, the interior of the mixing bin 710 is uniformly provided with micro beads 731, and one end of one side of the grinding barrel bin 300 is hinged with an anti-splashing mechanism 800 through a hinge shaft;
furthermore, the surface of the second linkage 715 is uniformly sleeved with a rotary material-conveying sheet 716, and the rotary material-conveying sheet 716 is spiral, when the first conical gear 714 is continuously engaged with the second conical gear 717, the second linkage 715 drives the rotary material-conveying sheet 716 to rapidly rotate inside the mixing bin 710, and when the rotary material-conveying sheet 716 is spiral, the rotary material-conveying sheet 716 continuously forms a stirring force for the micro beads 731 stored inside the mixing bin 710, so that the micro beads 731 rapidly rolls inside the mixing bin 710 to be fully contacted with each other after being stressed;
further, the inner wall of the fixed ring 711 is uniformly and fixedly connected with a tooth block, the surface of the collision block 712 is uniformly and fixedly connected with a tooth block, when the mixing bin 710 rotates, the mixing bin 710 continuously drives the first linkage rod 713 and the collision block 712 to rotate in the same direction, the collision block 712 continuously and rapidly collides with the teeth inside the fixed ring 711, after the collision block 712 is stressed, the first linkage rod 713 is rapidly driven to rotate, and when the first linkage rod 713 rotates, the first conical gear 714 is driven to simultaneously rotate and continuously meshes with the second conical gear 717, so that the second linkage rod 715 is linked;
further, a sealing gasket is glued on the surface of the piston member 722, the surface of the sealing gasket is attached to the inner wall of the piston pipe 718, and the sealing gasket glued on the surface of the piston member 722 ensures that the air tightness inside the piston pipe 718 is well ensured when the piston member 722 runs inside the piston pipe 718;
furthermore, one side of the first sealing plate 725 and one side of the second seal 730 are fixedly connected with a plug, the surface of the plug is glued with a rubber pad, the plug is fixedly connected with one side of the first sealing plate 725 and one side of the second seal 730, and the surface of the plug is glued with the rubber pad, when the pressure difference is formed between the interior of the mixing bin 710 and the interior of the grinding barrel bin 300, the first sealing plate 725 and the second seal 730 move to drive the plug at one side to enter the interior of the first fixing piece 724 or the second fixing piece 728, and the rubber pad is mutually attached to the inner wall of the first fixing piece 724 or the second fixing piece 728, so that the air tightness of the interior can be effectively ensured;
further, the anti-splashing mechanism 800 comprises a cover plate 810, a fixing plate 812 is arranged on one side of the cover plate 810, one end of the fixing plate 812 is fixedly connected with one end of the grinding barrel bin 300, a slot 811 is formed in one side, close to the fixing plate 812, of the cover plate 810, a screwing threaded rod 813 is inserted into one side of the fixing plate 812 in a penetrating manner, a screwing block 814 is fixedly connected to one side of the screwing threaded rod 813, when the anti-splashing mechanism 800 is used by a user, the cover plate 810 is pulled by the user, the cover plate 810 rapidly performs circular motion through an articulated shaft, one end of the cover plate 810 covers the surface of one end of the grinding barrel bin 300, the interior of the grinding barrel bin 300 can be effectively sealed relatively, and graphene raw liquid thrown in the grinding barrel bin 300 is prevented from being stirred and splashing outwards when the dispersion machine main body 100 is opened;
furthermore, one side of the screwing threaded rod 813 is semicircular, the inner wall of one end of the slot 811 is inclined, a rubber pad is glued on the surface of one side of the screwing threaded rod 813, one side of the screwing threaded rod 813 is semicircular and the inner wall of one end of the slot 811 is inclined, when one end of the screwing threaded rod 813 continuously extends into the slot 811, one end of the screwing threaded rod 813 continuously abuts against the inner wall of one end of the slot 811 at the same time, certain extrusion force is rapidly formed on the cover plate 810, the cover plate 810 can be rapidly attached to the surface of one end of the grinding barrel bin 300 in a stressed mode, and the interior of the grinding barrel bin 300 is relatively sealed;
furthermore, the surface of the screwing block 814 is glued with an anti-slip pad, the surface of the anti-slip pad is provided with anti-slip threads, and the surface of the screwing block 814 is glued with the anti-slip pad, so that the friction force generated by the hand of a user during screwing can be increased, and the slipping phenomenon is avoided;
furthermore, a sealing ring is glued at one end of the cover plate 810, the surface of the sealing ring is attached to the surface of one end of the grinding barrel bin 300, and the sealing ring glued at one end of the cover plate 810 can effectively ensure the air tightness inside the grinding barrel bin 300 when one end of the cover plate 810 is attached to the surface of one end of the grinding barrel bin 300.
A cleaning method of a grinding dispersion machine for graphene preparation is characterized by comprising the following steps: the method comprises the following specific operation steps:
the method comprises the following steps: after finishing processing graphite, a user continuously injects moisture into the grinding barrel bin 300, and then starts the disperser main body 100;
step two: after the dispersion machine main body 100 is opened, the rotating rod 500, the stator and rotor 600 and the auxiliary grinding mechanism 700 rapidly rotate in the grinding barrel bin 300, and the rotation of the stator and rotor 600 continuously generates a certain vortex in the grinding barrel bin 300, so that the residual stains on the barrel wall can be effectively removed when the grinding barrel bin 300 is machined;
step three: the rotating rod 500 is when the rotation, constantly drive the supplementary grinding mechanism 700 and carry out the rotation inside grinding barrel storehouse 300 simultaneously, the movable block 720 can drive the piston part 722 to make sliding motion in the inside of piston pipeline 718 fast according to the rotating rod 500 rotation direction, make the inside water source of grinding barrel storehouse 300 not end to flow to the inside of mixing storehouse 710, cooperation second trace 715 drives the rotation of rotatory defeated material piece 716 in mixing storehouse 710 inside, can accomplish simultaneously fast and accomplish the clearance back to the inside clearance completion of mixing storehouse 710, through discharge gate 400, can discharge outside to the inside sewage of grinding barrel storehouse 300 fast.
The working principle is as follows: when a user uses the device, the user can directly put graphene raw materials to be ground into the grinding barrel bin 300, then the dispersant feeding pipe 200 is opened, so that the dispersant feeding pipe 200 continuously injects a certain dispersant into the grinding barrel bin 300, after such operation is completed, the user can quickly pull the cover plate 810, the cover plate 810 quickly makes circular motion through the hinge shaft until one end of the cover plate 810 covers the surface of one end of the grinding barrel bin 300, then the user can quickly screw the screwing block 814, the screwing block 814 is matched with the thread structure arranged on the fixing plate 812, so that one end of the screwing threaded rod 813 continuously extends into the slot 811, one end of the screwing threaded rod 813 continuously abuts against the inner wall of one end of the slot 811, a certain extrusion force is quickly formed on the cover plate 810, the cover plate 810 can be stressed quickly to be attached to the surface of one end of the grinding barrel bin 300, the inside of the grinding barrel bin 300 is relatively sealed;
then, the user can open the dispenser body 100 in the forward direction, so that the output end of the dispenser body 100 continuously drives the rotating rod 500 to drive the stator and rotor 600 to rotate in the grinding barrel bin 300 in the forward direction at a high speed, a certain vortex is generated by the rotation of the stator and rotor 600, the graphene raw material put in the interior of the grinding barrel bin is stirred and ground, due to the rotation of the rotating rod 500, the mixing bin 710 rotates in the same direction in the grinding barrel bin 300 at a high speed, the mixing bin 710 simultaneously drives the first connecting rod 713 and the collision block 712 to rotate in the same direction, the collision block 712 continuously collides with the teeth inside the fixing ring 711 in the fixing ring 711, after the collision block 712 is stressed, the first connecting rod 713 is rapidly driven to rotate, the first connecting rod 713 drives the first bevel gear 714 to rotate simultaneously while rotating, and meshes with the second bevel gear 717, after the second bevel gear 717 is engaged, the second linkage bar 715 is rapidly driven to rotate in the mixing bin 710, when the second linkage bar 715 rotates in the mixing bin 710, the rotary material conveying sheet 716 can rapidly rotate and stir the micro beads 731 stored in the mixing bin 710, meanwhile, as the mixing bin 710 rotates in the disperser main body 100, the moving block 720 at one end is continuously driven to rotate in the same direction, the moving block 720 is in the fixed pipeline 719, through the mutual cooperation of the thread structures, the moving block 720 can continuously generate a downward sliding force in the fixed pipeline, the pull rod 721 and the piston 722 are driven to generate a downward displacement in the piston pipeline 718, the piston 722 is driven, so that the pressure in the mixing bin 710 gradually starts to increase, the pressure in the mixing bin 710 is rapidly increased with the pressure in the grinding barrel bin 300 to form a certain pressure difference, and through the pressure difference formed in the grinding barrel bin 300, the second seal 730 can be stressed continuously and move towards one side of the interior of the grinding barrel bin 300 rapidly, the second seal 730 can continuously pull the second spring part 729 while moving, the second spring part 729 is stressed and deformed, the interior of the second fixing part 728 is opened outwards, graphene raw liquid ground inside the grinding barrel bin 300 is rapidly sucked into the interior of the mixing bin 710 through the second fixing part 728, the graphene raw liquid ground inside the grinding barrel bin 300 is matched with the rotating transmission sheet 716 to stir the micro beads 731, the micro beads 731 are mutually collided and fully contacted with the graphene raw liquid absorbed inside the mixing bin 710, the graphene raw liquid is ground and dispersed continuously, the grinding and dispersing effect on graphene is enhanced by matching with the stator and rotor 600, otherwise, a user operates the dispersion machine main body 100, reversely rotates the rotating rod 500 inside the grinding barrel bin 300, and can enable the mixing bin 710 to reversely rotate inside the grinding barrel bin 300, in the same way, the moving block 720 can rotate reversely inside the fixed pipeline 719, the moving block 720 can drive the pull rod 721 and the piston 722 to move upwards inside the piston pipeline 718, so as to suck the pressure inside the mixing bin 710 quickly, and form a pressure difference with the pressure inside the grinding barrel bin 300 again, so that the first sealing plate 725 is subjected to the pressure difference and moves quickly to the inside of the mixing bin 710, while the first sealing plate 725 moves, the first spring 726 can be continuously pulled, so that the first spring 726 is deformed when being stressed, and graphene stock solution well dispersed inside the mixing bin 710 can be effectively discharged to the inside of the grinding barrel bin 300 through the first fixing part 724.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Claims (10)
1. The utility model provides a graphite alkene preparation is with grinding dispenser, includes dispenser main part (100), its characterized in that: one side of the dispersion machine main body (100) is fixedly connected with a dispersant blanking pipe (200), one end of one side of the dispersion machine main body (100) is fixedly connected with a grinding barrel bin (300), one end of one side of the grinding barrel bin (300) is provided with a discharge hole (400), a rotary rod (500) is arranged inside the discharge hole (400), one end of the rotary rod (500) is connected with the output end of the dispersion machine main body (100), the surface of the rotary rod (500) is sleeved with a stator and rotor (600), the other end of the rotary rod (500) is fixedly connected with an auxiliary grinding mechanism (700), the auxiliary grinding mechanism (700) comprises a mixing bin (710), one end of the mixing bin (710) is provided with a fixing ring (711), one side of the inside of the fixing ring (711) is provided with a touch block (712), and one end of the touch block (712) is fixedly connected with a first connecting rod (713), one end of the first linkage rod (713) penetrates through the mixing bin (710) and extends into the mixing bin (710), a first conical gear (714) is sleeved on the surface of one end of the first linkage rod (713), a second linkage rod (715) is arranged inside the mixing bin (710), two ends of the second linkage rod (715) are connected with the inner wall of the mixing bin (710) through embedded bearings, a second conical gear (717) is sleeved on the surface of one end of the second linkage rod (715), the second conical gear (717) is meshed with the first conical gear (714), a piston pipeline (718) is arranged in the middle of the surface of one end of the mixing bin (710), a fixed pipeline (719) is arranged at one end of the piston pipeline (718), the periphery of the fixed pipeline (719) is connected with the inner wall of the grinding barrel bin (300) through a support frame, and a moving block (720) is arranged inside the fixed pipeline (719), one end of the moving block (720) is fixedly connected with a pull rod (721), one end of the pull rod (721) penetrates through the piston pipeline (718) and extends into the piston pipeline (718), one end of the pull rod (721) is fixedly connected with a piston component (722), one side of the mixing bin (710) is provided with a liquid inlet (723), the inner wall of the liquid inlet (723) is fixedly connected with a first fixing component (724), one side of the first fixing component (724) is provided with a first sealing plate (725), the surface of the first fixing component (724) is sleeved with a first spring (726), one end of the first spring (726) is fixedly connected with the surface of the first fixing component (724), the other end of the first spring (726) is connected with the first sealing plate (725), the other side of the mixing bin (710) is provided with a liquid outlet (727), the inner wall of the liquid outlet (727) is fixedly connected with a second fixing component (728), one side of second mounting (728) is provided with the sealed (730) of second, the surface cover of second mounting (728) is equipped with second spring part (729), and the one end of second spring part (729) and the one end fixed connection of the sealed (730) of second, the other end of second spring part (729) and the fixed surface connection of second mounting (728), the inside of mixing storehouse (710) evenly is provided with microballon (731), the one end of grinding barrel storehouse (300) one side is articulated through the articulated shaft and is had to prevent outer splash mechanism (800).
2. The grinding dispersion machine for graphene preparation according to claim 1, characterized in that: the surface of the second linkage rod (715) is uniformly sleeved with a rotary material conveying sheet (716), and the rotary material conveying sheet (716) is spiral.
3. The grinding dispersion machine for graphene preparation according to claim 1, characterized in that: the inner wall of the fixing ring (711) is uniformly and fixedly connected with tooth blocks, and the surface of the contact block (712) is uniformly and fixedly connected with tooth blocks.
4. The grinding dispersion machine for graphene preparation according to claim 1, wherein: the surface of the piston piece (722) is glued with a sealing gasket, and the surface of the sealing gasket is attached to the inner wall of the piston pipeline (718).
5. The grinding dispersion machine for graphene preparation according to claim 1, characterized in that: one side of the first sealing plate (725) and one side of the second sealing plate (730) are fixedly connected with plugs, and rubber pads are glued on the surfaces of the plugs.
6. The grinding dispersion machine for graphene preparation according to claim 1, characterized in that: prevent outer mechanism (800) of spattering including apron (810), one side of apron (810) is provided with fixed plate (812), and the one end of fixed plate (812) and the one end looks fixed connection who grinds bucket storehouse (300), slot (811) have been seted up to one side that apron (810) and fixed plate (812) are close to mutually, one side of fixed plate (812) is run through to be inserted and is equipped with and twist threaded rod (813), and twists one side fixedly connected with of threaded rod (813) and twist piece (814).
7. The grinding dispersion machine for graphene preparation according to claim 6, characterized in that: one side of the screwing threaded rod (813) is semicircular, the inner wall of one end of the slot (811) is inclined, and a rubber pad is glued on the surface of one side of the screwing threaded rod (813).
8. The grinding dispersion machine for graphene preparation according to claim 6, characterized in that: the surface of the screwing block (814) is glued with a non-slip mat, and the surface of the non-slip mat is provided with non-slip lines.
9. The grinding dispersion machine for graphene preparation according to claim 6, characterized in that: and a sealing ring is glued at one end of the cover plate (810), and the surface of the sealing ring is attached to the surface of one end of the grinding barrel bin (300).
10. A cleaning method of a grinding dispersion machine for graphene preparation is characterized by comprising the following steps: the method comprises the following specific operation steps:
the method comprises the following steps: after finishing processing graphite, a user continuously injects moisture into the grinding barrel bin (300), and then starts the disperser main body (100);
step two: after the dispersion machine main body (100) is opened, the rotating rod (500), the stator and rotor (600) and the auxiliary grinding mechanism (700) rapidly rotate in the grinding barrel bin (300), and certain vortex is continuously generated in the grinding barrel bin (300) due to the rotation of the stator and rotor (600), so that residual stains on the barrel wall can be effectively removed when the grinding barrel bin (300) is machined;
step three: when the rotation of rotary rod (500), constantly drive simultaneously and assist grinding mechanism (700) and carry out the rotation in grinding barrel storehouse (300) inside simultaneously, movable block (720) can be according to rotary rod (500) rotation direction, it makes sliding motion to drive piston spare (722) fast in the inside of piston pipeline (718), make the inside water source of grinding barrel storehouse (300) not end to the inside of mixing storehouse (710) flow, cooperation second trace (715) drive rotatory defeated tablet (716) at the inside rotation of mixing storehouse (710), can accomplish simultaneously fast and accomplish the clearance back to the inside clearance completion in mixing storehouse (710), through discharge gate (400), can discharge outside to the inside sewage of grinding barrel storehouse (300) fast.
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