CN114602409B - Preparation method of compound for anodic oxidation normal-temperature rapid oxidant - Google Patents
Preparation method of compound for anodic oxidation normal-temperature rapid oxidant Download PDFInfo
- Publication number
- CN114602409B CN114602409B CN202210291258.6A CN202210291258A CN114602409B CN 114602409 B CN114602409 B CN 114602409B CN 202210291258 A CN202210291258 A CN 202210291258A CN 114602409 B CN114602409 B CN 114602409B
- Authority
- CN
- China
- Prior art keywords
- rod
- block
- preparation
- reaction
- matching
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/02—Anodisation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
A preparation method of a compound for an anodic oxidation normal-temperature rapid oxidant belongs to the technical field of compound preparation, and aims to solve the problems that a preparation device is complex and heavy in components, difficult to operate, long in preparation period, high in preparation cost, easy to cause dirt to enter a reaction container in the repeated opening process, and influence the preparation quality, and the wall surface of the reaction container is easy to be contaminated with materials, so that the proportion of each reaction component is influenced; according to the invention, the opening and closing of the arc-shaped baffle plate can be controlled by rotating the tray body for one circle, so that the reaction raw materials can be conveniently added in different reaction time without opening the reaction container; according to the invention, the stirring assembly can be controlled to stir and mix the reaction materials by repeatedly rotating the driving gear in the forward direction, and the two ends of the arc body round rod can be controlled to repeatedly strike the container shell, so that the materials stained on the inner wall surface naturally drop, the integrity of the reaction materials is maintained, a plurality of linkage mechanisms can be realized by one power component, the operation is convenient, and the preparation cost can be saved.
Description
Technical Field
The invention relates to the technical field of compound preparation, in particular to a preparation method of a compound for an anodic normal-temperature rapid oxidant.
Background
The oxidizing agent is a substance that obtains electrons in a redox reaction, the oxidizing agent has oxidizing property to obtain electrons having a reduced valence, a reduction reaction is performed to obtain a reduced product, and the substance that obtains electrons in the redox reaction is called an oxidizing agent, and accordingly, the substance that loses electrons is called a reducing agent, and in a narrow sense, the oxidizing agent may refer to a substance that can obtain oxygen from another substance, and the fluorinating agent may refer to a substance that can obtain fluorine from a substance, a chlorinating agent, a brominating agent, and the like.
In the preparation process of the oxidant compound, all the reaction components are required to be mixed and stirred according to the distribution ratio of each reaction component, the adding time of each reaction component is different, the reaction container is required to be continuously started, the components of the preparation device are complicated and heavy, the operation is difficult, the preparation period is prolonged, the preparation cost is high, dirt is easy to enter the reaction container in the repeated starting process, the preparation quality is influenced, and the wall surface of the reaction container is easy to be contaminated with materials, so that the distribution ratio of each reaction component is influenced.
Aiming at the problems, the prior device is improved, and a preparation method of a compound for anodic oxidation normal-temperature rapid oxidant is provided.
Disclosure of Invention
The invention aims to provide a preparation method of a compound for an anodic oxidation normal-temperature rapid oxidant, which solves the problems that in the preparation process of the oxidant compound in the background technology, all reaction components are required to be mixed and stirred according to the distribution ratio of the reaction components, the addition time of the reaction components is different, a reaction container is required to be started continuously, the components of a preparation device are complicated and heavy, the operation is difficult, the preparation period is prolonged, the preparation cost is high, dirt is easy to enter the reaction container in the repeated opening process, the preparation quality is influenced, the wall surface of the reaction container is easy to be polluted, and the distribution ratio of the reaction components is influenced.
In order to achieve the above purpose, the present invention provides the following technical solutions: a preparation method of a compound for an anodic oxidation normal-temperature rapid oxidant comprises the following steps:
s01: at the initial stage of preparation: pouring a reaction solvent into a reaction container filled with purified water with a specified proportioning amount according to the proportioning, and fully stirring the solution by a stirring assembly to obtain a mixed solution;
s02: the preparation medium period: performing heat treatment on the mixed solution obtained in the initial stage, cooling and standing, layering the mixed solution, and classifying and storing the liquid of each layer;
s03: and (3) in the later preparation stage: and adding a subsequent reaction solvent into the liquid collected in the middle stage, and then carrying out drying heat treatment on the mixture to obtain oxidant powder.
Further, in S01, the reaction solvent is a compound of an acidic auxiliary agent, an oxidation-reduction auxiliary agent and a high polymer, and comprises, by weight:
10-20 parts of sulfuric acid;
5-10 parts of oxalic acid;
1-2 parts of formic acid;
1-2 parts of tartaric acid;
3-5 parts of urea;
3-5 parts of anhydrous sodium sulfate;
0.5-1 part of polymaleic acid;
2000.5-1 parts of polyethylene glycol;
0.5-1 part of glycerol;
100 parts of pure water.
Further, the lower extreme of reaction vessel is provided with a rest seat, the last surface mounting of rest seat has actuating mechanism, actuating mechanism's upper end is provided with traction mechanism, force application mechanism is installed to one side of traction mechanism, reaction vessel sets up the lower extreme at force application mechanism, hammering mechanism is installed in the outside of reaction vessel, rest seat includes the rest bottom plate and sets up the first spout that matches at rest bottom plate upper surface, the second spout that matches is seted up to one side of first spout that matches, first spout that matches is linked together with the second spout that matches, extension curb plate is installed to one side of rest bottom plate, the one end of extension curb plate is provided with vertical backplate, the top of vertical backplate is provided with the beam pole, the side surface of vertical backplate is provided with the extension diaphragm, limit profile cover is installed to the one end of extension diaphragm, traction mechanism includes traction carousel and sets up the first notch annular tooth face at traction carousel side surface, the outside of first notch annular tooth face is provided with the conveyer belt, traction carousel lower surface's central authorities install the traction pole setting, force application mechanism includes the reference column piece and sets up the rolling pier piece in the reference column piece lower extreme, the upper surface of reference column piece sets up the extension column piece, the one end is provided with the connecting rod through the installation groove, the connecting rod one end of connecting rod, the connecting rod one side of connecting rod is located to the stirring assembly, the stirring device is located the inside the connecting rod assembly.
Further, the rotation mound piece includes driven fluted disc and installs the spacing piece that rotates at driven fluted disc upper surface, driven fluted disc is connected with the reference column piece through spacing piece that rotates, the annular flank of second notch has been seted up to driven fluted disc's side surface, driven fluted disc's lower surface is provided with the splice piece, the conveyer belt is connected with first notch annular flank of tooth and the annular flank of second notch meshing, the stirring subassembly includes the center ball piece and sets up the inlet pipe in center ball piece one end, the discharging pipe is installed to the other end of center ball piece, center ball piece and spacing profile sleeve assorted, the ring handle has been cup jointed in the outside of discharging pipe one end, stirring horizontal pole is installed to the side surface of ring handle, stirring sharp teeth are installed to the one end of stirring horizontal pole, the ball chamber has been seted up to the inside of center ball piece, the inside of ball chamber is provided with holds the spherical shell, splice thin pole is installed to the both sides of holding the spherical shell, the one end of splice thin pole is connected with the inner wall of center ball piece.
Further, the upper end that holds the spherical shell is provided with arc baffle, the central authorities of arc baffle lower surface install the top depression bar, the one end of top depression bar is provided with spacing ball, the both sides of top depression bar all are provided with first connecting spring, first connecting spring's one end is connected with arc baffle, first connecting spring's the other end is connected with holding the spherical shell, the upper surface that holds the spherical shell has been seted up and has been slided the hole, it is connected with the top depression bar to slide the hole, the inside that holds the spherical shell is provided with the semicircle bottom block, reserve the movable groove has been seted up to the upper surface of semicircle bottom block, the upper end of reserving the movable groove is provided with the adjustment and establishes the carousel.
Further, transfer and establish the carousel and include the disk body and install the traction column piece at disk body side, traction column piece's one end is provided with extension joint strip pole, the adapter ring is installed to extension joint strip pole's one end, install the standing strip in one side of disk body, the one end of installing the standing strip is connected with the upper surface of semicircle bottom block, the other end of installing the standing strip is provided with semicircle and supports the briquetting, the lower surface mounting of disk body has the splice box, the connection draw-in groove has been seted up on the surface of disk body and splice box, the interior bottom surface of connection draw-in groove is provided with reset spring, reset spring's one end is connected with traction column piece's lower surface.
Further, the driving mechanism comprises a driving gear and a side flat toothed plate arranged on one side of the driving gear, the side flat toothed plate is meshed with the driving gear, a first matching strip is mounted on the lower surface of the side flat toothed plate, one end of the traction vertical rod is connected with the driving gear, and the first matching strip is connected with a second matching sliding groove.
Further, hammering mechanism includes the horizontal sliding plate that is connected with side flat pinion rack one end and installs the second matching strip at horizontal sliding plate lower surface, the second matching strip is connected with first matching spout, the upper surface of horizontal sliding plate is provided with horizontal flat tooth face, movable adjustment groove has all been seted up at the both ends of horizontal sliding plate, the upper end of horizontal sliding plate is provided with the arc round bar, the lower surface of arc round bar is provided with the arc tooth face, the arc tooth face is connected with horizontal flat tooth face meshing, the both ends of arc round bar all are provided with hammer hook, the pendulum rod is all installed to the both sides of arc round bar, the pendulum rod is provided with four groups of regulation.
Further, one end of the adjusting swing rod is provided with a rotating handle column, the center of the rotating handle column is provided with a sleeved rotating rod, the rotating handle column is arranged on the side surface of the arc body round rod, the rotating handle column is connected with one end of the adjusting swing rod through the sleeved rotating rod, the other end of the adjusting swing rod is provided with a movable pushing thin rod, and the movable pushing thin rod is connected with the movable adjusting groove.
Further, the reaction vessel is including setting up the container shell at extension diaphragm lower surface and installing the oblique strip pole of matching in container shell both sides, and the surface mounting of matching oblique strip pole has the laminating piece, and the hammer hook is laminated with the laminating piece mutually, and the inboard of matching oblique strip pole is provided with the striking piece, and the both ends of matching oblique strip pole all are provided with second coupling spring, and the one end of second coupling spring is connected with the surface of container shell.
Compared with the prior art, the invention has the beneficial effects that:
1. according to the preparation method of the compound for the normal-temperature rapid oxidant for anodic oxidation, which is provided by the invention, the driving gear is started, the traction upright rod drives the traction turntable to rotate in the same direction, the conveyer belt is connected with the first notch annular tooth surface and the second notch annular tooth surface in a meshed manner, the rotary pier block rotates along with the first notch annular tooth surface, the rotary pier block rotates relative to the positioning column block through the limiting rotating piece, the stirring assembly integrally rotates by taking the central sphere block as the axis under the acting force of the connecting rod, the limiting contour sleeve limits the central sphere block, the discharging pipe drives the stirring cross rod and the stirring sharp teeth to stir at multiple angles in the container shell, the moving direction of the discharging pipe is matched with the inner cavity of the container shell, the full mixing of reaction raw materials in the reaction container can be facilitated, the preparation period can be shortened, and the working efficiency can be improved.
2. According to the preparation method of the compound for the normal-temperature rapid oxidant for anodic oxidation, which is provided by the invention, the disc body is started, when the traction column block rotates to the semicircular pressing block, the top end of the traction column block is attached to the round end of the semicircular pressing block, along with the rotation of the disc body, the traction column block is positioned at the right lower end of the semicircular pressing block, the traction column block is extruded into the connecting through groove, the extended long connecting rod is pressed down along with the semicircular pressing block, the connecting ring is clamped with the limiting ball block, the top pressing rod drives the arc baffle to move down, the arc baffle is separated from the communicating part between the ball cavity and the inner part of the feeding pipe, when reaction raw materials are needed to be added at fixed time, the reaction raw materials enter the ball cavity through the feeding pipe and then enter the reaction container along the discharging pipe, when the traction column block is separated from the semicircular pressing block, the arc baffle can be restored to the original position by utilizing the elasticity of the first connecting spring and the reset spring, the arc baffle can be closed again, the opening and closing of the arc baffle can be controlled by rotating the disc body for a circle, the opening and closing of the arc baffle can be further convenient for adding reaction raw materials in different reaction time without disconnecting the inner part, and the inner part of the reaction container is prevented from being polluted, and the preparation efficiency is further avoided.
3. According to the preparation method of the compound for the normal-temperature rapid oxidant for anodic oxidation, when the driving gear is started, the driving gear is in meshed connection with the side flat toothed plate, the side flat toothed plate drives the transverse sliding plate to translate to one side, the arc round rod is driven to overturn to one side by virtue of meshed connection of the transverse flat toothed plate and the arc toothed plate, one end of the arc round rod is hammered to strike the laminating block, the laminating block drives the matched inclined rod to integrally approach the container shell, the plurality of groups of striking blocks collide with the outer wall of the container shell, so that materials adhered to the inner wall are easy to shake off, the materials are re-fused into a mixed solution, the proportion of each reaction component is prevented from being influenced, resources can be saved, further, under the repeated forward rotation of the driving gear, the stirring assembly can be controlled to stir and mix the reaction materials, the two ends of the arc round rod can be controlled to repeatedly strike the container shell, so that the materials stained on the inner wall face naturally drop, the integrity of the reaction materials can be maintained, a power component can realize a plurality of linkage mechanisms, the operation is convenient, and the preparation cost can be saved.
Drawings
FIG. 1 is a flow chart of a compound preparation method for anodic oxidation of a normal temperature rapid oxidizer according to the invention;
FIG. 2 is a schematic diagram of the overall structure of a preparation method of a compound for anodic oxidation of a normal-temperature rapid oxidant;
FIG. 3 is a schematic diagram of a bracket seat structure of a compound preparation method for anodic oxidation of a normal-temperature rapid oxidant;
FIG. 4 is a schematic diagram of the assembled structure of the traction mechanism and the force application mechanism of the compound preparation method for anodic oxidation of the normal-temperature rapid oxidant;
FIG. 5 is a schematic diagram of the structure of a rotary pier block according to the preparation method of the compound for anodic oxidation of the normal-temperature rapid oxidant;
FIG. 6 is a schematic diagram of a stirring assembly of a compound preparation method for anodic oxidation of a normal temperature rapid oxidant according to the invention;
FIG. 7 is a schematic diagram of the internal planar structure of a central sphere of the preparation method of the compound for anodic oxidation of a normal-temperature rapid oxidant;
FIG. 8 is a schematic diagram of a turntable for adjusting the preparation method of a compound for anodic oxidation of a normal-temperature rapid oxidant;
FIG. 9 is an enlarged view of the invention at A of FIG. 7;
FIG. 10 is a schematic diagram of the driving mechanism of the method for preparing the compound for anodic oxidation of the normal-temperature rapid oxidant according to the invention;
FIG. 11 is a schematic diagram of a hammering mechanism of the compound preparation method for anodic oxidation of a normal temperature rapid oxidant according to the present invention;
FIG. 12 is a schematic structural diagram of a reaction vessel of the compound preparation method for anodic oxidation of a normal-temperature rapid oxidant.
In the figure: 1. a support bracket seat; 11. supporting the bottom plate; 12. the first matching chute; 13. a second matching chute; 14. extending the side plates; 15. a vertical backboard; 16. a beam; 17. an extension cross plate; 18. a limiting contour sleeve; 2. a driving mechanism; 21. a drive gear; 22. side flat toothed plates; 23. a first matching bar; 3. a traction mechanism; 31. traction turntable; 32. a first notched annular tooth surface; 33. a conveyor belt; 34. traction upright posts; 4. a force application mechanism; 41. positioning a column block; 42. rotating the pier blocks; 421. a driven fluted disc; 422. a limit rotating member; 423. a second notched annular tooth surface; 424. splicing blocks; 43. installing an embedding groove; 44. a connecting rod; 45. a stirring assembly; 451. a center ball block; 452. a feed pipe; 453. a discharge pipe; 454. a ring handle; 455. a stirring cross bar; 456. stirring the sharp teeth; 457. a ball cavity; 4571. an arc baffle; 4572. a pressing rod is pressed; 4573. limiting ball blocks; 4574. a first connecting spring; 458. accommodating the spherical shell; 4581. a slip hole; 4582. a semicircular bottom block; 4583. reserving a movable groove; 4584. setting a rotating disc; 45841. a tray body; 45842. traction column blocks; 45843. extending the extension bar rod; 45844. an engagement ring; 45845. a semicircular pressing block; 45846. installing a vertical strip; 45847. a splice box; 45848. connecting the through groove; 45849. a return spring; 459. splicing thin rods; 5. a reaction vessel; 51. a container housing; 52. matching diagonal bars; 53. a bonding block; 54. an impact block; 55. a second connecting spring; 6. a hammering mechanism; 61. a lateral sliding plate; 62. a second matching bar; 63. a transverse flat tooth surface; 64. a movable adjusting groove; 65. an arc body round rod; 66. arc tooth surfaces; 67. hammer hook; 68. adjusting the swinging rod; 681. rotating the stem; 682. sleeving a rotating rod; 683. the thin rod is movably pushed.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
In order to solve the technical problems that the adding time of each reaction component is different, and the reaction vessel is required to be started, the components of the preparation device are complicated and heavy, the operation is not easy, and the preparation period is prolonged, as shown in fig. 1-4, the following preferable technical scheme is provided:
a preparation method of a compound for an anodic oxidation normal-temperature rapid oxidant comprises the following steps:
s01: at the initial stage of preparation: pouring a reaction solvent into a reaction container 5 containing purified water with a specified proportioning amount according to the proportioning, and fully stirring the solution by a stirring assembly 45 to obtain a mixed solution;
s02: the preparation medium period: performing heat treatment on the mixed solution obtained in the initial stage, cooling and standing, layering the mixed solution, and classifying and storing the liquid of each layer;
s03: and (3) in the later preparation stage: and adding a subsequent reaction solvent into the liquid collected in the middle stage, and then carrying out drying heat treatment on the mixture to obtain oxidant powder.
In S01, the reaction solvent is a compound of an acid auxiliary agent, an oxidation-reduction auxiliary agent and a high polymer, and comprises the following components in parts by weight:
10-20 parts of sulfuric acid;
5-10 parts of oxalic acid;
1-2 parts of formic acid;
1-2 parts of tartaric acid;
3-5 parts of urea;
3-5 parts of anhydrous sodium sulfate;
0.5-1 part of polymaleic acid;
2000.5-1 parts of polyethylene glycol;
0.5-1 part of glycerol;
100 parts of pure water.
The lower extreme of reaction vessel 5 is provided with a rest seat 1, the upper surface mounting of rest seat 1 has actuating mechanism 2, actuating mechanism 2's upper end is provided with traction mechanism 3, force application mechanism 4 is installed to one side of traction mechanism 3, reaction vessel 5 sets up the lower extreme at force application mechanism 4, hammering mechanism 6 is installed in the outside of reaction vessel 5, rest seat 1 includes rest bottom plate 11 and sets up the first matching slide groove 12 at rest bottom plate 11 upper surface, second matching slide groove 13 has been seted up to one side of first matching slide groove 12, first matching slide groove 12 and second matching slide groove 13 are linked together, one side of rest bottom plate 11 is installed and is extended curb plate 14, the one end of extension curb plate 14 is provided with vertical backplate 15, the top of vertical backplate 15 is provided with beam 16, the side surface of vertical backplate 15 is provided with extension diaphragm 17, limit contour sleeve 18 is installed to the one end of extension diaphragm 17, traction mechanism 3 includes traction turntable 31 and sets up the first notch annular tooth face 32 at traction turntable 31 side surface, the outside of first notch annular tooth face 32 is provided with conveyer belt 33, the end of a locating block 45 is installed to the lower surface mounting flange block 45 of traction turntable 31 and is provided with the connecting rod assembly 41 through the end of the connecting rod 45, the end of the setting up end of the locating column assembly 41 of end 45 of end of the setting up end 45 of the connecting rod 41 of the setting up in the setting up end 45 of the connecting rod assembly 41, the connecting rod assembly 41 is installed to the connecting rod 45.
Specifically, the driving gear 21 is started, the traction upright rod 34 drives the traction turntable 31 to rotate in the same direction, the conveyor belt 33 is utilized to be connected with the first notch annular tooth surface 32 and the second notch annular tooth surface 423, the rotation pier block 42 rotates along with the rotation of the rotation pier block 42, the rotation pier block 42 rotates relative to the positioning column block 41 through the limiting rotation piece 422, the whole stirring assembly 45 rotates with the center ball block 451 as the axis under the acting force of the connecting rod 44, the limiting contour sleeve 18 limits the center ball block 451, the discharging pipe 453 drives the stirring cross rod 455 and the stirring sharp teeth 456 to stir at multiple angles in the container shell 51, the moving direction of the discharging pipe 453 is matched with the inner cavity of the container shell 51, the full mixing of the reaction raw materials in the reaction container 5 is facilitated, the preparation period can be shortened, and the working efficiency is improved.
In order to solve the technical problem that dirt is easy to enter the reaction vessel and the preparation quality is affected in the repeated opening process, as shown in fig. 7-9, the following preferable technical scheme is provided:
the upper end of the accommodating spherical shell 458 is provided with an arc-shaped baffle 4571, the center of the lower surface of the arc-shaped baffle 4571 is provided with a top pressing rod 4572, one end of the top pressing rod 4572 is provided with a limiting ball block 4573, two sides of the top pressing rod 4572 are provided with first connecting springs 4574, one end of each first connecting spring 4574 is connected with the arc-shaped baffle 4571, the other end of each first connecting spring 4574 is connected with the accommodating spherical shell 458, the upper surface of the accommodating spherical shell 458 is provided with a sliding hole 4581, the sliding hole 4581 is connected with the top pressing rod 4572, the inside of the accommodating spherical shell 458 is provided with a semicircular bottom block 4582, the upper surface of the semicircular bottom block 4582 is provided with a reserved movable groove 4583, the upper end of the reserved movable groove 4583 is provided with an adjusting turntable 4584, the adjusting turntable 4584 comprises a tray body 45841 and a traction column block 45842 arranged at the side end of the tray body 45841, one end of the traction column block 45842 is provided with an extension connecting bar 45843, one end of the extension connecting bar 45843 is provided with a joint ring 45844, one side of the tray body 45841 is provided with an installation vertical bar 45846, one end of the installation vertical bar 45846 is connected with the upper surface of the semicircular bottom block 4582, the other end of the installation vertical bar 45846 is provided with a semicircular pressing block 45845, the lower surface of the tray body 45841 is provided with a splicing box 45847, the surfaces of the tray body 45841 and the splicing box 45847 are provided with a connecting groove 45848, the inner bottom surface of the connecting groove 45848 is provided with a return spring 45849, and one end of the return spring 45849 is connected with the lower surface of the traction column block 45842.
Specifically, start disk body 45841, when traction column piece 45842 changes to semicircle butt briquetting 45845 department, traction column piece 45842's top is laminated with semicircle butt briquetting 45845's round end mutually, along with disk body 45841's rotation, traction column piece 45842 is located semicircle butt briquetting 45845's just lower extreme, extrude traction column piece 45842 in connecting slot 45848, extend long joint bar 45843 and push down thereupon, because of joint ring 45844 and spacing ball piece 4573 looks joint, top depression bar 4572 drives arc baffle 4571 and moves down, arc baffle 4571 breaks away from the intercommunication department of ball chamber 457 and inlet pipe 452 inside, when the timing adds the reaction raw materials, it is in the ball chamber 457 to get into along arc baffle 457 through inlet pipe 4571, again in the reaction vessel 5 along discharging pipe 453, when traction column piece 45842 breaks away from semicircle butt briquetting 45845, utilize the elasticity of first connecting spring 457 and reset spring 45849 can make arc baffle 4571 normal position, arc baffle 457 carries out the intercommunication department in ball chamber and inlet pipe 452 inside again, it is difficult to open and close the reaction vessel with the inside with the arc baffle 457, can not need to control the rotation of arc baffle 457, and can not open and close the reaction vessel 45 in a week, wherein, can avoid further reaction efficiency to open and close the reaction vessel is difficult to open and close in the preparation container, wherein, no further reaction is opened and no need to open and close the reaction vessel is opened.
In order to solve the technical problems that the wall surface of the reaction vessel is easy to be contaminated with materials, the proportion of each reaction component is influenced, and the preparation cost is high, as shown in fig. 5, 6 and 10-12, the following preferable technical scheme is provided:
the rotary pier block 42 comprises a driven fluted disc 421 and a limiting rotary piece 422 arranged on the upper surface of the driven fluted disc 421, the driven fluted disc 421 is connected with the positioning column block 41 through the limiting rotary piece 422, a second notch annular tooth surface 423 is arranged on the side surface of the driven fluted disc 421, a splicing block 424 is arranged on the lower surface of the driven fluted disc 421, a conveying belt 33 is meshed with the first notch annular tooth surface 32 and the second notch annular tooth surface 423, the stirring assembly 45 comprises a central ball block 451 and a feeding pipe 452 arranged at one end of the central ball block 451, a discharging pipe 453 is arranged at the other end of the central ball block 451, the central ball block 451 is matched with the limiting contour sleeve 18, a ring handle 454 is sleeved on the outer side of one end of the discharging pipe 453, a stirring cross rod 455 is arranged on the side surface of the ring handle 454, stirring sharp teeth 456 are arranged at one end of the stirring cross rod 455, a ball cavity 457 is arranged in the center ball cavity 457, a containing ball shell 458 is arranged in the center ball cavity 458, splicing thin rods 459 are arranged on two sides of the containing ball shell 458, and one end of the splicing thin rods 459 is connected with the inner wall of the central ball block 451.
The driving mechanism 2 comprises a driving gear 21 and a side flat toothed plate 22 arranged on one side of the driving gear 21, the side flat toothed plate 22 is meshed with the driving gear 21, a first matching strip 23 is arranged on the lower surface of the side flat toothed plate 22, one end of a traction vertical rod 34 is connected with the driving gear 21, the first matching strip 23 is connected with a second matching sliding groove 13, the hammering mechanism 6 comprises a transverse sliding plate 61 connected with one end of the side flat toothed plate 22 and a second matching strip 62 arranged on the lower surface of the transverse sliding plate 61, the second matching strip 62 is connected with the first matching sliding groove 12, the upper surface of the transverse sliding plate 61 is provided with a transverse flat tooth surface 63, both ends of the transverse sliding plate 61 are provided with movable regulating grooves 64, the upper end of the transverse sliding plate 61 is provided with an arc round rod 65, the lower surface of the arc round rod 65 is provided with an arc tooth surface 66, the arc tooth surface 66 is meshed with the transverse flat tooth surface 63, hammer hooks 67 are arranged at two ends of the arc body round rod 65, adjusting swing rods 68 are arranged at two sides of the arc body round rod 65, four groups of adjusting swing rods 68 are arranged at the four groups of adjusting swing rods 68, a rotating handle column 681 is arranged at one end of each adjusting swing rod 68, a sleeved rotating rod 682 is arranged in the center of each rotating handle column 681, each rotating handle column 681 is arranged on the side surface of each arc body round rod 65, each rotating handle column 681 is connected with one end of each adjusting swing rod 68 through the sleeved rotating rod 682, a movable pushing thin rod 683 is arranged at the other end of each adjusting swing rod 68, the movable pushing thin rod 683 is connected with the corresponding movable adjusting groove 64, the reaction vessel 5 comprises a vessel shell 51 arranged on the lower surface of the extending transverse plate 17 and matching diagonal rods 52 arranged at two sides of the vessel shell 51, the surface of each matching diagonal rod 52 is provided with a fitting block 53, the hammer hooks 67 are fitted with the fitting blocks 53, impact blocks 54 are arranged on the inner sides of the matching diagonal rods 52, two ends of each matching diagonal rod 52 are provided with second connecting springs 55, one end of the second connection spring 55 is connected to the outer surface of the container housing 51.
Specifically, when the driving gear 21 is started, the driving gear 21 is engaged with the side flat toothed plate 22, the side flat toothed plate 22 drives the transverse sliding plate 61 to translate to one side, the transverse flat toothed plate 63 is engaged with the arc toothed surface 66, the arc round rod 65 is driven to overturn to one side, one end of the arc round rod 65 is impacted by the hammer hook 67 to the attaching block 53, the attaching block 53 drives the matching inclined bar 52 to be integrally close to the container shell 51, the plurality of groups of impact blocks 54 collide with the outer wall of the container shell 51, so that materials adhered to the inner wall are easy to shake off, and are re-blended into the mixed solution, the proportion of each reaction component is prevented from being influenced, resources are saved, further, under the repeated forward rotation of the driving gear 21, the stirring assembly 45 can be controlled to stir and mix the reaction materials, the two ends of the arc round rod 65 can be controlled to repeatedly impact the container shell 51, so that the materials stained on the inner wall face naturally drop, the integrity of the reaction materials is maintained, a plurality of linkage mechanisms can be realized by one power member, the operation is convenient, and the preparation cost is saved.
The foregoing is only a preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art, who is within the scope of the present invention, should be covered by the protection scope of the present invention by making equivalents and modifications to the technical solution and the inventive concept thereof.
Claims (3)
1. A preparation method of a compound for an anodic oxidation normal-temperature rapid oxidant is characterized by comprising the following steps: the method comprises the following steps:
s01: at the initial stage of preparation: pouring a reaction solvent into a reaction container (5) filled with purified water with a specified proportioning amount according to the proportioning, and fully stirring the solution by a stirring assembly (45) to obtain a mixed solution;
s02: the preparation medium period: performing heat treatment on the mixed solution obtained in the initial stage, cooling and standing, layering the mixed solution, and classifying and storing the liquid of each layer;
s03: and (3) in the later preparation stage: adding a subsequent reaction solvent into the liquid collected in the middle stage, and then carrying out drying heat treatment on the mixture to obtain oxidant powder;
the lower extreme of reaction vessel (5) is provided with a support frame seat (1), the upper surface mounting of support frame seat (1) has actuating mechanism (2), the upper end of actuating mechanism (2) is provided with traction mechanism (3), force application mechanism (4) are installed to one side of traction mechanism (3), reaction vessel (5) set up the lower extreme at force application mechanism (4), hammering mechanism (6) are installed in the outside of reaction vessel (5), support frame seat (1) includes support bottom plate (11) and sets up first matching spout (12) at support bottom plate (11) upper surface, second matching spout (13) have been seted up to one side of first matching spout (12), one side of support bottom plate (11) is installed and is extended curb plate (14), one end of extension curb plate (14) is provided with vertical backplate (15), the top of vertical backplate (15) is provided with beam (16), the side surface of vertical backplate (15) is provided with extension diaphragm (17), profile (18) of extension diaphragm (17) one end is installed and is spacing;
the traction mechanism (3) comprises a traction rotary table (31) and a first notch annular tooth surface (32) arranged on the side surface of the traction rotary table (31), a conveyor belt (33) is arranged on the outer side of the first notch annular tooth surface (32), a traction vertical rod (34) is arranged in the center of the lower surface of the traction rotary table (31), the force application mechanism (4) comprises a positioning column block (41) and a rotary pier block (42) arranged at the lower end of the positioning column block (41), an installation jogging groove (43) is arranged on the upper surface of the positioning column block (41), the positioning column block (41) is connected with one end of a beam rod (16) through the installation jogging groove (43), a connecting rod (44) is arranged on one side of the rotary pier block (42), a stirring component (45) is arranged at one end of the connecting rod (44), and the stirring component (45) is arranged in the reaction container (5);
the rotary pier block (42) comprises a driven fluted disc (421) and a limiting rotary piece (422) arranged on the upper surface of the driven fluted disc (421), the driven fluted disc (421) is connected with a positioning column block (41) through the limiting rotary piece (422), a second notch annular tooth surface (423) is arranged on the side surface of the driven fluted disc (421), a splicing block (424) is arranged on the lower surface of the driven fluted disc (421), a conveying belt (33) is meshed with the first notch annular tooth surface (32) and the second notch annular tooth surface (423), a stirring assembly (45) comprises a central ball block (451) and a feeding pipe (452) arranged at one end of the central ball block (451), a discharging pipe (453) is arranged at the other end of the central ball block (451), the central ball block (451) is matched with a limiting contour sleeve (18), a ring handle (454) is sleeved on the outer side of one end of the discharging pipe (453), stirring cross bars (455) are arranged on the side surface of the side surfaces of the ring handles (454), the stirring cross bars (455) are provided with splicing blocks (456), ball cavities (457) are arranged in the inner parts of the central ball block (451), the ball cavities (457) are arranged in the inner parts of the ball cavities (458) and contain ball shells (45), one end of the spliced thin rod (459) is connected with the inner wall of the central ball block (451);
the driving mechanism (2) comprises a driving gear (21) and a side flat toothed plate (22) arranged on one side of the driving gear (21), the side flat toothed plate (22) is in meshed connection with the driving gear (21), a first matching strip (23) is arranged on the lower surface of the side flat toothed plate (22), one end of a traction vertical rod (34) is connected with the driving gear (21), and the first matching strip (23) is connected with a second matching chute (13);
the hammering mechanism (6) comprises a transverse sliding plate (61) connected with one end of the side flat toothed plate (22) and a second matching strip (62) arranged on the lower surface of the transverse sliding plate (61), the second matching strip (62) is connected with the first matching sliding groove (12), the upper surface of the transverse sliding plate (61) is provided with a transverse flat toothed surface (63), both ends of the transverse sliding plate (61) are provided with movable adjusting grooves (64), the upper end of the transverse sliding plate (61) is provided with an arc round rod (65), the lower surface of the arc round rod (65) is provided with an arc toothed surface (66), the arc toothed surface (66) is meshed with the transverse flat toothed surface (63), both ends of the arc round rod (65) are provided with hammer hooks (67), both sides of the arc round rod (65) are provided with adjusting swinging rods (68), and the adjusting swinging rods (68) are provided with four groups;
a rotary handle column (681) is arranged at one end of the adjusting swing rod (68), a sleeved rotary rod (682) is arranged in the center of the rotary handle column (681), the rotary handle column (681) is arranged on the side surface of the arc round rod (65), the rotary handle column (681) is connected with one end of the adjusting swing rod (68) through the sleeved rotary rod (682), a movable pushing thin rod (683) is arranged at the other end of the adjusting swing rod (68), and the movable pushing thin rod (683) is connected with the movable adjusting groove (64);
the reaction vessel (5) is including setting up in the container shell (51) of extension diaphragm (17) lower surface and installing in the matching diagonal bar (52) of container shell (51) both sides, the surface mounting of matching diagonal bar (52) has laminating piece (53), hammer hook (67) laminating with laminating piece (53) mutually, the inboard of matching diagonal bar (52) is provided with striking piece (54), the both ends of matching diagonal bar (52) all are provided with second coupling spring (55), the one end of second coupling spring (55) is connected with the surface of container shell (51).
2. The method for preparing the compound for the anodic oxidation normal-temperature rapid oxidant, which is characterized in that: the upper end that holds spherical shell (458) is provided with arc baffle (4571), the central authorities of arc baffle (4571) lower surface install top depression bar (4572), the one end of top depression bar (4572) is provided with spacing ball piece (4573), the both sides of top depression bar (4572) all are provided with first connecting spring (4574), the one end of first connecting spring (4574) is connected with arc baffle (4571), the other end of first connecting spring (4574) is connected with holds spherical shell (458), the upper surface that holds spherical shell (458) has seted up sliding hole (4581), sliding hole (4581) are connected with top depression bar (4572), the inside that holds spherical shell (458) is provided with semicircle bottom piece (4582), reservation movable groove (4583) have been seted up to the upper surface of semicircle bottom piece (4582), the upper end of reservation movable groove (4583) is provided with and transfers and establishes carousel (4584).
3. The method for preparing the compound for the anodic oxidation normal-temperature rapid oxidant according to claim 2, which is characterized in that: the adjusting turntable (4584) comprises a tray body (45841) and a traction column block (45842) arranged at the side end of the tray body (45841), an extension connecting rod (45843) is arranged at one end of the traction column block (45842), a joint ring (45844) is arranged at one end of the extension connecting rod (45843), an installation vertical rod (45846) is arranged at one side of the tray body (45841), one end of the installation vertical rod (45846) is connected with the upper surface of a semicircular bottom block (4582), a semicircular pressing block (45845) is arranged at the other end of the installation vertical rod (45846), a splicing box (45847) is arranged on the lower surface of the tray body (45841), a connecting groove (45848) is formed in the surfaces of the tray body (45841) and the splicing box (45847), a reset spring (45849) is arranged on the inner bottom surface of the connecting groove (45848), and one end of the reset spring (45849) is connected with the lower surface of the traction column block (45842).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210291258.6A CN114602409B (en) | 2022-03-23 | 2022-03-23 | Preparation method of compound for anodic oxidation normal-temperature rapid oxidant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210291258.6A CN114602409B (en) | 2022-03-23 | 2022-03-23 | Preparation method of compound for anodic oxidation normal-temperature rapid oxidant |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN114602409A CN114602409A (en) | 2022-06-10 |
| CN114602409B true CN114602409B (en) | 2023-09-26 |
Family
ID=81864809
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210291258.6A Active CN114602409B (en) | 2022-03-23 | 2022-03-23 | Preparation method of compound for anodic oxidation normal-temperature rapid oxidant |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN114602409B (en) |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107442055A (en) * | 2017-09-22 | 2017-12-08 | 济宁新创化工科技有限公司 | A kind of efficiently chemical industry stirred tank reaction unit |
| CN109621874A (en) * | 2019-01-24 | 2019-04-16 | 杨韦韦 | Mix reaction equipment is used in industrial chemicals production |
| CN210646385U (en) * | 2019-08-26 | 2020-06-02 | 福建鸿燕化工有限公司 | Raw materials ration mixing arrangement is used in cellulose acetate butyrate production |
| CN111704812A (en) * | 2020-05-07 | 2020-09-25 | 阳泉灿坤工贸有限公司 | Titanium dioxide organic coating preparation process |
| CN214716627U (en) * | 2021-04-20 | 2021-11-16 | 淮安宏图新材料有限公司 | Silane coupling agent small-dose synthesis device |
| KR20210138243A (en) * | 2020-05-12 | 2021-11-19 | 한성의료산업(주) | treatment device of mixture |
| CN113908760A (en) * | 2021-11-23 | 2022-01-11 | 徐州宏武纳米科技有限公司 | Dispersion machine for graphene processing |
| WO2022047872A1 (en) * | 2020-09-03 | 2022-03-10 | 黄春燕 | Chemical raw material rinsing device for chemical production |
| CN215996475U (en) * | 2021-08-06 | 2022-03-11 | 沈阳博奥医学检验所有限公司 | Medical dressing agitating unit |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101981131B1 (en) * | 2019-03-15 | 2019-05-22 | (주)티에스아이 | Slurry Mixer for Battery Electrode |
-
2022
- 2022-03-23 CN CN202210291258.6A patent/CN114602409B/en active Active
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107442055A (en) * | 2017-09-22 | 2017-12-08 | 济宁新创化工科技有限公司 | A kind of efficiently chemical industry stirred tank reaction unit |
| CN109621874A (en) * | 2019-01-24 | 2019-04-16 | 杨韦韦 | Mix reaction equipment is used in industrial chemicals production |
| CN210646385U (en) * | 2019-08-26 | 2020-06-02 | 福建鸿燕化工有限公司 | Raw materials ration mixing arrangement is used in cellulose acetate butyrate production |
| CN111704812A (en) * | 2020-05-07 | 2020-09-25 | 阳泉灿坤工贸有限公司 | Titanium dioxide organic coating preparation process |
| KR20210138243A (en) * | 2020-05-12 | 2021-11-19 | 한성의료산업(주) | treatment device of mixture |
| WO2022047872A1 (en) * | 2020-09-03 | 2022-03-10 | 黄春燕 | Chemical raw material rinsing device for chemical production |
| CN214716627U (en) * | 2021-04-20 | 2021-11-16 | 淮安宏图新材料有限公司 | Silane coupling agent small-dose synthesis device |
| CN215996475U (en) * | 2021-08-06 | 2022-03-11 | 沈阳博奥医学检验所有限公司 | Medical dressing agitating unit |
| CN113908760A (en) * | 2021-11-23 | 2022-01-11 | 徐州宏武纳米科技有限公司 | Dispersion machine for graphene processing |
Also Published As
| Publication number | Publication date |
|---|---|
| CN114602409A (en) | 2022-06-10 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN112265145B (en) | Cement agitating unit for building | |
| CN107670563A (en) | A kind of lead-acid storage battery production colloid mixed stirring device | |
| CN114602409B (en) | Preparation method of compound for anodic oxidation normal-temperature rapid oxidant | |
| CN112717826A (en) | Intensive mixing device is used in alloy material production and processing | |
| CN114471313A (en) | Natural ferment soap of fruit ferment and production equipment thereof | |
| CN114656130A (en) | Smelting furnace for processing glass products | |
| CN114345194A (en) | Granulator for processing mica powder with uniform feeding | |
| CN111943118B (en) | Filling system is used in shower bath processing | |
| CN113181808A (en) | Raw materials stirring mixing arrangement in batches is used in preparation of onychomycosis medicine | |
| CN113264705A (en) | Concrete water reducing agent and processing technology thereof | |
| CN218025561U (en) | Novel advanced oxidation treatment equipment for lithium battery wastewater | |
| CN112108066A (en) | Facial mask processing raw materials charge-in system | |
| CN110936493A (en) | Preparation device and preparation process of cement-based material with regularly-arranged pore structure | |
| CN216471018U (en) | Automatic reagent feeding device for sewage treatment | |
| CN218012778U (en) | Photosensitizer generating device | |
| CN218077378U (en) | Automatic stirring equipment is used in antibacterial gel production | |
| CN218290887U (en) | Preparation device of composite biological enzyme | |
| CN208340146U (en) | A kind of reactive distillation kettle can be used for the production of methacrylic acid special type ester | |
| CN214973672U (en) | Compounding device is used in production of organic inorganic compound fertilizer | |
| CN220546832U (en) | Concrete waterproof compacting agent blending device | |
| CN212701525U (en) | A mix machine for animal remedy production | |
| CN110420592B (en) | Chemical solution automatic configuration equipment | |
| CN218170979U (en) | Particle hybrid processing equipment with preheating structure | |
| CN214553003U (en) | Agitated vessel is used in preparation of o chlorobenzene glycine | |
| CN219463397U (en) | A multilayer formula stirring retort for sodium hydride generates |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |