CN114602409A - Preparation method of compound for anodic oxidation normal-temperature rapid oxidant - Google Patents
Preparation method of compound for anodic oxidation normal-temperature rapid oxidant Download PDFInfo
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- CN114602409A CN114602409A CN202210291258.6A CN202210291258A CN114602409A CN 114602409 A CN114602409 A CN 114602409A CN 202210291258 A CN202210291258 A CN 202210291258A CN 114602409 A CN114602409 A CN 114602409A
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- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
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- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
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Abstract
A compound preparation method for an anodic oxidation normal-temperature rapid oxidant belongs to the technical field of compound preparation, and aims to solve the problems that components of a preparation device are complex and heavy, the operation is not easy, the preparation period is prolonged, the preparation cost is high, dirt is easy to enter a reaction container in the repeated opening process to influence the preparation quality, and the wall surface of the reaction container is easy to be stained with materials to influence the proportioning degree of each reaction component; the opening and closing of the arc-shaped baffle plate can be controlled by rotating the plate body for one circle, so that reaction raw materials can be conveniently added in different reaction time without continuously opening the reaction container; according to the invention, the driving gear rotates forwards and repeatedly, so that the stirring assembly can be controlled to stir and mix reaction materials, and the two ends of the arc round rod can be controlled to repeatedly impact the container shell, so that the materials contaminated on the inner wall surface naturally fall off, the integrity of the reaction materials is kept, a plurality of linkage mechanisms can be realized by one power member, the operation is convenient and fast, and the preparation cost can be saved.
Description
Technical Field
The invention relates to the technical field of compound preparation, in particular to a preparation method of a compound for an anodic oxidation normal-temperature rapid oxidant.
Background
The oxidizing agent is a substance which obtains electrons in a redox reaction, the oxidizing agent has an oxidizing property, the valence of the obtained electrons is reduced, a reduction reaction occurs, and a reduction product is obtained.
In the preparation process of the oxidant compound, all reaction components need to be mixed and stirred according to the mixing ratio of the reaction components, the adding time of the reaction components is different, and then the reaction container needs to be opened continuously, the components of the preparation device are complicated and heavy, the operation is not easy, the preparation period is prolonged, the preparation cost is high, in the process of repeatedly opening, dirt is easy to enter the reaction container to influence the preparation quality, and the wall surface of the reaction container is easy to be stained with materials to influence the mixing ratio of the reaction components.
Aiming at the problems, the prior device is improved, and a preparation method of a compound for anodizing normal-temperature rapid oxidant is provided.
Disclosure of Invention
The invention aims to provide a preparation method of a compound for an anodic oxidation normal-temperature rapid oxidant, which solves the problems that in the background technology, in the preparation process of an oxidant compound, all reaction components need to be mixed and stirred according to the mixing ratio of the reaction components, the adding time of the reaction components is different, and further a reaction container needs to be continuously opened, the preparation device has complicated and heavy components, the operation is difficult, the preparation period is prolonged, the preparation cost is high, in the repeated opening process, dirt is easy to enter the reaction container to influence the preparation quality, and the wall surface of the reaction container is easy to be stained with materials to influence the mixing ratio of the reaction components.
In order to achieve the purpose, the invention provides the following technical scheme: a preparation method of a compound for an anodic oxidation normal-temperature rapid oxidant comprises the following steps:
s01: in the initial preparation stage: pouring a reaction solvent into a reaction container filled with purified water with a specified proportion according to the proportion, and fully stirring the solution by a stirring component to obtain a mixed solution;
s02: the preparation middle stage: carrying out heat treatment on the mixed liquid obtained in the initial stage, cooling and standing, layering the mixed liquid, and classifying and storing the liquids in all layers;
s03: the later stage of preparation: and adding a subsequent reaction solvent into the liquid collected in the middle stage, and drying and thermally treating the mixture to obtain the oxidant powder.
Further, in S01, the reaction solvent is a mixture of an acidic assistant, an oxidation-reduction assistant and a high-molecular polymer, and comprises the following components by weight:
10-20 parts of sulfuric acid;
5-10 parts of oxalic acid;
1-2 parts of formic acid;
1-2 parts of tartaric acid;
3-5 parts of urea;
3-5 parts of anhydrous sodium sulphate;
0.5-1 part of polymaleic acid;
2000.5-1 parts of polyethylene glycol;
0.5-1 part of glycerol;
100 parts of pure water.
Furthermore, a support bracket seat is arranged at the lower end of the reaction vessel, a driving mechanism is arranged on the upper surface of the support bracket seat, a traction mechanism is arranged at the upper end of the driving mechanism, a force application mechanism is arranged at one side of the traction mechanism, the reaction vessel is arranged at the lower end of the force application mechanism, a hammering mechanism is arranged at the outer side of the reaction vessel, the support bracket seat comprises a support bottom plate and a first matching chute arranged on the upper surface of the support bottom plate, a second matching chute is arranged at one side of the first matching chute, the first matching chute is communicated with the second matching chute, an extension side plate is arranged at one side of the support bottom plate, a vertical back plate is arranged at one end of the extension side plate, a beam rod is arranged at the top end of the vertical back plate, an extension transverse plate is arranged on the side surface of the vertical back plate, a limiting profile sleeve is arranged at one end of the extension transverse plate, the traction mechanism comprises a traction turntable and a first notch annular tooth surface arranged on the side surface of the traction turntable, the outside of first notch ring flank of tooth is provided with the conveyer belt, and the central authorities of pulling the carousel lower surface install and pull the pole setting, and force applying mechanism includes location column piece and the rotation mound piece of setting at location column piece lower extreme, and the installation gomphosis groove has been seted up to the upper surface of location column piece, and the location column piece is connected with the one end of roof beam pole through the installation gomphosis groove, rotates one side of mound piece and installs the extension rod, and the one end of extension rod is provided with the stirring subassembly, and the inside of reaction vessel is located to the stirring subassembly.
Further, the mound piece rotates and includes driven fluted disc and installs the spacing rotation piece at driven fluted disc upper surface, driven fluted disc is connected with the reference column piece through spacing rotation piece, second notch annular flank of tooth has been seted up to the side surface of driven fluted disc, the lower surface of driven fluted disc is provided with the concatenation piece, the conveyer belt is connected with first notch annular flank of tooth and the meshing of second notch annular flank of tooth, the stirring subassembly includes central ball piece and the inlet pipe of setting in central ball piece one end, the discharging pipe is installed to the other end of central ball piece, central ball piece and spacing profile cover phase-match, the ring handle has been cup jointed in the outside of discharging pipe one end, the stirring horizontal pole is installed to the side surface of ring handle, sharp stirring tooth is installed to the one end of stirring horizontal pole, the ball chamber has been seted up to the inside of central ball piece, the inside of ball chamber is provided with holds the spherical shell, the concatenation pin is installed to the both sides that hold the spherical shell, the one end of concatenation pin is connected with the inner wall of central ball piece.
Further, the upper end that holds the spherical shell is provided with cowl, the roof pressure pole is installed to the central authorities of cowl lower surface, the one end of roof pressure pole is provided with spacing ball piece, the both sides of roof pressure pole all are provided with first connecting spring, first connecting spring's one end is connected with cowl, first connecting spring's the other end with hold the spherical shell and be connected, the hole of sliding has been seted up to the upper surface that holds the spherical shell, the hole of sliding is connected with the roof pressure pole, the inside that holds the spherical shell is provided with the semicircle bottom piece, the reserve movable groove has been seted up to the upper surface of semicircle bottom piece, the upper end of reserving the movable groove is provided with the accent and establishes the carousel.
Further, transfer and establish the carousel and include the disk body and install the post piece that pulls at the disk body side, the one end of pulling the post piece is provided with the extension and connects the stick, the extension is connected the one end of stick and is installed the engaging ring, the installation vertical bar is installed to one side of disk body, the one end of installation vertical bar is connected with the upper surface of semicircle bottom piece, the other end of installation vertical bar is provided with semicircle abutting block, the lower surface mounting of disk body has the concatenation box, the connection logical groove has been seted up on the surface of disk body and concatenation box, the interior bottom surface that connects logical groove is provided with reset spring, reset spring's one end is connected with the lower surface of pulling the post piece.
Further, actuating mechanism includes drive gear and the side pinion rack that sets up in drive gear one side, and the side pinion rack is connected with drive gear meshing, and the lower surface mounting of side pinion rack has first matching strip, and the one end of pulling the pole setting is connected with drive gear, and first matching strip is connected with the second matching spout.
Furthermore, the hammering mechanism comprises a transverse sliding plate and a second matching strip, the transverse sliding plate is connected with one end of a side flat toothed plate, the second matching strip is installed on the lower surface of the transverse sliding plate and connected with a first matching sliding groove, a transverse flat toothed surface is arranged on the upper surface of the transverse sliding plate, movable adjusting grooves are formed in the two ends of the transverse sliding plate, an arc round rod is arranged at the upper end of the transverse sliding plate, an arc toothed surface is arranged on the lower surface of the arc round rod and meshed with the transverse flat toothed surface, hammer hooks are arranged at the two ends of the arc round rod, adjusting swing rods are installed on the two sides of the arc round rod, and four groups of adjusting swing rods are arranged.
Furthermore, a rotating handle column is installed at one end of the adjusting swing rod, a sleeved rotating rod is arranged in the center of the rotating handle column, the rotating handle column is arranged on the side surface of the arc round rod, the rotating handle column is connected with one end of the adjusting swing rod through the sleeved rotating rod, a movable pushing thin rod is arranged at the other end of the adjusting swing rod, and the movable pushing thin rod is connected with the movable adjusting groove.
Further, reaction vessel is including setting up at the vessel shell of extension diaphragm lower surface and installing the matching sloping pole in the vessel shell both sides, and the surface mounting who matches the sloping pole has the laminating piece, and the hammer hook is laminated with the laminating piece mutually, and the inboard that matches the sloping pole is provided with the striking piece, and the both ends that match the sloping pole all are provided with second connecting spring, and second connecting spring's one end is connected with the surface of vessel shell.
Compared with the prior art, the invention has the beneficial effects that:
1. the invention provides a preparation method of a compound for an anodic oxidation normal-temperature rapid oxidant, which comprises the steps of starting a driving gear, driving a traction turntable to rotate in the same direction by a traction upright rod, utilizing a conveyor belt to be meshed and connected with a first concave annular tooth surface and a second concave annular tooth surface, rotating a pier block along with the rotation of the traction upright rod, rotating the rotary pier block relative to a positioning column block through a limiting rotating piece, rotating a whole stirring assembly by taking a central ball block as an axis under the action of an engaging rod, limiting the central ball block by a limiting contour sleeve, driving a stirring cross rod and stirring sharp teeth to stir at multiple angles in a container shell by a discharge pipe, matching the moving direction of the discharge pipe with an inner cavity of the container shell, being beneficial to rapidly and fully mixing reaction raw materials in a reaction container, shortening the preparation period and improving the working efficiency.
2. The invention provides a preparation method of a compound for an anodic oxidation normal-temperature rapid oxidant, which comprises the steps of starting a disk body, when a traction column block rotates to a semicircular pressing block, the top end of the traction column block is attached to the rounded end of the semicircular pressing block, the traction column block is positioned right below the semicircular pressing block along with the rotation of the disk body, the traction column block is extruded into a connecting through groove, an extension connecting rod is pressed downwards along with the extension connecting rod, a joint ring is clamped with a limiting ball block, a jacking rod drives an arc-shaped baffle plate to move downwards, the arc-shaped baffle plate is separated from the communicating part between a ball cavity and the interior of a feeding pipe, when reaction raw materials need to be added at regular time, the arc-shaped baffle plate enters the ball cavity along a feeding pipe and then enters a reaction container along a discharging pipe, when the traction column block is separated from the semicircular pressing block, the arc-shaped baffle plate can be restored to the original position by utilizing the elasticity of a first connecting spring and a return spring, the arc-shaped baffle plate covers the communicating part between the ball cavity and the interior of the feeding pipe again, through rotating disk body a week, can control cowl's opening and shutting, and then be convenient for add reaction raw materials in different reaction time, need not constantly to open reaction vessel, avoid dirty entering wherein, further promote preparation efficiency.
3. The invention provides a preparation method of a compound for an anodic oxidation normal-temperature rapid oxidant, when a driving gear is started, the driving gear is meshed with a side flat toothed plate, the side flat toothed plate drives a transverse sliding plate to translate to one side, a circular arc rod is driven to turn to one side by the meshed connection of the transverse flat toothed surface and an arc toothed surface, one end of the circular arc rod is hammered and collided with an attaching block, the attaching block drives a matched oblique bar to be integrally close to a container shell, a plurality of groups of impacting blocks collide with the outer wall of the container shell, so that materials adhered to the inner wall are favorably shaken off and are re-melted into a mixed liquid, the influence on the ratio of each reaction component is avoided, resources can be saved, and further, under the repeated forward rotation of the driving gear, not only can a stirring component be controlled to stir and mix reaction materials, but also the two ends of the circular arc rod can be controlled to repeatedly impact the container shell so as to enable the materials adhered to naturally fall off the inner wall surface, the integrity of the reaction materials is kept, a plurality of linkage mechanisms can be realized by one power member, the operation is convenient, and the preparation cost can be saved.
Drawings
FIG. 1 is a flow chart of the preparation method of the compound for the anodic oxidation normal temperature rapid oxidizer of the present invention;
FIG. 2 is a schematic diagram of the overall structure of the preparation method of the compound for the anodic oxidation normal-temperature rapid oxidizer of the present invention;
FIG. 3 is a schematic view of the bracket holder structure of the preparation method of the compound for the anodic oxidation normal temperature rapid oxidizer of the present invention;
FIG. 4 is a schematic diagram of an assembly structure of a traction mechanism and a force application mechanism of a compound preparation method for an anodic oxidation normal-temperature rapid oxidant according to the present invention;
FIG. 5 is a schematic view of a rotary pier block structure of the preparation method of the compound for the anodic oxidation normal temperature rapid oxidizer of the present invention;
FIG. 6 is a schematic structural diagram of a stirring component of a compound preparation method for an anodic oxidation normal-temperature rapid oxidant of the invention;
FIG. 7 is a schematic view of the inner plane structure of a central ball block in the preparation method of the compound for the anodic oxidation normal-temperature rapid oxidizer according to the present invention;
FIG. 8 is a schematic structural diagram of a turntable for adjusting the preparation method of the compound for the anodic oxidation normal-temperature rapid oxidizer according to the present invention;
FIG. 9 is an enlarged view taken at A of FIG. 7 in accordance with the present invention;
FIG. 10 is a schematic structural diagram of a compound preparation method driving mechanism for an anodic oxidation normal-temperature rapid oxidizer according to the present invention;
FIG. 11 is a schematic structural view of a hammering mechanism of a compound preparation method for an anodic oxidation normal-temperature rapid oxidizer according to the present invention;
FIG. 12 is a schematic structural diagram of a reaction vessel of a preparation method of a compound for an anodic oxidation normal-temperature rapid oxidizer according to the present invention.
In the figure: 1. a bracket holder; 11. a support base plate; 12. a first matching chute; 13. a second matching chute; 14. an extension side plate; 15. a vertical back plate; 16. a beam; 17. extending the transverse plate; 18. a limiting outline sleeve; 2. a drive mechanism; 21. a drive gear; 22. a side flat toothed plate; 23. a first matching bar; 3. a traction mechanism; 31. a traction turntable; 32. a first concave-annular tooth surface; 33. a conveyor belt; 34. drawing the vertical rod; 4. a force application mechanism; 41. positioning the column block; 42. rotating the pier blocks; 421. a driven fluted disc; 422. limiting the rotating piece; 423. a second concave annular tooth surface; 424. splicing blocks; 43. installing and embedding grooves; 44. a connecting rod; 45. a stirring assembly; 451. a central ball block; 452. a feed pipe; 453. a discharge pipe; 454. a ring handle; 455. a stirring cross bar; 456. stirring sharp teeth; 457. a ball cavity; 4571. an arc-shaped baffle plate; 4572. a top pressure rod; 4573. a limiting ball block; 4574. a first connecting spring; 458. accommodating the spherical shell; 4581. a sliding hole; 4582. a semicircular bottom block; 4583. reserving a movable groove; 4584. adjusting a turntable; 45841. a tray body; 45842. a traction column block; 45843. extending the connecting rod; 45844. a mating ring; 45845. a semicircular pressing block; 45846. mounting a vertical bar; 45847. splicing the boxes; 45848. a connecting through groove; 45849. a return spring; 459. splicing the thin rods; 5. a reaction vessel; 51. a container housing; 52. matching the diagonal rods; 53. fitting blocks; 54. an impact block; 55. a second connecting spring; 6. a hammering mechanism; 61. a transverse sliding plate; 62. a second matching bar; 63. a transverse flat tooth surface; 64. a movable adjusting groove; 65. an arc round bar; 66. an arcuate tooth surface; 67. a hammer hook; 68. adjusting a swing rod; 681. rotating the handle post; 682. a rotating rod is sleeved; 683. the thin rod is movably pushed.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In order to solve the technical problems that the adding time of each reaction component is different, and further a reaction container needs to be continuously opened, the components of a preparation device are complicated and heavy, the operation is not easy, and the preparation period is prolonged, as shown in figures 1 to 4, the following preferred technical scheme is provided:
a preparation method of a compound for an anodic oxidation normal-temperature rapid oxidant comprises the following steps:
s01: in the initial preparation stage: in a reaction vessel 5 containing purified water with a specified proportion, pouring a reaction solvent into the reaction vessel 5 according to the proportion, and fully stirring the solution by a stirring component 45 to obtain a mixed solution;
s02: the preparation middle stage: carrying out heat treatment on the mixed liquid obtained at the initial stage, cooling and standing, layering the mixed liquid, and classifying and storing the liquid of each layer;
s03: the later stage of preparation: and adding a subsequent reaction solvent into the liquid collected in the middle stage, and drying and thermally treating the mixture to obtain the oxidant powder.
In S01, the reaction solvent is a mixture of an acidic assistant, an oxidation-reduction assistant and a polymer, and comprises the following components by weight:
10-20 parts of sulfuric acid;
5-10 parts of oxalic acid;
1-2 parts of formic acid;
1-2 parts of tartaric acid;
3-5 parts of urea;
3-5 parts of anhydrous sodium sulphate;
0.5-1 part of polymaleic acid;
2000.5-1 parts of polyethylene glycol;
0.5-1 part of glycerol;
100 parts of pure water.
The lower end of a reaction vessel 5 is provided with a support bracket seat 1, the upper surface of the support bracket seat 1 is provided with a driving mechanism 2, the upper end of the driving mechanism 2 is provided with a traction mechanism 3, one side of the traction mechanism 3 is provided with a force application mechanism 4, the reaction vessel 5 is arranged at the lower end of the force application mechanism 4, the outer side of the reaction vessel 5 is provided with a hammering mechanism 6, the support bracket seat 1 comprises a support bottom plate 11 and a first matching chute 12 arranged on the upper surface of the support bottom plate 11, one side of the first matching chute 12 is provided with a second matching chute 13, the first matching chute 12 is communicated with the second matching chute 13, one side of the support bottom plate 11 is provided with an extension side plate 14, one end of the extension side plate 14 is provided with a vertical back plate 15, the top end of the vertical back plate 15 is provided with a beam rod 16, the side surface of the vertical back plate 15 is provided with an extension transverse plate 17, and one end of the extension transverse plate 17 is provided with a limit profile sleeve 18, the traction mechanism 3 comprises a traction turntable 31 and a first concave annular tooth surface 32 arranged on the side surface of the traction turntable 31, a conveyor belt 33 is arranged on the outer side of the first concave annular tooth surface 32, a traction upright rod 34 is installed in the center of the lower surface of the traction turntable 31, the force application mechanism 4 comprises a positioning column block 41 and a rotating pier block 42 arranged at the lower end of the positioning column block 41, an installation and embedding groove 43 is formed in the upper surface of the positioning column block 41, the positioning column block 41 is connected with one end of a beam 16 through the installation and embedding groove 43, an engagement rod 44 is installed on one side of the rotating pier block 42, a stirring assembly 45 is arranged at one end of the engagement rod 44, and the stirring assembly 45 is arranged in the reaction container 5.
Specifically, the driving gear 21 is started, the traction upright stanchion 34 drives the traction turntable 31 to rotate in the same direction, the conveyor belt 33 is engaged with the first notched annular tooth surface 32 and the second notched annular tooth surface 423, the rotary pier block 42 rotates along with the rotary pier block 42, the rotary pier block 42 rotates relative to the positioning column block 41 through the limiting rotary piece 422, under the action of the connecting rod 44, the whole stirring assembly 45 rotates by taking the central ball block 451 as an axis, the limiting contour sleeve 18 limits the central ball block 451, the discharge pipe 453 drives the stirring cross rod 455 and the stirring sharp teeth 456 to stir in multiple angles in the container shell 51, the moving direction of the discharge pipe 453 is matched with the inner cavity of the container shell 51, so that the reaction raw materials in the reaction container 5 can be rapidly and sufficiently mixed, the preparation period can be shortened, and the working efficiency can be improved.
In order to solve the technical problem that in the process of repeatedly opening, dirt is easily caused to enter a reaction container to influence the preparation quality, as shown in fig. 7-9, the following preferred technical scheme is provided:
an arc-shaped baffle 4571 is arranged at the upper end of the accommodating ball shell 458, a top pressure rod 4572 is arranged in the center of the lower surface of the arc-shaped baffle 4571, a limiting ball block 4573 is arranged at one end of the top pressure rod 4572, first connecting springs 4574 are arranged on both sides of the top pressure rod 4572, one end of each first connecting spring 4574 is connected with the arc-shaped baffle 4571, the other end of each first connecting spring 4574 is connected with the accommodating ball shell 458, a sliding hole 4581 is formed in the upper surface of the accommodating ball shell 458, the sliding hole 4581 is connected with the top pressure rod 4572, a semicircular bottom block 4582 is arranged inside the accommodating ball shell 458, a reserved movable groove 4583 is formed in the upper surface of the semicircular bottom block 4582, an adjusting turntable 4584 is arranged at the upper end of the reserved movable groove 4583, the adjusting turntable 4584 comprises a plate body 45841 and a traction column block 45842 mounted at the side end of the plate 45841, an extension connecting rod 45843 is arranged at one end of the traction column 45842, an extension connecting rod 45843 is mounted with a joint ring 45844, an installation vertical bar 45846 is installed on one side of the tray body 45841, one end of the installation vertical bar 45846 is connected with the upper surface of the semicircular bottom block 4582, the other end of the installation vertical bar 45846 is provided with a semicircular pressing block 45845, the lower surface of the tray body 45841 is provided with a splicing box 45847, the surfaces of the tray body 45841 and the splicing box 45847 are provided with a connecting through groove 45848, the inner bottom surface of the connecting through groove 45848 is provided with a return spring 45849, and one end of the return spring 45849 is connected with the lower surface of the traction column block 45842.
Specifically, the tray 45841 is started, when the pulling column block 45842 rotates to the semicircular pressing block 45845, the top end of the pulling column block 45842 is attached to the rounded end of the semicircular pressing block 45845, the pulling column block 45842 is located at the lower end of the semicircular pressing block 45845 along with the rotation of the tray 45841, the pulling column block 45842 is pressed into the connecting through slot 45848, the extended long connecting rod 45843 is pressed downwards, because the connecting ring 45844 is clamped with the limiting ball block 4573, the top pressing rod 4572 drives the arc-shaped baffle 4571 to move downwards, the arc-shaped baffle 4571 is separated from the communication between the ball cavity 457 and the interior of the feeding pipe 452, when reaction raw materials are required to be added at regular time, the reaction raw materials enter the ball cavity 457 along the arc-shaped baffle 4571 through the feeding pipe 452, then enter the discharging pipe 453 into the reaction vessel 5, when the pulling column block 45842 is separated from the pressing block 45845, the arc-shaped baffle 4574 and the return spring 45849 can restore the arc-shaped baffle 4571 to the original position, and the arc-shaped baffle 4571 re-covered the inlet pipe 457, through rotating disk body 45841 a week, can control the opening and shutting of cowl 4571, and then be convenient for add reaction raw materials in different reaction time, need not constantly to open reaction vessel 5, avoid dirty entering wherein, further promote preparation efficiency.
In order to solve the technical problems that the wall surface of the reaction vessel is easy to be contaminated by materials, the proportioning degree of each reaction component is influenced, and the preparation cost is high, as shown in fig. 5, fig. 6 and fig. 10 to fig. 12, the following preferred technical solutions are provided:
the rotating pier block 42 comprises a driven fluted disc 421 and a limiting rotating member 422 arranged on the upper surface of the driven fluted disc 421, the driven fluted disc 421 is connected with the positioning column block 41 through the limiting rotating member 422, a second notched annular tooth surface 423 is arranged on the side surface of the driven fluted disc 421, a splicing block 424 is arranged on the lower surface of the driven fluted disc 421, the conveyor belt 33 is meshed with the first notched annular tooth surface 32 and the second notched annular tooth surface 423, the stirring assembly 45 comprises a central ball block 451 and a feed pipe 452 arranged at one end of the central ball block 451, a discharge pipe 453 is arranged at the other end of the central ball block 451, the central ball block 451 is matched with the limiting profile sleeve 18, a ring handle 454 is sleeved on the outer side of one end of the discharge pipe 453, a stirring cross bar 455 is arranged on the side surface of the ring handle 454, a stirring sharp tooth 456 is arranged at one end of the stirring cross bar 455, a ball cavity 457 is arranged inside the central ball cavity 451, and a ball containing shell is arranged inside the ball cavity 458, the splice pin 459 is mounted on both sides of the receiving ball shell 458, and one end of the splice pin 459 is connected to the inner wall of the central ball block 451.
The driving mechanism 2 comprises a driving gear 21 and a side flat toothed plate 22 arranged on one side of the driving gear 21, the side flat toothed plate 22 is meshed with the driving gear 21, a first matching strip 23 is arranged on the lower surface of the side flat toothed plate 22, one end of a traction upright rod 34 is connected with the driving gear 21, the first matching strip 23 is connected with a second matching chute 13, the hammering mechanism 6 comprises a transverse sliding plate 61 connected with one end of the side flat toothed plate 22 and a second matching strip 62 arranged on the lower surface of the transverse sliding plate 61, the second matching strip 62 is connected with the first matching chute 12, a transverse flat toothed surface 63 is arranged on the upper surface of the transverse sliding plate 61, movable adjusting grooves 64 are respectively arranged at two ends of the transverse sliding plate 61, an arc round rod 65 is arranged at the upper end of the transverse sliding plate 61, an arc toothed surface 66 is arranged on the lower surface of the arc round rod 65, and the arc toothed surface 66 is meshed with the transverse flat toothed surface 63, hammer hooks 67 are arranged at two ends of an arc round rod 65, adjusting swing rods 68 are arranged at two sides of the arc round rod 65, four groups of adjusting swing rods 68 are arranged, a rotating handle column 681 is arranged at one end of each adjusting swing rod 68, a sleeve rotating rod 682 is arranged at the center of each rotating handle column 681, each rotating handle column 681 is arranged on the side surface of the arc round rod 65, each rotating handle column 681 is connected with one end of each adjusting swing rod 68 through the sleeve rotating rod 682, a movable pushing thin rod 683 is arranged at the other end of each adjusting swing rod 68, each movable pushing thin rod 683 is connected with a movable adjusting groove 64, each reaction container 5 comprises a container shell 51 arranged on the lower surface of the extending transverse plate 17 and matching oblique rods 52 arranged on two sides of the container shell 51, a fitting block 53 is arranged on the surface of each matching oblique rod 52, each hammer hook 67 is fitted with the fitting block 53, an impact block 54 is arranged on the inner side of each matching oblique rod 52, and second connecting springs 55 are arranged at two ends of each matching oblique rod 52, one end of the second connection spring 55 is connected to the outer surface of the container case 51.
Specifically, when the driving gear 21 is started, the driving gear 21 is engaged with the side flat toothed plate 22, the side flat toothed plate 22 drives the transverse sliding plate 61 to move to one side, the transverse flat toothed surface 63 is engaged with the arc toothed surface 66 to drive the arc round rod 65 to turn to one side, the hammer hook 67 at one end of the arc round rod 65 impacts the attaching block 53, the attaching block 53 drives the matching diagonal rod 52 to be integrally close to the container shell 51, a plurality of groups of impacting blocks 54 impact the outer wall of the container shell 51 to facilitate shaking off the materials adhered to the inner wall, the materials are re-melted into the mixed liquid, the influence on the matching degree of each reaction component is avoided, resources can be saved, and further, under the repeated forward rotation of the driving gear 21, not only the stirring component 45 can be controlled to stir and mix the reaction materials, but also the two ends of the arc round rod 65 can be controlled to repeatedly impact the container shell 51 to enable the materials stained to naturally fall off, the integrity of the reaction materials is kept, a plurality of linkage mechanisms can be realized by one power member, the operation is convenient, and the preparation cost can be saved.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be able to cover the technical solutions and the inventive concepts of the present invention within the technical scope of the present invention.
Claims (10)
1. A preparation method of a compound for an anodic oxidation normal-temperature rapid oxidant is characterized by comprising the following steps: the method comprises the following steps:
s01: in the initial preparation stage: pouring a reaction solvent into a reaction container (5) filled with purified water with a specified proportion according to the proportion, and fully stirring the solution by a stirring component (45) to obtain a mixed solution;
s02: the preparation middle stage: carrying out heat treatment on the mixed liquid obtained in the initial stage, cooling and standing, layering the mixed liquid, and classifying and storing the liquids in all layers;
s03: the later stage of preparation: and adding a subsequent reaction solvent into the liquid collected in the middle stage, and drying and thermally treating the mixture to obtain the oxidant powder.
2. The preparation method of the compound for the anodic oxidation normal-temperature rapid oxidant according to claim 1, is characterized in that: in S01, the reaction solvent is a mixture of an acidic assistant, an oxidation-reduction assistant and a polymer, and comprises the following components by weight:
10-20 parts of sulfuric acid;
5-10 parts of oxalic acid;
1-2 parts of formic acid;
1-2 parts of tartaric acid;
3-5 parts of urea;
3-5 parts of anhydrous sodium sulphate;
0.5-1 part of polymaleic acid;
2000.5-1 parts of polyethylene glycol;
0.5-1 part of glycerol;
100 parts of pure water.
3. The preparation method of the compound for the anodic oxidation normal-temperature rapid oxidant according to claim 1, is characterized in that: the lower end of the reaction vessel (5) is provided with a bracket seat (1), the upper surface of the bracket seat (1) is provided with a driving mechanism (2), the upper end of the driving mechanism (2) is provided with a traction mechanism (3), one side of the traction mechanism (3) is provided with a force application mechanism (4), the reaction vessel (5) is arranged at the lower end of the force application mechanism (4), the outer side of the reaction vessel (5) is provided with a hammering mechanism (6), the bracket seat (1) comprises a supporting bottom plate (11) and a first matching chute (12) arranged on the upper surface of the supporting bottom plate (11), one side of the first matching chute (12) is provided with a second matching chute (13), the first matching chute (12) is communicated with the second matching chute (13), one side of the supporting bottom plate (11) is provided with an extending side plate (14), one end of the extending side plate (14) is provided with a vertical backboard (15), the top end of the vertical back plate (15) is provided with a beam rod (16), the side surface of the vertical back plate (15) is provided with an extension transverse plate (17), one end of the extension transverse plate (17) is provided with a limiting profile sleeve (18), the traction mechanism (3) comprises a traction turntable (31) and a first notch annular tooth surface (32) arranged on the side surface of the traction turntable (31), the outer side of the first notch annular tooth surface (32) is provided with a conveyor belt (33), the center of the lower surface of the traction turntable (31) is provided with a traction upright rod (34), the force application mechanism (4) comprises a positioning column block (41) and a rotating pier block (42) arranged at the lower end of the positioning column block (41), the upper surface of the positioning column block (41) is provided with an installation groove (43), the positioning column block (41) is connected with one end of the beam rod (16) through the installation and embedding groove (43), one side of the rotating pier block (42) is provided with an adapter rod (44), one end of the connecting rod (44) is provided with a stirring component (45), and the stirring component (45) is arranged in the reaction vessel (5).
4. The preparation method of the compound for the anodic oxidation normal-temperature rapid oxidant according to claim 3, is characterized in that: the rotating pier block (42) comprises a driven fluted disc (421) and a limiting rotating part (422) arranged on the upper surface of the driven fluted disc (421), the driven fluted disc (421) is connected with the positioning column block (41) through the limiting rotating part (422), a second notched annular tooth surface (423) is arranged on the side surface of the driven fluted disc (421), a splicing block (424) is arranged on the lower surface of the driven fluted disc (421), a conveying belt (33) is meshed and connected with the first notched annular tooth surface (32) and the second notched annular tooth surface (423), a stirring assembly (45) comprises a central ball block (451) and a feeding pipe (452) arranged at one end of the central ball block (451), a discharging pipe (453) is arranged at the other end of the central ball block (451), the central ball block (451) is matched with the limiting profile sleeve (18), a ring handle (454) is sleeved on the outer side of one end of the discharging pipe (453), and a stirring cross rod (455) is arranged on the side surface of the ring handle (454), stirring sharp teeth (456) are installed at one end of the stirring cross bar (455), a ball cavity (457) is formed in the center ball block (451), a containing ball shell (458) is arranged in the ball cavity (457), splicing slender rods (459) are installed on two sides of the containing ball shell (458), and one end of each splicing slender rod (459) is connected with the inner wall of the center ball block (451).
5. The preparation method of the compound for the anodic oxidation normal-temperature rapid oxidant according to claim 4, characterized in that: the upper end of holding ball shell (458) is provided with cowl (4571), center mounting of cowl (4571) lower surface has top pressure pole (4572), the one end of top pressure pole (4572) is provided with spacing ball piece (4573), the both sides of top pressure pole (4572) all are provided with first connecting spring (4574), the one end of first connecting spring (4574) is connected with cowl (4571), the other end of first connecting spring (4574) is connected with holding ball shell (458), slip hole (4581) has been seted up to the upper surface of holding ball shell (458), slip hole (4581) is connected with top pressure pole (4572), the inside of holding ball shell (458) is provided with semicircle bottom block (4582), reserve activity groove (4583) has been seted up to the upper surface of semicircle bottom block (4582), the upper end of reserving activity groove (4583) is provided with adjusts and establishes carousel (4584).
6. The preparation method of the compound for the anodic oxidation normal-temperature rapid oxidizer according to claim 5, wherein the preparation method comprises the following steps: the adjusting turntable (4584) comprises a turntable body (45841) and a traction column block (45842) installed at the side end of the turntable body (45841), one end of the traction column block (45842) is provided with an extension connecting rod (45843), one end of the extension connecting rod (45843) is provided with a joint ring (45844), one side of the turntable body (45841) is provided with an installation vertical rod (45846), one end of the installation vertical rod (45846) is connected with the upper surface of a semicircular bottom block (4582), the other end of the installation vertical rod (45846) is provided with a semicircular pressing block (45845), the lower surface of the turntable body (45841) is provided with a splicing box (45847), the surfaces of the turntable body (45841) and the splicing box (45847) are provided with a connecting through groove (45848), the inner bottom surface of the connecting through groove (45848) is provided with a return spring (45849), and one end of the return spring (45849) is connected with the lower surface of the traction column block (45842).
7. The preparation method of the compound for the anodic oxidation normal-temperature rapid oxidizer according to claim 3, is characterized by comprising the following steps: actuating mechanism (2) are including drive gear (21) and side flat rack (22) of setting in drive gear (21) one side, and side flat rack (22) are connected with drive gear (21) meshing, and the lower surface mounting of side flat rack (22) has first matching strip (23), and the one end of pulling pole setting (34) is connected with drive gear (21), and first matching strip (23) are connected with second matching spout (13).
8. The preparation method of the compound for the anodic oxidation normal-temperature rapid oxidizer according to claim 7, which is characterized in that: hammering mechanism (6) include transverse sliding plate (61) that are connected with side fishback (22) one end and install second matching strip (62) at transverse sliding plate (61) lower surface, second matching strip (62) are connected with first matching spout (12), the upper surface of transverse sliding plate (61) is provided with horizontal flat flank (63), activity adjustment tank (64) have all been seted up at the both ends of transverse sliding plate (61), the upper end of transverse sliding plate (61) is provided with arc body round bar (65), the lower surface of arc body round bar (65) is provided with arc flank (66), arc flank (66) are connected with horizontal flat flank (63) meshing, the both ends of arc body round bar (65) all are provided with hammer hook (67), adjust pendulum rod (68) are all installed to the both sides of arc body round bar (65), it is provided with four groups to adjust pendulum rod (68).
9. The preparation method of the compound for the anodic oxidation normal-temperature rapid oxidizer according to claim 8, wherein the preparation method comprises the following steps: a rotating handle column (681) is installed at one end of the adjusting swing rod (68), a sleeved rotating rod (682) is arranged in the center of the rotating handle column (681), the rotating handle column (681) is arranged on the side surface of the arc round rod (65), the rotating handle column (681) is connected with one end of the adjusting swing rod (68) through the sleeved rotating rod (682), a movable pushing thin rod (683) is arranged at the other end of the adjusting swing rod (68), and the movable pushing thin rod (683) is connected with the movable adjusting groove (64).
10. The preparation method of the compound for the anodic oxidation normal-temperature rapid oxidant according to claim 3, is characterized in that: the reaction vessel (5) comprises a vessel shell (51) arranged on the lower surface of the extending transverse plate (17) and matching oblique rods (52) arranged on two sides of the vessel shell (51), wherein a fitting block (53) is arranged on the surface of each matching oblique rod (52), a hammer hook (67) is fitted with the fitting block (53), an impact block (54) is arranged on the inner side of each matching oblique rod (52), second connecting springs (55) are arranged at two ends of each matching oblique rod (52), and one ends of the second connecting springs (55) are connected with the outer surface of the vessel shell (51).
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