CN114568738A - Low-temperature heating non-combustible product prepared from flexible carbonized exocarpium citri rubrum particles and application - Google Patents
Low-temperature heating non-combustible product prepared from flexible carbonized exocarpium citri rubrum particles and application Download PDFInfo
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- CN114568738A CN114568738A CN202111482906.8A CN202111482906A CN114568738A CN 114568738 A CN114568738 A CN 114568738A CN 202111482906 A CN202111482906 A CN 202111482906A CN 114568738 A CN114568738 A CN 114568738A
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- exocarpium citri
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel
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Abstract
The invention discloses a low-temperature heating non-combustible product prepared by flexible carbonized tangerine particles and application thereof, wherein a proper amount of alcohol is added into tangerine, and solid parts are separated out by hot reflux to obtain tangerine residues; igniting the herbaceous or woody plants to fully burn the herbaceous or woody plants, and sieving the remaining ash with a 80-mesh sieve to obtain undersize fine powder to obtain plant carbon ash; adding the prepared exocarpium Citri rubrum residue into boiling or non-boiling plant carbon ash, keeping the mixture of the two in boiling state, fully and flexibly carbonizing the exocarpium Citri rubrum residue for a fixed time, and separating to remove the plant carbon ash to obtain flexibly carbonized exocarpium Citri rubrum; and crushing and screening the prepared flexible carbonized exocarpium citri rubrum to obtain flexible carbonized exocarpium citri rubrum particles with required granularity. The flexible carbonized exocarpium citri grandis particles prepared by the invention are applied to heating non-combustible products, so that the prepared heating non-combustible products have natural exocarpium citri grandis fragrance and flavor characteristics, and the smoking quality of the particles is integrally improved.
Description
Technical Field
The invention relates to the field of heating non-combustible products, in particular to a low-temperature heating non-combustible product prepared from flexible carbonized exocarpium citri rubrum particles and application thereof.
Background
The heat-not-burn product is a tobacco substitute product, and is prepared by adding an extract liquid to plant particles to obtain heat-not-burn particles, and making them into a cigarette bullet or the like. When the particle baking device is used, heating equipment is used for heating and baking the particle baking device, and the temperature is controlled to be lower than the ignition point of the particles (generally 200-400 ℃) so as to be smoked by smokers.
The non-combustible product heated has the advantages that the atomization temperature of the product is low, the characteristic fragrant substances are retained to the maximum extent, and the particles can adsorb the fragrant substances in a saturated manner, so that the smoking quality is more elegant and lingering; the heating non-combustible product also has the characteristics of controllable chemical components of atomized smoke, effective reduction of harmful substances and the like. However, the conventional non-combustible heating product has the problems that the characteristic aroma substances are not obvious, part of particles have obvious bitter taste, and the like.
Disclosure of Invention
The invention aims to provide a preparation method of flexible carbonized exocarpium citri rubrum particles, and the obtained flexible carbonized exocarpium citri rubrum particles are applied to low-temperature heating non-combustible products to improve characteristic aroma and improve smoking quality.
In order to achieve the purpose, the preparation method of the flexible carbonized exocarpium citri rubrum particles comprises the following steps:
1) preparing orange residue: adding a proper amount of alcohol into the dried tangerine peel tablets, fully soaking, carrying out hot reflux for 0.5-1.5 h at the temperature of 55-75 ℃, dissolving out the part of soluble alcohol after extraction, and obtaining tangerine peel residues from the solid part;
2) preparing plant carbon ash: igniting the herbaceous or woody plants to fully burn the herbaceous or woody plants, and sieving the remaining ash with a 80-mesh sieve to obtain undersize fine powder to obtain plant carbon ash;
3) flexible carbonization: adding the tangerine peel residues prepared in the step 1) into boiling or non-boiling plant carbon ash, keeping the mixture of the tangerine peel residues and the plant carbon ash in a boiling state, fully and flexibly carbonizing the tangerine peel residues within a fixed time, and separating and removing the plant carbon ash to obtain flexibly carbonized tangerine peel;
the plant carbon ash is heated to a boiling state for flexible carbonization, and the purpose is as follows: heating to raise heat and lift the plant carbon ash upwards, returning to the original place of descent by self gravity to present a hot buoyancy boiling state (namely boiling), carbonizing in the state, wherein the carbonization process is helpful for degrading substances such as sugar, amino acid, pectin and the like, and simultaneously the carbonization process can lock fragrance to the maximum extent and retain the flavor of the red tangerine peel.
4) Preparing into particles: and (4) crushing and screening the flexible carbonized red oranges prepared in the step 3) to obtain flexible carbonized red oranges with required granularity.
Preferably, the concentration of the alcohol in the step 1) is 50% by mass, and the adding amount of the alcohol is 8-12 times of the mass of the extracted red tangerine peel.
Preferably, the herbaceous or woody plants in the step 2) comprise but are not limited to one or more of straws and rice straws.
Preferably, in the step 3), the temperature of the boiling state is kept at 180-300 ℃ for 5-10 min, and the moisture content of the orange granules obtained after flexible carbonization and separation is 8-15% by mass.
Preferably, in the step 4), the particle size of the flexible carbonized exocarpium citri rubrum particles is 12-50 meshes in a standard mesh number.
The invention also discloses an application method of the flexible carbonized exocarpium citri rubrum particles in low-temperature heating of non-combustible products.
Preferably, the adding amount of the flexible carbonized exocarpium citri rubrum particles is preferably 20 to 50 percent of the total mass of the low-temperature heating non-combustible product.
The article is typically tubular in shape similar to a conventional cigarette, but may have other shapes. The specific filling and packaging method using the prior art is not an improvement of the present invention and is therefore omitted.
Compared with the prior art, the invention has the beneficial effects that:
1) according to the method, firstly, the dried orange slices are soaked in alcohol and subjected to reflux treatment at a specific temperature and time, and the soluble parts of the dried orange slices are dissolved out by the alcohol to obtain soft orange residues with fine gaps.
2) The evaluation of the low-temperature heating non-combustible product prepared by the invention shows that the addition of the flexible carbonized exocarpium citri rubrum particles can effectively improve the adsorption capacity of the particles, cover burnt odor and obviously improve the smoking quality of the low-temperature heating non-combustible product.
3) The invention firstly makes the flexible carbonized red tangerine peel into the base material of the low-temperature heating non-combustible product, has simple preparation method, easy operation and low cost, is suitable for popularization and application, and fills the blank in the technical field of the low-temperature heating non-combustible product.
Drawings
FIG. 1 is an appearance diagram of a dried orange slice produced by the process of the present invention;
FIG. 2 is an appearance diagram of exocarpium Citri rubrum residue obtained in the preparation process of the present invention;
FIG. 3 is an appearance diagram of a flexible carbonized exocarpium Citri Grandis residue prepared in the process of the present invention;
FIG. 4 is an appearance diagram of orange granules prepared according to the present invention.
Detailed Description
The present invention will be described in further detail with reference to specific examples.
Example 1
As shown in fig. 1 to 4, in the case of exocarpium citri rubrum, flexible carbonized exocarpium citri rubrum granules were prepared and added to low-temperature-heat-incombustible granules to prepare a low-temperature-heat-incombustible product 1.
1) Preparing the tangerine peel residues: adding alcohol with the mass of 8 times of the batch size for hot reflux extraction twice. Extracting at 55 deg.C for 0.5h, and naturally air drying the solid part after extraction to obtain the residue.
2) Preparing plant ash: igniting the straws with carbon, fully burning the straws to obtain straw ash powder, and sieving the straw ash powder with a 80-mesh sieve to obtain fine powder;
3) preparing flexible carbonized red tangerine peel particles: heating plant ash to a boiling state, adding the tangerine peel residues, performing full flexible carbonization, keeping the temperature at 180 ℃ for 5min to obtain flexible carbonized tangerine peel residues, and screening the flexible carbonized tangerine peel residues by using a 12-mesh standard sieve to obtain flexible carbonized tangerine peel particles, wherein the water content of the flexible carbonized tangerine peel particles is 11.5%;
4) preparation of low-temperature heating non-combustible product: the soft carbonized exocarpium Citri rubrum particles are added into the non-combustible particles under heating, the addition amount is 20%, and the low-temperature non-combustible heated product 1 is obtained.
The samples of the low-temperature heating non-combustible product 1 and the samples without the flexible carbonized exocarpium citri rubrum particles (hereinafter referred to as a control group) are randomly numbered, sensory evaluation is carried out by an evaluation group, and the evaluation test result shows that the flexible carbonized exocarpium citri rubrum particles are harmonious with the low-temperature heating non-combustible product, the fragrance amount is slightly increased, the smoke quality is good, and the scorched smell is slightly reduced, which is detailed in table 1.
TABLE 1 evaluation of smoking quality of non-combustible product 1 heated at low temperature
Sensory quality assessment noun interpretation:
1) the aroma refers to the aroma of the smoke inherent in the smoke of the non-combustible product heated at low temperature. Higher scores represent more fragrance.
2) The aroma amount refers to the smoke amount of a non-combustible product heated at low temperature. A higher score indicates a more adequate fragrance quantity.
3) Aftertaste refers to the taste sensation left by smoke from the oral cavity and nasal cavity. Including comfort, cleanliness, and dryness. A higher score indicates a cleaner aftertaste.
4) The harmony refers to the harmonious and consistent fragrance, and the characteristics of a certain monomer in the fragrance cannot be sensed. Higher scores represent harmonious or harmonious coordination.
5) Miscellaneous gases mean slight and noticeable unpleasant odors that do not have the intrinsic odor of a non-low temperature heat-not-combustible product. Higher scores represent more prominent miscellaneous gas.
Example 2
The main steps of this example are repeated with example 1, with the only difference that:
the addition amount of the flexible carbonized exocarpium Citri rubrum particles was changed to 35%, and the number of the manufactured low-temperature heating non-combustible product was sample 2.
The result of the smoke panel tests shows that the flexible carbonized red tangerine peel particles are compatible with low-temperature heating non-combustible products, the fragrance amount is increased, the smoke quality is elegant, and the scorched smell is reduced. See table 2 for details.
Table 2 sample 2 aspiration quality evaluation
Although the present invention has been described in detail with reference to certain specific embodiments thereof, it will be understood by those skilled in the art that the foregoing examples are for the purpose of illustration only and are not intended to limit the scope of the invention. It will be appreciated by those skilled in the art that modifications may be made to the above embodiments without departing from the scope and spirit of the invention. The scope of protection of the invention is defined by the appended claims.
Claims (7)
1. A preparation process of flexible carbonized exocarpium citri rubrum particles is characterized by comprising the following steps:
1) preparing orange residue: adding a proper amount of alcohol into the dried tangerine peel tablets, carrying out hot reflux for 0.5-1.5 h at the temperature of 55-75 ℃, and separating out a solid part to obtain tangerine peel residues;
2) preparing plant carbon ash: igniting the herbaceous or woody plants to fully burn the herbaceous or woody plants, and sieving the rest ash with a 80-mesh sieve to obtain undersize fine powder, namely plant carbon ash;
3) flexible carbonization: adding the tangerine peel residues prepared in the step 1) into boiling or non-boiling plant carbon ash, keeping the mixture of the tangerine peel residues and the plant carbon ash in a boiling state, fully and flexibly carbonizing the tangerine peel residues within a fixed time, and separating and removing the plant carbon ash to obtain flexibly carbonized tangerine peel;
4) preparing into particles: and (3) crushing and screening the flexible carbonized exocarpium citri rubrum prepared in the step 3) to obtain flexible carbonized exocarpium citri rubrum particles with the required granularity.
2. The process for preparing flexible carbonized exocarpium citri rubrum particles according to claim 1, wherein the concentration of the alcohol in step 1) is 50% by mass, and the addition amount is 8-12 times of the mass of the extracted exocarpium citri rubrum.
3. The process for preparing flexible carbonized exocarpium citri rubrum particles according to claim 1, wherein the herbaceous or woody plants in step 2) include but are not limited to one or more of straws and rice straws.
4. The process for preparing the flexible carbonized exocarpium citri rubrum particles according to claim 1, wherein the boiling temperature in the step 3) is kept at 180-300 ℃ for 5-10 min, and the moisture content of the exocarpium citri rubrum particles obtained after flexible carbonization and separation is 8-15% by mass.
5. The process for preparing flexible carbonized exocarpium citri grandis granules according to claim 1, wherein: the granularity of the flexible carbonized red tangerine peel particles in the step 4) is 12-50 meshes in terms of standard screen mesh number.
6. Use of the flexible carbonized red tangerine particles prepared by the preparation method according to any one of claims 1 to 5 in low temperature heating of non-combustible products.
7. The use of the flexible carbonized exocarpium Citri rubrum particles in a low-temperature heating non-combustible product according to claim 6, wherein the addition amount of the flexible carbonized exocarpium Citri rubrum particles is 20-50% of the total mass of the low-temperature heating non-combustible product.
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Citations (6)
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| CN109222230A (en) * | 2018-09-11 | 2019-01-18 | 云南中烟工业有限责任公司 | A kind of soft quasi- carbonization ferment particulate of corn Radix Glycyrrhizae blood-snow tea, preparation method and the usage |
| CN109330016A (en) * | 2018-11-14 | 2019-02-15 | 河南中烟工业有限责任公司 | A kind of Exocarpium Citri Grandis medicinal extract, preparation method and the application in cigarette |
| CN109549250A (en) * | 2018-10-18 | 2019-04-02 | 云南中烟工业有限责任公司 | The soft quasi- carbonization ferment particulate of the small blueness mandarin orange of one kind, preparation method and the usage |
| CN110292203A (en) * | 2018-10-18 | 2019-10-01 | 云南中烟工业有限责任公司 | A kind of soft quasi- carbonization ferment particulate of plant, preparation method and the usage |
| CN112237297A (en) * | 2020-11-09 | 2021-01-19 | 云南纯旭生物科技有限公司 | High-smoke-concentration heating non-combustible product |
| CN212545525U (en) * | 2020-05-25 | 2021-02-19 | 云南中烟工业有限责任公司 | Flexible carbonization device |
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2021
- 2021-12-07 CN CN202111482906.8A patent/CN114568738B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109222230A (en) * | 2018-09-11 | 2019-01-18 | 云南中烟工业有限责任公司 | A kind of soft quasi- carbonization ferment particulate of corn Radix Glycyrrhizae blood-snow tea, preparation method and the usage |
| CN109549250A (en) * | 2018-10-18 | 2019-04-02 | 云南中烟工业有限责任公司 | The soft quasi- carbonization ferment particulate of the small blueness mandarin orange of one kind, preparation method and the usage |
| CN110292203A (en) * | 2018-10-18 | 2019-10-01 | 云南中烟工业有限责任公司 | A kind of soft quasi- carbonization ferment particulate of plant, preparation method and the usage |
| CN109330016A (en) * | 2018-11-14 | 2019-02-15 | 河南中烟工业有限责任公司 | A kind of Exocarpium Citri Grandis medicinal extract, preparation method and the application in cigarette |
| CN212545525U (en) * | 2020-05-25 | 2021-02-19 | 云南中烟工业有限责任公司 | Flexible carbonization device |
| CN112237297A (en) * | 2020-11-09 | 2021-01-19 | 云南纯旭生物科技有限公司 | High-smoke-concentration heating non-combustible product |
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