CN114432199B - Peony pistil superfine powder micelle solution and preparation method and application thereof - Google Patents
Peony pistil superfine powder micelle solution and preparation method and application thereof Download PDFInfo
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Images
Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/49—Solubiliser, Solubilising system
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/522—Antioxidants; Radical scavengers
Abstract
The invention discloses a peony pistil submicron powder micellar solution and a preparation method and application thereof. The peony pistil superfine powder micelle solution comprises the following raw materials in parts by weight: 2-9.8 parts of peony pistil ultra-fine powder, 30-40 parts of polyglycerol-4 oleate, 60-65 parts of meadowfoam seed oil and 0.5-3 parts of tocopherol. According to the invention, the stability of the peony pistil ultrafine powder micelle in a solution is regulated and controlled by regulating the proportion of glyceride substances in the peony pistil ultrafine powder, polyglycerol-4 oleate and white pooling seed oil, so that the prepared peony pistil micelle has better stability, can retain effective components in the peony pistil, has the effects of whitening, resisting aging and the like, and has a good application prospect in the field of cosmetics.
Description
Technical Field
The invention belongs to the technical field of peony processing, and particularly relates to a peony stamen ultrafine powder micellar solution, and a preparation method and application thereof.
Background
The peony has high ornamental value and medicinal value, the carbohydrate content in the stamen of the peony is higher than 55.49 percent, the protein content reaches 24.83 percent and is far higher than the protein content of the petals of the same peony, the fat content in the plant species is medium and low, the total sugar content is 14.24 percent and is far lower than the total sugar content of common energy foods, and researches find that the stamen of the peony has the effects of reducing blood fat, preventing and assisting in treating cardiovascular and cerebrovascular diseases and the like, has positive auxiliary treatment effects on gastrointestinal dysfunction and constipation, has auxiliary treatment and recovery effects on prostatitis and prostatic hyperplasia, the crude fiber content is higher than the crude fiber content of bee pollen, the VC content is 39.3mg/100g, the VE content is 23.2mg/100g, and belongs to high category in a Chinese food nutrition ingredient table. The peony stamen contains 18 kinds of amino acids, the total amount of the amino acids accounts for 10.56%, the content of essential amino acids accounts for 38.26%, the content of the essential amino acids is higher than that of rose (34.42%) by nearly 4%, 8 kinds of essential amino acids are complete and reasonable, the content of the essential amino acids is 1.47% of glutamic acid at the highest, 0.13% of methionine at the lowest, the content of other 6 kinds of essential amino acids is higher and uniform, and the formed protein content is high and excellent in quality; the peony stamen has reasonable fatty acid composition, the contents of oleic acid, linoleic acid and linolenic acid are high, the total content of 156 unsaturated fatty acid exceeds 70%, the content ratio of unsaturated fatty acid to saturated fatty acid reaches more than 2.5 and is far greater than the world health organization recommended value (not less than 0.7), and the peony stamen has very reasonable fatty acid composition and high nutritional value. The lutein content in stamen of peony flower is 8.4mg/kg, which shows that the product has the unique functions of improving eyesight and protecting vision, and especially preventing chronic eye diseases such as age-related macular degeneration, cataract and the like.
Although the medicinal value, the food value and the like of the peony are higher, the development and the utilization of deep-processed products of the peony are seriously lagged, and the peony pistil products obtained by the prior art are not easy to store, so that the waste is caused because the utilization rate of effective components in the peony pistil is low.
Disclosure of Invention
The invention aims to provide a peony pistil submicron powder micellar solution and a preparation method and application thereof aiming at the defects of the prior art.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows: the peony pistil submicron powder micelle solution comprises the following raw materials in parts by weight: 2-9.8 parts of peony pistil ultra-fine powder, 30-40 parts of polyglycerol-4 oleate, 60-65 parts of meadowfoam seed oil and 0.5-3 parts of tocopherol.
The polyglycerol-4 oleate is used as a solubilizer, so that the formation of micro-micelles in the solution of peony pistil micro-powder in scarfing can be ensured; on one hand, the main component of the meadowfoam seed oil is glyceride, so that the micellae can be better suspended in the same oil, and the stable state of the micellae is ensured; on the other hand, the meadowfoam seed oil has good skin permeability as vegetable oil, and can improve the application of the micro-micelle in cosmetics; meanwhile, the tocopherol is added to play an antioxidation role of the peony pistil micelle full-oil system. Through compounding of the raw materials, the prepared peony pistil superfine powder micellar solution has good stability, and effective ingredients in peony pistil can be retained to the maximum extent.
As a preferred embodiment of the invention, the particle size of the peony pistil ultra-micro powder is 400-600 meshes.
The stability of the peony pistil superfine powder micellar solution can be directly influenced by the particle size of the peony pistil superfine powder, and the peony pistil superfine powder has the particle size of 400-600 meshes, so that the stability of the peony pistil superfine powder micellar solution can be still better after a later-stage shearing process. As a preferred embodiment of the invention, the preparation method of the peony stamen ultrafine powder comprises the following steps: and (3) carrying out superfine grinding on the peony pistil, and screening and separating pollen to obtain the peony pistil superfine powder.
As a preferred embodiment of the invention, the ultramicro pulverization is characterized in that the wall breaking is carried out by a planetary ball mill in an ultramicro way, the rotating speed is 600-1000r/min, the pulverizing time is 0.5-1h, and the ball-to-material ratio is 5-9:1.
As a preferred embodiment of the invention, the screening is carried out by using a shaking screen, and the screen mesh of the shaking screen is 400-600 meshes.
The invention also claims a preparation method of the peony pistil submicron powder micellar solution, which comprises the following steps:
dispersing the peony pistil superfine powder in polyglycerol-4 oleate, adding tocopherol and meadowfoam seed oil, and shearing under a vacuum condition until the tocopherol and the meadowfoam seed oil are completely dissolved to obtain the peony pistil superfine powder micellar solution.
In the system, the peony pistil superfine powder can be dissolved in polyglycerol-4 oleate and glyceride substances in white pooling seed oil, a PS-PI diblock copolymer is formed by adjusting the proportion of PS and PI in a mixed solvent and at a certain shearing rate and preparation temperature, the PS-PI diblock copolymer can form a micro-micelle body with PS as a core and PI as a shell, and the micelle body is uniformly dispersed in a stable micro-opalescence uniform dispersion system.
Treating the peony pistil submicron powder micelle solution by a quenching process for preservation; the quenching process is to rapidly reduce the temperature of the peony pistil submicron powder micelle solution to 0-minus 18 ℃. The quenching process specifically comprises the following steps: placing the peony pistil submicron powder micellar solution into a container, and placing the container into a vessel loaded with ice-water mixture to cool the peony pistil submicron powder micellar solution to 0 ℃.
As a preferred embodiment of the invention, the rotation speed of the shearing treatment is 13000-15000r/min, and the temperature is 30-45 ℃.
The stability of the peony pistil ultra-pure micro powder micelle body is optimized by adjusting the temperature of the shearing treatment. If the temperature is not within the limited range of the invention, the activity of the peony pistil ultra-pure micro-powder micelle body can be influenced, and the micelle body is agglomerated and separated out due to gelatinization.
The invention also claims application of the peony pistil submicron powder micellar solution in cosmetics.
A cosmetic comprises said peony pistil ultra-micro micelle solution.
As a preferred embodiment of the invention, the content of the peony pistil submicron powder micelle solution in the cosmetic is 1-10% by mass.
Compared with the prior art, the invention has the following beneficial effects: according to the invention, the stability of the peony pistil ultrafine powder micelle in the solution is regulated and controlled by regulating the proportion of glyceride substances in the peony pistil ultrafine powder, polyglycerol-4 oleate and white pooling seed oil, so that the peony pistil ultrafine powder, the polyglycerol-4 oleate, the white pooling seed oil and the tocopherol are compounded, and the prepared peony pistil micro-micelle has better stability on one hand; on the other hand, compared with the traditional active ingredient extraction method, the peony pistil micro-micelle solution disclosed by the invention can furthest retain the active ingredients in the peony pistil, so that the peony pistil micro-micelle has the effects of whitening, resisting aging and the like, and the defect that the peony pistil ultra-micro powder can only serve as a toner role due to the fact that the peony pistil ultra-micro powder is not fused with other components of cosmetics in skin care products is overcome, and the application of the peony pistil powder in the field of cosmetics is better expanded.
Drawings
FIG. 1 is a microstructure diagram of ultra-pure micro-powder micelle of peony pistil.
Detailed Description
To better illustrate the objects, technical solutions and advantages of the present invention, the present invention will be further described with reference to specific examples.
FIG. 1 is a microstructure diagram of ultra-pure micro-powder micelle of peony pistil. As can be seen from the figure, the peony pistil ultra-fine powder can be dissolved in polyglycerol-4 oleate and glyceride substances in white pooled seed oil, and a PS-PI diblock copolymer can be formed by adjusting the proportion of PS and PI in a mixed solvent and at a certain shearing rate and preparation temperature, wherein the PS-PI diblock copolymer can form a micelle body with PS as a core and PI as a shell.
Example 1
The peony pistil submicron powder micelle solution comprises the following raw materials in parts by weight: 2 parts of peony pistil superfine powder, 30 parts of polyglycerol-4 oleate, 63 parts of chinaroot greenbrier seed oil and 2 parts of tocopherol.
The preparation method of the peony pistil submicron powder micelle solution comprises the following steps:
(1) Ultramicro wall breaking is carried out on peony pistil by using a planetary ball mill, and then pollen is screened and separated by using a 600-mesh vibrating screen to obtain peony pistil ultramicro powder; the rotation speed of the ultramicro wall breaking is 600r/min, the crushing time is 0.5h, and the ball-to-material ratio is 7:1;
(2) Dispersing the peony pistil superfine powder in polyglycerol-4 oleate, then adding tocopherol and meadowfoam seed oil, and shearing at 13000r/min under vacuum condition and 40 ℃ until the peony pistil superfine powder is completely dissolved to obtain the peony pistil superfine powder micellar solution.
Example 2
The peony pistil submicron powder micelle solution comprises the following raw materials in parts by weight: 6 parts of peony pistil superfine powder, 35 parts of polyglycerol-4 oleate, 60 parts of chinaroot greenbrier seed oil and 0.5 part of tocopherol.
The preparation method of the peony pistil submicron powder micelle solution comprises the following steps:
(1) Ultramicro wall breaking is carried out on peony pistil by using a planetary ball mill, and then pollen is screened and separated by using a 500-mesh vibrating screen to obtain peony pistil ultramicro powder; the rotation speed of the ultramicro wall breaking is 800r/min, the crushing time is 1h, and the ball-material ratio is 5:1;
(2) Dispersing the peony pistil superfine powder in polyglycerol-4 oleate, then adding tocopherol and meadowfoam seed oil, and shearing at 13000r/min under vacuum condition and 30 ℃ until the peony pistil superfine powder is completely dissolved to obtain the peony pistil superfine powder micellar solution.
Example 3
The peony pistil submicron powder micelle solution comprises the following raw materials in parts by weight: 9.8 parts of peony pistil superfine powder, 40 parts of polyglycerol-4 oleate, 65 parts of white chinaberry seed oil and 3 parts of tocopherol.
The preparation method of the peony pistil submicron powder micelle solution comprises the following steps:
(1) Ultramicro wall breaking is carried out on peony pistil by using a planet ball mill, and then pollen is screened and separated by using a 700-mesh vibrating screen to obtain peony pistil ultramicro powder; the rotation speed of the ultramicro wall breaking is 1000r/min, the crushing time is 0.8h, and the ball-to-material ratio is 9:1;
(2) Dispersing the peony pistil superfine powder in polyglycerol-4 oleate, then adding tocopherol and meadowfoam seed oil, and shearing at 15000r/min under vacuum condition and 45 ℃ until the peony pistil superfine powder is completely dissolved to obtain the peony pistil superfine powder micellar solution.
Example 4
The raw material components of the peony pistil submicron powder micelle solution in the embodiment are the same as those in the embodiment 1.
The preparation method of the peony pistil submicron powder micelle solution is only different from that of the peony pistil submicron powder micelle solution in the embodiment 1: in the step (1), the mesh number of the screen of the oscillating screen is 500 meshes.
Example 5
The raw material components of the peony pistil submicron powder micellar solution in the embodiment are the same as those in the embodiment 1.
The preparation method of the peony pistil submicron powder micelle solution is only different from that of the peony pistil submicron powder micelle solution in the embodiment 1: in the step (1), the mesh number of the screen of the oscillating screen is 450 meshes.
Example 6
The raw material components of the peony pistil submicron powder micelle solution in the embodiment are the same as those in the embodiment 1.
The preparation method of the peony pistil submicron powder micelle solution is only different from that of the peony pistil submicron powder micelle solution in the embodiment 1: in the step (1), the mesh number of the screen of the oscillating screen is 400 meshes.
Example 7
The raw material components of the peony pistil submicron powder micelle solution in the embodiment are the same as those in the embodiment 1.
The preparation method of the peony pistil submicron powder micellar solution in the embodiment is only different from that in the embodiment 1: in the step (2), the temperature of the shearing treatment is 30 ℃.
Example 8
The raw material components of the peony pistil submicron powder micellar solution in the embodiment are the same as those in the embodiment 1.
The preparation method of the peony pistil submicron powder micelle solution is only different from that of the peony pistil submicron powder micelle solution in the embodiment 1: in the step (2), the temperature of the shearing treatment is 35 ℃.
Example 9
The raw material components of the peony pistil submicron powder micelle solution in the embodiment are the same as those in the embodiment 1.
The preparation method of the peony pistil submicron powder micellar solution in the embodiment is only different from that in the embodiment 1: in the step (2), the temperature of the shearing treatment is 45 ℃.
Example 10
The peony pistil submicron powder micelle solution comprises the following raw materials in parts by weight: 2 parts of peony pistil superfine powder, 35 parts of polyglycerol-4 oleate, 63 parts of chinaroot greenbrier seed oil and 2 parts of tocopherol.
The preparation method of the peony pistil submicron powder micelle solution is the same as that of the embodiment 1.
Example 11
The peony pistil submicron powder micelle solution comprises the following raw materials in parts by weight: 2 parts of peony pistil superfine powder, 40 parts of polyglycerol-4 oleate, 63 parts of chinaroot greenbrier seed oil and 2 parts of tocopherol.
The preparation method of the peony pistil submicron powder micelle solution is the same as that of the embodiment 1.
Comparative example 1
The raw material components of the peony pistil submicron powder micellar solution in the comparative example are the same as those in the example 1.
The preparation method of the peony pistil submicron powder micellar solution in the comparative example is only different from that in the example 1: in the step (1), the mesh number of the screen of the oscillating screen is 300 meshes.
Comparative example 2
The raw material components of the peony pistil submicron powder micelle solution in the comparative example are the same as those in the example 1.
The preparation method of the peony pistil submicron powder micellar solution in the comparative example is only different from that in the example 1: in the step (1), the mesh number of the screen of the oscillating screen is 800 meshes.
Comparative example 3
The raw material components of the peony pistil submicron powder micelle solution in the comparative example are the same as those in the example 1.
The preparation method of the peony pistil submicron powder micellar solution in the comparative example is only different from that in the example 1 in that: in the step (2), the temperature of the shearing treatment is 20 ℃.
Comparative example 4
The raw material components of the peony pistil submicron powder micellar solution in the comparative example are the same as those in the example 1.
The preparation method of the peony pistil submicron powder micellar solution in the comparative example is only different from that in the example 1: in the step (2), the temperature of the shearing treatment is 50 ℃.
Comparative example 5
The peony pistil submicron powder micelle solution comprises the following raw materials in parts by weight: 2 parts of peony pistil ultrafine powder, 20 parts of polyglycerol-4 oleate, 63 parts of white pool flower seed oil and 2 parts of tocopherol.
The preparation method of the peony pistil submicron powder micelle solution in the comparative example is the same as that of the example 1.
Comparative example 6
The peony pistil submicron powder micelle solution comprises the following raw materials in parts by weight: 2 parts of peony pistil superfine powder, 50 parts of polyglycerol-4 oleate, 63 parts of chinaroot greenbrier seed oil and 2 parts of tocopherol.
The preparation method of the peony pistil submicron powder micelle solution in the comparative example is the same as that of the example 1.
Effect example 1
The stability test was performed on the peony pistil ultra fine powder micelle solutions prepared in examples 1 to 11 and comparative examples 1 to 6 and the cosmetics prepared from the peony pistil ultra fine powder micelle solutions.
Test samples: peony pistil ultra-fine powder micelle solutions prepared in examples 1 to 11 and comparative examples 1 to 6
Test method 1:
and observing the state of the tested sample, wherein when the sample is a light yellow transparent oily solution, the sample is stable, and if the sample is in a turbid state, the sample is unstable.
TABLE 1 stability results for peony pistil submicron micelle solutions
According to the data in the table 1, the examples of the present invention can prepare stable state peony pistil ultra-fine powder micellar solution which is light yellow transparent oil solution.
Test method 2
And (3) mixing the test sample with grease GTCC according to the mass ratio of 1:10, mixing uniformly, respectively placing the mixture under the conditions of-18 ℃ in dark, 45 ℃ in dark and 1 week in light, observing the state of the sample, indicating that the sample is stable when the appearance of the sample is not changed, and indicating that the sample is unstable if the appearance of the sample is changed, such as conglomeration, discoloration and precipitation.
TABLE 2 stability results for cosmetics prepared from peony pistil ultra-micro powder micellar solution
According to the data in table 2, compared to the comparative example, the cosmetic products prepared in the examples have no change under the conditions of-18 ℃ in the dark, 45 ℃ in the dark and 1 week in the light, which indicates that the peony pistil ultrafine micelle solution can be stably applied to the cosmetics. Effect example 2
Effect example 2
The effect example is an effective component content test of the peony stamen ultrafine micelle solution prepared in examples 1-11, and the effective content of protein, lutein, polysaccharide and vitamins in each 100g of the peony stamen ultrafine micelle solution is tested.
TABLE 3 determination of the active ingredient content of peony pistil ultra-fine powder micellar solution
| Protein | Xanthophyll | Polysaccharides | Vitamins and their use as anti-inflammatory agents | |
| Example 1 | 12.80g | 0.18mg | 8.80g | 2.65mg |
| Example 2 | 13.49g | 0.50mg | 9.24g | 4.25mg |
| Example 3 | 14.13g | 0.80mg | 9.80g | 4.53mg |
| Example 4 | 12.65g | 0.20mg | 8.85g | 2.53mg |
| Example 5 | 12.76g | 0.25mg | 8.82g | 2.58mg |
| Example 6 | 12.89g | 0.28mg | 8.75g | 2.60mg |
| Example 7 | 12.68g | 0.16mg | 8.72g | 2.58mg |
| Example 8 | 12.50g | 0.18mg | 8.79g | 2.28mg |
| Example 9 | 12.78g | 0.20mg | 8.82g | 2.70mg |
| Example 10 | 12.45g | 0.17mg | 8.68g | 2.25mg |
| Example 11 | 11.87g | 0.160mg | 8.24g | 2.04mg |
The products prepared in comparative examples 1 to 6 are turbid oil liquids and are in unstable states, so that the content of specific components cannot be calibrated. Therefore, the peony pistil submicron powder micellar solution prepared by the embodiment of the invention can be stably applied to cosmetics and is fused with other components in the cosmetics, and the peony pistil submicron powder micellar solution can reserve effective components in peony pistils to the maximum extent, so that the peony pistil submicron powder micellar solution has the effects of whitening, resisting aging and the like.
Although the present invention has been described in detail with reference to the preferred embodiments, it will be understood by those skilled in the art that various changes may be made and equivalents may be substituted for elements thereof without departing from the true spirit and scope of the present invention.
Claims (7)
1. The peony pistil superfine powder micellar solution is characterized by comprising the following raw materials in parts by weight: 2-9.8 parts of peony pistil superfine powder, 30-40 parts of polyglycerol-4 oleate, 60-65 parts of meadowfoam seed oil and 0.5-3 parts of tocopherol; the particle size of the peony pistil ultra-fine powder is 400-600 meshes; the preparation method of the peony pistil submicron powder micelle solution comprises the following steps: dispersing the peony pistil superfine powder in polyglycerol-4 oleate, adding tocopherol and chinaroot greenbrier seed oil, and shearing under vacuum condition until the tocopherol and the chinaroot greenbrier seed oil are completely dissolved, wherein the reaction temperature is 30-45 ℃, so as to obtain the peony pistil superfine powder micellar solution.
2. The peony stamen ultrafine powder micellar solution as claimed in claim 1, wherein the preparation method of said peony stamen ultrafine powder comprises the following steps: and (3) carrying out superfine grinding on the peony pistil, and screening and separating pollen to obtain the peony pistil superfine powder.
3. The peony pistil submicron powder micellar solution as claimed in claim 2, wherein the ultramicro pulverization is characterized in that the wall breaking is carried out by a planetary ball mill in an ultramicro way, the rotating speed is 600-1000r/min, the pulverization time is 0.5-1h, and the ball-to-material ratio is 5-9:1.
4. The method for preparing the peony pistil submicron powder micellar solution as in claim 1, wherein the rotation speed of the shearing treatment is 13000-15000r/min.
5. The use of peony pistil submicron powder micellar solution as defined in claim 1 in cosmetics.
6. A cosmetic comprising the peony pistil submicron micelle solution as set forth in claim 1.
7. The cosmetic according to claim 6, wherein the content of the peony pistil submicron micelle solution in the cosmetic is 1-10% by mass.
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Denomination of invention: A peony stamen ultrafine powder micelle solution and its preparation method and application Effective date of registration: 20231008 Granted publication date: 20221028 Pledgee: Guotou Taikang Trust Co.,Ltd. Pledgor: Meichulai (Hangzhou) Cosmetics Co.,Ltd. Registration number: Y2023980060101 |
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