CN114407451A - Flame-retardant anti-dripping multifunctional knitted fabric and preparation method thereof - Google Patents
Flame-retardant anti-dripping multifunctional knitted fabric and preparation method thereof Download PDFInfo
- Publication number
- CN114407451A CN114407451A CN202111669975.XA CN202111669975A CN114407451A CN 114407451 A CN114407451 A CN 114407451A CN 202111669975 A CN202111669975 A CN 202111669975A CN 114407451 A CN114407451 A CN 114407451A
- Authority
- CN
- China
- Prior art keywords
- flame
- retardant
- layer
- yarn
- yarns
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 title claims abstract description 88
- 239000003063 flame retardant Substances 0.000 title claims abstract description 88
- 239000004744 fabric Substances 0.000 title claims abstract description 61
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 238000004519 manufacturing process Methods 0.000 title description 2
- 239000000835 fiber Substances 0.000 claims abstract description 70
- 229920000742 Cotton Polymers 0.000 claims abstract description 48
- 241000219146 Gossypium Species 0.000 claims abstract description 30
- 229920000728 polyester Polymers 0.000 claims abstract description 28
- 238000009940 knitting Methods 0.000 claims abstract description 26
- 238000002156 mixing Methods 0.000 claims abstract description 18
- 240000000047 Gossypium barbadense Species 0.000 claims abstract description 17
- 235000009429 Gossypium barbadense Nutrition 0.000 claims abstract description 17
- 229920002821 Modacrylic Polymers 0.000 claims abstract description 17
- 238000009941 weaving Methods 0.000 claims abstract description 15
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 9
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 9
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 9
- 239000011425 bamboo Substances 0.000 claims abstract description 9
- 239000003610 charcoal Substances 0.000 claims abstract description 9
- 238000000034 method Methods 0.000 claims abstract description 6
- 244000082204 Phyllostachys viridis Species 0.000 claims abstract 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 30
- 238000010438 heat treatment Methods 0.000 claims description 25
- 239000002131 composite material Substances 0.000 claims description 18
- 238000001816 cooling Methods 0.000 claims description 15
- 238000001035 drying Methods 0.000 claims description 15
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 claims description 10
- 239000002202 Polyethylene glycol Substances 0.000 claims description 10
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 10
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 10
- 239000000853 adhesive Substances 0.000 claims description 10
- 230000001070 adhesive effect Effects 0.000 claims description 10
- 238000007598 dipping method Methods 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 10
- 229920001223 polyethylene glycol Polymers 0.000 claims description 10
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 claims description 10
- 238000005096 rolling process Methods 0.000 claims description 10
- 238000007493 shaping process Methods 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 230000004048 modification Effects 0.000 claims description 7
- 238000012986 modification Methods 0.000 claims description 7
- XKCJSHHFLBYYOA-UHFFFAOYSA-N 3-[butyl(3-hydroxypropyl)phosphoryl]propan-1-ol Chemical compound CCCCP(=O)(CCCO)CCCO XKCJSHHFLBYYOA-UHFFFAOYSA-N 0.000 claims description 5
- AMUTYVGRCVFCCD-UHFFFAOYSA-N 5,6-diaminopyridine-3-carboxylic acid Chemical compound NC1=CC(C(O)=O)=CN=C1N AMUTYVGRCVFCCD-UHFFFAOYSA-N 0.000 claims description 5
- 239000004114 Ammonium polyphosphate Substances 0.000 claims description 5
- WQSKCGPDUVGMGX-UHFFFAOYSA-N C1(CCCCCCC1)P(CCCO)=O Chemical compound C1(CCCCCCC1)P(CCCO)=O WQSKCGPDUVGMGX-UHFFFAOYSA-N 0.000 claims description 5
- 229920000877 Melamine resin Polymers 0.000 claims description 5
- 235000006679 Mentha X verticillata Nutrition 0.000 claims description 5
- 235000002899 Mentha suaveolens Nutrition 0.000 claims description 5
- 235000001636 Mentha x rotundifolia Nutrition 0.000 claims description 5
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 5
- 235000019826 ammonium polyphosphate Nutrition 0.000 claims description 5
- 229920001276 ammonium polyphosphate Polymers 0.000 claims description 5
- 229960002442 glucosamine Drugs 0.000 claims description 5
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 claims description 5
- 239000005543 nano-size silicon particle Substances 0.000 claims description 5
- 235000012239 silicon dioxide Nutrition 0.000 claims description 5
- 238000002791 soaking Methods 0.000 claims description 5
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 5
- 239000000341 volatile oil Substances 0.000 claims description 5
- 240000002853 Nelumbo nucifera Species 0.000 claims description 2
- 235000006508 Nelumbo nucifera Nutrition 0.000 claims description 2
- 235000006510 Nelumbo pentapetala Nutrition 0.000 claims description 2
- 239000003921 oil Substances 0.000 claims description 2
- 230000008569 process Effects 0.000 abstract description 2
- 241001330002 Bambuseae Species 0.000 description 6
- 238000002485 combustion reaction Methods 0.000 description 3
- 229940119170 jojoba wax Drugs 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/18—Synthetic fibres consisting of macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/26—Polymers or copolymers of unsaturated carboxylic acids or derivatives thereof
- D06M2101/28—Acrylonitrile; Methacrylonitrile
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
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- D—TEXTILES; PAPER
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- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/30—Flame or heat resistance, fire retardancy properties
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Abstract
The invention provides a flame-retardant anti-dripping multifunctional knitted fabric which comprises a flame-retardant layer, a knitted layer and a cotton cloth layer; the flame-retardant layer is formed by interweaving first warp yarns and first weft yarns, the first warp yarns are modacrylic fiber yarns, and the first weft yarns are yarns formed by blending modacrylic fibers and flame-retardant anti-molten-drop polyester fibers; the knitting layer is formed by knitting a second yarn I and a second yarn II through a weft knitting machine, the second yarn I is made of long-staple cotton fibers, and the second yarn II is made of polyester fibers and long-staple cotton fibers through blending; the cotton cloth layer is formed by weaving third warp yarns and third weft yarns, the third warp yarns are bamboo charcoal fiber yarns, and the third weft yarns are formed by interweaving fine denier polyester fibers and pima cotton blended yarns. The preparation method of the flame-retardant anti-dripping multifunctional knitted fabric provided by the invention is simple in process, low in cost and wide in application prospect.
Description
Technical Field
The invention relates to the technical field of knitted fabric preparation, in particular to a flame-retardant anti-dripping multifunctional knitted fabric and a preparation method thereof.
Background
With social progress and development of times, the danger of fire is increased, and the hazard of fire is increased. Along with the improvement of living standard and the enhancement of people oriented security consciousness, the fire-proof anti-dripping knitwear and the flame retardant property are more and more concerned by people.
The existing flame-retardant fireproof fabric has good flame-retardant performance, but poor flexibility, poor wear resistance, poor air permeability and poor sweat absorption.
Disclosure of Invention
The invention aims to provide a flame-retardant anti-dripping multifunctional knitted fabric and a preparation method thereof aiming at the difference of the prior art.
The invention adopts the following technical scheme for solving the technical problems:
the invention provides a flame-retardant anti-dripping multifunctional knitted fabric, which comprises a flame-retardant layer, a knitted layer and a cotton cloth layer; the flame-retardant layer is formed by interweaving first warp yarns and first weft yarns, the first warp yarns are modacrylic fiber yarns, and the first weft yarns are yarns formed by blending modacrylic fibers and flame-retardant anti-molten-drop polyester fibers; the knitting layer is formed by knitting a second yarn I and a second yarn II through a weft knitting machine, the second yarn I is made of long-staple cotton fibers, and the second yarn II is made of polyester fibers and long-staple cotton fibers through blending; the cotton cloth layer is formed by weaving third warp yarns and third weft yarns, the third warp yarns are bamboo charcoal fiber yarns, and the third weft yarns are formed by interweaving fine denier polyester fibers and pima cotton blended yarns.
Furthermore, tough composite fibers are filled between the flame-retardant layer and the knitted layer.
Furthermore, heat-resistant composite fibers are filled between the knitting layer and the cotton cloth layer.
Furthermore, the lower surface of the cotton cloth layer is covered with a layer of flame-retardant film.
The invention provides a preparation method of a flame-retardant anti-molten drop multifunctional knitted fabric, which comprises the following steps:
step one, blending modacrylic fiber and flame-retardant anti-molten-drop polyester fiber to prepare first weft yarn, and then interweaving the first weft yarn and a first warp yarn modacrylic fiber yarn to obtain a flame-retardant base layer;
step two, sequentially adding 6-10 parts of melamine, 3-6 parts of triethanolamine, 15-25 parts of nano silicon dioxide and 15-25 parts of polyethylene glycol into 350 parts of water, heating and uniformly stirring, and then adjusting the pH value to 5-6 by using 12-16 parts of citric acid to obtain a modified solution I;
step three, placing the flame-retardant base layer obtained in the step one into the modification liquid I obtained in the step two for second soaking and second rolling, wherein the rolling residual rate is 70-80%, drying, shaping and cooling to obtain the flame-retardant layer;
step four, sequentially adding 5-6.8 parts of beta-1, 4-poly-glucosamine, 2.4-7.2 parts of isooctyl palmitate, 0.4-1.7 parts of lotus oil, 0.3-0.6 part of mint essential oil, 4-12 parts of citric acid, 20-30 parts of polyethylene glycol and 4-10 parts of sodium carbonate into 185 parts of water, heating and uniformly stirring, and naturally cooling to obtain a modified solution II;
step five, blending the polyester fiber and the long stapled cotton fiber into a second yarn II, and then weaving the second yarn II with the long stapled cotton fiber of the first yarn I by using a weft knitting machine to obtain a knitting base layer; meanwhile, the fine denier polyester fiber and the pima cotton are blended to form a third weft yarn, and the third weft yarn and the third warp yarn bamboo charcoal fiber yarn are interwoven to obtain a cotton cloth base layer;
step six, simultaneously dipping the knitted base layer and the cotton cloth base layer obtained in the step five into the modified liquid II obtained in the step four, heating to 45-50 ℃, continuously dipping for 35-45min, drying, shaping and cooling;
and seventhly, quilting the flame-retardant layer obtained in the third step and the knitted layer together through tough composite fibers, and connecting the quilted layer and the cotton cloth layer together through heat-resistant composite fibers or flame-retardant adhesives to obtain the flame-retardant anti-dripping multifunctional knitted fabric.
Further, in the second step, the heating temperature is 50-60 ℃.
Further, in the third step, the drying temperature is 100-.
Further, in the seventh step, the flame-retardant adhesive is one or more of resorcinol bis-diphenyl phosphate, hydroquinone bis-diphenyl phosphite, n-butyl bis-hydroxypropyl phosphine oxide, cyclooctyl hydroxypropyl phosphine oxide or ammonium polyphosphate.
Further, in the fourth step, the heating temperature is 55-65 ℃.
By adopting the technical scheme, compared with the prior art, the invention has the following technical effects:
the flame-retardant anti-dripping multifunctional knitted fabric prepared by the invention can increase the viscosity of ash after combustion during combustion, thereby preventing dripping during combustion of the fabric. The flame-retardant layer adopts the modacrylic fiber and the flame-retardant anti-molten-drop polyester fiber as raw materials, so that the flame-retardant performance of the flame-retardant layer is improved, and the strength of the fabric is improved by the filled tough composite fiber; the heat-resistant composite fiber filled between the knitting layer and the cotton cloth layer increases the heat resistance of the knitting layer.
The preparation method of the flame-retardant anti-dripping multifunctional knitted fabric provided by the invention is simple in process, low in cost and wide in application prospect.
Detailed Description
The present invention is further illustrated by the following specific examples, which are not to be construed as limiting the invention thereto. It should be noted that the embodiments and features of the embodiments may be combined with each other without conflict.
Example 1
The first aspect of the present embodiment provides a flame-retardant anti-dripping multifunctional knitted fabric, which includes a flame-retardant layer, a knitted layer, and a cotton layer; the flame-retardant layer is formed by interweaving first warp yarns and first weft yarns, the first warp yarns are modacrylic fiber yarns, and the first weft yarns are yarns formed by blending modacrylic fibers and flame-retardant anti-molten-drop polyester fibers; the knitting layer is formed by knitting a second yarn I and a second yarn II through a weft knitting machine, the second yarn I is made of long-staple cotton fibers, and the second yarn II is made of polyester fibers and long-staple cotton fibers through blending; the cotton cloth layer is formed by weaving third warp yarns and third weft yarns, the third warp yarns are bamboo charcoal fiber yarns, and the third weft yarns are formed by interweaving fine denier polyester fibers and pima cotton blended yarns.
As a preferable example, tough composite fibers are filled between the flame-retardant layer and the knitting layer.
As a preferable example, heat-resistant composite fibers are filled between the knitted layer and the cotton cloth layer.
As a preferable example, the lower surface of the cotton cloth layer is covered with a layer of flame-retardant film.
The second aspect of the present embodiment provides a method for preparing a flame-retardant anti-dripping multifunctional knitted fabric, including the following steps:
step one, blending modacrylic fiber and flame-retardant anti-molten-drop polyester fiber to prepare first weft yarn, and then interweaving the first weft yarn and a first warp yarn modacrylic fiber yarn to obtain a flame-retardant base layer;
step two, sequentially adding 6 parts of melamine, 3 parts of triethanolamine, 15 parts of nano silicon dioxide and 15 parts of polyethylene glycol into 250 parts of water, heating and uniformly stirring, and then adjusting the pH value to 5.5 by using 12 parts of citric acid to obtain a modified solution I;
step three, placing the flame-retardant base layer obtained in the step one in the modification liquid I obtained in the step two for second soaking and second rolling, wherein the rolling residual rate is 70%, drying, shaping and cooling to obtain the flame-retardant layer;
step four, sequentially adding 5 parts of beta-1, 4-poly-glucosamine, 2.4 parts of isooctyl palmitate, 0.4 part of jojoba oil, 0.3 part of mint essential oil, 4 parts of citric acid, 20 parts of polyethylene glycol and 4 parts of sodium carbonate into 185 parts of water, heating and uniformly stirring, and naturally cooling to obtain a modified solution II;
step five, blending the polyester fiber and the long stapled cotton fiber into a second yarn II, and then weaving the second yarn II with the long stapled cotton fiber of the second yarn I by using a weft knitting machine to obtain a knitting base layer; meanwhile, fine denier polyester fiber and pima cotton are blended and woven to form third weft yarn, and then the third weft yarn and the third warp yarn bamboo charcoal fiber are mutually woven to obtain a cotton cloth base layer;
step six, simultaneously dipping the knitted base layer and the cotton cloth base layer obtained in the step five into the modified liquid II obtained in the step four, heating to 45 ℃, continuously dipping for 45min, drying, shaping and cooling;
seventhly, quilting the flame-retardant layer obtained in the third step and the knitted layer together through tough composite fibers, and connecting the quilting layer and the cotton cloth layer together through heat-resistant composite fibers or flame-retardant adhesive to obtain the flame-retardant anti-dripping multifunctional knitted fabric
As a preferable example, in the second step, the heating temperature is 50 ℃.
As a preferred example, in the third step, the drying temperature is 100 ℃, and the setting temperature is 170 ℃.
As a preferable example, in the fourth step, the heating temperature is 55 ℃.
As a preferred example, in step seven, the flame-retardant adhesive is one or more of resorcinol bis-diphenyl phosphate, hydroquinone bis-diphenyl phosphite, n-butyl bis-hydroxypropyl phosphine oxide, cyclooctyl hydroxypropyl phosphine oxide or ammonium polyphosphate.
Example 2
The embodiment provides a preparation method of a flame-retardant anti-dripping multifunctional knitted fabric, which comprises the following steps:
step one, blending and weaving modacrylic fibers and flame-retardant anti-molten-drop polyester fibers to form first weft yarns, and then mutually weaving the first weft yarns and the first warp yarns to obtain a flame-retardant base layer;
step two, sequentially adding 8 parts of melamine, 5 parts of triethanolamine, 20 parts of nano silicon dioxide and 20 parts of polyethylene glycol into 300 parts of water, heating and uniformly stirring, and adjusting the pH value to 5.3 by using 14 parts of citric acid to obtain a modified solution I;
step three, placing the flame-retardant base layer obtained in the step one in the modification liquid I obtained in the step two for second soaking and second rolling, wherein the rolling residual rate is 75%, drying, shaping and cooling to obtain the flame-retardant layer;
step four, sequentially adding 5.4 parts of beta-1, 4-poly-glucosamine, 4.8 parts of isooctyl palmitate, 1.1 parts of jojoba oil, 0.45 part of mint essential oil, 8 parts of citric acid, 25 parts of polyethylene glycol and 7 parts of sodium carbonate into 190 parts of water, heating to 60 ℃, uniformly stirring, and naturally cooling to obtain a modified solution II;
step five, blending and weaving the polyester yarns and the long stapled cotton fibers into second yarns II, and weaving the second yarns II and the second yarns I with the long stapled cotton fibers by a weft knitting machine to obtain a knitting base layer; meanwhile, fine denier polyester fiber and pima cotton are blended and woven to form third weft yarn, and then the third weft yarn and the third warp yarn bamboo charcoal fiber are mutually woven to obtain a cotton cloth base layer;
step six, simultaneously dipping the knitted base layer and the cotton cloth base layer obtained in the step five into the modified liquid II obtained in the step four, heating to 47 ℃, continuously dipping for 40min, drying, shaping and cooling;
and seventhly, quilting the flame-retardant layer obtained in the third step and the knitted layer together through tough composite fibers, and connecting the quilted layer and the cotton cloth layer together through heat-resistant composite fibers or flame-retardant adhesives to obtain the flame-retardant anti-dripping multifunctional knitted fabric.
As a preferable example, in the second step, the heating temperature is 55 ℃.
As a preferred example, in the third step, the drying temperature is 110 ℃ and the setting temperature is 150 ℃.
As a preferable example, in the fourth step, the heating temperature is 60 ℃.
As a preferred example, in step seven, the flame-retardant adhesive is one or more of resorcinol bis-diphenyl phosphate, hydroquinone bis-diphenyl phosphite, n-butyl bis-hydroxypropyl phosphine oxide, cyclooctyl hydroxypropyl phosphine oxide or ammonium polyphosphate.
Example 3
The embodiment provides a preparation method of a flame-retardant anti-dripping multifunctional knitted fabric, which comprises the following steps:
step one, blending and weaving modacrylic fibers and flame-retardant anti-molten-drop polyester fibers to form first weft yarns, and then mutually weaving the first weft yarns and the first warp yarns to obtain a flame-retardant base layer;
step two, sequentially adding 10 parts of melamine, 6 parts of triethanolamine, 25 parts of nano silicon dioxide and 25 parts of polyethylene glycol into 350 parts of water, heating and uniformly stirring, and adjusting the pH value to 5 by using 16 parts of citric acid to obtain a modified solution I;
step three, placing the flame-retardant base layer obtained in the step one in the modification liquid I obtained in the step two for second soaking and second rolling, wherein the rolling residual rate is 80%, drying, shaping and cooling to obtain the flame-retardant layer;
step four, sequentially adding 6.8 parts of beta-1, 4-poly-glucosamine, 7.2 parts of isooctyl palmitate, 1.7 parts of jojoba oil, 0.6 part of mint essential oil, 12 parts of citric acid, 30 parts of polyethylene glycol and 10 parts of sodium carbonate into 195 parts of water, heating to 65 ℃, uniformly stirring, and naturally cooling to obtain a modified solution II;
and step five, blending and weaving the polyester yarns and the long stapled cotton fibers into second yarns II, and then weaving the second yarns II with the long stapled cotton fibers of the second yarns I. Knitting by a weft knitting machine to obtain a knitting base layer; meanwhile, fine denier polyester fiber and pima cotton are blended and woven to form third weft yarn, and then the third weft yarn and the third warp yarn bamboo charcoal fiber are mutually woven to obtain a cotton cloth base layer;
step six, simultaneously dipping the knitted base layer and the cotton cloth base layer obtained in the step five into the modified liquid II obtained in the step four, heating to 50 ℃, continuously dipping for 35min, drying, shaping and cooling;
and seventhly, quilting the flame-retardant layer obtained in the third step and the knitted layer together through tough composite fibers, and connecting the quilted layer and the cotton cloth layer together through heat-resistant composite fibers or flame-retardant adhesives to obtain the flame-retardant anti-dripping multifunctional knitted fabric.
As a preferable example, in the second step, the heating temperature is 60 ℃.
As a preferred example, in the third step, the drying temperature is 120 ℃ and the setting temperature is 175 ℃.
As a preferable example, in the fourth step, the heating temperature is 65 ℃.
As a preferred example, in step seven, the flame-retardant adhesive is one or more of resorcinol bis-diphenyl phosphate, hydroquinone bis-diphenyl phosphite, n-butyl bis-hydroxypropyl phosphine oxide, cyclooctyl hydroxypropyl phosphine oxide or ammonium polyphosphate.
The embodiments of the present invention have been described in detail, but the embodiments are merely examples, and the present invention is not limited to the embodiments described above. Any equivalent modifications or alterations to this practice will occur to those skilled in the art and are intended to be within the scope of this invention. Accordingly, equivalent changes and modifications made without departing from the spirit and scope of the present invention should be covered by the present invention.
Claims (9)
1. The flame-retardant anti-dripping multifunctional knitted fabric is characterized by comprising a flame-retardant layer, a knitted layer and a cotton cloth layer; the flame-retardant layer is formed by interweaving first warp yarns and first weft yarns, the first warp yarns are modacrylic fiber yarns, and the first weft yarns are yarns formed by blending modacrylic fibers and flame-retardant anti-molten-drop polyester fibers; the knitted layer is formed by knitting a second yarn I and a second yarn II through a warp and weft knitting machine, the second yarn I is long-staple cotton fiber, and the second yarn II is polyester fiber and long-staple cotton fiber in a blending mode; the cotton cloth layer is formed by weaving third warp yarns and third weft yarns, the third warp yarns are bamboo charcoal fiber yarns, and the third weft yarns are formed by interweaving fine denier polyester fibers and pima cotton blended yarns.
2. The flame-retardant anti-dripping multifunctional knitted fabric according to claim 1, wherein tough composite fibers are filled between the flame-retardant layer and the knitted layer.
3. The flame-retardant anti-dripping multifunctional knitted fabric according to claim 1, wherein heat-resistant composite fibers are filled between the knitted layer and the cotton cloth layer.
4. The flame-retardant anti-dripping multifunctional knitted fabric according to claim 1, wherein the lower surface of the cotton cloth layer is further covered with a flame-retardant film.
5. The method for preparing a flame-retardant anti-dripping multifunctional knitted fabric according to any one of claims 1 to 4, comprising the steps of:
step one, blending modacrylic fiber and flame-retardant anti-molten-drop polyester fiber to prepare first weft yarn, and then interweaving the first weft yarn and a first warp yarn modacrylic fiber yarn to obtain a flame-retardant base layer;
step two, sequentially adding 6-10 parts of melamine, 3-6 parts of triethanolamine, 15-25 parts of nano silicon dioxide and 15-25 parts of polyethylene glycol into 350 parts of water, heating and uniformly stirring, and then adjusting the pH value to 5-6 by using 12-16 parts of citric acid to obtain a modified solution I;
step three, placing the flame-retardant base layer obtained in the step one into the modification liquid I obtained in the step two for second soaking and second rolling, wherein the rolling residual rate is 70-80%, drying, shaping and cooling to obtain the flame-retardant layer;
step four, sequentially adding 5-6.8 parts of beta-1, 4-poly-glucosamine, 2.4-7.2 parts of isooctyl palmitate, 0.4-1.7 parts of lotus oil, 0.3-0.6 part of mint essential oil, 4-12 parts of citric acid, 20-30 parts of polyethylene glycol and 4-10 parts of sodium carbonate into 185 parts of water, heating and uniformly stirring, and naturally cooling to obtain a modified solution II;
step five, blending the polyester fiber and the long stapled cotton fiber into a second yarn II, and then weaving the second yarn II with the long stapled cotton fiber of the second yarn I by using a weft knitting machine to obtain a knitting base layer; meanwhile, the fine denier polyester fiber and the pima cotton are blended to form a third weft yarn, and the third weft yarn and the third warp yarn bamboo charcoal fiber yarn are interwoven to obtain a cotton cloth base layer;
step six, simultaneously dipping the knitted base layer and the cotton cloth base layer obtained in the step five into the modified liquid II obtained in the step four, heating to 45-50 ℃, continuously dipping for 35-45min, drying, shaping and cooling;
and seventhly, quilting the flame-retardant layer obtained in the third step and the knitted layer together through tough composite fibers, and connecting the quilted layer and the cotton cloth layer together through heat-resistant composite fibers or flame-retardant adhesives to obtain the flame-retardant anti-dripping multifunctional knitted fabric.
6. The preparation method of the flame-retardant anti-dripping multifunctional knitted fabric according to claim 5, wherein in the second step, the heating temperature is 50-60 ℃.
7. The method for preparing the flame-retardant and anti-dripping multifunctional knitted fabric according to claim 5, wherein in the third step, the drying temperature is 100-120 ℃, and the setting temperature is 125-175 ℃.
8. The preparation method of the flame-retardant anti-dripping multifunctional knitted fabric according to claim 5, wherein in the fourth step, the heating temperature is 55-65 ℃.
9. The method for preparing the flame-retardant anti-dripping multifunctional knitted fabric according to claim 5, wherein in the seventh step, the flame-retardant adhesive is one or more of resorcinol bis-diphenyl phosphate, hydroquinone bis-diphenyl phosphite, n-butyl bis-hydroxypropyl phosphine oxide, cyclooctyl hydroxypropyl phosphine oxide or ammonium polyphosphate.
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CN101580979A (en) * | 2008-05-16 | 2009-11-18 | 中国纺织科学研究院 | Fire-retardant anti-molten droplet fiber, method for preparing same and application thereof |
CN201738090U (en) * | 2010-07-14 | 2011-02-09 | 山东泰丰纺织有限公司 | Bamboo charcoal fiber, pima cotton and fine denier tencel jacquard fabric |
CN105172247A (en) * | 2015-09-08 | 2015-12-23 | 泉州迈特富纺织科技有限公司 | Fireproof flame retardant anti-bacterial fabric as well as preparation method and application thereof |
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CN101580979A (en) * | 2008-05-16 | 2009-11-18 | 中国纺织科学研究院 | Fire-retardant anti-molten droplet fiber, method for preparing same and application thereof |
CN201738090U (en) * | 2010-07-14 | 2011-02-09 | 山东泰丰纺织有限公司 | Bamboo charcoal fiber, pima cotton and fine denier tencel jacquard fabric |
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