CN114396817A - Liquid metal heat pipe packaging device and method - Google Patents
Liquid metal heat pipe packaging device and method Download PDFInfo
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- CN114396817A CN114396817A CN202210015055.4A CN202210015055A CN114396817A CN 114396817 A CN114396817 A CN 114396817A CN 202210015055 A CN202210015055 A CN 202210015055A CN 114396817 A CN114396817 A CN 114396817A
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- liquid metal
- heat pipe
- vacuum
- valve
- storage tank
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F28—HEAT EXCHANGE IN GENERAL
- F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
- F28D15/00—Heat-exchange apparatus with the intermediate heat-transfer medium in closed tubes passing into or through the conduit walls ; Heat-exchange apparatus employing intermediate heat-transfer medium or bodies
- F28D15/02—Heat-exchange apparatus with the intermediate heat-transfer medium in closed tubes passing into or through the conduit walls ; Heat-exchange apparatus employing intermediate heat-transfer medium or bodies in which the medium condenses and evaporates, e.g. heat pipes
- F28D15/0283—Means for filling or sealing heat pipes
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F04—POSITIVE - DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS FOR LIQUIDS OR ELASTIC FLUIDS
- F04B—POSITIVE-DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS
- F04B37/00—Pumps having pertinent characteristics not provided for in, or of interest apart from, groups F04B25/00 - F04B35/00
- F04B37/10—Pumps having pertinent characteristics not provided for in, or of interest apart from, groups F04B25/00 - F04B35/00 for special use
- F04B37/14—Pumps having pertinent characteristics not provided for in, or of interest apart from, groups F04B25/00 - F04B35/00 for special use to obtain high vacuum
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F04—POSITIVE - DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS FOR LIQUIDS OR ELASTIC FLUIDS
- F04B—POSITIVE-DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS
- F04B41/00—Pumping installations or systems specially adapted for elastic fluids
- F04B41/06—Combinations of two or more pumps
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- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Sustainable Development (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Vacuum Packaging (AREA)
Abstract
The invention discloses a liquid metal heat pipe packaging device and a method. The vacuum operation box provides a vacuum environment for filling the heat pipe; the inert gas storage tank provides inert gas; the vacuum pump unit exhausts the gas in the vacuum operation box and vacuumizes the heat pipe; the liquid metal storage tank stores liquid metal working media; the quality of the liquid metal working medium is measured and filled by the electromagnetic flowmeter; and a water oxygen detector, a helium mass spectrometer leak detector and a vacuum gauge are used for detecting the water oxygen content, the leakage rate and the vacuum degree in the filling process. The device has the advantages of simple structure, simple and convenient operation, controllable filling quality of the liquid metal and high filling vacuum degree of the heat pipe.
Description
Technical Field
The invention relates to the technical field of phase change heat exchange equipment, in particular to a high-temperature heat pipe working medium filling device and method.
Background
The high-temperature heat pipe usually adopts liquid metal as a working medium, and the liquid metal heat pipe can be applied to the fields of nuclear reactor systems, aerospace, ferrous metallurgy and the like due to the fact that the melting point and the boiling point of the liquid metal are high. Because the liquid metal is active in nature and is very easy to react with air, the generated oxide can block pores of the liquid absorption core and influence the working performance of the heat pipe. Meanwhile, because the working vapor pressure of the liquid metal is lower, the existence of non-condensable gas can greatly influence the isothermal performance and the heat transfer capacity of the heat pipe. The design provides a high-temperature heat pipe working medium filling device aiming at the high-temperature heat pipe filling process, and provides reference for high-quality filling of the high-temperature heat pipe.
Disclosure of Invention
The invention provides a liquid metal heat pipe packaging device and a liquid metal heat pipe packaging method for realizing high-quality packaging of a liquid metal heat pipe.
In order to achieve the purpose, the invention adopts the following technical scheme:
a high-temperature heat pipe working medium filling device and a method thereof comprise a vacuum operation box 100, an inert gas storage tank 200, a vacuum pump unit 300, a liquid metal storage tank 400, a connecting joint 500, a heat pipe 600, a gas inlet valve 201, a water oxygen detector 301, a helium mass spectrometer leak detector 302, a first valve 310, a second valve 320, a neck expanding cavity 311, a vacuum gauge 312, a sealing valve 313, an electromagnetic flowmeter 401 and a packaging valve 402; the inert gas storage tank 200 is connected to the bottom of the vacuum operation box 100 through a gas inlet valve 201, the outlet of the vacuum pump unit 300 is connected with a water oxygen detector 301 and a helium mass spectrometer leak detector 302, the inlet pipeline of the vacuum pump unit 300 penetrates through the upper side wall of the vacuum operation box 100 and then is divided into two paths, one path is communicated with the inside of the vacuum operation box 100 through a second valve 320, the other path is sequentially connected with a first valve 310, a neck expanding cavity 311 and a sealing valve 313 and then penetrates out of the bottom of the vacuum operation box 100 to be connected with the upper port of a connector 500, and a vacuum gauge 312 is arranged on the neck expanding cavity 311; the liquid metal storage tank 400 passes through the electromagnetic flow meter 401 and the packaging valve 402 and penetrates out of the bottom of the vacuum operation box 100 to be connected with the upper port of the connecting joint 500, and the lower port of the connecting joint 500 is connected with the heat pipe 600.
The gas stored in the inert gas storage tank 200 is nitrogen, helium, neon, argon or xenon.
The vacuum pump unit 300 is a multi-stage unit, and comprises one or more of ion pump, molecular pump, diffusion pump, jet pump, roots pump, rotary vane pump and piston pump, and the vacuum degree is 105~10-8Of the order of Pa.
The vacuum gauge 312 is a composite vacuum gauge, which is at least two of Pirani vacuum gauge, resistance vacuum gauge, thermocouple vacuum gauge, thermal radiation vacuum gauge, hot cathode ionization vacuum gauge, cold cathode ionization vacuum gauge, and viscous vacuum gauge, and the vacuum degree measurement cover 105~10-8Of the order of Pa.
The liquid metal in the liquid metal storage tank 400 is lithium, sodium, potassium, rubidium, cesium or mercury, and the temperature maintained in the liquid metal storage tank 400 causes the metal to be in a liquid state.
The sealing valve 313 and the packaging valve 402 are liquid metal valves, and the working temperature is 50 ℃ above the melting point of the liquid metal.
The connection joint 500 is a vacuum joint, a high vacuum flange, a threaded joint or a movable joint is selected, and a gasket used by the connection joint 500 is a graphite gasket, an epoxy copper gasket or a steel skeleton graphite gasket.
The baking temperature before filling the heat pipe 600 is 250 +/-50 ℃, and the filling vacuum degree of the heat pipe 600 is 10-4Pa, water oxygen content less than 10-10std cc/s, leak rate less than 10-9std cc/s。
Compared with the prior art, the invention has the following advantages:
the vacuum pump unit 300 is adopted to only vacuumize the inner cavity of the heat pipe 600, so that the problem of more global vacuumizing leakage points is avoided, the volume of the inner cavity of the heat pipe 600 is small, and higher vacuum degree can be realized; the quantitative filling method for the liquid metal storage tank 400 and the mutual checking method for the electromagnetic flowmeter 401 are adopted, so that the quantitative accuracy of the filling quality of the heat pipe 600 is ensured; working medium filling is completed in the vacuum operation box 100, so that the purity of the liquid metal working medium is ensured; the inert gas storage tank 200 is used for replacing air to avoid the oxidation of the working medium.
Drawings
FIG. 1 is a schematic diagram of a high-temperature heat pipe working medium filling device
Detailed Description
The invention will now be further described with reference to the following examples, and the accompanying drawings:
as shown in fig. 1, the liquid metal heat pipe packaging apparatus of the present invention includes a vacuum operation box 100, an inert gas storage tank 200, a vacuum pump unit 300, a liquid metal storage tank 400, a connection joint 500, a heat pipe 600, a gas inlet valve 201, a water oxygen detector 301, a helium mass spectrometer leak detector 302, a first valve 310, a second valve 320, a neck cavity 311, a vacuum gauge 312, a sealing valve 313, an electromagnetic flow meter 401, and a filling valve 402. The inert gas storage tank 200 is connected to the bottom of the vacuum operation box 100 through a gas inlet valve 201, the outlet of the vacuum pump unit 300 is connected with a water oxygen detector 301 and a helium mass spectrometer leak detector 302, the inlet pipeline of the vacuum pump unit 300 penetrates through the upper side wall of the vacuum operation box 100 and then is divided into two paths, one path is communicated with the inside of the vacuum operation box 100 through a second valve 320, the other path is sequentially connected with a first valve 310, a neck expanding cavity 311 and a sealing valve 313 and then penetrates out of the bottom of the vacuum operation box 100 to be connected with the upper port of a connector 500, and a vacuum gauge 312 is arranged on the neck expanding cavity 311; the liquid metal storage tank 400 passes through the electromagnetic flow meter 401 and the filling valve 402 and penetrates out of the bottom of the vacuum operation box 100 to be connected with the upper port of the connecting joint 500, and the lower port of the connecting joint 500 is connected with the heat pipe 600.
In a preferred embodiment of the present invention, the storage gas in the inert gas storage tank 200 is nitrogen, helium, neon, argon, or xenon.
As a preferred embodiment of the present invention, the aboveThe air pump unit 300 is a multi-stage unit, and comprises one or more of ion pump, molecular pump, diffusion pump, jet pump, Roots pump, rotary vane pump, and piston pump, and the vacuum degree is 105~10-8Pa magnitude; adopts multi-stage units to realize the atmospheric pressure of 10-8The Pa-order vacuum degree avoids the problem that the pumping range of a single vacuum pump is limited.
In a preferred embodiment of the present invention, the vacuum gauge 312 is a composite vacuum gauge, the composite vacuum gauge is at least two of a pirani vacuum gauge, a resistance vacuum gauge, a thermocouple vacuum gauge, a thermal radiation vacuum gauge, a hot cathode ionization vacuum gauge, a cold cathode ionization vacuum gauge, and a viscous vacuum gauge, and the vacuum degree measurement cover 10 is provided5~10-8Of the order of Pa. By adopting the composite vacuum gauge, the pressure from atmospheric pressure to 10 can be realized-8The measurement of Pa magnitude vacuum degree avoids the defects of measurement range limitation and insufficient precision of a single vacuum gauge. In a preferred embodiment of the present invention, the liquid metal in the liquid metal storage tank 400 is lithium, sodium, potassium, rubidium, cesium or mercury, and the temperature maintained in the liquid metal storage tank 400 is such that the metal is in a liquid state, for example, when the liquid metal is lithium, the temperature maintained in the liquid metal storage tank 400 is 200 to 300 ℃; if the liquid metal is sodium or potassium, the temperature in the liquid metal storage tank 400 is maintained at 150-250 ℃; if the liquid metal is rubidium or cesium, the temperature in the liquid metal storage tank 400 is maintained at 50-100 ℃; if the liquid metal is mercury, the temperature of the liquid metal storage tank 400 is maintained at 20-50 ℃.
In a preferred embodiment of the present invention, the sealing valve 313 and the filling valve 402 are liquid metal valves, and the working temperature is 50 ℃ above the melting point of the liquid metal. The liquid metal valve is adopted, the defect that rubber substances in the traditional valve react with liquid metal is overcome, and the purity of the liquid metal and the reliability of the device are improved.
As a preferred embodiment of the present invention, the connection joint 500 is a vacuum joint, and is a high vacuum flange, a threaded joint, or a loose joint, and the gasket used by the connection joint 500 is a graphite gasket, an epoxy copper gasket, or a steel skeleton graphite gasket, so that the disadvantage of the occurrence of the rubber sealing ring and the liquid metal can be avoided, and reliable sealing connection can be achieved.
As a preferred embodiment of the invention, the baking temperature of the heat pipe 600 before filling is 250 ℃ +/-50 ℃, and water vapor in the cavity of the heat pipe 600 is removed by baking, so that the oxidation of the liquid metal working medium is reduced. The filling vacuum degree of the heat pipe 600 is 10-4Pa, water oxygen content less than 10-10std cc/s, leak rate less than 10-9std cc/s, provides higher vacuum for the cavity of the heat pipe 600, and ensures the packaging quality of the heat pipe 600.
The working principle of the invention is as follows: opening the gas inlet valve 201 and the second valve 320, starting the vacuum pump unit 300 and the water oxygen detector 301, performing water removal and oxygen removal operation on the interior of the vacuum operation box 100, and displaying that the water oxygen content is less than 10 by the water oxygen detector 301-10std cc/s, the gas inlet valve 201 and the second valve 320 are closed, and a fixed amount of liquid metal working medium is charged into the liquid metal storage tank 400 through the vacuum operation box 100 and is kept at a temperature 50 ℃ above the melting point of the liquid metal working medium. After the heat pipe 600 is connected with the connecting joint 500, baking is carried out at 250 +/-50 ℃, the first valve 310 and the sealing valve 313 are opened to only vacuumize the inner cavity of the heat pipe 600, the helium mass spectrometer leak detector 302 is started, and when the water oxygen detector 301 shows that the water oxygen content is less than 10-10std cc/s, helium mass spectrometer leak detector 302 showed leak rates less than 10-9std cc/s, the first valve 310 and the sealing valve 313 are closed. And opening the packaging valve 402, and closing the packaging valve 402 after the reading of the electromagnetic flowmeter 401 is consistent with the mass of the liquid metal working medium. After the heat pipe 600 is cooled to room temperature, the first valve 310 and the sealing valve 313 are opened until the vacuum gauge number is lower than 10-4And after Pa, closing the sealing valve 313, and performing thermal pinch-off on the liquid charging pipe of the heat pipe 600 to complete the packaging of the heat pipe 600.
Claims (10)
1. A liquid metal heat pipe packaging hardware which characterized in that: the device comprises a vacuum operation box (100), an inert gas storage tank (200), a vacuum pump unit (300), a liquid metal storage tank (400), a connecting joint (500), a heat pipe (600), a gas inlet valve (201), a water oxygen detector (301), a helium mass spectrometer leak detector (302), a first valve (310), a second valve (320), a neck expanding cavity (311), a vacuum gauge (312), a sealing valve (313), an electromagnetic flowmeter (401) and a packaging valve (402); the inert gas storage tank (200) is connected to the bottom of the vacuum operation box (100) through a gas inlet valve (201), an outlet of a vacuum pump unit (300) is connected with a water oxygen detector (301) and a helium mass spectrometer leak detector (302), an inlet pipeline of the vacuum pump unit (300) penetrates through the upper side wall of the vacuum operation box (100) and then is divided into two paths, one path is communicated with the inside of the vacuum operation box (100) through a second valve (320), the other path is sequentially connected with a first valve (310), a neck expanding cavity (311) and a sealing valve (313) and then penetrates out of the bottom of the vacuum operation box (100) to be connected with an upper port of a connecting joint (500), and the neck expanding cavity (311) is provided with a vacuum gauge (312); the liquid metal storage tank (400) penetrates out of the bottom of the vacuum operation box (100) through the electromagnetic flowmeter (401) and the packaging valve (402) to be connected with the upper port of the connecting joint (500), and the lower port of the connecting joint (500) is connected with the heat pipe (600).
2. The liquid metal heat pipe packaging apparatus of claim 1, wherein: the gas stored in the inert gas storage tank (200) is nitrogen, helium, neon, argon or xenon.
3. The liquid metal heat pipe packaging apparatus of claim 1, wherein: the vacuum pump unit (300) is a multistage unit, and comprises one or more of ion pump, molecular pump, diffusion pump, jet pump, roots pump, rotary vane pump and piston pump, and the vacuum degree covers 105~10-8Of the order of Pa.
4. The liquid metal heat pipe packaging apparatus of claim 1, wherein: the vacuum gauge (312) is a composite vacuum gauge, the composite vacuum gauge is at least two of a Pirani vacuum gauge, a resistance vacuum gauge, a thermocouple vacuum gauge, a thermal radiation vacuum gauge, a hot cathode ionization vacuum gauge, a cold cathode ionization vacuum gauge and a viscous vacuum gauge, and the vacuum degree measurement cover 105~10- 8Of the order of Pa.
5. The liquid metal heat pipe packaging apparatus of claim 1, wherein: the liquid metal in the liquid metal storage tank (400) is lithium, sodium, potassium, rubidium, cesium or mercury, and the temperature maintained in the liquid metal storage tank (400) is such that the metal is liquid.
6. The liquid metal heat pipe packaging apparatus of claim 1, wherein: the sealing valve (313) and the packaging valve (402) are liquid metal valves, and the working temperature is 50 ℃ above the melting point of the liquid metal.
7. The liquid metal heat pipe packaging apparatus of claim 1, wherein: the connecting joint (500) is a vacuum joint, a high vacuum flange, a threaded joint or a movable joint is selected, and a gasket used by the connecting joint (500) is a graphite gasket, an epoxy copper gasket or a steel skeleton graphite gasket.
8. The liquid metal heat pipe packaging apparatus of claim 1, wherein: the baking temperature before filling the heat pipe (600) is 250 +/-50 ℃, and the filling vacuum degree of the heat pipe (600) is 10-4Pa, water oxygen content less than 10-10std cc/s, leak rate less than 10-9std cc/s。
9. The liquid metal heat pipe packaging apparatus of claim 1, wherein: the inner diameter of the heat pipe (600) is less than or equal to 50mm, and the length of the heat pipe is less than or equal to 2 m.
10. A method of operating a liquid metal heat pipe enclosure as claimed in any one of claims 1 to 9, wherein: opening the gas inlet valve (201) and the second valve (320), starting the vacuum pump set (300) and the water oxygen detector (301), performing water removal and oxygen removal operation on the interior of the vacuum operation box (100), and displaying that the water oxygen content is less than 10 by the water oxygen detector (301)-10After std cc/s, closing the gas inlet valve (201) and the second valve (320), loading a quantitative liquid metal working medium into a liquid metal storage tank (400) through a vacuum operation box (100), and keeping the temperature to be 50 ℃ above the melting point of the liquid metal working medium; after the heat pipe (600) is connected with the connecting joint (500)Baking at 250 +/-50 ℃, opening the first valve (310) and the sealing valve (313) to only vacuumize the inner cavity of the heat pipe (600), starting the helium mass spectrometer leak detector (302), and waiting for the water oxygen detector (301) to display that the water oxygen content is less than 10-10std cc/s, helium mass spectrometer leak detector (302) showed leak rates below 10-9After std cc/s, closing the first valve (310) and the sealing valve (313); opening the packaging valve (402), and closing the packaging valve (402) after the reading of the electromagnetic flowmeter (401) is consistent with the mass of the liquid metal working medium; after the heat pipe (600) is cooled to the room temperature, the first valve (310) and the sealing valve (313) are opened until the vacuum gauge number is lower than 10-4And after Pa, closing the sealing valve (313), and performing thermal pinch-off on the liquid charging pipe of the heat pipe (600) to finish the packaging of the heat pipe (600).
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114719642A (en) * | 2022-05-20 | 2022-07-08 | 西安交通大学 | High-temperature sodium heat pipe filling device and method |
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JPH06323768A (en) * | 1993-05-18 | 1994-11-25 | Hitachi Ltd | Heat pipe |
CN201634406U (en) * | 2009-12-23 | 2010-11-17 | 四川盛阳太阳能应用技术有限公司 | Device for leading working medium to be placed in split type heat pipe solar flat plate collector |
CN102331204A (en) * | 2011-09-07 | 2012-01-25 | 济南大学 | Integrated equipment for preparing water-based nano-fluid and filling heat pipe |
CN103968693A (en) * | 2014-05-21 | 2014-08-06 | 海康创业(北京)科技有限公司 | Active integrated heat pipe injection device and injection method using same |
CN105403086A (en) * | 2015-12-24 | 2016-03-16 | 中国航空工业集团公司北京航空制造工程研究所 | Storage tank and device for filling of alkali-metal heat pipe as well as method for filling heat pipe with alkali metal |
CN106931814A (en) * | 2017-03-09 | 2017-07-07 | 广东工业大学 | A kind of flat-plate type micro heat pipe evacuation priming device and its method |
CN107436106A (en) * | 2017-09-12 | 2017-12-05 | 大连海事大学 | A kind of charging device and method of liquid metal high temperature pulsating heat pipe |
CN108106471A (en) * | 2017-12-15 | 2018-06-01 | 陕西仙童科技有限公司 | A kind of accurate filling system of heat-pipe working medium and filling method |
CN110243212A (en) * | 2019-05-31 | 2019-09-17 | 西安交通大学 | A kind of hot filling circuit system of high-temperature alkali metal heat pipe and method |
CN111486729A (en) * | 2020-04-23 | 2020-08-04 | 西安交通大学 | High-temperature alkali metal heat pipe cold filling system and method |
CN113758321A (en) * | 2021-08-24 | 2021-12-07 | 西安交通大学 | High-temperature heat pipe quantitative liquid filling device and method |
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2022
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JPH06323768A (en) * | 1993-05-18 | 1994-11-25 | Hitachi Ltd | Heat pipe |
CN201634406U (en) * | 2009-12-23 | 2010-11-17 | 四川盛阳太阳能应用技术有限公司 | Device for leading working medium to be placed in split type heat pipe solar flat plate collector |
CN102331204A (en) * | 2011-09-07 | 2012-01-25 | 济南大学 | Integrated equipment for preparing water-based nano-fluid and filling heat pipe |
CN103968693A (en) * | 2014-05-21 | 2014-08-06 | 海康创业(北京)科技有限公司 | Active integrated heat pipe injection device and injection method using same |
CN105403086A (en) * | 2015-12-24 | 2016-03-16 | 中国航空工业集团公司北京航空制造工程研究所 | Storage tank and device for filling of alkali-metal heat pipe as well as method for filling heat pipe with alkali metal |
CN106931814A (en) * | 2017-03-09 | 2017-07-07 | 广东工业大学 | A kind of flat-plate type micro heat pipe evacuation priming device and its method |
CN107436106A (en) * | 2017-09-12 | 2017-12-05 | 大连海事大学 | A kind of charging device and method of liquid metal high temperature pulsating heat pipe |
CN108106471A (en) * | 2017-12-15 | 2018-06-01 | 陕西仙童科技有限公司 | A kind of accurate filling system of heat-pipe working medium and filling method |
CN110243212A (en) * | 2019-05-31 | 2019-09-17 | 西安交通大学 | A kind of hot filling circuit system of high-temperature alkali metal heat pipe and method |
CN111486729A (en) * | 2020-04-23 | 2020-08-04 | 西安交通大学 | High-temperature alkali metal heat pipe cold filling system and method |
CN113758321A (en) * | 2021-08-24 | 2021-12-07 | 西安交通大学 | High-temperature heat pipe quantitative liquid filling device and method |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN114719642A (en) * | 2022-05-20 | 2022-07-08 | 西安交通大学 | High-temperature sodium heat pipe filling device and method |
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