CN114367264B - Reation kettle convenient to sample detects - Google Patents
Reation kettle convenient to sample detects Download PDFInfo
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- CN114367264B CN114367264B CN202210062158.6A CN202210062158A CN114367264B CN 114367264 B CN114367264 B CN 114367264B CN 202210062158 A CN202210062158 A CN 202210062158A CN 114367264 B CN114367264 B CN 114367264B
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- 238000009826 distribution Methods 0.000 claims abstract description 41
- 238000005070 sampling Methods 0.000 claims abstract description 28
- 239000000463 material Substances 0.000 claims description 27
- 238000006243 chemical reaction Methods 0.000 abstract description 28
- 238000005273 aeration Methods 0.000 abstract description 20
- 230000000694 effects Effects 0.000 abstract description 19
- 238000001514 detection method Methods 0.000 abstract description 15
- 238000003756 stirring Methods 0.000 description 12
- 238000010586 diagram Methods 0.000 description 8
- 238000007599 discharging Methods 0.000 description 3
- 238000004880 explosion Methods 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000008602 contraction Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 238000003491 array Methods 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000012824 chemical production Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000001546 nitrifying effect Effects 0.000 description 1
- 230000000379 polymerizing effect Effects 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 230000001960 triggered effect Effects 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/10—Devices for withdrawing samples in the liquid or fluent state
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Analytical Chemistry (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Physics & Mathematics (AREA)
- Hydrology & Water Resources (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
The invention relates to a reaction kettle convenient for sampling and detection, which comprises a kettle body, wherein the inner wall of the top of the kettle body is rotationally connected with a main pipe, the bottom of the main pipe is communicated with an air distribution plate, the bottom of the air distribution plate is communicated with a plurality of air ducts, the top of the kettle body is fixedly provided with a first motor, one side of the top of the kettle body is fixedly penetrated by an exhaust pipe, the inner walls of the two sides of the exhaust pipe are both provided with guide blocks in a sliding manner, a reset spring is fixedly arranged between the guide blocks and the inner wall of the top of the guide block, an exhaust column is fixedly arranged between the two guide blocks, the circumferential outer wall of the exhaust column is provided with a plurality of air distribution holes, the bottom of the exhaust column is provided with a main air hole, the circumferential outer wall of the main pipe is provided with a circular groove, the circumferential outer wall of the circular groove is fixedly provided with a first air hole in a dense manner, the circular groove is sleeved with an air guide sleeve ring, the circumferential inner wall of the air guide sleeve is fixedly penetrated by a connecting pipe; when the invention utilizes the exhaust, part of gas is simultaneously introduced into the gas guide pipe to form an aeration effect, thereby utilizing energy.
Description
Technical Field
The invention relates to the technical field of reaction kettles, in particular to a reaction kettle convenient for sampling and detection.
Background
The reactor is one kind of important chemical equipment and is one pressure container for complete sulfurizing, nitrifying, hydrogenating, hydrocarbylating, polymerizing, condensing and other chemical technological process. The structural design of the reaction kettle is different according to different reaction condition requirements, but the structure of the reaction kettle generally comprises a kettle body, a transmission device, a stirring device, a heating device, a cooling device and a sealing device.
In chemical production, because in the partial chemical reaction process, its reaction efficiency and temperature are directly proportional, consequently, need at the in-process of reaction, heat reation kettle, promote the internal temperature of cauldron, simultaneously because the rising of the internal temperature of cauldron causes atmospheric pressure too big, consequently, still need exhaust the cauldron body, prevent to cause the damage to reation kettle, among the prior art, do not make full use of to the exhaust gas, cause the energy waste, so put forward a reation kettle of being convenient for sampling detection and solve the problem that above-mentioned was proposed.
In order to solve the problems, the invention provides a reaction kettle convenient for sampling and detection.
Disclosure of Invention
The invention aims to solve the problem of energy waste of the existing reaction kettle, adapt to the actual needs, and provide a reaction kettle convenient for sampling and detection so as to solve the technical problems.
In order to achieve the purpose of the invention, the technical scheme adopted by the invention is as follows:
the utility model provides a reation kettle convenient to sample and detect, the reactor comprises a kettle body, cauldron body top inner wall runs through and rotates through the bearing and is connected with the person in charge, be responsible for top closure, bottom opening, be responsible for bottom intercommunication has the gas distribution dish, gas distribution dish bottom intercommunication has a plurality of annular array distribution's air duct, the air duct cross-section sets up to the arc, cauldron body top has first motor through the bolt fastening, pass through bolt fastening between first motor output shaft and the person in charge, cauldron body top one side runs through and is fixed with the blast pipe, the guide slot has all been seted up to blast pipe both sides inner wall, sliding connection has the guide block in the guide slot, have same reset spring through bolt fastening between guide block and the guide slot top inner wall, same exhaust column through bolt fastening between two guide blocks, a plurality of gas distribution holes have been seted up to the exhaust column circumference outer wall, the main gas hole has been seted up to the exhaust column bottom, main gas hole and gas distribution hole intercommunication, annular groove has been seted up to main gas distribution circumference outer wall, annular groove circumference outer wall runs through the first gas hole of seting up the air duct, annular groove department cover has the first gas guide ring, the second gas hole of densely distributed is seted up to the circumference inner wall, the top of the cauldron body runs through and is fixed with the connecting pipe, the top, the mouth of pipe towards bottom one side of connecting pipe and gas guide ring intercommunication.
Preferably, the top pipe orifice of the connecting pipe is in threaded connection with a gas gathering head, and the gas gathering head is arranged in a flaring shape.
Preferably, the top of the kettle body is fixedly penetrated by a feeding pipe, the bottom of the kettle body is fixedly penetrated by a discharging pipe, and valves are arranged on the feeding pipe and the discharging pipe.
Preferably, the fixed ring is fixed to the cover on being responsible for, and the equal welding of fixed ring both sides has the ear piece, and the round pin hub connection has the mounting panel on the ear piece, and movable groove has been seted up to the mounting panel bottom, and the inner wall of movable groove both sides all has a plurality of first springs through the bolt fastening, and the inboard of a plurality of springs of both sides all has same roof through the bolt fastening, and the roof cross-section sets up into the arc, and the intrados of roof has a plurality of evenly distributed's thimble through the bolt fastening, and the thimble runs through the lateral wall of mounting panel, is provided with trigger mechanism in the movable groove.
Preferably, the triggering mechanism comprises a first shaft rod, the first shaft rod is rotationally connected to the top inner wall of the movable groove through a bearing, a plurality of annular array distributed blades are fixed on the circumference outer wall of the first shaft rod through bolts, a plurality of evenly distributed flow gathering cups are fixedly penetrated at one end of the mounting plate, which is close to the first shaft rod, and the flow gathering cups are arranged in a funnel shape.
Preferably, the outer wall of the circumference of the thimble is provided with densely distributed needling heads, and the needling heads and the thimble are of an integrated structure.
Preferably, the main pipe is sleeved with the movable ring, the same connecting rod is connected between the movable ring and the mounting plate through a pin shaft, sliding grooves are formed in two sides of the main pipe, sliding blocks are connected in the sliding grooves in a sliding mode, the same second spring is fixed between the sliding blocks and the inner walls of the sliding grooves through bolts, and the sliding blocks and the movable ring are fixed through bolts.
Preferably, the pipe orifice of the air duct is communicated with a fixed pipe head, the outer side of the fixed pipe head is rotationally connected with a disc through a bearing, the outer side of the disc is communicated with a plurality of air distribution pipes distributed in annular arrays, the air distribution pipes are arranged in a Y shape, the inner side of the disc is fixedly provided with a second shaft rod through a bolt, and the inner side of the second shaft rod is fixedly provided with a blade through a bolt.
Preferably, the movable port is arranged at the top of the kettle body, the toothed bar is arranged in the movable port, the rear end of the toothed bar is provided with the directional groove, the directional block is connected in the directional groove in a sliding way, the directional block and the inner wall of the rear end of the movable port are fixed through bolts, the plunger is fixed at the bottom of the toothed bar through bolts, the sampling cup is fixed at the top of the plunger through bolts, the second motor is fixed at the top of the kettle body through bolts, the output shaft of the second motor is connected with the gear, and the gear is meshed with the toothed bar.
The beneficial effects are that:
1. when the reaction kettle works, the first motor is in a starting state, the output shaft of the first motor drives the main pipe, the gas distribution disc and the gas guide pipe to rotate, materials to be reacted are stirred, meanwhile, the kettle body is heated continuously, the temperature is high, the gas pressure pushes the gas discharge column upwards, the gas discharge column follows the guide block and moves upwards to form extrusion to the reset spring along the guide groove, when the gas distribution holes on the gas discharge column are exposed out of the exhaust pipe, high-temperature gas in the kettle body can enter from the main gas hole and be discharged from the gas distribution holes, and part of gas directly rushes into the connecting pipe due to the fact that the connecting pipe is opposite to the gas discharge column, then enters into the main pipe through the second gas hole and the first gas hole, is discharged from the gas guide pipe, an aeration effect is formed, the stirring degree of the materials is improved, the reaction efficiency is promoted, and energy utilization can be carried out.
2. When the main pipe rotates, the fixed ring, the lug blocks, the mounting plate and the ejector pins are synchronously driven to rotate, the ejector pins are used for conducting transverse scanning, large bubbles formed by aeration are broken, local explosion is formed, and accordingly stirring effect on materials is further promoted, the materials can be concentrated from the flow gathering cup, the materials enter the movable groove, impact is formed on the blades, the blades rotate around the first shaft rod, the rotating blades collide with the top plates, the two top plates respectively move upwards and downwards, the corresponding ejector pins are synchronously driven to move, at the moment, the top plates squeeze the first springs, reset, so that the ejector pins shrink, the large bubbles formed by aeration are further convenient to puncture, the top plate section is set into an arc shape, good stress fit can be conducted on one hand with the blades, on the other hand, the materials in the movable groove can be conveniently extruded, stirring on the two ends is further promoted, meanwhile, the resistance of the materials when the top plates reset is reduced, the shrinkage motion of the ejector pins is faster, the piercing heads of the cloth are arranged, the piercing heads can be improved, the corresponding ejector pins can be further rotated, the elastic connecting rods can be further matched with the first springs, the elastic connecting rods can be fully rotated, and the whole connecting rods can be fully rotated, and the elastic connecting rods can be further rotated, and the whole can be stretched, and the whole connecting rods can be fully rotated, and the vibration can be stretched, and the vibration can be fully move around the first springs, and have the vibration, and the vibration can be completely rotate.
3. When gas enters the fixed tube head from the gas guide tube, the air flow drives the blade to rotate, and then the second shaft rod, the disc and the gas distribution tube are synchronously driven to rotate, so that the gas is ejected in a rotary mode, the aeration effect is improved, and meanwhile, the gas distribution tube is arranged in a Y shape, multidirectional aeration can be formed, and the aeration effect is further improved. When taking a sample, start the second motor, the second motor output shaft drives gear rotation, and gear engagement drives the rack bar and moves down, takes a sample after the sample cup removes to suitable position, starts the reverse rotation of second motor then for the rack bar upwards moves to movable mouth position, accomplishes the sample, and the plunger forms sealedly to movable mouth this moment, convenient operation.
Drawings
FIG. 1 is a schematic diagram of the whole structure of a reaction kettle convenient for sampling and detection;
FIG. 2 is a schematic diagram of the internal structure of a reaction kettle for facilitating sampling and detection according to the present invention;
FIG. 3 is a schematic diagram of a split structure of an air guide sleeve ring of a reaction kettle for facilitating sampling and detection;
FIG. 4 is a schematic diagram of the internal structure of an exhaust pipe of the reaction kettle, which is convenient for sampling and detection;
FIG. 5 is an enlarged schematic view of the structure of the portion A of the reaction kettle which is convenient for sampling and detection;
FIG. 6 is a schematic diagram of the internal structure of a mounting plate of the reaction kettle, which is convenient for sampling and detection;
FIG. 7 is a schematic diagram of a thimble structure of a reaction kettle for facilitating sampling and detection according to the present invention;
FIG. 8 is a schematic diagram of the internal structure of a fixed tube head of the reaction kettle for facilitating sampling and detection;
fig. 9 is a schematic diagram of a rack bar structure of a reaction kettle convenient for sampling and detection.
The reference numerals are as follows:
1. a kettle body; 2. a main pipe; 3. an air distribution plate; 4. an air duct; 5. a ring groove; 6. a first air hole; 7. an air guide sleeve ring; 8. a second air hole; 9. a connecting pipe; 10. a gas gathering head; 11. an exhaust pipe; 12. a guide groove; 13. a guide block; 14. a return spring; 15. an exhaust column; 16. an air dividing hole; 17. a main air hole; 18. a first motor; 19. a fixing ring; 20. ear pieces; 21. a mounting plate; 22. a movable groove; 23. a top plate; 24. a thimble; 25. a first spring; 26. a first shaft; 27. a blade; 28. a flow gathering cup; 29. a movable ring; 30. a chute; 31. a slide block; 32. a second spring; 33. a connecting rod; 34. a piercing head; 35. fixing the tube head; 36. a disc; 37. a gas distribution pipe; 38. a second shaft; 39. a paddle; 40. a feed pipe; 41. a discharge pipe; 42. a movable opening; 43. a toothed bar; 44. a directional groove; 45. an orientation block; 46. a plunger; 47. a sampling cup; 48. a second motor; 49. a gear.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments.
The invention is further illustrated by the following examples in connection with figures 1-9:
in this embodiment, as shown in fig. 1-4, a reaction kettle convenient for sampling and detection, including a kettle body 1, kettle body 1 top inner wall runs through and is connected with a main pipe 2 through the bearing rotation, be responsible for 2 top closures, the bottom opening, be responsible for 2 bottom intercommunication has a gas distribution dish 3, gas distribution dish 3 bottom intercommunication has a plurality of annular array distributed air duct 4, the air duct 4 cross-section sets up into the arc, kettle body 1 top is fixed with first motor 18 through the bolt, pass through the bolt fastening between first motor 18 output shaft and the main pipe 2, kettle body 1 top one side runs through and is fixed with blast pipe 11, guide slot 12 has all been seted up to blast pipe 11 both sides inner wall, sliding connection has guide block 13 in the guide slot 12, be fixed with same reset spring 14 through the bolt fastening between guide block 13 and the guide slot 12 top inner wall, be fixed with same exhaust column 15 through the bolt fastening between two guide blocks 13, a plurality of gas distribution holes 16 have been seted up to the circumference outer wall of exhaust column 15, main gas hole 17 and gas distribution column 15 bottom has been seted up main gas distribution 17, main pipe 2 circumference outer wall has annular groove 5, 5 annular groove 5 is set up to the circumference outer wall, 5 circumference outer wall has run through and has been seted up first gas hole 6 of seting up, 5 gas distribution ring 7, 7 is equipped with gas distribution ring 7 towards ring 7 and gas distribution 7, 9 top one side of the top of the connecting pipe 9 is fixed with the top of the connecting pipe, top 9 is connected to the top of the connecting pipe, top 9 is fixed to the gas distribution ring 9.
Further, the gas gathering head 10 is connected to the pipe orifice of the top of the connecting pipe 9 in a threaded manner, and the gas gathering head 10 is arranged in a flaring shape, so that gas can be conveniently gathered.
Further, the top of the kettle body 1 is fixedly penetrated by a feed pipe 40, the bottom of the kettle body 1 is fixedly penetrated by a discharge pipe 41, and valves are arranged on the feed pipe 40 and the discharge pipe 41, so that the feeding and the discharging can be facilitated.
In this embodiment, referring to fig. 5-7, a fixed ring 19 is sleeved and fixed on a main pipe 2, ear blocks 20 are welded on two sides of the fixed ring 19, a mounting plate 21 is connected to the ear blocks 20 through pins, a movable groove 22 is formed in the bottom of the mounting plate 21, a plurality of first springs 25 are fixed on inner walls of two sides of the movable groove 22 through bolts, a same top plate 23 is fixed on inner sides of the plurality of springs on two sides through bolts, the section of the top plate 23 is set to be arc-shaped, a plurality of uniformly distributed ejector pins 24 are fixed on the inner arc-shaped surface of the top plate 23 through bolts, the ejector pins 24 penetrate through the side wall of the mounting plate 21, and a triggering mechanism is arranged in the movable groove 22, so that bubbles can be punctured by the ejector pins 24.
Further, the triggering mechanism comprises a first shaft rod 26, the first shaft rod 26 is rotatably connected to the top inner wall of the movable groove 22 through a bearing, a plurality of annular array distributed blades 27 are fixedly arranged on the circumferential outer wall of the first shaft rod 26 through bolts, a plurality of evenly distributed flow gathering cups 28 are fixedly penetrated at one end of the mounting plate 21, which is close to the first shaft rod 26, and the flow gathering cups 28 are arranged in a funnel shape, so that the action of the ejector pins 24 can be triggered through the rotation of the blades 27.
Further, the outer wall of the circumference of the thimble 24 is provided with densely distributed piercing heads 34, and the piercing heads 34 and the thimble 24 are of an integrated structure, so that the piercing effect on bubbles can be improved.
Further, the main pipe 2 is sleeved with the movable ring 29, the movable ring 29 and the mounting plate 21 are connected with the same connecting rod 33 through a pin shaft, the two sides of the main pipe 2 are provided with the sliding grooves 30, the sliding grooves 30 are connected with the sliding blocks 31 in a sliding manner, the same second springs 32 are fixed between the sliding blocks 31 and the inner walls of the sliding grooves 30 through bolts, and the whole mounting plate 21 can be made to rotate in a reciprocating manner through the bolts between the sliding blocks 31 and the movable ring 29.
In this embodiment, referring to fig. 8, a fixed tube head 35 is connected to the tube opening of the air duct 4, a disc 36 is rotatably connected to the outer side of the fixed tube head 35 through a bearing, a plurality of air distribution tubes 37 distributed in a ring array are connected to the outer side of the disc 36, the air distribution tubes 37 are arranged in a Y shape, a second shaft 38 is fixed to the inner side of the disc 36 through bolts, and a blade 39 is fixed to the inner side of the second shaft 38 through bolts, so that the aeration effect can be improved.
In this embodiment, referring to fig. 2 and 9, a movable opening 42 is formed at the top of the kettle body 1, a toothed bar 43 is disposed in the movable opening 42, a directional groove 44 is formed at the rear end of the toothed bar 43, a directional block 45 is slidably connected in the directional groove 44, the directional block 45 is fixed with the inner wall of the rear end of the movable opening 42 through a bolt, a plunger 46 is fixed at the bottom of the toothed bar 43 through a bolt, a sampling cup 47 is fixed at the top of the plunger 46 through a bolt, a second motor 48 is fixed at the top of the kettle body 1 through a bolt, a gear 49 is connected with the output shaft of the second motor 48, and the gear 49 is meshed with the toothed bar 43, so that sampling can be facilitated.
The invention has the beneficial effects that:
when the reaction kettle works, the first motor 18 is in a starting state, the output shaft of the first motor 18 drives the main pipe 2, the gas distribution disc 3 and the gas guide pipe 4 to rotate, the reacted materials are stirred, meanwhile, the kettle body 1 is heated continuously, the temperature is high, the gas pressure pushes the gas discharge column 15 upwards, the gas discharge column 15 follows the guide block 13 and moves upwards along the guide groove 12 to extrude the reset spring 14, when the gas distribution holes 16 on the gas discharge column 15 are exposed to the outside of the gas discharge pipe 11, high-temperature gas in the kettle body 1 can enter from the main gas holes 17 and be discharged in a dispersed manner from the plurality of gas distribution holes 16, and as the connecting pipe 9 is opposite to the gas discharge column 15, a part of gas directly rushes into the connecting pipe 9 and then enters into the main pipe 2 through the second gas holes 8 and the first gas holes 6, and is discharged from the gas guide pipe 4, so that an aeration effect is formed, the stirring degree of the materials is improved, and the reaction efficiency is promoted, and the energy utilization can be carried out.
Further, when the main pipe 2 rotates, the fixing ring 19, the ear blocks 20, the mounting plate 21 and the ejector pins 24 are synchronously driven to rotate, the ejector pins 24 are used for conducting transverse scanning, large bubbles formed by aeration are broken to form local explosion, the stirring effect on materials is further promoted, at the moment, the materials are concentrated from the collecting cup 28 and enter the movable groove 22, impact is formed on the blade 27, the blade 27 rotates around the first shaft rod 26, the rotating blade 27 collides with the top plate 23, the two top plates 23 respectively move upwards and downwards, the corresponding ejector pins 24 are synchronously driven to move, at the moment, the top plate 23 extrudes the first spring 25 and performs reset action under the elastic force, so that the ejector pins 24 are contracted, the large bubbles formed by aeration are further facilitated to be broken, the section of the top plate 23 is arranged into an arc shape, on one hand, the blade 27 can be well matched with stress, on the other hand, when the reset action is carried out, the materials in the movable groove 22 can be conveniently extruded and discharged to the two ends, the stirring of the materials is further promoted, meanwhile, the resistance of the materials to the reset of the top plate 23 is reduced, the contraction action of the thimble 24 is quicker, and the densely distributed piercing heads 34 are arranged, so that the piercing effect on bubbles can be improved, further, when the mounting plate 21 rotates, the mounting plate 21 is subjected to centrifugal force, the whole mounting plate 21 rotates around the ear block 20, the movable ring 29 is pulled upwards through the connecting rod 33, the sliding block 31 stretches the second spring 32, at the moment, the materials have multidirectional fluidity due to the stirring of the materials, have a certain shaking effect, and the whole mounting plate 21 can carry out small-range reciprocating rotation in cooperation with the elasticity of the second spring 32, so that the piercing action on the bubbles is further promoted, the materials are fully stirred.
Further, when the gas enters the fixed tube head 35 from the gas guide tube 4, the air flow drives the blade 39 to rotate, and then synchronously drives the second shaft rod 38, the circular disc 36 and the gas distribution tube 37 to rotate, so that the gas is ejected in a rotating manner, the aeration effect is improved, and meanwhile, the gas distribution tube 37 is arranged in a Y shape, so that multidirectional aeration can be formed, and the aeration effect is further improved.
Further, when sampling is performed, the second motor 48 is started, the output shaft of the second motor 48 drives the gear 49 to rotate, the gear 49 is meshed with the gear 43 to drive the toothed bar 43 to move downwards until the sampling cup 47 moves to a proper position for sampling, then the second motor 48 is started to rotate reversely, so that the toothed bar 43 moves upwards to the position of the movable port 42 to finish sampling, and at the moment, the plunger 46 seals the movable port 42, so that the operation is convenient.
Working principle: when the reaction kettle works, the first motor 18 is in a starting state, the output shaft of the first motor 18 drives the main pipe 2, the gas distribution disc 3 and the gas guide pipe 4 to rotate, the reacted materials are stirred, meanwhile, the kettle body 1 is continuously heated, the temperature is high, the gas pressure pushes the gas discharge column 15 upwards, the gas discharge column 15 follows the guide block 13 and moves upwards along the guide groove 12 to extrude the reset spring 14, when the gas distribution holes 16 on the gas discharge column 15 are exposed out of the gas discharge pipe 11, high-temperature gas in the kettle body 1 can enter from the main gas holes 17 and be dispersed and discharged from the plurality of gas distribution holes 16, as the connecting pipe 9 is opposite to the gas discharge column 15, a part of gas directly rushes into the connecting pipe 9, then enters into the main pipe 2 through the second gas holes 8 and the first gas holes 6 and is discharged from the gas guide pipe 4, the aeration effect is formed, the stirring degree of the materials is improved, the reaction efficiency is promoted, the energy can be utilized, further, when the main pipe 2 rotates, the fixed ring 19, the ear blocks 20, the mounting plate 21 and the ejector pins 24 are synchronously driven to rotate, the ejector pins 24 are used for conducting transverse scanning, large bubbles formed by aeration are broken to form local explosion, the stirring effect on materials is further promoted, at the moment, the materials can be concentrated from the flow collecting cup 28 and enter the movable groove 22, impact is formed on the blade 27, the blade 27 rotates around the first shaft rod 26, the rotating blade 27 collides with the top plate 23, the two top plates 23 respectively move upwards and downwards, then the corresponding ejector pins 24 are synchronously driven to move, at the moment, the top plate 23 extrudes the first spring 25, and under the action of elasticity, reset action is conducted, so that the ejector pins 24 are enabled to conduct shrinkage action, the large bubbles formed by aeration are further facilitated to be torn, the section of the top plate 23 is arranged into an arc shape, on the one hand, the movable groove 22 can be conveniently extruded and discharged to two ends when in reset action, the stirring of the materials is further promoted, meanwhile, the resistance of the materials to the reset of the top plate 23 is reduced, the contraction action of the thimble 24 is quicker, the puncture effect on bubbles can be improved by arranging densely-distributed puncture heads 34, further, when the mounting plate 21 rotates, the mounting plate 21 integrally rotates around the ear blocks 20 due to centrifugal force, the movable ring 29 is pulled upwards through the connecting rod 33, the sliding block 31 stretches the second spring 32, the materials have multidirectional mobility due to the stirring of the materials, have a certain shaking effect and the small-range reciprocating rotation of the whole mounting plate 21 is realized by matching with the elasticity of the second spring 32, the puncture action of bubbles is further promoted, the materials are fully stirred, further, when gas enters the fixed tube head 35 from the gas guide tube 4, the air flow drives the paddle 39 to rotate, then the second shaft rod 38, the disc 36 and the gas distribution tube 37 are synchronously driven to rotate, so that the gas is rotationally sprayed out, the aeration effect is improved, meanwhile, the gas distribution tube 37 is arranged into a Y shape, the multidirectional aeration can be formed, the aeration effect is further improved, further, during sampling, the second motor 48 is started, the output shaft of the second motor 48 drives the gear 49 to rotate, the gear 49 is meshed to drive the toothed bar 43 to move downwards until the sampling cup 47 moves to a proper position for sampling, then the second motor 48 is started to reversely rotate, the toothed bar 43 is upwards moved to the position of the movable opening 42, the sampling is completed, the plunger 46 forms sealing for the movable opening 42, the operation is convenient.
The embodiments of the present invention are disclosed as preferred embodiments, but not limited thereto, and those skilled in the art will readily appreciate from the foregoing description that various extensions and modifications can be made without departing from the spirit of the present invention.
Claims (1)
1. The utility model provides a reation kettle convenient to sample and detect, including the cauldron body (1), a serial communication port, cauldron body (1) top inner wall runs through and rotates and is connected with main pipe (2), be responsible for (2) top and seal, bottom opening, be responsible for (2) bottom intercommunication and have branch gas dish (3), branch gas dish (3) bottom intercommunication has a plurality of annular array distributed air duct (4), air duct (4) cross-section sets up to the arc, cauldron body (1) top fixedly connected with first motor (18), fixed connection between first motor (18) output shaft and main pipe (2), cauldron body (1) top one side runs through and is fixed with blast pipe (11), guide slot (12) have all been seted up to blast pipe (11) both sides inner wall, sliding connection has guide block (13) in guide slot (12), fixedly connected with between guide block (13) and guide slot (12) top inner wall has same reset spring (14), fixedly connected with same exhaust column (15) between two guide block (13), a plurality of gas holes (16) have been seted up to exhaust column (15) circumference outer wall, main gas hole (17) bottom opening, main gas hole (17) and gas hole (17) are seted up to main pipe (6) circumference (5) outer wall, circumference (5) are seted up and are penetrated to ring groove (5), the annular groove (5) is sleeved with an air guide sleeve ring (7), the inner wall of the circumference of the air guide sleeve ring (7) is provided with densely distributed second air holes (8), a connecting pipe (9) is fixedly penetrated at the top of the kettle body (1), the top pipe orifice of the connecting pipe (9) faces one side of an air exhaust column (15), and the bottom of the connecting pipe (9) is communicated with the air guide sleeve ring (7);
the top pipe orifice of the connecting pipe (9) is in threaded connection with a gas gathering head (10), and the gas gathering head (10) is arranged in a flaring shape;
the top of the kettle body (1) is fixedly penetrated by a feed pipe (40), the bottom of the kettle body (1) is fixedly penetrated by a discharge pipe (41), and valves are arranged on the feed pipe (40) and the discharge pipe (41);
the main pipe (2) is sleeved and fixed with a fixing ring (19), ear blocks (20) are welded on two sides of the fixing ring (19), a mounting plate (21) is connected to the ear blocks (20) through pin shafts, a movable groove (22) is formed in the bottom of the mounting plate (21), a plurality of first springs (25) are fixedly connected to the inner walls of two sides of the movable groove (22), the inner sides of the springs on each side are fixedly connected with the same top plate (23), the section of the top plate (23) is arc-shaped, a plurality of thimble (24) which are uniformly distributed are fixedly connected to the intrados of the top plate (23), the thimble (24) penetrates through the side wall of the mounting plate (21), and a triggering mechanism is arranged in the movable groove (22);
the triggering mechanism comprises a first shaft lever (26), the first shaft lever (26) is rotationally connected to the top inner wall of the movable groove (22), a plurality of blades (27) distributed in an annular array are fixedly connected to the circumferential outer wall of the first shaft lever (26), a plurality of evenly distributed flow gathering cups (28) penetrate and are fixedly arranged at one end, close to the first shaft lever (26), of the mounting plate (21), and the flow gathering cups (28) are arranged in a funnel shape;
the outer wall of the circumference of the thimble (24) is provided with densely distributed thorn heads (34), and the thorn heads (34) and the thimble (24) are of an integrated structure;
the main pipe (2) is sleeved with a movable ring (29), the same connecting rod (33) is connected between the movable ring (29) and the mounting plate (21) through a pin shaft, sliding grooves (30) are formed in two sides of the main pipe (2), sliding blocks (31) are connected in the sliding grooves (30) in a sliding manner, the same second spring (32) is fixedly connected between the sliding blocks (31) and the inner walls of the sliding grooves (30), and the sliding blocks (31) are fixedly connected with the movable ring (29);
the pipe mouth of the air duct (4) is communicated with a fixed pipe head (35), the outer side of the fixed pipe head (35) is rotationally connected with a disc (36), the outer side of the disc (36) is communicated with a plurality of air distribution pipes (37) distributed in a ring-shaped array, the air distribution pipes (37) are arranged in a Y shape, the inner side of the disc (36) is fixedly connected with a second shaft rod (38), and the inner side of the second shaft rod (38) is fixedly connected with a blade (39);
a movable opening (42) is formed in the top of the kettle body (1), a toothed bar (43) is arranged in the movable opening (42), a directional groove (44) is formed in the rear end of the toothed bar (43), a directional block (45) is connected in a sliding manner in the directional groove (44), the directional block (45) is fixedly connected with the inner wall of the rear end of the movable opening (42), a plunger (46) is fixedly connected to the bottom of the toothed bar (43), a sampling cup (47) is fixedly connected to the top of the plunger (46), a second motor (48) is fixedly connected to the top of the kettle body (1), a gear (49) is connected to an output shaft of the second motor (48), and the gear (49) is connected with the toothed bar (43) in a meshed manner;
when the main pipe (2) rotates, materials are concentrated from the flow gathering cup (28) and enter the movable groove (22), impact is formed on the blade plate (27), the blade plate (27) rotates around the first shaft rod (26), the rotating blade plate (27) collides with the top plates (23), the two top plates (23) move upwards and downwards respectively, and then the corresponding ejector pins (24) are synchronously driven to move.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210062158.6A CN114367264B (en) | 2022-01-19 | 2022-01-19 | Reation kettle convenient to sample detects |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202210062158.6A CN114367264B (en) | 2022-01-19 | 2022-01-19 | Reation kettle convenient to sample detects |
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| CN114367264A CN114367264A (en) | 2022-04-19 |
| CN114367264B true CN114367264B (en) | 2023-12-29 |
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| CN212855725U (en) * | 2020-06-08 | 2021-04-02 | 上海立科化学科技有限公司 | Pressure regulating reaction kettle for gas-liquid synthesis |
| CN112705140A (en) * | 2020-12-07 | 2021-04-27 | 李会娟 | Colloid reaction equipment |
| CN112934061A (en) * | 2021-02-06 | 2021-06-11 | 广州市浩杰玩具有限公司 | Mixing equipment for civil construction |
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Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109772251A (en) * | 2017-11-14 | 2019-05-21 | 张松彬 | A kind of reaction kettle convenient for sample detection |
| CN210613682U (en) * | 2019-06-28 | 2020-05-26 | 马鞍山科英合成材料有限公司 | Production equipment for improving preparation efficiency of closed isocyanate |
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| CN212855725U (en) * | 2020-06-08 | 2021-04-02 | 上海立科化学科技有限公司 | Pressure regulating reaction kettle for gas-liquid synthesis |
| CN111977874A (en) * | 2020-09-01 | 2020-11-24 | 杨锦 | Medical sewage treatment equipment |
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| CN114367264A (en) | 2022-04-19 |
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Effective date of registration: 20231204 Address after: 044000 Salt Lake Industrial Park, Yuncheng City, Shanxi Province Applicant after: SHANXI QIYOU BUILDING MATERIALS TECHNOLOGY Co.,Ltd. Address before: 100000 No. 210, Nanhu Xiyuan, Chaoyang District, Beijing Applicant before: Wang Yuantang |
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