CN109772251A - A kind of reaction kettle convenient for sample detection - Google Patents
A kind of reaction kettle convenient for sample detection Download PDFInfo
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- CN109772251A CN109772251A CN201711123087.1A CN201711123087A CN109772251A CN 109772251 A CN109772251 A CN 109772251A CN 201711123087 A CN201711123087 A CN 201711123087A CN 109772251 A CN109772251 A CN 109772251A
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- China
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- autoclave body
- reaction kettle
- gear
- sample detection
- kettle convenient
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Abstract
The invention provides a kind of reaction kettle convenient for sample detection, including autoclave body, agitating shaft is equipped with inside the autoclave body, the agitating shaft is equipped with the first agitating paddle and the second agitating paddle, and first agitating paddle be located at agitating shaft bottom end, the agitating shaft upper end stretches out autoclave body and is connected with the motor for being located at autoclave body outside top, sales kit (SK) is additionally provided with inside the autoclave body, the sales kit (SK) side wall is equipped with feed opening, rack gear is fixedly connected with above sales kit (SK), the upper end of the rack stretches out autoclave body and straight up by being located at the limit hole on the outside of autoclave body, the rack gear side is equipped with the gear engaged, the gear is located on the outside of autoclave body, gear is connected to motor.Sales kit (SK) is equipped in a kind of reaction kettle convenient for sample detection of the present invention, by the position of motor control gear and the adjustable sales kit (SK) of rack gear, the sample that can extract any position inside autoclave body is detected, and realizes the real time monitoring to reaction.
Description
Technical field
The invention belongs to field of chemical equipment, more particularly, to a kind of reaction kettle convenient for sample detection.
Background technique
Reaction kettle is a kind of important chemical industry equipment, is to be mainly used to complete vulcanization, nitrification, hydrogenation, hydrocarbonylation, polymerization, contracting
The pressure vessel of the chemical enginnering process such as conjunction.According to different reaction condition needs, the structure design of reaction kettle be will be different,
But its structure is generally made of autoclave body, transmission device, agitating device, heating device, cooling device, sealing device.
It needs to extract reactant in Chemical Manufacture, in reaction process and be detected, the process of real-time monitoring reaction, when anti-
When answering kettle larger, it is larger that reaction liquid difficulty is extracted with suction pipe.
Summary of the invention
In view of this, the invention is directed to a kind of reaction kettle convenient for sample detection in extract real-time reaction kettle
Reactant, convenient for detection reaction process.
In order to achieve the above objectives, the technical solution of the invention is achieved in that
A kind of reaction kettle convenient for sample detection, including autoclave body, the autoclave body top side are equipped with feed inlet, and the other side is set
There is sample tap, the autoclave body bottom is equipped with discharge port, and agitating shaft is equipped with inside the autoclave body, and the agitating shaft is equipped with first and stirs
Paddle and the second agitating paddle are mixed, and the first agitating paddle is located at agitating shaft bottom end, the agitating shaft upper end stretches out autoclave body and is located at autoclave body
The motor of outside top is connected, and sales kit (SK) is additionally provided with inside the autoclave body, and the sales kit (SK) side wall is equipped with feed opening, sales kit (SK)
Top is fixedly connected with rack gear, and the upper end of the rack stretches out autoclave body and straight up by being located at the limit hole on the outside of autoclave body, described
Rack gear side is equipped with the gear engaged, and the gear is located on the outside of autoclave body, and gear is connected to motor.
Further, it is provided with fixation kit on the outside of the autoclave body, the fixation kit includes rack platform and is located at branch
Fixed link above body panel, the rack platform are equipped with gear locking device, and the motor is placed on rack platform, institute
Limit hole is stated in fixed link.
Further, the first agitating paddle of institute and the second agitating paddle are W-shaped, and jagged protrusion is provided on blade.
Further, the diameter of the feed opening is 5-10mm；Distance of the feed opening apart from sales kit (SK) top is 10-
20mm；Supporting leg is equipped with below the autoclave body.
Further, the supporting leg is removable frame.
Further, the limit hole (6) is long hole.
Compared with the existing technology, a kind of described in the invention to be had the advantage that convenient for the reaction kettle of sample detection
It is equipped with sales kit (SK) in a kind of reaction kettle convenient for sample detection of the present invention, passes through motor control gear and tooth
The position of the adjustable sales kit (SK) of item, the sample that can extract any position inside autoclave body are detected, and realize the reality to reaction
When monitor, simple and convenient, while the agitating paddle of W shape can cause flow-disturbing to mixture, the protrusion on paddle can eliminate mixture
In bubble, accelerate the dissolution of reactant.
Detailed description of the invention
The attached drawing for constituting a part of the invention is used to provide to further understand the invention, present invention wound
The illustrative embodiments and their description made are used to explain the present invention creation, do not constitute the improper restriction to the invention.?
In attached drawing:
Fig. 1 is a kind of structural schematic diagram of the reaction kettle convenient for sample detection described in the invention embodiment.
Description of symbols:
1- autoclave body；2- feed inlet；3- agitating shaft；4- motor；5- rack gear；6- limit hole；7- gear；8- sample tap；9- sample
Product case, 10- discharge port；The first agitating paddle of 11-；The second agitating paddle of 12-；13- motor；14- feed opening.
Specific embodiment
It should be noted that in the absence of conflict, the feature in embodiment and embodiment in the invention can
To be combined with each other.
In the description of the invention, it is to be understood that term " center ", " longitudinal direction ", " transverse direction ", "upper", "lower",
The orientation or positional relationship of the instructions such as "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outside" is
It is based on the orientation or positional relationship shown in the drawings, is merely for convenience of description the invention and simplifies description, rather than indicate
Or imply that signified device or element must have a particular orientation, be constructed and operated in a specific orientation, therefore cannot understand
For the limitation to the invention.In addition, term " first ", " second " etc. are used for description purposes only, and should not be understood as indicating
Or it implies relative importance or implicitly indicates the quantity of indicated technical characteristic." first ", " second " etc. are defined as a result,
Feature can explicitly or implicitly include one or more of the features.In the description of the invention, unless separately
It is described, the meaning of " plurality " is two or more.
In the description of the invention, it should be noted that unless otherwise clearly defined and limited, term " peace
Dress ", " connected ", " connection " shall be understood in a broad sense, for example, it may be being fixedly connected, may be a detachable connection, or integrally
Connection；It can be mechanical connection, be also possible to be electrically connected；Can be directly connected, can also indirectly connected through an intermediary,
It can be the connection inside two elements.For the ordinary skill in the art, on being understood by concrete condition
State concrete meaning of the term in the invention.
The present invention will be described in detail below with reference to the accompanying drawings and embodiments creates.
A kind of reaction kettle convenient for sample detection, as shown in Figure 1, including autoclave body 1, the autoclave body top side is equipped with charging
Mouth 2, the other side are equipped with sample tap 8, and the autoclave body bottom is equipped with discharge port 10, and agitating shaft 3 is equipped with inside the autoclave body, described to stir
Axis is mixed equipped with the first agitating paddle 11 and the second agitating paddle 12, and the first agitating paddle is located at agitating shaft bottom end, on the agitating shaft
End stretches out autoclave body and is connected with the motor 4 for being located at autoclave body outside top, and sales kit (SK) 9, the sales kit (SK) are additionally provided with inside the autoclave body
Side wall is equipped with feed opening, is fixedly connected with rack gear 5 above sales kit (SK), the upper end of the rack stretches out autoclave body straight up and passes through position
Limit hole 6 on the outside of autoclave body, the rack gear side are equipped with the gear 7 engaged, and the gear is located on the outside of autoclave body, gear
It is connect with motor 13.
Fixation kit is provided on the outside of the autoclave body, the fixation kit includes rack platform and is located above rack platform
Fixed link, the rack platform is equipped with gear locking device, and the motor is placed on rack platform, and the limit hole is set
In in fixed link.
The first agitating paddle 11 of institute and the second agitating paddle 12 are W-shaped, and jagged protrusion is provided on blade.
The diameter of the feed opening is 5-10mm；Distance of the feed opening apart from sales kit (SK) top is 10-20mm；It is described
Supporting leg is equipped with below autoclave body.For the ease of movement, the supporting leg is designed to removable frame.Meanwhile it adjusting for convenience
Section, the limit hole (6) is preferably long hole.
A kind of specific work process of the reaction kettle convenient for sample detection described in the invention are as follows:
A kind of reaction kettle convenient for sample detection described in the invention, in use, raw material enters kettle from feed inlet 2
Body, motor 4 drive agitating shaft 3 to rotate, and the first agitating paddle 11 and the second agitating paddle 12 play stirring action, the protrusion being arranged on blade
Bubble in energy elimination reaction liquid, keeps dissolution of raw material more abundant, in reaction process, reaction liquid enters sample by feed opening
In product case, when need to extract reaction liquid detected when, open motor 13, gear 7 with carry-over bar 5 move up and down, realize sample
The up and down motion of product case, can extract the reaction liquid of different location in autoclave body as needed, and rack drives sales kit (SK) 9 reaches sampling
Below mouthful, the reaction solution sample in sales kit (SK) is extracted by specific purpose tool, by the fixed gear of locking device after extraction, instead
Product is discharged by discharge port 10 after answering.
The foregoing is merely the preferred embodiments of the invention, are not intended to limit the invention creation, all at this
Within the spirit and principle of innovation and creation, any modification, equivalent replacement, improvement and so on should be included in the invention
Protection scope within.
Claims (8)
1. a kind of reaction kettle convenient for sample detection, it is characterised in that: including autoclave body (1), the autoclave body top side be equipped with into
Material mouth (2), the other side are equipped with sample tap (8), and the autoclave body bottom is equipped with discharge port (10), and agitating shaft is equipped with inside the autoclave body
(3), the agitating shaft is equipped with the first agitating paddle (11) and the second agitating paddle (12), and the first agitating paddle is located at agitating shaft bottom
End, the agitating shaft upper end stretch out autoclave body and are connected with the motor (4) for being located at autoclave body outside top, are additionally provided with sample inside the autoclave body
Product case (9), the sales kit (SK) side wall are equipped with feed opening (14), are fixedly connected with rack gear (5), the upper end of the rack above sales kit (SK)
Autoclave body is stretched out straight up and by being located at the limit hole (6) on the outside of autoclave body, the rack gear side is equipped with the gear that engages
(7), the gear is located on the outside of autoclave body, and gear is connect with motor (13).
2. a kind of reaction kettle convenient for sample detection according to claim 1, it is characterised in that: setting on the outside of the autoclave body
There is a fixation kit, the fixation kit includes rack platform and the fixed link above rack platform, on the rack platform
Equipped with gear locking device, the motor (13) is placed on rack platform, and the limit hole (6) is set in fixed link.
3. a kind of reaction kettle convenient for sample detection according to claim 2, it is characterised in that: the first agitating paddle of institute (11)
It is W-shaped with the second agitating paddle (12), and is provided with jagged protrusion on blade.
4. a kind of reaction kettle convenient for sample detection according to claim 2, it is characterised in that: the diameter of the feed opening
For 5-10mm.
5. a kind of reaction kettle convenient for sample detection according to claim 1, it is characterised in that: the feed opening is apart from sample
The distance on product case top is 10-20mm.
6. a kind of reaction kettle convenient for sample detection according to claim 1 or 5, it is characterised in that: below the autoclave body
Equipped with supporting leg.
7. a kind of reaction kettle convenient for sample detection according to claim 6, it is characterised in that: the supporting leg is removable
Dynamic structure.
8. a kind of reaction kettle convenient for sample detection according to claim 2, it is characterised in that: the limit hole (6) is
Long hole.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711123087.1A CN109772251A (en) | 2017-11-14 | 2017-11-14 | A kind of reaction kettle convenient for sample detection |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711123087.1A CN109772251A (en) | 2017-11-14 | 2017-11-14 | A kind of reaction kettle convenient for sample detection |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109772251A true CN109772251A (en) | 2019-05-21 |
Family
ID=66494114
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711123087.1A Pending CN109772251A (en) | 2017-11-14 | 2017-11-14 | A kind of reaction kettle convenient for sample detection |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109772251A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110585954A (en) * | 2019-09-19 | 2019-12-20 | 英鸿纳米科技股份有限公司 | Special nanometer coating production line of nanometer super capacitor battery |
| CN111389334A (en) * | 2020-04-18 | 2020-07-10 | 杨明清 | Water-reducing agent reation kettle convenient to sample detection |
| CN113834699A (en) * | 2021-10-11 | 2021-12-24 | 格林爱科(荆门)新能源材料有限公司 | Liquid sampling system |
| CN114367264A (en) * | 2022-01-19 | 2022-04-19 | 王渊堂 | Reation kettle convenient to sampling test |
-
2017
- 2017-11-14 CN CN201711123087.1A patent/CN109772251A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110585954A (en) * | 2019-09-19 | 2019-12-20 | 英鸿纳米科技股份有限公司 | Special nanometer coating production line of nanometer super capacitor battery |
| CN111389334A (en) * | 2020-04-18 | 2020-07-10 | 杨明清 | Water-reducing agent reation kettle convenient to sample detection |
| CN113834699A (en) * | 2021-10-11 | 2021-12-24 | 格林爱科(荆门)新能源材料有限公司 | Liquid sampling system |
| CN114367264A (en) * | 2022-01-19 | 2022-04-19 | 王渊堂 | Reation kettle convenient to sampling test |
| CN114367264B (en) * | 2022-01-19 | 2023-12-29 | 山西其右建材科技有限公司 | Reation kettle convenient to sample detects |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20190521 |
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| WD01 | Invention patent application deemed withdrawn after publication |