CN206424961U - A kind of graphite intercalation reactor - Google Patents
A kind of graphite intercalation reactor Download PDFInfo
- Publication number
- CN206424961U CN206424961U CN201720073244.1U CN201720073244U CN206424961U CN 206424961 U CN206424961 U CN 206424961U CN 201720073244 U CN201720073244 U CN 201720073244U CN 206424961 U CN206424961 U CN 206424961U
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- China
- Prior art keywords
- kettle
- flow
- stopping plate
- reactor
- graphite intercalation
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Abstract
The utility model discloses a kind of graphite intercalation reactor, including far-infrared heating stove, kettle and motor, flow-stopping plate is provided with the kettle, the kettle is horizontally installed in far-infrared heating stove by bearing, the motor drives kettle to rotate by transmission belt.The utility model can be such that material uniformly mixes by kettle spinning, in the absence of dead angle, and kettle heating surface area is bigger, be heated evenly, can effectively improve intercalation effect.Meanwhile, because reducing rabbling mechanism, also reach the purpose for simplifying reactor structure.
Description
Technical field
The utility model belongs to field of graphene, in particular to a kind of graphite intercalation reactor, is mainly used in stone
Ink carries out intercalation processing.
Background technology
In recent years, with the rise of nanometer technology, people gradually recognize the huge superiority of nanoscale product, start
Various fine technologies are studied, wherein, a kind of super-fine processing that intercalation technique grows up aiming at layer mineral feature
Method.
Intercalation technique refers to that the small molecule of some organic or inorganics enters the interlayer of layer mineral under certain conditions,
So as to slacken the interlaminar action power of layer mineral, a kind of New Processing of monomer peeling effect is reached.
At present, intercalation technique is generally completed by the reactor of stirring-type, and such as Chinese patent notification number is
The prior art of " CN204544193U " disclosed a kind of industrialization solid phase intercalation reactor, its technology on the 12nd in August in 2015
Scheme is that the reactor includes kettle, and kettle, which is provided with charging aperture and discharging opening, the kettle, is provided with agitator, the kettle
The outside of body is provided with heating system, and the cooling air channel in gap, the top cover of kettle are formed between the heating system and kettle outer wall
It is provided with flushing hole, thermometer hole, vacuum port and gauge port.Using the patent as the prior art of representative, mainly pass through stirring
Effect realize intercalation, but in actual application, for the reaction of solid-phase material, stirring-type reaction kettle exists due to bottom
Dead angle is stirred, partial material mixing can be caused uneven, intercalation effect is influenceed；In addition, stirring-type reaction kettle is due to internal structure
Complexity, can cause difficulty to cleaning；Agitator and the sealing of kettle junction also easily go wrong.
Utility model content
The purpose of this utility model is that solve the above-mentioned problems in the prior art reacts there is provided a kind of graphite intercalation
Kettle, the utility model can be such that material uniformly mixes by kettle spinning, in the absence of dead angle, and kettle heating surface area is bigger, by
Heat evenly, can effectively improve intercalation effect.Meanwhile, because reducing rabbling mechanism, also reach and simplified reactor structure
Purpose.
To achieve the above object, the technical solution adopted in the utility model is as follows：
A kind of graphite intercalation reactor, it is characterised in that：Including far-infrared heating stove, kettle and motor, in the kettle
Flow-stopping plate is provided with, the kettle is horizontally installed in far-infrared heating stove by bearing, and the motor is driven by transmission belt
Kettle is rotated.
The flow-stopping plate vertical welding is on inner wall of kettle.
The height of the flow-stopping plate is 4-6cm.
The junction of the flow-stopping plate and kettle is S-shaped.
The quantity of the flow-stopping plate is polylith, and polylith flow-stopping plate is uniformly arranged in kettle.
One end of the kettle by swivel joint be connected with vacuum interface, pressure gauge connection, pressure sensor interface and
Temperature sensor interface, the other end is connected with relief valve connection by bearing.
Described reactor also includes feeding device and drawing mechanism, and the feeding device includes funnel and the branch with roller
Frame, the funnel is fixed on support；The drawing mechanism includes deflector chute and the support with roller, and the deflector chute is fixed on
On support.
Using the utility model has the advantage of：
First, in the utility model, flow-stopping plate is set in kettle, and kettle lateral rotation is arranged on far-infrared heating stove
Interior structure, can be such that material uniformly mixes by kettle spinning, in the absence of dead angle, and kettle heating surface area is bigger, be heated more
Uniformly, intercalation effect can be effectively improved.Meanwhile, compared with prior art, the utility model also reduces rabbling mechanism, reaches
Simplify the purpose of reactor structure.
2nd, in the utility model, during the course of the reaction, the junction of flow-stopping plate and kettle is S-shaped, and the height of flow-stopping plate
4-6cm structure is set to, kettle materials inside can be made to be mixed both axially and radially under collective effect of the flow-stopping plate with kettle
It is even.On the one hand the structure design of flow-stopping plate can make material mixing more uniform, on the other hand make the discharging and kettle cleaning of material
It is more thorough.
3rd, in the utility model, the structure of polylith flow-stopping plate is uniformly arranged in kettle, material can be further reduced equal
The time of even mixing, meanwhile, it is capable to further improve intercalation effect.
4th, in the utility model, by single feeding device and drawing mechanism, avoid the need for setting valve on kettle
Door so that material mixed process will not accumulated plugging, meanwhile, kettle internal structure is simple so that cleaning more facilitate.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model；
Fig. 2 is structural representation when the utility model feeds；
Fig. 3 is structural representation when the utility model discharges；
In figure marked as：1st, far-infrared heating stove, 2, vacuum interface, 3, pressure gauge connection, 4, pressure sensor interface, 5,
Temperature sensor interface, 6, flow-stopping plate, 7, motor, 8, relief valve connection, 9, kettle, 10, funnel, 11, deflector chute.
Embodiment
Gear is provided with a kind of graphite intercalation reactor, including far-infrared heating stove 1, kettle 9 and motor 7, the kettle 9
Plate 6 is flowed, the kettle 9 is horizontally installed in far-infrared heating stove 1 by bearing, the motor 7 passes through transmission belt and kettle 9
Right-hand member is connected, and the motor 7 drives kettle 9 to rotate by transmission belt；The left end of the kettle 9 is connected with very by swivel joint
Null interface 2, pressure gauge connection 3, pressure sensor interface 4 and temperature sensor interface 5, right-hand member is connected with safety valve by bearing
Interface 8.
In the utility model, the flow-stopping plate 6 is veneer, and its quantity is polylith, and every piece of flow-stopping plate 6 vertically stands on kettle 9
Inner side, the height of every piece of flow-stopping plate 6 is 4-6cm, and the junction of every piece of flow-stopping plate 6 and kettle 9 is S-shaped, every piece of flow-stopping plate 6
Length is consistent, and spacing is consistent.During the course of the reaction, kettle 9 at the uniform velocity rotates vertically, and materials inside is in flow-stopping plate 6 and kettle 9
It is well mixed both axially and radially under collective effect.On the one hand the structure design of flow-stopping plate 6 can make material mixing more uniform, separately
On the one hand the discharging of material and kettle 9 is made to clean more thorough.
Further, preferably the quantity of flow-stopping plate is 12 pieces.
In the utility model, described reactor also includes feeding device and drawing mechanism, and the feeding device includes leakage
Bucket 10 and the support with roller, the funnel 10 are fixed on support；The drawing mechanism includes deflector chute 11 and with roller
Support, the deflector chute 11 is fixed on support.
In the utility model, the charging and discharging of the kettle 9 can be complete by removing the swivel joint of the left end of kettle 9
Into.
Operation principle of the present utility model is：
1, the swivel joint of the left end of kettle 9 is removed, the lower end of funnel 10 is stretched into kettle 9 from the left end of kettle 9, to kettle
Material is added in 9, after material addition is finished, swivel joint is resetted.
2, kettle 9 is heated by far-infrared heating stove 1, drives kettle 9 to rotate by motor 7, in the presence of flow-stopping plate 6,
Material is uniformly mixed.
3, after the completion of material mixing, the swivel joint of the left end of kettle 9 is removed again, kettle is stretched into the upper end of deflector chute 11
In 9, while rotating kettle 9, in the presence of flow-stopping plate 6, mixed material is discharged from deflector chute 11.
Claims (7)
1. a kind of graphite intercalation reactor, it is characterised in that：Including far-infrared heating stove（1）, kettle（9）And motor（7）, it is described
Kettle（9）Inside it is provided with flow-stopping plate（6）, the kettle（9）Far-infrared heating stove is horizontally installed on by bearing（1）It is interior, it is described
Motor（7）Kettle is driven by transmission belt（9）Rotate.
2. a kind of graphite intercalation reactor as claimed in claim 1, it is characterised in that：The flow-stopping plate（6）Vertical welding in
Kettle（9）On inwall.
3. a kind of graphite intercalation reactor as claimed in claim 1, it is characterised in that：The flow-stopping plate（6）Height for 4-
6cm。
4. a kind of graphite intercalation reactor as claimed in claim 1, it is characterised in that：The flow-stopping plate（6）With kettle（9）'s
Junction is S-shaped.
5. a kind of graphite intercalation reactor as any one of claim 1-4, it is characterised in that：The flow-stopping plate（6）
Quantity be polylith, polylith flow-stopping plate（6）It is uniformly arranged on kettle（9）It is interior.
6. a kind of graphite intercalation reactor as claimed in claim 1, it is characterised in that：The kettle（9）One end pass through rotation
Adapter is connected with vacuum interface（2）, pressure gauge connection（3）, pressure sensor interface（4）And temperature sensor interface（5）, separately
One end is connected with relief valve connection by bearing（8）.
7. a kind of graphite intercalation reactor as claimed in claim 1, it is characterised in that：Described reactor also includes charging dress
Put and drawing mechanism, the feeding device includes funnel（10）With the support with roller, the funnel（10）It is fixed on support；
The drawing mechanism includes deflector chute（11）With the support with roller, the deflector chute（11）It is fixed on support.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720073244.1U CN206424961U (en) | 2017-01-21 | 2017-01-21 | A kind of graphite intercalation reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720073244.1U CN206424961U (en) | 2017-01-21 | 2017-01-21 | A kind of graphite intercalation reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206424961U true CN206424961U (en) | 2017-08-22 |
Family
ID=59582725
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720073244.1U Active CN206424961U (en) | 2017-01-21 | 2017-01-21 | A kind of graphite intercalation reactor |
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| Country | Link |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108380148A (en) * | 2018-03-07 | 2018-08-10 | 中国工程物理研究院激光聚变研究中心 | A kind of drop revolution curing reaction system of simulated microgravity |
| CN109499516A (en) * | 2018-12-14 | 2019-03-22 | 武汉科技大学 | A kind of rotary pressure reacting furnace |
| CN113041643A (en) * | 2020-09-11 | 2021-06-29 | 禹城鼎盛天成生物科技有限公司 | Nervonic acid oil spin crystallization device and method thereof |
-
2017
- 2017-01-21 CN CN201720073244.1U patent/CN206424961U/en active Active
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108380148A (en) * | 2018-03-07 | 2018-08-10 | 中国工程物理研究院激光聚变研究中心 | A kind of drop revolution curing reaction system of simulated microgravity |
| CN108380148B (en) * | 2018-03-07 | 2019-12-13 | 中国工程物理研究院激光聚变研究中心 | droplet gyration solidification reaction system of simulation microgravity |
| CN109499516A (en) * | 2018-12-14 | 2019-03-22 | 武汉科技大学 | A kind of rotary pressure reacting furnace |
| CN113041643A (en) * | 2020-09-11 | 2021-06-29 | 禹城鼎盛天成生物科技有限公司 | Nervonic acid oil spin crystallization device and method thereof |
| CN113041643B (en) * | 2020-09-11 | 2023-11-24 | 禹城鼎盛天成生物科技有限公司 | Nervonic acid grease spin crystallization device and method thereof |
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