CN114315311A - Tiancha star purple sand pug and preparation method thereof - Google Patents
Tiancha star purple sand pug and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a Tiancha star purple sand pug which comprises the following components in percentage by weight: 8 to 12 percent of red leather dragon purple sand raw ore, 25 to 35 percent of white clay purple sand raw ore, 15 to 20 percent of indigenous green clay purple sand raw ore, 15 to 20 percent of golden clay purple sand raw ore, 3 to 8 percent of white clay purple sand raw ore, 3 to 8 percent of rock red clay purple sand raw ore and 3 to 8 percent of green gray purple clay purple sand raw ore. The invention provides the Tiancha star purple sand pug which is simple in process, low in pug shrinkage rate, high in finished product rate and rich in finished product color after firing and the preparation method thereof.
Description
Technical Field
The invention relates to the technical field of purple sand pug, and particularly relates to Tiancha star purple sand pug and a preparation method thereof.
Background
The purple sand is a ceramic product between pottery and porcelain, and is characterized by compact structure, nearly vitrified property, high strength, fine particles, shell-shaped or stone-shaped fracture, but no translucency of porcelain body. The purple sand ware has various mud colors, commonly called 'five-color soil', and has various colors such as white mud, black mud, yellow mud, pine flower mud and the like besides red mud, purple mud, segment mud, black mud and blackish green mud which are mainly 'five colors', the purple sand ware does not hang glaze, but fully utilizes the natural color of the mud, the color is warm and moist after firing, the purple sand ware is elegant and lovely, the surface of the purple sand ware also has a matte effect, the reflection of light energy can be weakened, and the vivid effects of the shape, the decoration and the natural color of the ware can be clearly expressed.
The existing purple sand pug has single color after being fired, and the color pattern of the finished purple sand product which is accidentally furnace-transmuted is uncontrollable. The purple sand pug which is rich in color, small in firing shrinkage deformation and high in yield is urgently needed in the market.
Disclosure of Invention
In order to solve the problems, the invention provides the Tiancha xing purple sand pug which is simple in process, low in pug shrinkage rate, high in finished product rate and rich in finished product color after firing and the preparation method thereof.
According to one aspect of the invention, the Tiancha star purple sand pug comprises the following components in percentage by weight: 8 to 12 percent of red leather dragon purple sand raw ore, 25 to 35 percent of white clay purple sand raw ore, 15 to 20 percent of indigenous green clay purple sand raw ore, 15 to 20 percent of golden clay purple sand raw ore, 3 to 8 percent of white clay purple sand raw ore, 3 to 8 percent of rock red clay purple sand raw ore and 3 to 8 percent of green gray purple clay purple sand raw ore.
In some embodiments, the red-skin Longzi red porcelain raw ore is yellow-skin Longzi wild mountain red mud, and the red-skin Longzi red porcelain raw ore is made of 50.6% SiO2, 20.6% Al 2O3, 9.8% Fe 2O3, 0.84% CaO, 0.64% MgO, 2.15% K2O, 0.21% Na2O and 0.82% TiO;
the white clay purple sand raw ore is No. four mine white clay, and is prepared from 55-57% of SiO2, 19-22% of Al 2O3, 1.4% of Fe 2O3, 0.5-0.8% of CaO, 0.5-0.8% of MgO, 2-3% of K2O, 0.01-0.08% of Na2O and 1-1.2% of TiO;
the raw red porcelain ore of the mountain green mud is No. four mine green mud, and is prepared from 55-57% of SiO2, 2% of A l 2O3, 8-9% of Fe 2O3, 0.5-0.8% of CaO, 0.5-0.8% of MgO, 2-3% of K2O, 0.01-0.08% of Na2O and 1-1.2% of TiO;
the raw red porcelain ore of the gold group mud is the Huang Long mountain group mud, and is prepared from 55 to 57 percent of SiO2, 1.8 percent of Al 2O3, 8 to 9 percent of Fe 2O3, 0.5 to 0.8 percent of CaO, 0.5 to 0.8 percent of MgO, 2 to 3 percent of K2O, 0.01 to 0.08 percent of Na2O and 1 to 1.2 percent of TiO;
the raw white mud purple sand ore is yellow Longshan white mud, and is prepared from 55-57% of SiO2, 19-22% of Al 2O3, 4-5% of Fe 2O3, 0.5-0.8% of CaO, 0.5-0.8% of MgO, 2-3% of K2O, 0.01-0.08% of Na2O and 1-1.2% of TiO;
the raw material of the red stoneware purple sand is yellow Longshan red stoneware, and is prepared from 56.3 percent of SiO2, 19 to 22 percent of Al 2O3, 8 to 9 percent of Fe 2O3, 0.5 to 0.8 percent of CaO, 0.5 to 0.8 percent of MgO, 2 to 3 percent of K2O, 0.01 to 0.08 percent of Na2O and 1 to 1.2 percent of TiO;
the green-gray purple mud is purple mud in a large pool mining area, and is prepared from 55-57% of SiO2, 19-22% of Al 2O3, 8-9% of Fe 2O3, 0.5-0.8% of CaO, 0.5-0.8% of MgO, 2-3% of K2O, 0.01-0.08% of Na2O and 1-1.2% of TiO.
According to one aspect of the invention, the preparation method of the Tiancha star purple sand pug comprises the following steps:
step (1), selecting materials: sorting the red leather dragon purple sand raw ore, the white clay purple sand raw ore, the Benshan green clay purple sand raw ore, the gold clay purple sand raw ore, the white clay purple sand raw ore, the red clay purple sand raw ore and the green gray purple clay purple sand raw ore one by one, and removing obvious impurities in the ore materials;
step (2), weathering: placing the sorted ore materials in open air in different areas, and naturally weathering for more than 3 months;
step (3), crushing: crushing the mineral aggregates one by utilizing a ring roller mill, and screening the crushed mineral aggregates;
and (4) purifying: purifying the mineral aggregate by a dry absorption method or a wet absorption method;
and (5) ageing: respectively adding clean water into the purified mineral aggregate obtained in the step (4), and uniformly stirring to form slurry, wherein the slurry is in a closed environment with the temperature of 15-20 ℃ and the relative humidity of 20-30% for 3-6 months;
step (6), pre-sintering: drying the red pitaya, the golden ball mud, the red mud and the green ash purple mud ore materials obtained in the step (5) into granules, and then sintering the granules in a kiln;
step (7), blending: fully mixing the fired purple sand particles with aged purple sand mineral aggregate according to the proportion;
step (8), pugging: repeatedly beating and extruding the pug mixed in the step (7) by using equipment; .
And (9) warehousing: and packaging the pug of the purple sand subjected to pugging and warehousing for later use.
In some embodiments, the firing temperature of the red leather dragon red porcelain mineral aggregate in the step (6) is 1150-1165 ℃, and the firing time is 4-6 hours.
In some embodiments, the firing temperature of the golden ball mud purple sand mineral aggregate in the step (6) is 1135 ℃ to 1140 ℃ and the firing time is 4 to 6 hours.
In some embodiments, the firing temperature of the red mud purple sand mineral aggregate in the step (6) is 1160-1165 ℃, and the firing time is 4-6 hours.
In some embodiments, the firing temperature of the purple sand ore material of the grey purple mud in the step (6) is 1180-1185 ℃, and the firing time is 4-6 hours.
Compared with the prior art, the invention has the beneficial effects that: simple process, low shrinkage of the pug, high yield and rich color of the finished product after firing. In the invention, the novel pug disclosed by the invention is prepared by pre-firing raw purple sand pug, embodying the colors of different pugs at different firing temperatures and mixing pre-fired pug particles.
Detailed Description
The present invention is described in detail below with reference to various embodiments, but it should be understood that these embodiments are not intended to limit the present invention, and those skilled in the art should be able to make equivalent changes or substitutions in function, method, or structure based on these embodiments without departing from the scope of the present invention.
In the description of the present invention, it should be noted that, unless otherwise specified and limited, the terms "mounted," "connected," and "connected" are to be construed broadly, and may be, for example, mechanically or electrically connected, or two elements communicating with each other, directly or indirectly through an intermediate medium, and specific meanings of the terms may be understood by those skilled in the art according to specific situations.
The invention relates to a Tiancha star purple sand pug which comprises the following components in percentage by weight: 8 to 12 percent of red leather dragon purple sand raw ore, 25 to 35 percent of white clay purple sand raw ore, 15 to 20 percent of indigenous green clay purple sand raw ore, 15 to 20 percent of golden clay purple sand raw ore, 3 to 8 percent of white clay purple sand raw ore, 3 to 8 percent of rock red clay purple sand raw ore and 3 to 8 percent of green gray purple clay purple sand raw ore. In the invention, the novel pug disclosed by the invention is prepared by pre-firing raw purple sand pug, embodying the colors of different pugs at different firing temperatures and mixing pre-fired pug particles.
The preparation method of the Tiancha star purple sand pug comprises the following steps:
step (1), selecting materials: sorting the red leather dragon purple sand raw ore, the white clay purple sand raw ore, the Benshan green clay purple sand raw ore, the gold clay purple sand raw ore, the white clay purple sand raw ore, the red clay purple sand raw ore and the green gray purple clay purple sand raw ore one by one, and removing obvious impurities in the ore materials;
step (2), weathering: placing the sorted ore materials in open air in different areas, and naturally weathering for more than 3 months;
step (3), crushing: crushing the mineral aggregates one by utilizing a ring roller mill, and screening the crushed mineral aggregates;
and (4) purifying: purifying the mineral aggregate by a dry absorption method or a wet absorption method;
and (5) ageing: respectively adding clean water into the purified mineral aggregate obtained in the step (4), and uniformly stirring to form slurry, wherein the slurry is in a closed environment with the temperature of 15-20 ℃ and the relative humidity of 20-30% for 3-6 months;
step (6), pre-sintering: drying the red pitaya, the golden ball mud, the red mud and the green ash purple mud ore materials obtained in the step (5) into granules, and then sintering the granules in a kiln;
step (7), blending: fully mixing the fired purple sand particles with aged purple sand mineral aggregate according to the proportion;
step (8), pugging: repeatedly beating and extruding the pug mixed in the step (7) by using equipment; .
And (9) warehousing: and packaging the pug of the purple sand subjected to pugging and warehousing for later use.
The red leather dragon purple sand raw ore is yellow dragon mountain wild mountain red mud, and is prepared from 50.6% of SiO2, 20.6% of Al 2O3, 9.8% of Fe 2O3, 0.84% of CaO, 0.64% of MgO, 2.15% of K2O, 0.21% of Na2O and 0.82% of T iO. The yellow dragon mountain wild mountain red mud is produced at the lower part of a superficial yellow stone layer, the mineral aggregate is red brown compact block in appearance, is relatively hard, contains a certain amount of fine mica fragments, and has purple brown stripes, light green spots and stripe shapes, and rusty color and white waxy shapes on the surface.
The red leather dragon and red porcelain mineral aggregate in the step (3) is optimally screened into particles with 60 meshes, the firing temperature of the red leather dragon and red porcelain mineral aggregate in the step (6) is 1150-1165 ℃, and the firing time is 4-6 hours. The red leather dragon purple sand mineral aggregate particles after being fired are light brown.
The white clay purple sand raw ore is No. four mine white clay, and is prepared from 55-57% of SiO2, 19-22% of Al 2O3, 1.4% of Fe 2O3, 0.5-0.8% of CaO, 0.5-0.8% of MgO, 2-3% of K2O, 0.01-0.08% of Na2O and 1-1.2% of TiO. The appearance of the white clay purple sand raw ore is in a fusion symbiotic shape of green clay and purple clay, and the white clay purple sand raw ore is fragile and not hard. The cooked mud is fine and smooth, and has silt property during molding and manufacturing with good plasticity.
Optimally screening the white clay purple sand raw ore in the step (3) into 40-mesh particles.
The raw red porcelain ore of the mountain green mud is No. four mine green mud, and is prepared from 55-57% of SiO2, 2% of A l 2O3, 8-9% of Fe 2O3, 0.5-0.8% of CaO, 0.5-0.8% of MgO, 2-3% of K2O, 0.01-0.08% of Na2O and 1-1.2% of TiO. The raw ore of the mountain green mud purple sand has uniform and fine appearance texture, is light green compact block-shaped, has a slightly hard surface, has rusty color on the surface, is fine and smooth in cooked mud, and has silt property when being molded and manufactured with good plasticity.
In the step (3), the raw ore of the Benshan green mud purple sand is optimally screened into particles of 60 meshes.
The raw red porcelain ore of the gold group mud is the Huang Long mountain group mud, and is prepared from 55-57% of SiO2, 1.8% of Al 2O3, 8-9% of Fe 2O3, 0.5-0.8% of CaO, 0.5-0.8% of MgO, 2-3% of K2O, 0.01-0.08% of Na2O and 1-1.2% of TiO. The raw ore of the golden ball mud purple sand is produced in a superficial vermilion mud sticking layer, the ore content is low, and the appearance is in a symbiosis state of vermilion mud and green mud. The argillaceous block structure is softer breakable, has rusty color on the mineral aggregate, and ripe mud is more exquisite, and plasticity is good, and mud nature is heavier during the preparation.
The golden group mud purple sand mineral aggregate in the step (3) is optimally screened into particles of 60 meshes, and the firing temperature of the golden group mud purple sand mineral aggregate in the step (6) is 1135-1140 ℃, and the firing time is 4-6 hours. The yellow granules of the gold group mud purple sand ore material after being fired are red yellow, and the yellow granules are hidden on the surface.
The raw white clay purple sand ore is yellow Longshan white clay, and is prepared from 55-57% of SiO2, 19-22% of Al 2O3, 4-5% of Fe 2O3, 0.5-0.8% of CaO, 0.5-0.8% of MgO, 2-3% of K2O, 0.01-0.08% of Na2O and 1-1.2% of TiO. The product is produced in a superficial tope yellow stone layer, has light bluish white and grayish white compact blocks, is softer and fragile, contains a small amount of mica fragments, is fine and smooth in cooked mud, has general plasticity, and has silt property during molding and manufacturing.
And (4) optimally screening the white mud purple sand mineral aggregate in the step (3) into particles of 60 meshes.
The raw material of the red stoneware purple sand is yellow Longshan red stoneware, and is prepared from 56.3 percent of SiO2, 19 to 22 percent of Al 2O3, 8 to 9 percent of Fe 2O3, 0.5 to 0.8 percent of CaO, 0.5 to 0.8 percent of MgO, 2 to 3 percent of K2O, 0.01 to 0.08 percent of Na2O and 1 to 1.2 percent of TiO. The interlayer produced in the yellow stone rock stratum is produced in a multilayer shape, has uneven appearance texture, is dark red compact block, is as hard as stone, contains more mica fragments, has poor plasticity of cooked mud, is easy to crack and break during molding, has heavier sand property during manufacturing, and is not suitable for being molded independently.
In the step (3), the rock red mud purple sand mineral aggregate is optimally screened into particles of 60 meshes.
The green-gray purple mud is purple mud in a large pool mining area, and is prepared from 55-57% of SiO2, 19-22% of Al 2O3, 8-9% of Fe 2O3, 0.5-0.8% of CaO, 0.5-0.8% of MgO, 2-3% of K2O, 0.01-0.08% of Na2O and 1-1.2% of TiO. The Tianqing mud and the mineral layer are produced, the appearance of the Tianqing mud is in a grey purple brown compact block shape, the Tianqing mud is relatively hard, a small amount of fine white mica fragments are contained, the mineral aggregate is in a light green bean spot shape, and the surface of the mineral aggregate is in a texture shape.
The green-gray purple clay purple sand ore material in the step (3) is optimally screened into particles with 60 meshes, the firing temperature of the green-gray purple clay purple sand ore material in the step (6) is 1180-1185 ℃, and the firing time is 4-6 hours. The green-gray purple clay purple sand mineral aggregate particles after being fired are in a green gray color, and the surfaces of the green-gray purple clay purple sand mineral aggregate particles are pure and smooth.
Example one
The invention discloses a Tiancha star purple sand pug which comprises the following components in parts by weight:
example two
The invention discloses a Tiancha star purple sand pug which comprises the following components in parts by weight:
EXAMPLE III
The invention discloses a Tiancha star purple sand pug which comprises the following components in parts by weight:
according to the proportioning of the pug, the components of the three embodiments are proportioned, the plasticity of the mixture in the first embodiment and the third embodiment is optimal in the process of molding the cooked pug, and the plasticity of the mixture in the second embodiment is general due to the fact that the red stoneware raw ore accounts for a high proportion; in a firing test, the shrinkage rate of the second embodiment and the third embodiment is 5%, the shrinkage rate of the first embodiment is 6%, and the lower shrinkage rate can reduce the proportion of cracking deformation of a finished product in the kiln firing process, so that the yield can be improved; from the color after firing completion: in the third embodiment, the white mud is lighter in the ratio of the white mud to the white mud, and the rest of the dull red, yellow and dark cyan sand points are obviously displayed, and the quantity and the distribution are harmonious.
Compared with the prior art, the invention has the beneficial effects that: simple process, low shrinkage of the pug, high yield and rich color of the finished product after firing. In the invention, the novel pug disclosed by the invention is prepared by pre-firing raw purple sand pug, embodying the colors of different pugs at different firing temperatures and mixing pre-fired pug particles.
The foregoing describes only some embodiments of the present invention and modifications and variations thereof will be apparent to those skilled in the art without departing from the spirit and scope of the invention.
Claims (7)
1. The Tiancha star purple sand pug is characterized by comprising the following components in percentage by weight: 8 to 12 percent of red leather dragon purple sand raw ore, 25 to 35 percent of white clay purple sand raw ore, 15 to 20 percent of indigenous green clay purple sand raw ore, 15 to 20 percent of golden clay purple sand raw ore, 3 to 8 percent of white clay purple sand raw ore, 3 to 8 percent of rock red clay purple sand raw ore and 3 to 8 percent of green gray purple clay purple sand raw ore.
2. The Tiancha xing purple clay mud as claimed in claim 1, wherein the red pitaya red clay raw ore is yellow dragon mountain wild mountain red clay, and is made of 50.6% SiO2, 20.6% Al 2O3, 9.8% Fe 2O3, 0.84% CaO, 0.64% MgO, 2.15% K2O, 0.21% Na2O, and 0.82% TiO;
the white clay purple sand raw ore is No. four mine white clay, and is prepared from 55-57% of SiO2, 19-22% of Al 2O3, 1.4% of Fe 2O3, 0.5-0.8% of CaO, 0.5-0.8% of MgO, 2-3% of K2O, 0.01-0.08% of Na2O and 1-1.2% of TiO;
the raw red porcelain ore of the mountain green mud is No. four mine green mud, and is prepared from 55-57% of SiO2, 2% of Al 2O3, 8-9% of Fe 2O3, 0.5-0.8% of CaO, 0.5-0.8% of MgO, 2-3% of K2O, 0.01-0.08% of Na2O and 1-1.2% of TiO;
the gold group mud purple sand raw ore is yellow dragon mountain group mud, and is prepared from 55-57% of SiO2, 1.8% of Al 2O3, 8-9% of Fe 2O3, 0.5-0.8% of CaO, 0.5-0.8% of MgO, 2-3% of K2O, 0.01-0.08% of Na2O and 1-1.2% of TiO;
the raw white mud purple sand ore is yellow Longshan white mud, and is prepared from 55-57% of SiO2, 19-22% of Al 2O3, 4-5% of Fe 2O3, 0.5-0.8% of CaO, 0.5-0.8% of MgO, 2-3% of K2O, 0.01-0.08% of Na2O and 1-1.2% of TiO;
the raw material of the red stoneware purple sand is yellow Longshan red mud, and is prepared from 56.3 percent of SiO2, 19 to 22 percent of Al 2O3, 8 to 9 percent of Fe 2O3, 0.5 to 0.8 percent of CaO, 0.5 to 0.8 percent of MgO, 2 to 3 percent of K2O, 0.01 to 0.08 percent of Na2O and 1 to 1.2 percent of TiO;
the blue-gray purple mud is purple mud in a large pool mining area, and is prepared from 55-57% of SiO2, 19-22% of Al 2O3, 8-9% of Fe 2O3, 0.5-0.8% of CaO, 0.5-0.8% of MgO, 2-3% of K2O, 0.01-0.08% of Na2O and 1-1.2% of TiO.
3. The preparation method of Tiancha xing purple sand pug as claimed in claim 1, which is characterized by comprising the following steps:
step (1), selecting materials: sorting the red leather dragon purple sand raw ore, the white clay purple sand raw ore, the indigenous green clay purple sand raw ore, the gold clay purple sand raw ore, the white clay purple sand raw ore, the red clay purple sand raw ore and the green gray purple clay purple sand raw ore one by one, and removing obvious impurities in the raw ore;
step (2), weathering: placing the sorted ore materials in open air in different areas, and naturally weathering for more than 3 months;
step (3), crushing: crushing the mineral aggregates one by utilizing a ring roller mill, and screening the crushed mineral aggregates;
and (4) purifying: purifying the mineral aggregate by a dry absorption method or a wet absorption method;
and (5) ageing: respectively adding clean water into the purified mineral aggregate obtained in the step (4), and uniformly stirring to form slurry, wherein the slurry is in a closed environment with the temperature of 15-20 ℃ and the relative humidity of 20-30% for 3-6 months;
step (6), pre-sintering: drying the red pitaya, the golden ball mud, the red mud and the green ash purple mud ore materials obtained in the step (5) into granules, and then sintering the granules in a kiln;
step (7), blending: fully mixing the fired purple sand particles with the aged purple sand mineral aggregate according to the proportion;
step (8), pugging: repeatedly beating and extruding the pug mixed in the step (7) by using equipment; .
And (9) warehousing: and packaging the pug of the purple sand subjected to pugging and warehousing for later use.
4. The preparation method of Tiancha xing purple sand pug as claimed in claim 3, wherein the firing temperature of the red leather dragon purple sand mineral aggregate in the step (6) is 1150-1165 ℃ and the firing time is 4-6 hours.
5. The preparation method of Tiancha xing purple sand pug as claimed in claim 3, wherein the firing temperature of the gold group pug purple sand mineral aggregate in the step (6) is 1135 ℃ to 1140 ℃ and the firing time is 4 to 6 hours.
6. The preparation method of Tiancha xing purple sand pug as claimed in claim 3, wherein the firing temperature of the red mud purple sand mineral aggregate in the step (6) is 1160-1165 ℃ and the firing time is 4-6 hours.
7. The preparation method of Tiancha xing purple sand pug as claimed in claim 3, wherein the firing temperature of the lime purple sand ore material in the step (6) is 1180-1185 ℃ and the firing time is 4-6 hours.
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