CN114272181B - Moisturizing and skin-tendering mask and preparation method thereof - Google Patents
Moisturizing and skin-tendering mask and preparation method thereof Download PDFInfo
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- CN114272181B CN114272181B CN202210101093.1A CN202210101093A CN114272181B CN 114272181 B CN114272181 B CN 114272181B CN 202210101093 A CN202210101093 A CN 202210101093A CN 114272181 B CN114272181 B CN 114272181B
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- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 claims description 26
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- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims description 25
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- Cosmetics (AREA)
Abstract
The invention discloses a moisturizing and skin-tendering mask and a preparation method thereof, and particularly relates to the technical field of masks. The invention can effectively improve the antibacterial performance of the moisturizing and skin-tendering mask, can effectively sterilize bacteria on the surface of the mask, and simultaneously ensures the antibacterial performance of the mask under illumination conditions, thereby avoiding the reduction of the antibacterial performance of the mask after illumination; after the silver nitrate is subjected to blending and compounding treatment on the polyvinyl alcohol, the starch and the resveratrol, electrostatic spinning is performed on the surface of the non-woven fabric base fabric to form nano composite fibers, so that nano silver can be effectively compounded into the nano composite fibers, and the nano silver particles perform antibacterial treatment on the mask by taking the nano composite fibers as carriers, so that the antibacterial treatment effect of the mask is further enhanced; the chitosan and gelatin are mixed and mixed into the mask liquid, so that the antibacterial performance of the mask can be further enhanced, the contact and combination effects of the mask liquid and the non-woven fabric base cloth are enhanced, and the utilization rate of the mask liquid is ensured.
Description
Technical Field
The invention relates to the technical field of masks, in particular to a moisturizing and skin-tendering mask and a preparation method thereof.
Background
The facial mask is a skin care product for moisturizing skin, and also has multiple functions of moisturizing, nourishing, improving appearance, deep cleaning and the like. The facial mask is covered on the horny layer of the skin to provide moisture for the horny layer, so that the horny layer is fully hydrated, thereby improving the appearance and elasticity of the skin. The mask can be classified into a mask type: peeling, wiping or washing, peeling after solidification and main stream sticking in the market; wherein paste cloth formula facial mask includes: two forms of gel-containing non-woven fabric sticking cloth type and dipping non-woven fabric sticking cloth type facial masks; the gel-containing non-woven fabric sticking cloth is formed by coating a layer of gel-type preparation on the surface of the non-woven fabric, cutting the non-woven fabric into a face shape, and sealing the face shape in a package; impregnated nonwoven masks are more commonly used, and are made by impregnating nonwoven with a mask solution.
The existing moisturizing and skin-tendering mask has poor antibacterial performance, and particularly the antibacterial performance of the mask is further reduced after the external package of the mask is subjected to illumination.
Disclosure of Invention
In order to overcome the defects in the prior art, the embodiment of the invention provides a moisturizing and skin-tendering mask and a preparation method thereof.
The moisturizing and skin-tendering mask comprises non-woven fabric base cloth, a supplement and mask liquid, wherein the supplement, the non-woven fabric base cloth and the mask liquid are in part by weight: 1:120-160:400-500.
Further, the supplement comprises the following components in percentage by weight: 19.60-20.60% of polyvinyl alcohol, 2.60-3.60% of silk peptide, 2.40-3.40% of hyaluronic acid, 3.60-4.60% of silver nitrate, 3.40-4.40% of starch, 19.40-20.40% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.40 to 3.40 percent of ginsenoside, 2.40 to 3.40 percent of pilose antler peptide, 1.80 to 2.80 percent of sodium hyaluronate, 4.60 to 5.60 percent of cod collagen, 0.8 to 1.2 percent of croaker alcohol extract, 0.8 to 1.2 percent of marathon alcohol extract, 9.60 to 10.60 percent of chitosan, 14.40 to 15.40 percent of gelatin and the balance of deionized water.
Further, the supplement, the non-woven fabric base cloth and the mask liquid are prepared from the following components in parts by weight: 1:120:400; the supplement comprises the following components in percentage by weight: 19.60% of polyvinyl alcohol, 2.60% of silk peptide, 2.40% of hyaluronic acid, 3.60% of silver nitrate, 3.40% of starch, 19.40% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.40% of ginsenoside, 2.40% of pilose antler peptide, 1.80% of sodium hyaluronate, 4.60% of cod collagen, 0.8% of croaker alcohol extract, 0.8% of malassezia alcohol extract, 9.60% of chitosan, 14.40% of gelatin and the balance of deionized water.
Further, the supplement, the non-woven fabric base cloth and the mask liquid are prepared from the following components in parts by weight: 1:160:500; the supplement comprises the following components in percentage by weight: 20.60% of polyvinyl alcohol, 3.60% of silk peptide, 3.40% of hyaluronic acid, 4.60% of silver nitrate, 4.40% of starch, 20.40% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 3.40% of ginsenoside, 3.40% of pilose antler peptide, 2.80% of sodium hyaluronate, 5.60% of cod collagen, 1.2% of croaker alcohol extract, 1.2% of malassezia alcohol extract, 10.60% of chitosan, 15.40% of gelatin and the balance of deionized water.
Further, the supplement, the non-woven fabric base cloth and the mask liquid are prepared from the following components in parts by weight: 1:140:450; the supplement comprises the following components in percentage by weight: 20.10% of polyvinyl alcohol, 3.10% of silk peptide, 2.90% of hyaluronic acid, 4.10% of silver nitrate, 3.90% of starch, 19.90% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.90% of ginsenoside, 2.90% of pilose antler peptide, 2.30% of sodium hyaluronate, 5.10% of cod collagen, 1.0% of croaker alcohol extract, 1.0% of malassezia alcohol extract, 10.10% of chitosan, 14.90% of gelatin and the balance of deionized water.
A preparation method of a moisturizing and skin-tendering mask comprises the following specific preparation steps:
Step one: according to the weight parts, the raw materials of the non-woven fabric base cloth, the supplement agent comprise polyvinyl alcohol, silk peptide, hyaluronic acid, silver nitrate, starch, resveratrol, deionized water and ginsenoside, pilose antler peptide, sodium hyaluronate, cod collagen, the extraction liquid of the crotalaria sinica, the extraction liquid of the marylalcohol, chitosan, gelatin and deionized water;
Step two: raw materials of the supplement are as follows: polyvinyl alcohol, silk peptide, hyaluronic acid, silver nitrate, starch, resveratrol and deionized water are blended, and the premix is obtained after water bath ultrasonic treatment for 20 to 30 minutes;
step three: performing ultrasonic treatment on the premix prepared in the second step for 10-30 minutes to obtain spinning solution;
step four: taking the non-woven fabric base cloth in the first step as a receiving matrix, and forming a nanofiber-shaped supplement on the surface of the non-woven fabric base cloth in the third step in an electrostatic spinning mode to obtain the composite mask base cloth;
step five: raw materials of the mask liquid are as follows: mixing ginsenoside, pilose antler peptide, sodium hyaluronate, cod collagen, a croaker alcohol extract, a marmalade alcohol extract, chitosan, gelatin and deionized water, and performing water bath ultrasonic treatment for 20-30 minutes to obtain a mask liquid;
Step six: immersing the composite mask base cloth prepared in the fourth step into the mask liquid prepared in the fifth step, and carrying out ultrasonic treatment for 5-10 minutes to obtain the moisturizing and skin-tendering mask.
Further, in the second step, the water bath temperature is 50-60 ℃, the ultrasonic treatment frequency is 25-29 KHz, and the power is 1250-1350W; in the third step, the ultrasonic treatment frequency is 1.8-2.0 MHz, and the power is 300-400W; in the fourth step, the spinning voltage is 22 KV to 24KV, the liquid feeding rate is 0.5 mL/h to 0.6mL/h, and the receiving distance is 15cm to 17cm; in the fifth step, the water bath temperature is 40-50 ℃, the ultrasonic treatment frequency is 23-25 KHz, and the power is 1250-1350W; in the sixth step, the ultrasonic treatment frequency is 1.6-1.8 MHz, and the power is 300-400W.
Further, in the second step, the water bath temperature is 50 ℃, the ultrasonic treatment frequency is 25KHz, and the power is 1250W; in the third step, the ultrasonic processing frequency is 1.8MHz, and the power is 300W; in the fourth step, the spinning voltage is 22KV, the liquid feeding rate is 0.5mL/h, and the receiving distance is 15cm; in the fifth step, the water bath temperature is 40 ℃, the ultrasonic treatment frequency is 23KHz, and the power is 1250W; in step six, the ultrasonic treatment frequency is 1.6MHz and the power is 300W.
Further, in the second step, the water bath temperature is 60 ℃, the ultrasonic treatment frequency is 29KHz, and the power is 1350W; in the third step, the ultrasonic processing frequency is 2.0MHz, and the power is 400W; in the fourth step, the spinning voltage is 24KV, the liquid feeding rate is 0.6mL/h, and the receiving distance is 17cm; in the fifth step, the water bath temperature is 50 ℃, the ultrasonic treatment frequency is 25KHz, and the power is 1350W; in step six, the ultrasonic treatment frequency is 1.8MHz and the power is 400W.
Further, in the second step, the water bath temperature is 55 ℃, the ultrasonic treatment frequency is 27KHz, and the power is 1300W; in the third step, the ultrasonic processing frequency is 1.9MHz, and the power is 350W; in the fourth step, the spinning voltage is 23KV, the liquid feeding rate is 0.55mL/h, and the receiving distance is 16cm; in the fifth step, the water bath temperature is 45 ℃, the ultrasonic treatment frequency is 24KHz, and the power is 1300W; in step six, the ultrasonic treatment frequency is 1.7MHz and the power is 350W.
The invention has the technical effects and advantages that:
1. The moisturizing and skin-tendering mask prepared by adopting the raw material formula can effectively improve the antibacterial performance of the moisturizing and skin-tendering mask, can effectively sterilize bacteria on the surface of the mask, and can ensure the antibacterial performance of the mask under the illumination condition, so that the reduction of the antibacterial performance of the mask after illumination is avoided; the supplement is prepared by blending polyvinyl alcohol, silk peptide and hyaluronic acid on the surface of a non-woven fabric base fabric to form nano composite fibers through electrostatic spinning, so that the moisturizing and skin tendering performances of the mask can be effectively ensured, the skin-friendly effect is better, and the mask application effect is good; after the blending and compounding treatment of the polyvinyl alcohol, the starch and the resveratrol, the nano-composite fiber is formed on the surface of the non-woven fabric base cloth by electrostatic spinning, so that the nano-silver can be effectively compounded into the nano-composite fiber, the antibacterial effect of the mask is further effectively enhanced, the water vapor light transmittance coefficient and the moisture absorption performance of the mask are ensured, the nano-silver particles perform antibacterial treatment on the mask by taking the nano-composite fiber as a carrier, and the antibacterial treatment effect of the mask is further enhanced; the facial mask liquid is prepared by mixing and compounding ginsenoside, pilose antler peptide, sodium hyaluronate and cod collagen, and is rapidly compounded under ultrasonic treatment, so that the ultraviolet resistance and ageing resistance of the facial mask can be effectively ensured; the chitosan and gelatin are mixed and mixed into the mask liquid, so that the antibacterial performance of the mask can be further enhanced, the contact and combination effect of the mask liquid and the non-woven fabric base cloth is enhanced, and the utilization rate of the mask liquid is ensured;
2. In the process of preparing the moisturizing and skin-tendering mask, in the second step, the polyvinyl alcohol, the silk peptide, the hyaluronic acid, the silver nitrate, the starch and the resveratrol can be effectively subjected to rapid reaction compounding, so that the reaction process is accelerated; in the third step, the uniform dispersion of materials in the spinning solution can be effectively ensured, and the more uniform effective substances in the nano composite fiber generated by the subsequent electrostatic spinning treatment can be ensured; in the fourth step, the antibacterial enhancement and supplementation effect of the supplement on the mask can be effectively enhanced; in the fifth step, the rapid reaction and compounding are carried out under the ultrasonic treatment of 23KHz at 40 ℃ to accelerate the reaction process; in the sixth step, the composite mask base cloth is immersed into the mask liquid and subjected to ultrasonic treatment at 1.7MHz, so that the active ingredients in the mask liquid are ensured to be rapidly compounded with the composite mask base cloth, and the moisturizing and skin tendering effects and the antibacterial effects of the mask are further enhanced.
Detailed Description
The following description will clearly and fully describe the technical solutions of the embodiments of the present invention, and it is apparent that the described embodiments are only some embodiments of the present invention, not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Example 1:
the invention provides a moisturizing and skin-tendering mask which comprises non-woven fabric base cloth, a supplement and mask liquid, wherein the supplement, the non-woven fabric base cloth and the mask liquid are in parts by weight: 1:120:400; the supplement comprises the following components in percentage by weight: 19.60% of polyvinyl alcohol, 2.60% of silk peptide, 2.40% of hyaluronic acid, 3.60% of silver nitrate, 3.40% of starch, 19.40% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.40% of ginsenoside, 2.40% of pilose antler peptide, 1.80% of sodium hyaluronate, 4.60% of cod collagen, 0.8% of croaker alcohol extract, 0.8% of malassezia alcohol extract, 9.60% of chitosan, 14.40% of gelatin and the balance of deionized water;
the invention also provides a preparation method of the moisturizing and skin-tendering mask, which comprises the following specific preparation steps:
Step one: according to the weight parts, the raw materials of the non-woven fabric base cloth, the supplement agent comprise polyvinyl alcohol, silk peptide, hyaluronic acid, silver nitrate, starch, resveratrol, deionized water and ginsenoside, pilose antler peptide, sodium hyaluronate, cod collagen, the extraction liquid of the crotalaria sinica, the extraction liquid of the marylalcohol, chitosan, gelatin and deionized water;
step two: raw materials of the supplement are as follows: polyvinyl alcohol, silk peptide, hyaluronic acid, silver nitrate, starch, resveratrol and deionized water are blended, and water bath ultrasonic treatment is carried out for 20 minutes to obtain premix;
step three: performing ultrasonic treatment on the premix prepared in the second step for 10 minutes to obtain spinning solution;
step four: taking the non-woven fabric base cloth in the first step as a receiving matrix, and forming a nanofiber-shaped supplement on the surface of the non-woven fabric base cloth in the third step in an electrostatic spinning mode to obtain the composite mask base cloth;
Step five: raw materials of the mask liquid are as follows: mixing ginsenoside, cornu Cervi Pantotrichum peptide, sodium hyaluronate, cod collagen, ethanol extract of Rhynchosia volubilis, ethanol extract of Maryland, chitosan, gelatin and deionized water, and performing ultrasonic treatment in water bath for 20min to obtain facial mask solution;
step six: and (3) immersing the composite mask base cloth prepared in the step (IV) into the mask liquid prepared in the step (V), and carrying out ultrasonic treatment for 5 minutes to obtain the moisturizing and skin-tendering mask.
In the second step, the water bath temperature is 50 ℃, the ultrasonic treatment frequency is 25KHz, and the power is 1250W; in the third step, the ultrasonic processing frequency is 1.8MHz, and the power is 300W; in the fourth step, the spinning voltage is 22KV, the liquid feeding rate is 0.5mL/h, and the receiving distance is 15cm; in the fifth step, the water bath temperature is 40 ℃, the ultrasonic treatment frequency is 23KHz, and the power is 1250W; in step six, the ultrasonic treatment frequency is 1.6MHz and the power is 300W.
Example 2:
Unlike example 1, the supplement, the non-woven fabric base cloth and the mask liquid are in parts by weight: 1:160:500; the supplement comprises the following components in percentage by weight: 20.60% of polyvinyl alcohol, 3.60% of silk peptide, 3.40% of hyaluronic acid, 4.60% of silver nitrate, 4.40% of starch, 20.40% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 3.40% of ginsenoside, 3.40% of pilose antler peptide, 2.80% of sodium hyaluronate, 5.60% of cod collagen, 1.2% of croaker alcohol extract, 1.2% of malassezia alcohol extract, 10.60% of chitosan, 15.40% of gelatin and the balance of deionized water.
Example 3:
Different from the embodiment 1-2, the supplement, the non-woven fabric base cloth and the mask liquid are prepared from the following components in parts by weight: 1:140:450; the supplement comprises the following components in percentage by weight: 20.10% of polyvinyl alcohol, 3.10% of silk peptide, 2.90% of hyaluronic acid, 4.10% of silver nitrate, 3.90% of starch, 19.90% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.90% of ginsenoside, 2.90% of pilose antler peptide, 2.30% of sodium hyaluronate, 5.10% of cod collagen, 1.0% of croaker alcohol extract, 1.0% of malassezia alcohol extract, 10.10% of chitosan, 14.90% of gelatin and the balance of deionized water.
The moisturizing and tendering mask prepared in the above examples 1 to 3 and the moisturizing and tendering mask of the first control group, the moisturizing and tendering mask of the second control group, the moisturizing and tendering mask of the third control group, the moisturizing and tendering mask of the fourth control group, the moisturizing and tendering mask of the fifth control group and the moisturizing and tendering mask of the sixth control group are respectively taken, the moisturizing and tendering mask of the first control group and the polyvinyl alcohol of the third control group are respectively compared with the polyvinyl alcohol of the third control group, the moisturizing and tendering mask of the second control group and the silver nitrate is not compared with the third control group, the moisturizing and tendering mask of the third control group and the starch is not compared with the third control group, the moisturizing and tendering mask of the fourth control group and the alcohol extract of the third control group are respectively tested, the moisturizing and tendering mask of the sixth control group and the chitosan is respectively tested with the third control group and the fourth control group, each moisturizing and tendering mask of the third control group and the fourth control group is respectively tested with the third control group and the fourth control group, and the fifth control group are respectively tested, and the moisturizing and tendering mask is 30; the test results are shown in Table one:
Table one:
As shown in the first table, when the moisturizing and skin-tendering mask comprises the following raw materials in proportion: the supplement, the non-woven fabric base cloth and the mask liquid are prepared from the following components in parts by weight: 1:140:450; the supplement comprises the following components in percentage by weight: 20.10% of polyvinyl alcohol, 3.10% of silk peptide, 2.90% of hyaluronic acid, 4.10% of silver nitrate, 3.90% of starch, 19.90% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.90% of ginsenoside, 2.90% of pilose antler peptide, 2.30% of sodium hyaluronate, 5.10% of cod collagen, 1.0% of croaker alcohol extract, 1.0% of marylalcohol extract, 10.10% of chitosan, 14.90% of gelatin and the balance of deionized water, the antibacterial performance of the moisturizing and skin-tendering facial mask can be effectively improved, bacteria on the surface of the facial mask can be effectively sterilized, and meanwhile, the antibacterial performance of the facial mask is guaranteed under the illumination condition, so that the reduction of the antibacterial performance of the facial mask after illumination is avoided; example 3 is a preferred embodiment of the invention, the supplement is prepared by blending polyvinyl alcohol, silk peptide and hyaluronic acid on the surface of a non-woven fabric base fabric to form nano composite fibers through electrostatic spinning, so that the moisturizing and skin tendering performances of the mask can be effectively ensured, the skin-friendly effect is better, and the mask application effect is good; after the blending and compounding treatment of the polyvinyl alcohol, the starch and the resveratrol, the nano-composite fiber is formed on the surface of the non-woven fabric base cloth by electrostatic spinning, so that the nano-silver can be effectively compounded into the nano-composite fiber, the antibacterial effect of the mask is further effectively enhanced, the water vapor light transmittance coefficient and the moisture absorption performance of the mask are ensured, the nano-silver particles perform antibacterial treatment on the mask by taking the nano-composite fiber as a carrier, and the antibacterial treatment effect of the mask is further enhanced; the facial mask liquid is prepared by mixing and compounding ginsenoside, pilose antler peptide, sodium hyaluronate and cod collagen, and is rapidly compounded under ultrasonic treatment, so that the ultraviolet resistance and ageing resistance of the facial mask can be effectively ensured; the alcohol extract of the large-leaf holly can effectively improve the antibacterial, anti-ultraviolet and oxidation resistance of the mask; the maryland alcohol extract has the effects of clearing heat and detoxicating, cooling blood and stopping bleeding, promoting diuresis and relieving swelling, and can effectively strengthen the antibacterial effect of the mask; the chitosan and gelatin are mixed and mixed into the mask liquid, so that the antibacterial performance of the mask can be further enhanced, the contact and combination effect of the mask liquid and the non-woven fabric base cloth is enhanced, and the utilization rate of the mask liquid is ensured; the chitosan and the ginsenoside are compounded, so that the antibacterial effect of the facial mask can be further enhanced, and the protection effect of the facial mask on the skin using the facial mask is improved; the chitosan and the sodium hyaluronate are compounded, so that the repairing effect of the mask on the skin can be effectively enhanced.
Example 4:
The invention provides a moisturizing and skin-tendering mask which comprises non-woven fabric base cloth, a supplement and mask liquid, wherein the supplement, the non-woven fabric base cloth and the mask liquid are in parts by weight: 1:140:450; the supplement comprises the following components in percentage by weight: 20.10% of polyvinyl alcohol, 3.10% of silk peptide, 2.90% of hyaluronic acid, 4.10% of silver nitrate, 3.90% of starch, 19.90% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.90% of ginsenoside, 2.90% of pilose antler peptide, 2.30% of sodium hyaluronate, 5.10% of cod collagen, 1.0% of croaker alcohol extract, 1.0% of malassezia alcohol extract, 10.10% of chitosan, 14.90% of gelatin and the balance of deionized water;
the invention also provides a preparation method of the moisturizing and skin-tendering mask, which comprises the following specific preparation steps:
Step one: according to the weight parts, the raw materials of the non-woven fabric base cloth, the supplement agent comprise polyvinyl alcohol, silk peptide, hyaluronic acid, silver nitrate, starch, resveratrol, deionized water and ginsenoside, pilose antler peptide, sodium hyaluronate, cod collagen, the extraction liquid of the crotalaria sinica, the extraction liquid of the marylalcohol, chitosan, gelatin and deionized water;
Step two: raw materials of the supplement are as follows: polyvinyl alcohol, silk peptide, hyaluronic acid, silver nitrate, starch, resveratrol and deionized water are blended, and water bath ultrasonic treatment is carried out for 25 minutes to obtain premix;
step three: performing ultrasonic treatment on the premix prepared in the second step for 20 minutes to obtain spinning solution;
step four: taking the non-woven fabric base cloth in the first step as a receiving matrix, and forming a nanofiber-shaped supplement on the surface of the non-woven fabric base cloth in the third step in an electrostatic spinning mode to obtain the composite mask base cloth;
Step five: raw materials of the mask liquid are as follows: mixing ginsenoside, cornu Cervi Pantotrichum peptide, sodium hyaluronate, cod collagen, ethanol extract of Rhynchosia volubilis, ethanol extract of Maryland, chitosan, gelatin and deionized water, and performing ultrasonic treatment in water bath for 25 min to obtain facial mask solution;
Step six: and (3) immersing the composite mask base cloth prepared in the step (IV) into the mask liquid prepared in the step (V), and carrying out ultrasonic treatment for 7 minutes to obtain the moisturizing and skin-tendering mask.
In the second step, the water bath temperature is 50 ℃, the ultrasonic treatment frequency is 25KHz, and the power is 1250W; in the third step, the ultrasonic processing frequency is 1.8MHz, and the power is 300W; in the fourth step, the spinning voltage is 22KV, the liquid feeding rate is 0.5mL/h, and the receiving distance is 15cm; in the fifth step, the water bath temperature is 40 ℃, the ultrasonic treatment frequency is 23KHz, and the power is 1250W; in step six, the ultrasonic treatment frequency is 1.6MHz and the power is 300W.
Example 5:
Unlike example 4, in step two, the water bath temperature was 60 ℃, the ultrasonic treatment frequency was 29KHz, and the power was 1350W; in the third step, the ultrasonic processing frequency is 2.0MHz, and the power is 400W; in the fourth step, the spinning voltage is 24KV, the liquid feeding rate is 0.6mL/h, and the receiving distance is 17cm; in the fifth step, the water bath temperature is 50 ℃, the ultrasonic treatment frequency is 25KHz, and the power is 1350W; in step six, the ultrasonic treatment frequency is 1.8MHz and the power is 400W.
Example 6:
Unlike examples 4-5, in step two, the water bath temperature was 55deg.C, the ultrasonic treatment frequency was 27KHz, and the power was 1300W; in the third step, the ultrasonic processing frequency is 1.9MHz, and the power is 350W; in the fourth step, the spinning voltage is 23KV, the liquid feeding rate is 0.55mL/h, and the receiving distance is 16cm; in the fifth step, the water bath temperature is 45 ℃, the ultrasonic treatment frequency is 24KHz, and the power is 1300W; in step six, the ultrasonic treatment frequency is 1.7MHz and the power is 350W.
The moisturizing and tendering mask prepared in examples 4 to 6 above was taken separately from the moisturizing and tendering mask of control group seven, the moisturizing and tendering mask of control group eight, the moisturizing and tendering mask of control group nine and the moisturizing and tendering mask of control group ten, the moisturizing and tendering mask of control group seven was compared with example six without the operation of water bath ultrasonic treatment in step three, the moisturizing and tendering mask of control group eight was compared with example six without the operation of water bath ultrasonic treatment in step four, the moisturizing and tendering mask of control group nine was compared with example six without the operation of water bath ultrasonic treatment in step five, the moisturizing and tendering mask of control group ten was compared with example six without the operation of ultrasonic treatment in step six, the moisturizing and tendering mask prepared in three examples and the moisturizing and tendering mask of four control groups were tested separately, each control group and example produced 30 sets of moisturizing and tendering masks, and the test results were shown in table two:
and (II) table:
As can be seen from Table II, example 6 is a preferred embodiment of the present invention; in the second step, the polyvinyl alcohol, the silk peptide, the hyaluronic acid, the silver nitrate, the starch, the resveratrol and the deionized water are subjected to ultrasonic treatment at 55 ℃ and 27KHz, so that the polyvinyl alcohol, the silk peptide, the hyaluronic acid, the silver nitrate, the starch and the resveratrol can be subjected to rapid reaction and compounding, and the reaction process is accelerated; in the third step, the premix is treated under 1.9MHz ultrasonic treatment, so that the uniform dispersion of materials in the spinning solution can be effectively ensured, and the more uniform effective substances in the nano composite fiber generated by the subsequent electrostatic spinning treatment can be ensured; in the fourth step, the spinning solution is compounded on the surface of the non-woven fabric base cloth in an electrostatic spinning mode, so that the antibacterial enhancement and supplementation effect of the supplement on the mask can be effectively enhanced; in the fifth step, ginsenoside, pilose antler peptide, sodium hyaluronate, cod collagen, milpa alcohol extract, maryland alcohol extract, chitosan, gelatin and deionized water are subjected to rapid reaction and compounding under the ultrasonic treatment of 23KHz at 40 ℃ to accelerate the reaction process; in the sixth step, the composite mask base cloth is immersed into the mask liquid and subjected to ultrasonic treatment at 1.7MHz, so that the active ingredients in the mask liquid are ensured to be rapidly compounded with the composite mask base cloth, and the moisturizing and skin tendering effects and the antibacterial effects of the mask are further enhanced.
It is noted that relational terms such as first and second, and the like are used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Moreover, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Finally, it should be noted that: the foregoing description is only a preferred embodiment of the present invention, and the present invention is not limited thereto, but it is to be understood that modifications and equivalents of some of the technical features described in the foregoing embodiments may be made by those skilled in the art, although the present invention has been described in detail with reference to the foregoing embodiments. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (9)
1. A moisturizing and skin-rejuvenating mask is characterized in that: the face mask comprises non-woven fabric base cloth, a supplement and face mask liquid, wherein the supplement, the non-woven fabric base cloth and the face mask liquid are in weight part ratio: 1:120-160:400-500; the supplement comprises the following components in percentage by weight: 19.60-20.60% of polyvinyl alcohol, 2.60-3.60% of silk peptide, 2.40-3.40% of hyaluronic acid, 3.60-4.60% of silver nitrate, 3.40-4.40% of starch, 19.40-20.40% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.40 to 3.40 percent of ginsenoside, 2.40 to 3.40 percent of pilose antler peptide, 1.80 to 2.80 percent of sodium hyaluronate, 4.60 to 5.60 percent of cod collagen, 0.8 to 1.2 percent of croaker alcohol extract, 0.8 to 1.2 percent of marathon alcohol extract, 9.60 to 10.60 percent of chitosan, 14.40 to 15.40 percent of gelatin and the balance of deionized water.
2. The moisturizing and skin-rejuvenating mask as recited in claim 1, wherein: the supplement, the non-woven fabric base cloth and the mask liquid are prepared from the following components in parts by weight: 1:120:400; the supplement comprises the following components in percentage by weight: 19.60% of polyvinyl alcohol, 2.60% of silk peptide, 2.40% of hyaluronic acid, 3.60% of silver nitrate, 3.40% of starch, 19.40% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.40% of ginsenoside, 2.40% of pilose antler peptide, 1.80% of sodium hyaluronate, 4.60% of cod collagen, 0.8% of croaker alcohol extract, 0.8% of malassezia alcohol extract, 9.60% of chitosan, 14.40% of gelatin and the balance of deionized water.
3. The moisturizing and skin-rejuvenating mask as recited in claim 1, wherein: the supplement, the non-woven fabric base cloth and the mask liquid are prepared from the following components in parts by weight: 1:160:500; the supplement comprises the following components in percentage by weight: 20.60% of polyvinyl alcohol, 3.60% of silk peptide, 3.40% of hyaluronic acid, 4.60% of silver nitrate, 4.40% of starch, 20.40% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 3.40% of ginsenoside, 3.40% of pilose antler peptide, 2.80% of sodium hyaluronate, 5.60% of cod collagen, 1.2% of croaker alcohol extract, 1.2% of malassezia alcohol extract, 10.60% of chitosan, 15.40% of gelatin and the balance of deionized water.
4. The moisturizing and skin-rejuvenating mask as recited in claim 1, wherein: the supplement, the non-woven fabric base cloth and the mask liquid are prepared from the following components in parts by weight: 1:140:450; the supplement comprises the following components in percentage by weight: 20.10% of polyvinyl alcohol, 3.10% of silk peptide, 2.90% of hyaluronic acid, 4.10% of silver nitrate, 3.90% of starch, 19.90% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.90% of ginsenoside, 2.90% of pilose antler peptide, 2.30% of sodium hyaluronate, 5.10% of cod collagen, 1.0% of croaker alcohol extract, 1.0% of malassezia alcohol extract, 10.10% of chitosan, 14.90% of gelatin and the balance of deionized water.
5. A preparation method of a moisturizing and skin-tendering mask is characterized by comprising the following steps: the preparation method comprises the following specific steps:
Step one: according to the weight parts, the raw materials of the non-woven fabric base cloth, the supplement agent comprise polyvinyl alcohol, silk peptide, hyaluronic acid, silver nitrate, starch, resveratrol, deionized water and ginsenoside, pilose antler peptide, sodium hyaluronate, cod collagen, the extraction liquid of the crotalaria sinica, the extraction liquid of the marylalcohol, chitosan, gelatin and deionized water;
Step two: raw materials of the supplement are as follows: polyvinyl alcohol, silk peptide, hyaluronic acid, silver nitrate, starch, resveratrol and deionized water are blended, and the premix is obtained after water bath ultrasonic treatment for 20 to 30 minutes;
step three: performing ultrasonic treatment on the premix prepared in the second step for 10-30 minutes to obtain spinning solution;
step four: taking the non-woven fabric base cloth in the first step as a receiving matrix, and forming a nanofiber-shaped supplement on the surface of the non-woven fabric base cloth in the third step in an electrostatic spinning mode to obtain the composite mask base cloth;
step five: raw materials of the mask liquid are as follows: mixing ginsenoside, pilose antler peptide, sodium hyaluronate, cod collagen, a croaker alcohol extract, a marmalade alcohol extract, chitosan, gelatin and deionized water, and performing water bath ultrasonic treatment for 20-30 minutes to obtain a mask liquid;
Step six: immersing the composite mask base cloth prepared in the fourth step into the mask liquid prepared in the fifth step, and carrying out ultrasonic treatment for 5-10 minutes to obtain the moisturizing and skin-tendering mask.
6. The method for preparing the moisturizing and skin-rejuvenating mask according to claim 5, wherein the method comprises the following steps: in the second step, the water bath temperature is 50-60 ℃, the ultrasonic treatment frequency is 25-29 KHz, and the power is 1250-1350W; in the third step, the ultrasonic treatment frequency is 1.8-2.0 MHz, and the power is 300-400W; in the fourth step, the spinning voltage is 22 KV to 24KV, the liquid feeding rate is 0.5 mL/h to 0.6mL/h, and the receiving distance is 15 cm to 17cm; in the fifth step, the water bath temperature is 40-50 ℃, the ultrasonic treatment frequency is 23-25 KHz, and the power is 1250-1350W; in the sixth step, the ultrasonic treatment frequency is 1.6-1.8 MHz, and the power is 300-400W.
7. The method for preparing the moisturizing and skin-rejuvenating mask according to claim 6, wherein the method comprises the following steps: in the second step, the water bath temperature is 50 ℃, the ultrasonic treatment frequency is 25KHz, and the power is 1250W; in the third step, the ultrasonic treatment frequency is 1.8MHz, and the power is 300W; in the fourth step, the spinning voltage is 22KV, the liquid feeding rate is 0.5mL/h, and the receiving distance is 15cm; in the fifth step, the water bath temperature is 40 ℃, the ultrasonic treatment frequency is 23KHz, and the power is 1250W; in step six, the sonication frequency was 1.6MHz and the power was 300W.
8. The method for preparing the moisturizing and skin-rejuvenating mask according to claim 6, wherein the method comprises the following steps: in the second step, the water bath temperature is 60 ℃, the ultrasonic treatment frequency is 29KHz, and the power is 1350W; in the third step, the ultrasonic treatment frequency is 2.0MHz, and the power is 400W; in the fourth step, the spinning voltage is 24KV, the liquid feeding rate is 0.6mL/h, and the receiving distance is 17cm; in the fifth step, the water bath temperature is 50 ℃, the ultrasonic treatment frequency is 25KHz, and the power is 1350W; in step six, the sonication frequency was 1.8MHz and the power was 400W.
9. The method for preparing the moisturizing and skin-rejuvenating mask according to claim 6, wherein the method comprises the following steps: in the second step, the water bath temperature is 55 ℃, the ultrasonic treatment frequency is 27KHz, and the power is 1300W; in the third step, the ultrasonic treatment frequency is 1.9MHz, and the power is 350W; in the fourth step, the spinning voltage is 23KV, the liquid feeding rate is 0.55mL/h, and the receiving distance is 16cm; in the fifth step, the water bath temperature is 45 ℃, the ultrasonic treatment frequency is 24KHz, and the power is 1300W; in step six, the sonication frequency was 1.7MHz and the power was 350W.
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