CN114272181A - Moisturizing and skin-tendering mask and preparation method thereof - Google Patents

Moisturizing and skin-tendering mask and preparation method thereof Download PDF

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CN114272181A
CN114272181A CN202210101093.1A CN202210101093A CN114272181A CN 114272181 A CN114272181 A CN 114272181A CN 202210101093 A CN202210101093 A CN 202210101093A CN 114272181 A CN114272181 A CN 114272181A
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mask
ultrasonic treatment
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moisturizing
skin
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CN114272181B (en
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杨鹏
赖振东
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Guangdong Yingteng Biotechnology Co ltd
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Guangdong Yingteng Biotechnology Co ltd
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Abstract

The invention discloses a moisturizing and skin-tendering mask and a preparation method thereof, and particularly relates to the technical field of masks. The invention can effectively improve the antibacterial performance of the moisturizing and skin-tendering mask, can effectively sterilize bacteria on the surface of the mask, and simultaneously ensures the antibacterial performance of the mask under the illumination condition, thereby avoiding the reduction of the antibacterial performance of the mask after illumination; after blending and compounding treatment of the polyvinyl alcohol, the starch and the resveratrol, the silver nitrate is subjected to electrostatic spinning on the surface of the non-woven fabric base cloth to form nano-composite fibers, so that nano-silver can be effectively compounded into the nano-composite fibers, and nano-silver particles perform antibacterial treatment on the facial mask by taking the nano-composite fibers as carriers, so that the antibacterial treatment effect of the facial mask is further enhanced; the chitosan and the gelatin are blended, compounded and doped into the mask liquid, so that the antibacterial performance of the mask can be further enhanced, the contact and combination effect of the mask liquid and the non-woven fabric base cloth is enhanced, and the utilization rate of the mask liquid is ensured.

Description

Moisturizing and skin-tendering mask and preparation method thereof
Technical Field
The invention relates to the technical field of facial masks, in particular to a moisturizing and skin-tendering facial mask and a preparation method thereof.
Background
The facial mask is a skin care product for moisturizing skin, and also has multiple functions of moisturizing, nourishing, improving appearance, deeply cleaning and the like. The mask covers the stratum corneum layer of the skin, and provides water to the stratum corneum layer, so that the stratum corneum layer is fully hydrated, and the appearance and the elasticity of the skin are improved. The facial mask can be classified according to the facial mask form as follows: peeling, wiping or washing, curing and peeling and market mainstream sticking; wherein the cloth-sticking type face film comprises: gel-containing non-woven fabric coating and impregnated non-woven fabric coating facial mask; the gel-containing non-woven fabric is prepared by coating a gel-type preparation on the surface of a non-woven fabric, cutting into a facial shape, and sealing in a package; impregnated nonwoven masks are more commonly used and are made by impregnating a nonwoven with a mask solution.
The existing moisturizing and skin tendering mask has poor antibacterial performance, and especially after the mask is externally packaged and irradiated by light, the antibacterial performance of the mask is further reduced.
Disclosure of Invention
In order to overcome the above defects in the prior art, embodiments of the present invention provide a moisturizing and skin-tendering mask and a preparation method thereof.
The moisturizing and skin-tendering mask comprises a non-woven fabric base cloth, an extender and a mask liquid, wherein the extender, the non-woven fabric base cloth and the mask liquid are as follows by weight: 1: 120-160: 400-500.
Further, the supplement comprises the following components in percentage by weight: 19.60-20.60% of polyvinyl alcohol, 2.60-3.60% of silk peptide, 2.40-3.40% of hyaluronic acid, 3.60-4.60% of silver nitrate, 3.40-4.40% of starch, 19.40-20.40% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.40-3.40% of ginsenoside, 2.40-3.40% of antler peptide, 1.80-2.80% of sodium hyaluronate, 4.60-5.60% of cod collagen, 0.8-1.2% of ethanol extract of maitake mushroom, 0.8-1.2% of ethanol extract of Indian kalimeris herb, 9.60-10.60% of chitosan, 14.40-15.40% of gelatin and the balance of deionized water.
Further, the supplement, the non-woven base cloth and the mask liquid are as follows according to the weight part ratio: 1: 120: 400; the supplement comprises the following components in percentage by weight: 19.60% of polyvinyl alcohol, 2.60% of silk peptide, 2.40% of hyaluronic acid, 3.60% of silver nitrate, 3.40% of starch, 19.40% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.40% of ginsenoside, 2.40% of cornua cervi pantotrichum peptide, 1.80% of sodium hyaluronate, 4.60% of cod collagen, 0.8% of alcohol extract of maitake mushroom, 0.8% of alcohol extract of Indian kalimeris herb, 9.60% of chitosan, 14.40% of gelatin and the balance of deionized water.
Further, the supplement, the non-woven base cloth and the mask liquid are as follows according to the weight part ratio: 1: 160: 500; the supplement comprises the following components in percentage by weight: 20.60% of polyvinyl alcohol, 3.60% of silk peptide, 3.40% of hyaluronic acid, 4.60% of silver nitrate, 4.40% of starch, 20.40% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 3.40% of ginsenoside, 3.40% of cornua cervi pantotrichum peptide, 2.80% of sodium hyaluronate, 5.60% of cod collagen, 1.2% of alcohol extract of maitake mushroom, 1.2% of alcohol extract of Indian kalimeris herb, 10.60% of chitosan, 15.40% of gelatin and the balance of deionized water.
Further, the supplement, the non-woven base cloth and the mask liquid are as follows according to the weight part ratio: 1: 140: 450; the supplement comprises the following components in percentage by weight: 20.10% of polyvinyl alcohol, 3.10% of silk peptide, 2.90% of hyaluronic acid, 4.10% of silver nitrate, 3.90% of starch, 19.90% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.90% of ginsenoside, 2.90% of cornua cervi pantotrichum peptide, 2.30% of sodium hyaluronate, 5.10% of cod collagen, 1.0% of alcohol extract of maitake mushroom, 1.0% of alcohol extract of Indian kalimeris herb, 10.10% of chitosan, 14.90% of gelatin and the balance of deionized water.
A preparation method of a moisturizing and skin-tendering mask comprises the following specific preparation steps:
the method comprises the following steps: weighing non-woven fabric base cloth, polyvinyl alcohol, silk peptide, hyaluronic acid, silver nitrate, starch, resveratrol and deionized water in the raw materials of the supplement according to the parts by weight, and ginsenoside, cornua cervi pantotrichum peptide, sodium hyaluronate, cod collagen, alcohol extract of maitake mushroom, alcohol extract of kalimeris indica, chitosan, gelatin and deionized water in the raw materials of the mask liquid;
step two: raw materials of the supplement are as follows: blending polyvinyl alcohol, silk peptide, hyaluronic acid, silver nitrate, starch, resveratrol and deionized water, and carrying out water bath ultrasonic treatment for 20-30 minutes to obtain a premix;
step three: carrying out ultrasonic treatment on the premix prepared in the second step for 10-30 minutes to obtain a spinning solution;
step four: taking the non-woven fabric base cloth in the step one as a receiving base body, and forming a nano fibrous extender on the surface of the non-woven fabric base cloth by using the spinning solution in the step three in an electrostatic spinning mode to obtain a composite mask base cloth;
step five: preparing the raw materials of the mask liquid: mixing ginsenoside, pantocrin, sodium hyaluronate, cod collagen, alcohol extract of maitake mushroom, alcohol extract of Indian kalimeris herb, chitosan, gelatin and deionized water, and carrying out ultrasonic treatment in water bath for 20-30 minutes to obtain a mask liquid;
step six: and (4) soaking the composite facial mask base cloth prepared in the fourth step into the facial mask liquid obtained in the fifth step, and carrying out ultrasonic treatment for 5-10 minutes to obtain the moisturizing and skin-tendering facial mask.
Further, in the second step, the water bath temperature is 50-60 ℃, the ultrasonic treatment frequency is 25-29 KHz, and the power is 1250-1350W; in the third step, the ultrasonic treatment frequency is 1.8-2.0 MHz, and the power is 300-400W; in the fourth step, the spinning voltage is 22-24 KV, the liquid feeding speed is 0.5-0.6 mL/h, and the receiving distance is 15-17 cm; in the fifth step, the water bath temperature is 40-50 ℃, the ultrasonic treatment frequency is 23-25 KHz, and the power is 1250-1350W; in the sixth step, the ultrasonic treatment frequency is 1.6-1.8 MHz, and the power is 300-400W.
Further, in the second step, the temperature of the water bath is 50 ℃, the ultrasonic treatment frequency is 25KHz, and the power is 1250W; in the third step, the ultrasonic treatment frequency is 1.8MHz, and the power is 300W; in the fourth step, the spinning voltage is 22KV, the liquid feeding speed is 0.5mL/h, and the receiving distance is 15 cm; in the fifth step, the temperature of the water bath is 40 ℃, the ultrasonic treatment frequency is 23KHz, and the power is 1250W; in the sixth step, the ultrasonic treatment frequency is 1.6MHz, and the power is 300W.
Further, in the second step, the water bath temperature is 60 ℃, the ultrasonic treatment frequency is 29KHz, and the power is 1350W; in the third step, the ultrasonic treatment frequency is 2.0MHz, and the power is 400W; in the fourth step, the spinning voltage is 24KV, the liquid feeding speed is 0.6mL/h, and the receiving distance is 17 cm; in the fifth step, the water bath temperature is 50 ℃, the ultrasonic treatment frequency is 25KHz, and the power is 1350W; in the sixth step, the ultrasonic treatment frequency is 1.8MHz, and the power is 400W.
Further, in the second step, the water bath temperature is 55 ℃, the ultrasonic treatment frequency is 27KHz, and the power is 1300W; in the third step, the ultrasonic treatment frequency is 1.9MHz, and the power is 350W; in the fourth step, the spinning voltage is 23KV, the liquid feeding speed is 0.55mL/h, and the receiving distance is 16 cm; in the fifth step, the water bath temperature is 45 ℃, the ultrasonic treatment frequency is 24KHz, and the power is 1300W; in the sixth step, the ultrasonic treatment frequency is 1.7MHz, and the power is 350W.
The invention has the technical effects and advantages that:
1. the moisturizing and skin-tendering facial mask prepared by the raw material formula can effectively improve the antibacterial performance of the moisturizing and skin-tendering facial mask, can effectively sterilize bacteria on the surface of the facial mask, and simultaneously ensures the antibacterial performance of the facial mask under the illumination condition, thereby avoiding the reduction of the antibacterial performance of the facial mask after illumination; the replenisher is formed by blending polyvinyl alcohol, silk peptide and hyaluronic acid and compounding the mixture on the surface of non-woven fabric base cloth in an electrostatic spinning manner to form nano-composite fibers, so that the moisturizing and skin-tendering performance of the mask can be effectively guaranteed, the skin-friendly effect is better, and the mask application effect is better; the use of silver nitrate, after the blending and compounding treatment of polyvinyl alcohol, starch and resveratrol, the nano-composite fiber is formed on the surface of the non-woven fabric base cloth through electrostatic spinning, nano-silver can be effectively compounded into the nano-composite fiber, so that the antibacterial effect of the mask is effectively enhanced, the water vapor light transmittance and the moisture absorption performance of the mask are ensured, and the nano-silver particles perform antibacterial treatment on the mask by taking the nano-composite fiber as a carrier, so that the antibacterial treatment effect of the mask is further enhanced; the ginsenoside, the antler peptide, the sodium hyaluronate and the cod collagen are blended and compounded in the facial mask liquid, and are quickly compounded under ultrasonic treatment, so that the uvioresistant performance and the anti-aging performance of the facial mask can be effectively guaranteed; the chitosan and the gelatin are blended, compounded and doped into the mask liquid, so that the antibacterial performance of the mask can be further enhanced, the contact and combination effect of the mask liquid and the non-woven base cloth is enhanced, and the utilization rate of the mask liquid is ensured;
2. in the process of preparing the moisturizing and skin-tendering mask, in the second step, the polyvinyl alcohol, the silk peptide, the hyaluronic acid, the silver nitrate, the starch and the resveratrol can be effectively reacted and compounded quickly, so that the reaction process is accelerated; in the third step, the materials in the spinning solution can be effectively ensured to be uniformly dispersed, and the effective substances in the nano composite fibers generated by the subsequent electrostatic spinning treatment are ensured to be more uniform; in the fourth step, the antibacterial enhancement supplement effect of the supplement on the facial mask can be effectively enhanced; in the fifth step, rapid reaction compounding is carried out under the ultrasonic treatment of 23KHz at 40 ℃, and the reaction process is accelerated; and step six, soaking the composite mask base cloth into the mask liquid, and performing ultrasonic treatment at 1.7MHz to ensure that the effective components in the mask liquid are quickly compounded with the composite mask base cloth, so that the moisturizing and skin-tendering effects and the antibacterial effects of the mask are further enhanced.
Detailed Description
The following will clearly and completely describe the technical solutions in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1:
the invention provides a moisturizing and skin-tendering mask which comprises a non-woven fabric base cloth, an extender and a mask liquid, wherein the extender, the non-woven fabric base cloth and the mask liquid are as follows by weight: 1: 120: 400; the supplement comprises the following components in percentage by weight: 19.60% of polyvinyl alcohol, 2.60% of silk peptide, 2.40% of hyaluronic acid, 3.60% of silver nitrate, 3.40% of starch, 19.40% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.40% of ginsenoside, 2.40% of cornua cervi pantotrichum peptide, 1.80% of sodium hyaluronate, 4.60% of cod collagen, 0.8% of alcohol extract of maitake mushroom, 0.8% of alcohol extract of Indian kalimeris herb, 9.60% of chitosan, 14.40% of gelatin and the balance of deionized water;
the invention also provides a preparation method of the moisturizing and skin-tendering mask, which comprises the following specific preparation steps:
the method comprises the following steps: weighing non-woven fabric base cloth, polyvinyl alcohol, silk peptide, hyaluronic acid, silver nitrate, starch, resveratrol and deionized water in the raw materials of the supplement according to the parts by weight, and ginsenoside, cornua cervi pantotrichum peptide, sodium hyaluronate, cod collagen, alcohol extract of maitake mushroom, alcohol extract of kalimeris indica, chitosan, gelatin and deionized water in the raw materials of the mask liquid;
step two: raw materials of the supplement are as follows: blending polyvinyl alcohol, silk peptide, hyaluronic acid, silver nitrate, starch, resveratrol and deionized water, and carrying out water bath ultrasonic treatment for 20 minutes to obtain a premix;
step three: carrying out ultrasonic treatment on the premix prepared in the step two for 10 minutes to obtain a spinning solution;
step four: taking the non-woven fabric base cloth in the step one as a receiving base body, and forming a nano fibrous extender on the surface of the non-woven fabric base cloth by using the spinning solution in the step three in an electrostatic spinning mode to obtain a composite mask base cloth;
step five: preparing the raw materials of the mask liquid: mixing ginsenoside, pantocrin, sodium hyaluronate, cod collagen, alcohol extract of maitake mushroom, alcohol extract of Kalimeris indica, chitosan, gelatin and deionized water, and performing ultrasonic treatment in water bath for 20 minutes to obtain facial mask liquid;
step six: and (5) soaking the composite facial mask base cloth prepared in the fourth step into the facial mask liquid obtained in the fifth step, and carrying out ultrasonic treatment for 5 minutes to obtain the moisturizing and skin-tendering facial mask.
In the second step, the water bath temperature is 50 ℃, the ultrasonic treatment frequency is 25KHz, and the power is 1250W; in the third step, the ultrasonic treatment frequency is 1.8MHz, and the power is 300W; in the fourth step, the spinning voltage is 22KV, the liquid feeding speed is 0.5mL/h, and the receiving distance is 15 cm; in the fifth step, the temperature of the water bath is 40 ℃, the ultrasonic treatment frequency is 23KHz, and the power is 1250W; in the sixth step, the ultrasonic treatment frequency is 1.6MHz, and the power is 300W.
Example 2:
different from the embodiment 1, the supplement, the non-woven base fabric and the mask liquid are as follows according to the weight part ratio: 1: 160: 500; the supplement comprises the following components in percentage by weight: 20.60% of polyvinyl alcohol, 3.60% of silk peptide, 3.40% of hyaluronic acid, 4.60% of silver nitrate, 4.40% of starch, 20.40% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 3.40% of ginsenoside, 3.40% of cornua cervi pantotrichum peptide, 2.80% of sodium hyaluronate, 5.60% of cod collagen, 1.2% of alcohol extract of maitake mushroom, 1.2% of alcohol extract of Indian kalimeris herb, 10.60% of chitosan, 15.40% of gelatin and the balance of deionized water.
Example 3:
different from the examples 1-2, the supplement, the non-woven base fabric and the mask liquid are as follows according to the weight part ratio: 1: 140: 450; the supplement comprises the following components in percentage by weight: 20.10% of polyvinyl alcohol, 3.10% of silk peptide, 2.90% of hyaluronic acid, 4.10% of silver nitrate, 3.90% of starch, 19.90% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.90% of ginsenoside, 2.90% of cornua cervi pantotrichum peptide, 2.30% of sodium hyaluronate, 5.10% of cod collagen, 1.0% of alcohol extract of maitake mushroom, 1.0% of alcohol extract of Indian kalimeris herb, 10.10% of chitosan, 14.90% of gelatin and the balance of deionized water.
The moisturizing and skin-tendering facial masks prepared in the above examples 1-3, the moisturizing and skin-tendering facial mask of the first control group, the moisturizing and skin-tendering facial mask of the second control group, the moisturizing and skin-tendering facial mask of the fourth control group, the moisturizing and skin-tendering facial mask of the fifth control group and the moisturizing and skin-tendering facial mask of the sixth control group were respectively taken, the moisturizing and skin-tendering facial mask of the first control group and the three phases of the example had no polyvinyl alcohol, the moisturizing and skin-tendering facial mask of the second control group and the three phases of the example had no silver nitrate, the moisturizing and skin-tendering facial mask of the third control group and the three phases of the example had no starch, the moisturizing and skin-tendering facial mask of the fourth control group and the three phases of the example had no lacquer and alcohol extract, the moisturizing and skin-tendering facial mask of the fifth control group and the three phases of the example had no manila alcohol extract, the moisturizing and skin-tendering facial masks of the six control groups were respectively tested, 30 groups of moisturizing and skin rejuvenating masks were prepared for each control group and example and tested; the test results are shown in table one:
table one:
Figure BDA0003492499370000061
as can be seen from table one, when the moisturizing and skin-tendering mask comprises the following raw materials in parts by weight: the replenisher, the non-woven fabric base cloth and the mask liquid are as follows by weight: 1: 140: 450; the supplement comprises the following components in percentage by weight: 20.10% of polyvinyl alcohol, 3.10% of silk peptide, 2.90% of hyaluronic acid, 4.10% of silver nitrate, 3.90% of starch, 19.90% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.90% of ginsenoside, 2.90% of cornua cervi pantotrichum peptide, 2.30% of sodium hyaluronate, 5.10% of cod collagen, 1.0% of a maitake japonica alcohol extract, 1.0% of a glauca ethanol extract, 10.10% of chitosan, 14.90% of gelatin and the balance of deionized water, so that the antibacterial performance of the moisturizing and skin-tendering mask can be effectively improved, bacteria on the surface of the mask can be effectively sterilized, the antibacterial performance of the mask can be guaranteed under the illumination condition, and the antibacterial performance of the mask after illumination is prevented from being reduced; embodiment 3 is a preferred embodiment of the present invention, the supplement is prepared by blending polyvinyl alcohol, silk peptide and hyaluronic acid and compounding the blend on the surface of the non-woven fabric base fabric to form the nano-composite fiber through electrostatic spinning, such that the moisturizing and skin-tendering performance of the facial mask can be effectively ensured, the skin-friendly effect is better, and the facial mask application effect is good; the use of silver nitrate, after the blending and compounding treatment of polyvinyl alcohol, starch and resveratrol, the nano-composite fiber is formed on the surface of the non-woven fabric base cloth through electrostatic spinning, nano-silver can be effectively compounded into the nano-composite fiber, so that the antibacterial effect of the mask is effectively enhanced, the water vapor light transmittance and the moisture absorption performance of the mask are ensured, and the nano-silver particles perform antibacterial treatment on the mask by taking the nano-composite fiber as a carrier, so that the antibacterial treatment effect of the mask is further enhanced; the ginsenoside, the antler peptide, the sodium hyaluronate and the cod collagen are blended and compounded in the facial mask liquid, and are quickly compounded under ultrasonic treatment, so that the uvioresistant performance and the anti-aging performance of the facial mask can be effectively guaranteed; the ethanol extract of the maitake mushroom can effectively improve the antibacterial, ultraviolet-resistant and antioxidant properties of the mask; the herba Kalimeridis alcohol extract has the effects of clearing heat and detoxicating, cooling blood and stopping bleeding, and promoting diuresis and detumescence, and can effectively enhance the antibacterial effect of the facial mask; the chitosan and the gelatin are blended, compounded and doped into the mask liquid, so that the antibacterial performance of the mask can be further enhanced, the contact and combination effect of the mask liquid and the non-woven base cloth is enhanced, and the utilization rate of the mask liquid is ensured; the chitosan and the ginsenoside are compounded, so that the antibacterial effect of the facial mask can be further enhanced, and the protective effect of the facial mask on the skin using the facial mask is improved; the chitosan and the sodium hyaluronate are compounded, so that the repairing treatment effect of the mask on the skin can be effectively enhanced.
Example 4:
the invention provides a moisturizing and skin-tendering mask which comprises a non-woven fabric base cloth, an extender and a mask liquid, wherein the extender, the non-woven fabric base cloth and the mask liquid are as follows by weight: 1: 140: 450; the supplement comprises the following components in percentage by weight: 20.10% of polyvinyl alcohol, 3.10% of silk peptide, 2.90% of hyaluronic acid, 4.10% of silver nitrate, 3.90% of starch, 19.90% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.90% of ginsenoside, 2.90% of cornua cervi pantotrichum peptide, 2.30% of sodium hyaluronate, 5.10% of cod collagen, 1.0% of alcohol extract of maitake mushroom, 1.0% of alcohol extract of Indian kalimeris herb, 10.10% of chitosan, 14.90% of gelatin and the balance of deionized water;
the invention also provides a preparation method of the moisturizing and skin-tendering mask, which comprises the following specific preparation steps:
the method comprises the following steps: weighing non-woven fabric base cloth, polyvinyl alcohol, silk peptide, hyaluronic acid, silver nitrate, starch, resveratrol and deionized water in the raw materials of the supplement according to the parts by weight, and ginsenoside, cornua cervi pantotrichum peptide, sodium hyaluronate, cod collagen, alcohol extract of maitake mushroom, alcohol extract of kalimeris indica, chitosan, gelatin and deionized water in the raw materials of the mask liquid;
step two: raw materials of the supplement are as follows: blending polyvinyl alcohol, silk peptide, hyaluronic acid, silver nitrate, starch, resveratrol and deionized water, and carrying out water bath ultrasonic treatment for 25 minutes to obtain a premix;
step three: carrying out ultrasonic treatment on the premix prepared in the step two for 20 minutes to obtain a spinning solution;
step four: taking the non-woven fabric base cloth in the step one as a receiving base body, and forming a nano fibrous extender on the surface of the non-woven fabric base cloth by using the spinning solution in the step three in an electrostatic spinning mode to obtain a composite mask base cloth;
step five: preparing the raw materials of the mask liquid: mixing ginsenoside, pantocrin, sodium hyaluronate, cod collagen, alcohol extract of maitake mushroom, alcohol extract of Kalimeris indica, chitosan, gelatin and deionized water, and performing ultrasonic treatment in water bath for 25 minutes to obtain facial mask liquid;
step six: and (4) soaking the composite facial mask base cloth prepared in the fourth step into the facial mask liquid obtained in the fifth step, and carrying out ultrasonic treatment for 7 minutes to obtain the moisturizing and skin-tendering facial mask.
In the second step, the water bath temperature is 50 ℃, the ultrasonic treatment frequency is 25KHz, and the power is 1250W; in the third step, the ultrasonic treatment frequency is 1.8MHz, and the power is 300W; in the fourth step, the spinning voltage is 22KV, the liquid feeding speed is 0.5mL/h, and the receiving distance is 15 cm; in the fifth step, the temperature of the water bath is 40 ℃, the ultrasonic treatment frequency is 23KHz, and the power is 1250W; in the sixth step, the ultrasonic treatment frequency is 1.6MHz, and the power is 300W.
Example 5:
different from the embodiment 4, in the second step, the water bath temperature is 60 ℃, the ultrasonic treatment frequency is 29KHz, and the power is 1350W; in the third step, the ultrasonic treatment frequency is 2.0MHz, and the power is 400W; in the fourth step, the spinning voltage is 24KV, the liquid feeding speed is 0.6mL/h, and the receiving distance is 17 cm; in the fifth step, the water bath temperature is 50 ℃, the ultrasonic treatment frequency is 25KHz, and the power is 1350W; in the sixth step, the ultrasonic treatment frequency is 1.8MHz, and the power is 400W.
Example 6:
different from the examples 4-5, in the second step, the water bath temperature is 55 ℃, the ultrasonic treatment frequency is 27KHz, and the power is 1300W; in the third step, the ultrasonic treatment frequency is 1.9MHz, and the power is 350W; in the fourth step, the spinning voltage is 23KV, the liquid feeding speed is 0.55mL/h, and the receiving distance is 16 cm; in the fifth step, the water bath temperature is 45 ℃, the ultrasonic treatment frequency is 24KHz, and the power is 1300W; in the sixth step, the ultrasonic treatment frequency is 1.7MHz, and the power is 350W.
Taking the moisturizing and skin-tendering facial masks prepared in the above examples 4-6 and the moisturizing and skin-tendering facial mask of the control group seven, the moisturizing and skin-tendering facial mask of the control group eight, the moisturizing and skin-tendering facial mask of the control group nine and the moisturizing and skin-tendering facial mask of the control group ten respectively, the moisturizing and skin-tendering facial mask of the control group seven has no operation of water bath ultrasonic treatment in step three compared with the example six, the moisturizing and skin-tendering facial mask of the control group eight has no operation of ultrasonic treatment in step four compared with the example six, the moisturizing and skin-tendering facial mask of the control group nine has no operation of water bath ultrasonic treatment in step five compared with the example six, the moisturizing and skin-tendering facial mask of the control group ten has no operation of ultrasonic treatment in step six compared with the example six, the moisturizing and skin-tendering facial masks of the three examples and the moisturizing and skin-tendering facial masks of the four control groups are respectively tested by the seven groups, 30 groups of moisturizing and skin-tendering facial masks are prepared by each of the control group and the example, the test was carried out, and the test results are shown in table two:
table two:
Figure BDA0003492499370000091
as can be seen from table two, example 6 is a preferred embodiment of the present invention; in the second step, the polyvinyl alcohol, the silk peptide, the hyaluronic acid, the silver nitrate, the starch, the resveratrol and the deionized water are subjected to ultrasonic treatment at 55 ℃ and 27KHz, so that the polyvinyl alcohol, the silk peptide, the hyaluronic acid, the silver nitrate, the starch and the resveratrol can be effectively subjected to rapid reaction and compounding, and the reaction process is accelerated; in the third step, the premix is treated under 1.9MHz ultrasonic treatment, so that the uniform dispersion of materials in the spinning solution can be effectively ensured, and the uniformity of effective substances in the nano composite fibers generated by the subsequent electrostatic spinning treatment is ensured; in the fourth step, the spinning solution is compounded on the surface of the non-woven fabric base cloth in an electrostatic spinning mode, so that the antibacterial enhancement supplement effect of the supplement on the mask can be effectively enhanced; in the fifth step, ginsenoside, antler peptide, sodium hyaluronate, cod collagen, alcohol extract of maitake mushroom, alcohol extract of Indian kalimeris herb, chitosan, gelatin and deionized water are subjected to rapid reaction and compounding under the ultrasonic treatment of 23KHz at 40 ℃ to accelerate the reaction process; and step six, soaking the composite mask base cloth into the mask liquid, and performing ultrasonic treatment at 1.7MHz to ensure that the effective components in the mask liquid are quickly compounded with the composite mask base cloth, so that the moisturizing and skin-tendering effects and the antibacterial effects of the mask are further enhanced.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (10)

1. The moisturizing and skin tendering mask is characterized in that: the mask liquid comprises a non-woven fabric base cloth, a supplement and a mask liquid, wherein the supplement, the non-woven fabric base cloth and the mask liquid are as follows by weight: 1: 120-160: 400-500.
2. The hydrating and rejuvenating mask as set forth in claim 1, wherein: the supplement comprises the following components in percentage by weight: 19.60-20.60% of polyvinyl alcohol, 2.60-3.60% of silk peptide, 2.40-3.40% of hyaluronic acid, 3.60-4.60% of silver nitrate, 3.40-4.40% of starch, 19.40-20.40% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.40-3.40% of ginsenoside, 2.40-3.40% of antler peptide, 1.80-2.80% of sodium hyaluronate, 4.60-5.60% of cod collagen, 0.8-1.2% of ethanol extract of maitake mushroom, 0.8-1.2% of ethanol extract of Indian kalimeris herb, 9.60-10.60% of chitosan, 14.40-15.40% of gelatin and the balance of deionized water.
3. The hydrating and rejuvenating mask as set forth in claim 2, wherein: the replenisher, the non-woven fabric base cloth and the mask liquid are as follows by weight: 1: 120: 400; the supplement comprises the following components in percentage by weight: 19.60% of polyvinyl alcohol, 2.60% of silk peptide, 2.40% of hyaluronic acid, 3.60% of silver nitrate, 3.40% of starch, 19.40% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.40% of ginsenoside, 2.40% of cornua cervi pantotrichum peptide, 1.80% of sodium hyaluronate, 4.60% of cod collagen, 0.8% of alcohol extract of maitake mushroom, 0.8% of alcohol extract of Indian kalimeris herb, 9.60% of chitosan, 14.40% of gelatin and the balance of deionized water.
4. The hydrating and rejuvenating mask as set forth in claim 2, wherein: the replenisher, the non-woven fabric base cloth and the mask liquid are as follows by weight: 1: 160: 500; the supplement comprises the following components in percentage by weight: 20.60% of polyvinyl alcohol, 3.60% of silk peptide, 3.40% of hyaluronic acid, 4.60% of silver nitrate, 4.40% of starch, 20.40% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 3.40% of ginsenoside, 3.40% of cornua cervi pantotrichum peptide, 2.80% of sodium hyaluronate, 5.60% of cod collagen, 1.2% of alcohol extract of maitake mushroom, 1.2% of alcohol extract of Indian kalimeris herb, 10.60% of chitosan, 15.40% of gelatin and the balance of deionized water.
5. The hydrating and rejuvenating mask as set forth in claim 2, wherein: the replenisher, the non-woven fabric base cloth and the mask liquid are as follows by weight: 1: 140: 450; the supplement comprises the following components in percentage by weight: 20.10% of polyvinyl alcohol, 3.10% of silk peptide, 2.90% of hyaluronic acid, 4.10% of silver nitrate, 3.90% of starch, 19.90% of resveratrol and the balance of deionized water; the mask liquid comprises the following components in percentage by weight: 2.90% of ginsenoside, 2.90% of cornua cervi pantotrichum peptide, 2.30% of sodium hyaluronate, 5.10% of cod collagen, 1.0% of alcohol extract of maitake mushroom, 1.0% of alcohol extract of Indian kalimeris herb, 10.10% of chitosan, 14.90% of gelatin and the balance of deionized water.
6. A preparation method of the facial mask for moisturizing and tendering skin is characterized by comprising the following steps: the preparation method comprises the following specific steps:
the method comprises the following steps: weighing non-woven fabric base cloth, polyvinyl alcohol, silk peptide, hyaluronic acid, silver nitrate, starch, resveratrol and deionized water in the raw materials of the supplement according to the parts by weight, and ginsenoside, cornua cervi pantotrichum peptide, sodium hyaluronate, cod collagen, alcohol extract of maitake mushroom, alcohol extract of kalimeris indica, chitosan, gelatin and deionized water in the raw materials of the mask liquid;
step two: raw materials of the supplement are as follows: blending polyvinyl alcohol, silk peptide, hyaluronic acid, silver nitrate, starch, resveratrol and deionized water, and carrying out water bath ultrasonic treatment for 20-30 minutes to obtain a premix;
step three: carrying out ultrasonic treatment on the premix prepared in the second step for 10-30 minutes to obtain a spinning solution;
step four: taking the non-woven fabric base cloth in the step one as a receiving base body, and forming a nano fibrous extender on the surface of the non-woven fabric base cloth by using the spinning solution in the step three in an electrostatic spinning mode to obtain a composite mask base cloth;
step five: preparing the raw materials of the mask liquid: mixing ginsenoside, pantocrin, sodium hyaluronate, cod collagen, alcohol extract of maitake mushroom, alcohol extract of Indian kalimeris herb, chitosan, gelatin and deionized water, and carrying out ultrasonic treatment in water bath for 20-30 minutes to obtain a mask liquid;
step six: and (4) soaking the composite facial mask base cloth prepared in the fourth step into the facial mask liquid obtained in the fifth step, and carrying out ultrasonic treatment for 5-10 minutes to obtain the moisturizing and skin-tendering facial mask.
7. The method for preparing the moisturizing and skin rejuvenating mask as claimed in claim 6, wherein: in the second step, the water bath temperature is 50-60 ℃, the ultrasonic treatment frequency is 25-29 KHz, and the power is 1250-1350W; in the third step, the ultrasonic treatment frequency is 1.8-2.0 MHz, and the power is 300-400W; in the fourth step, the spinning voltage is 22-24 KV, the liquid feeding speed is 0.5-0.6 mL/h, and the receiving distance is 15-17 cm; in the fifth step, the water bath temperature is 40-50 ℃, the ultrasonic treatment frequency is 23-25 KHz, and the power is 1250-1350W; in the sixth step, the ultrasonic treatment frequency is 1.6-1.8 MHz, and the power is 300-400W.
8. The method for preparing the moisturizing and skin rejuvenating mask as claimed in claim 7, wherein: in the second step, the water bath temperature is 50 ℃, the ultrasonic treatment frequency is 25KHz, and the power is 1250W; in the third step, the ultrasonic treatment frequency is 1.8MHz, and the power is 300W; in the fourth step, the spinning voltage is 22KV, the liquid feeding speed is 0.5mL/h, and the receiving distance is 15 cm; in the fifth step, the temperature of the water bath is 40 ℃, the ultrasonic treatment frequency is 23KHz, and the power is 1250W; in the sixth step, the ultrasonic treatment frequency is 1.6MHz, and the power is 300W.
9. The method for preparing the moisturizing and skin rejuvenating mask as claimed in claim 7, wherein: in the second step, the water bath temperature is 60 ℃, the ultrasonic treatment frequency is 29KHz, and the power is 1350W; in the third step, the ultrasonic treatment frequency is 2.0MHz, and the power is 400W; in the fourth step, the spinning voltage is 24KV, the liquid feeding speed is 0.6mL/h, and the receiving distance is 17 cm; in the fifth step, the water bath temperature is 50 ℃, the ultrasonic treatment frequency is 25KHz, and the power is 1350W; in the sixth step, the ultrasonic treatment frequency is 1.8MHz, and the power is 400W.
10. The method for preparing the moisturizing and skin rejuvenating mask as claimed in claim 7, wherein: in the second step, the water bath temperature is 55 ℃, the ultrasonic treatment frequency is 27KHz, and the power is 1300W; in the third step, the ultrasonic treatment frequency is 1.9MHz, and the power is 350W; in the fourth step, the spinning voltage is 23KV, the liquid feeding speed is 0.55mL/h, and the receiving distance is 16 cm; in the fifth step, the water bath temperature is 45 ℃, the ultrasonic treatment frequency is 24KHz, and the power is 1300W; in the sixth step, the ultrasonic treatment frequency is 1.7MHz, and the power is 350W.
CN202210101093.1A 2022-01-27 2022-01-27 Moisturizing and skin-tendering mask and preparation method thereof Active CN114272181B (en)

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JP2017133137A (en) * 2016-01-29 2017-08-03 株式会社Csl Antibacterial and antivirus composition for fiber and fiber product
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CN112726219A (en) * 2020-12-28 2021-04-30 广东广油华丰科技研究有限公司 Emulsion containing nano cuprous oxide/copper oxide/silver oxide for non-woven fabric and application thereof
KR102278638B1 (en) * 2020-12-14 2021-07-16 주식회사 엘라코스메틱 Maskpack with improved moisture content
CN113350246A (en) * 2021-04-06 2021-09-07 卢桂琼 Whitening mask with high antibacterial performance and preparation method thereof
CN113789001A (en) * 2021-09-15 2021-12-14 青岛奥盛塑胶有限公司 Waterproof shielding protective film for spraying and processing technology thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2017133137A (en) * 2016-01-29 2017-08-03 株式会社Csl Antibacterial and antivirus composition for fiber and fiber product
CN106110369A (en) * 2016-06-30 2016-11-16 江苏开源康达医疗器械有限公司 A kind of medical composite type hyaluronic acid dressing and preparation method thereof
KR102052921B1 (en) * 2018-09-13 2020-01-08 조석형 Anti-bacterial chitosan non-woven fabric and maskpack
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