CN114223908A - Mineral trace element and taurine composite product, preparation method and application - Google Patents

Mineral trace element and taurine composite product, preparation method and application Download PDF

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Publication number
CN114223908A
CN114223908A CN202111614703.XA CN202111614703A CN114223908A CN 114223908 A CN114223908 A CN 114223908A CN 202111614703 A CN202111614703 A CN 202111614703A CN 114223908 A CN114223908 A CN 114223908A
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taurine
parts
composite product
stirring
mineral
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罗江水
魏润宏
易滢婷
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Sichuan University
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Sichuan University
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    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/17—Amino acids, peptides or proteins
    • A23L33/175—Amino acids
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/105—Plant extracts, their artificial duplicates or their derivatives
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/115—Fatty acids or derivatives thereof; Fats or oils
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/15—Vitamins
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/16—Inorganic salts, minerals or trace elements
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/16—Inorganic salts, minerals or trace elements
    • A23L33/165—Complexes or chelates
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Food Science & Technology (AREA)
  • Nutrition Science (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mycology (AREA)
  • Polymers & Plastics (AREA)
  • Inorganic Chemistry (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Botany (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

The invention discloses a mineral trace element and taurine composite product, a preparation method and application, wherein the composite product is a complex obtained by fully reacting 10 parts of taurine, 7-21 parts of metal mineral elements and 0.5-5 parts of supplementary materials in parts by mole; the metal mineral element is one, two or more of sodium, copper, manganese, nickel, potassium, magnesium, iron, zinc and calcium; the supplementary material is one, two or more of anthocyanidin, xanthophyll, astaxanthin, vitamin C, microorganism E, coenzyme Q10, SOD, pycnogenol, lycopene and DHA. The product of the invention contains taurine and microelements required by human body, the preparation method is simple, the raw materials are cheap, and the obtained product has high purity and excellent quality.

Description

Mineral trace element and taurine composite product, preparation method and application
Technical Field
The invention relates to the technical field of food additives, in particular to a mineral trace element and taurine composite product, a preparation method and application.
Background
Taurine is a beta-sulphenyl amino acid widely distributed in animal tissue cells, and is an important substance for regulating normal physiological functions of organisms. Taurine not only plays an important role in the development of the brain, ovary, heart, liver, nervous system and other organisms of human bodies, but also has a plurality of physiological functions of resisting tumor, enhancing immunity, protecting heart, reducing blood pressure, reducing blood fat and blood sugar, relieving fatty liver, reducing transaminase, resisting aging and the like.
The human body trace elements mainly comprise iron, copper, manganese, zinc, cobalt, nickel, vanadium, fluorine, selenium, iodine, silicon, tin and the like. The weight of each element in the human body is between 0.01 and 0.005 percent. The microelements have important effects on maintaining metabolism, body function and immunity of human body. The trace elements are usually ingested by food, and if the diet is improperly prepared, food preference or certain diseases are suffered, deficiency is easily caused, and a series of body diseases are caused.
Most of the existing mineral trace element products are varieties with single components, such as taurine magnesium tablets, aspartic acid calcium effervescent tablets and the like, the components are single, and multiple products are usually needed to be matched for use in use, so that the administration is inconvenient. And generally the production process is complicated and requires expensive raw materials.
Disclosure of Invention
Aiming at the problems in the prior art, the invention provides a mineral trace element and taurine composite product with simple production process, high product purity and excellent quality, a preparation method and application.
The technical scheme adopted by the invention is as follows:
a mineral trace element and taurine composite product is a complex obtained by fully reacting 10 parts of taurine, 7-21 parts of metal mineral elements and 0.5-5 parts of supplementary materials in parts by mole;
the metal mineral element is one, two or more of sodium, copper, manganese, nickel, potassium, magnesium, iron, zinc and calcium;
the supplementary material is one, two or more of anthocyanidin, xanthophyll, astaxanthin, vitamin C, microorganism E, coenzyme Q10, SOD, pycnogenol, lycopene and DHA.
Further, the metal mineral elements comprise the following components in parts by mole: 1-3 parts of manganese, 1-3 parts of nickel ions, 1-3 parts of potassium, 1-3 parts of magnesium, 1-3 parts of iron, 1-3 parts of zinc and 1-3 parts of calcium.
Further, the supplementary materials comprise the following components in parts by mole: 0.1-1 part of anthocyanin, 0.1-1 part of lutein, 0.1-1 part of astaxanthin, 0.1-1 part of vitamin E and 0.1-1 part of DHA.
A preparation method of a mineral trace element and taurine composite product comprises the following steps:
step 1: dissolving taurine in an aqueous solution to obtain a taurine solution;
step 2: adding metal salt corresponding to the metal mineral element into the taurine solution obtained in the step 1, and fully mixing; fully reacting at 50-200 ℃;
and step 3: removing volatile substances from the reaction product in the step 2 to obtain the taurate coordination polymer;
and 4, step 4: and (3) adding a supplementary material into the taurate coordination polymer obtained in the step (3), fully reacting, cleaning and drying to obtain the required composite product.
Further, the mixing in the step 2 is performed by adopting a stirring method, and the stirring method is one of mechanical stirring, magnetic stirring, manual stirring, ultrasonic stirring and vibration stirring; step 4, stirring and reacting at 50 ℃. .
Further, the reaction time in the step 2 is 3-10 hours, and the reaction time in the step 4 is 1 hour.
Further, in the step 2, the heating is performed to a required temperature by one of heating rod heating, infrared heating and high-frequency electromagnetic heating.
Further, the mass concentration of taurine in the taurine acid solution in the step 1 is 5 wt.% to 50 wt.%.
Use of a composite product as an additive to a food or health food.
Further, the food or health food comprises one of a vitamin complex, a beverage and a dairy product.
The invention has the beneficial effects that:
(1) the composite product obtained by the invention can be rapidly dissociated in the acidic environment of gastric acid, the release amount of metal ions is promoted, and the absorption of inorganic salt by stomach is improved;
(2) the metal sulfonate is a porous soft structure with adsorption and catalysis properties, and is favorable for better combination of the metal sulfonate and other substances;
(3) the manganese ions, the iron ions and the copper ions can have a synergistic effect with other metal ions, so that the rapid generation of the metal sulfonate and the complex polymer thereof can be accelerated, and the reaction yield is increased;
(4) the supplements such as anthocyanin and the like in the invention have complexation with metal ions, and can present different colors, thereby being convenient for identification and distinction;
(5) the product of the invention contains taurine and microelements required by human body, the preparation method is simple, the raw materials are cheap, and the obtained product has high purity and excellent quality.
Detailed Description
The present invention is further illustrated by the following specific examples.
A mineral trace element and taurine composite product is a complex obtained by fully reacting 10 parts of taurine, 7-21 parts of metal mineral elements and 0.5-5 parts of supplementary materials in parts by mole;
the metal mineral element is one, two or more of sodium, copper, manganese, nickel, potassium, magnesium, iron, zinc and calcium; preferably, the metal mineral elements comprise the following components in parts by mole: 1-3 parts of manganese, 1-3 parts of nickel ions, 1-3 parts of potassium, 1-3 parts of magnesium, 1-3 parts of iron, 1-3 parts of zinc and 1-3 parts of calcium.
The supplementary material is one, two or more of anthocyanidin, xanthophyll, astaxanthin, vitamin C, microorganism E, coenzyme Q10, SOD, pycnogenol, lycopene and DHA. Preferably, the supplementary materials comprise the following components in parts by mole: 0.1-1 part of anthocyanin, 0.1-1 part of lutein, 0.1-1 part of astaxanthin, 0.1-1 part of vitamin E and 0.1-1 part of DHA.
A preparation method of a mineral trace element and taurine composite product comprises the following steps:
step 1: dissolving taurine in an aqueous solution to obtain a taurine solution, and placing the taurine solution in a reaction container; the mass concentration of the taurine in the taurine acid solution is 5 wt.% to 50 wt.%.
Step 2: adding metal salt corresponding to the metal mineral element into the taurine solution obtained in the step 1, and fully mixing; fully reacting at 50-200 ℃; the mixing is carried out by adopting a stirring method, and the stirring method is one of mechanical stirring, magnetic stirring, manual stirring, ultrasonic stirring and vibration stirring; the reaction time is 3-10 h. Heating to a required temperature by one of heating rod heating, infrared heating and high-frequency electromagnetic heating.
And step 3: removing volatile substances from the reaction product in the step 2 to obtain the taurate coordination polymer; volatile materials were removed by a reduced pressure distillation system.
And 4, step 4: and (3) adding a supplement into the taurate coordination polymer obtained in the step (3), stirring and reacting at 50 ℃, cleaning and drying to obtain the required composite product, wherein the reaction time is 1 h.
The composite product is used as additive for food or health food. The food or health food comprises one of compound vitamins, beverage, and milk product (such as cow milk, sheep milk, milk powder, yogurt, etc.); it can also be added into other food.
The taurine in the invention can be directly used as a ligand, and the ligand contains an amino nitrogen atom and a sulfooxy atom which can coordinate with different metal ions. In addition, the coordination mode of the sulfonate is various, and the sulfonate can be monodentate (namely, single oxygen atom is used for independent coordination), and can also be bidentate, tridentate, bridged (namely, two oxygen atoms or three oxygen atoms in the sulfonate are used for coordination) or chelate coordination (namely, nitrogen and one oxygen atom of the sulfonate are used for coordination with metal to form a chelate six-membered ring). The metal sulfonate has a porous soft structure with adsorption and catalysis properties, and the structure is favorable for better combination of the metal sulfonate and other substances and development and production of products. (for example, taurine binary polymer, crystal containing metal Ni ion and K ion, which form three-dimensional supermolecular framework structure through weak coordination and abundant hydrogen bond)
Manganese ions, iron ions and copper ions with catalytic properties have synergistic effect with other ions, can accelerate the rapid generation of metal sulfonate and a complex polymer thereof, and increase the reaction yield. At present, one of the most important means for resisting aging and diseases of human beings is antioxidation, and anthocyanin, lutein, astaxanthin, vitamin C, vitamin E, coenzyme Q10, SOD, pycnogenol, lycopene and the like have the antioxidation function. DHA (Docosahexaenoic acid), also known as brain gold, is a polyunsaturated fatty acid of the docosahexaenoic acid Omega-3 series. It has the important effects of promoting the development of visual acuity, improving the sleep quality of infants, improving immunity, resisting inflammation, improving memory problems of old people and other chronic health problems, enhancing the development of skeletal muscles, strengthening body, resisting cancers and the like.
The organic component and the inorganic component are combined to have mutual synergistic effect. For example, anthocyanin and astaxanthin can form a metal complex with metal ions, the molecular structure of anthocyanin contains a large amount of phenolic hydroxyl and substituent groups (such as methoxy), so that the chemical property of anthocyanin is more active, and the structure and color of anthocyanin can be changed due to the complexation of anthocyanin and metal ions, so that the color of composite medicine can be effectively adjusted, and the composite medicine can be used for medicine identification, differentiation and the like. After the anthocyanin and the metal element are subjected to a coordination reaction, the electronic configuration in the whole molecule is changed, so that hydrogen on the hydroxyl is unstable, and the anthocyanin has stronger oxidation resistance. The metal elements and hydroxyl groups at the ortho positions of the B ring in the anthocyanin molecule form stable five-membered rings, so that electron cloud distribution of the whole molecule is delocalized, and the lotus procyanidin forms a relatively stable free radical intermediate. The more stable this phenoxy radical, the more active the anthocyanin metal complex is at scavenging free radicals.
Examples
A preparation method of a mineral trace element and taurine composite product comprises the following steps:
step 1: dissolving 3mol of taurine in an aqueous solution to prepare a taurine solution with the taurine concentration of 50 wt.%, and placing the taurine solution in a reaction container.
Step 2: adding 1mol of MgCl into the taurine solution obtained in the step 12Heating to 70 ℃ in a reaction vessel, and preserving heat for 10h to generate magnesium taurate solution; then 1mol of K is added to the solution2CO3The weak alkaline solution reacts for 1 hour, and part of magnesium taurate generates magnesium taurate complexes due to the alkaline environment.
Then continuously adding 1mol of nickel acetate solution and 1MnCl with catalytic activity through a peristaltic pump2And mechanically stirring, heating to 150 ℃ by adopting high-frequency electromagnetic heating, and continuously preserving heat for 10 hours.
And step 3: and (3) obtaining the taurate coordination polymer by using the volatile substances of the reaction product in the step (2). Catalytically active MnCl2The coordination compound can be rapidly dissociated in the environment of gastric acid, promotes the release amount of metal and improves the absorption of inorganic salt by stomach.
And 4, step 4: cooling to 50 ℃, adding supplementary materials anthocyanin, lutein, astaxanthin and vitamin E into the taurate coordination polymer obtained in the step 3, and reacting for 1 h; after the reaction is full, volatilizing part of H by a reduced pressure distillation system2O, HCl, the metal ions which do not generate the complexes and the residual taurine generate a composite product of manganese taurate, nickel taurine, magnesium taurate and potassium taurine and a metal complex of anthocyanin and astaxanthin. And adding dry ice into the mixed solution, quickly cooling to normal temperature, and performing vacuum pumping, freezing and low-temperature drying to obtain the required composite product.
Taurine and metal salts produce taurates having the structure shown in the following table:
TABLE 1 chemical structural formula of taurate
Figure BDA0003436100840000051
The composite product obtained by the invention can be rapidly dissociated in the acidic environment of gastric acid, the release amount of metal ions is promoted, and the absorption of inorganic salt by stomach is improved; the metal sulfonate is a porous soft structure with adsorption and catalysis properties, and is favorable for better combination of the metal sulfonate and other substances; manganese ions, iron ions and copper ions can have a synergistic effect with other metal ions, so that the rapid generation of metal sulfonate and a complex polymer thereof can be accelerated, and the reaction yield is increased; it is common to have one of the manganese, iron, copper ions together, followed by the other metal ions listed above. The metal salt is usually a chloride salt, a carbonate salt or a carboxylate salt.
In the invention, the supplementary materials such as anthocyanin and the like and metal ions are subjected to complexation, and can present different colors, thereby being convenient for identification and distinction; the product contains taurine and trace elements required by human body, the preparation method is simple, the raw materials are cheap, and the obtained product has high purity and excellent quality.

Claims (10)

1. A mineral trace element and taurine composite product is characterized in that the composite product is a complex obtained by fully reacting 10 parts of taurine, 7-21 parts of metal mineral elements and 0.5-5 parts of supplementary materials in parts by mole;
the metal mineral element is one, two or more of sodium, copper, manganese, nickel, potassium, magnesium, iron, zinc and calcium;
the supplementary material is one, two or more of anthocyanidin, xanthophyll, astaxanthin, vitamin C, microorganism E, coenzyme Q10, SOD, pycnogenol, lycopene and DHA.
2. The mineral microelement and taurine composite product according to claim 1, wherein the metal mineral elements comprise, in terms of mole fraction: 1-3 parts of manganese, 1-3 parts of nickel ions, 1-3 parts of potassium, 1-3 parts of magnesium, 1-3 parts of iron, 1-3 parts of zinc and 1-3 parts of calcium.
3. The mineral microelement and taurine composite product according to claim 1, wherein the supplementary material comprises, in terms of mole parts: 0.1-1 part of anthocyanin, 0.1-1 part of lutein, 0.1-1 part of astaxanthin, 0.1-1 part of vitamin E and 0.1-1 part of DHA.
4. The method for preparing the composite product of mineral trace elements and taurine as claimed in any one of claims 1 to 3, comprising the steps of:
step 1: dissolving taurine in an aqueous solution to obtain a taurine solution;
step 2: adding metal salt corresponding to the metal mineral element into the taurine solution obtained in the step 1, and fully mixing; fully reacting at 50-200 ℃;
and step 3: removing volatile substances from the reaction product in the step 2 to obtain the taurate coordination polymer;
and 4, step 4: and (3) adding a supplementary material into the taurate coordination polymer obtained in the step (3), fully reacting, cleaning and drying to obtain the required composite product.
5. The preparation method according to claim 4, wherein the mixing in the step 2 is performed by a stirring method, and the stirring method is one of mechanical stirring, magnetic stirring, manual stirring, ultrasonic stirring and vibration stirring; step 4, stirring and reacting at 50 ℃.
6. The preparation method according to claim 4, wherein the reaction time in the step 2 is 3-10 h, and the reaction time in the step 4 is 1 h.
7. The method according to claim 4, wherein the heating to a desired temperature in step 2 is performed by one of heating with a heating rod, infrared heating, and high-frequency electromagnetic heating.
8. The method according to claim 4, wherein the mass concentration of taurine in the taurine acid solution in the step 1 is 5 wt.% to 50 wt.%.
9. Use of a composite product obtained by the method according to claims 4 to 8, wherein the composite product is used as an additive for food or health food.
10. The use of claim 9, wherein the food or health food comprises one of a vitamin complex, a beverage, and a dairy product.
CN202111614703.XA 2021-12-27 2021-12-27 Mineral trace element and taurine composite product, preparation method and application Pending CN114223908A (en)

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