CN114149872A - Novel washing powder and preparation method thereof - Google Patents
Novel washing powder and preparation method thereof Download PDFInfo
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- CN114149872A CN114149872A CN202111299060.4A CN202111299060A CN114149872A CN 114149872 A CN114149872 A CN 114149872A CN 202111299060 A CN202111299060 A CN 202111299060A CN 114149872 A CN114149872 A CN 114149872A
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- sodium
- washing powder
- powder
- slurry
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- 239000000843 powder Substances 0.000 title claims abstract description 73
- 238000005406 washing Methods 0.000 title claims abstract description 53
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000002245 particle Substances 0.000 claims abstract description 24
- 239000002250 absorbent Substances 0.000 claims abstract description 17
- 230000002745 absorbent Effects 0.000 claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 15
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 15
- 239000000835 fiber Substances 0.000 claims abstract description 15
- 239000004367 Lipase Substances 0.000 claims abstract description 13
- 102000004882 Lipase Human genes 0.000 claims abstract description 13
- 108090001060 Lipase Proteins 0.000 claims abstract description 13
- 229910000503 Na-aluminosilicate Inorganic materials 0.000 claims abstract description 13
- 108091005804 Peptidases Proteins 0.000 claims abstract description 13
- 239000004365 Protease Substances 0.000 claims abstract description 13
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims abstract description 13
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 claims abstract description 13
- PMYUVOOOQDGQNW-UHFFFAOYSA-N hexasodium;trioxido(trioxidosilyloxy)silane Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[O-][Si]([O-])([O-])O[Si]([O-])([O-])[O-] PMYUVOOOQDGQNW-UHFFFAOYSA-N 0.000 claims abstract description 13
- 235000019421 lipase Nutrition 0.000 claims abstract description 13
- 239000002736 nonionic surfactant Substances 0.000 claims abstract description 13
- 229920001467 poly(styrenesulfonates) Polymers 0.000 claims abstract description 13
- 229940051841 polyoxyethylene ether Drugs 0.000 claims abstract description 13
- 229920000056 polyoxyethylene ether Polymers 0.000 claims abstract description 13
- 235000012217 sodium aluminium silicate Nutrition 0.000 claims abstract description 13
- 239000000429 sodium aluminium silicate Substances 0.000 claims abstract description 13
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000001509 sodium citrate Substances 0.000 claims abstract description 13
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims abstract description 13
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 claims abstract description 13
- 239000003205 fragrance Substances 0.000 claims abstract description 9
- 239000002002 slurry Substances 0.000 claims description 33
- 239000000203 mixture Substances 0.000 claims description 29
- 238000003756 stirring Methods 0.000 claims description 27
- 239000000686 essence Substances 0.000 claims description 20
- 239000000463 material Substances 0.000 claims description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 8
- 239000003795 chemical substances by application Substances 0.000 claims description 8
- 239000008187 granular material Substances 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 230000001007 puffing effect Effects 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 6
- 238000001694 spray drying Methods 0.000 claims description 6
- 239000000126 substance Substances 0.000 claims description 6
- 238000005303 weighing Methods 0.000 claims description 6
- 238000000576 coating method Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 239000011347 resin Substances 0.000 claims description 4
- 229920005989 resin Polymers 0.000 claims description 4
- 239000011780 sodium chloride Substances 0.000 claims description 4
- 229960001922 sodium perborate Drugs 0.000 claims description 4
- 159000000000 sodium salts Chemical class 0.000 claims description 4
- YKLJGMBLPUQQOI-UHFFFAOYSA-M sodium;oxidooxy(oxo)borane Chemical compound [Na+].[O-]OB=O YKLJGMBLPUQQOI-UHFFFAOYSA-M 0.000 claims description 4
- 239000012467 final product Substances 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 102000004190 Enzymes Human genes 0.000 claims description 2
- 108090000790 Enzymes Proteins 0.000 claims description 2
- 102000004317 Lyases Human genes 0.000 claims description 2
- 108090000856 Lyases Proteins 0.000 claims description 2
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 2
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 2
- 238000000354 decomposition reaction Methods 0.000 claims description 2
- 238000004090 dissolution Methods 0.000 claims description 2
- MCPKSFINULVDNX-UHFFFAOYSA-N drometrizole Chemical compound CC1=CC=C(O)C(N2N=C3C=CC=CC3=N2)=C1 MCPKSFINULVDNX-UHFFFAOYSA-N 0.000 claims description 2
- 229930003935 flavonoid Natural products 0.000 claims description 2
- 150000002215 flavonoids Chemical class 0.000 claims description 2
- 235000017173 flavonoids Nutrition 0.000 claims description 2
- 150000008442 polyphenolic compounds Chemical class 0.000 claims description 2
- 235000013824 polyphenols Nutrition 0.000 claims description 2
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 2
- 239000002994 raw material Substances 0.000 claims description 2
- 229960001295 tocopherol Drugs 0.000 claims description 2
- 229930003799 tocopherol Natural products 0.000 claims description 2
- 235000010384 tocopherol Nutrition 0.000 claims description 2
- 239000011732 tocopherol Substances 0.000 claims description 2
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 claims description 2
- MRBKEAMVRSLQPH-UHFFFAOYSA-N 3-tert-butyl-4-hydroxyanisole Chemical compound COC1=CC=C(O)C(C(C)(C)C)=C1 MRBKEAMVRSLQPH-UHFFFAOYSA-N 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 5
- 230000003647 oxidation Effects 0.000 abstract description 5
- 238000007254 oxidation reaction Methods 0.000 abstract description 5
- 238000004140 cleaning Methods 0.000 abstract description 4
- 230000007774 longterm Effects 0.000 abstract description 2
- 238000001514 detection method Methods 0.000 description 2
- 239000003599 detergent Substances 0.000 description 2
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- CZBZUDVBLSSABA-UHFFFAOYSA-N butylated hydroxyanisole Chemical compound COC1=CC=C(O)C(C(C)(C)C)=C1.COC1=CC=C(O)C=C1C(C)(C)C CZBZUDVBLSSABA-UHFFFAOYSA-N 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/02—Preparation in the form of powder by spray drying
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/0005—Other compounding ingredients characterised by their effect
- C11D3/0036—Soil deposition preventing compositions; Antiredeposition agents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/0005—Other compounding ingredients characterised by their effect
- C11D3/0084—Antioxidants; Free-radical scavengers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/08—Silicates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
- C11D3/128—Aluminium silicates, e.g. zeolites
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3749—Polyolefins; Halogenated polyolefins; Natural or synthetic rubber; Polyarylolefins or halogenated polyarylolefins
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38609—Protease or amylase in solid compositions only
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38627—Preparations containing enzymes, e.g. protease or amylase containing lipase
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a novel washing powder, which comprises the following components in percentage by weight: 10-15% of sulfonated polystyrene, 5-12% of sodium aluminosilicate, 5-10% of sodium disilicate, 1-4% of fatty alcohol-polyoxyethylene ether, 3-5% of sodium dodecyl benzene sulfonate, 12-16% of nonionic surfactant, 5-7% of fiber antiscale, 1-3% of protease, 1-4% of lipase, 4-6% of sodium citrate, 7-9% of puffed powder, 6-15% of mixed particle essence, 1-3% of ultraviolet absorbent, 0.5-2% of antioxidant and the balance of water. The invention also discloses a preparation method of the novel washing powder, which can optimize the preparation process and improve the product control effect. The laundry clothes prepared by the invention have good cleaning effect, can reach or even exceed the common standard, and the clothes cleaned by the laundry powder have obvious fragrance which has multiple layers and can slowly diffuse for a long time; the washing powder has good oxidation resistance and can meet the requirement of long-term use in families.
Description
Technical Field
The invention relates to the technical field of detergents, in particular to novel washing powder and a preparation method thereof.
Background
Along with the improvement of living standard of people, people have better conditions to improve living environment and personal hygiene, and are in clean and tidy environment for a long time, not only can promote people's health, but also can make the human body happy. People generally need to ensure the cleanness of clothes besides ensuring the cleanness of their bodies, and washing powder and laundry detergent are the two most important clothes cleaning agents at present, can generate foams, remove various stains stained on the clothes and leave certain fragrance, and are popular among many people.
The washing powder has higher cost performance relatively, so the washing powder is more widely applied, but many washing powders on the market at present usually have simpler components, have common cleaning effect, are difficult to retain fragrance, are not easy to be liked by consumers, and have insufficient competitiveness. Meanwhile, in the storage process of the washing powder, when the washing powder is directly irradiated by sunlight for a long time, the washing powder is easy to oxidize and deteriorate. In view of the above, we propose a novel washing powder and a preparation method thereof.
Disclosure of Invention
The invention aims to provide a novel washing powder and a preparation method thereof, and aims to solve the problems in the background art.
In order to realize the purpose, the invention provides the following technical scheme, and the novel washing powder comprises the following components in percentage by weight: 10-15% of sulfonated polystyrene, 5-12% of sodium aluminosilicate, 5-10% of sodium disilicate, 1-4% of fatty alcohol-polyoxyethylene ether, 3-5% of sodium dodecyl benzene sulfonate, 12-16% of nonionic surfactant, 5-7% of fiber antiscale, 1-3% of protease, 1-4% of lipase, 4-6% of sodium citrate, 7-9% of puffed powder, 6-15% of mixed particle essence, 1-3% of ultraviolet absorbent, 0.5-2% of antioxidant and the balance of water.
Preferably, the fiber antiscaling agent is a mixed preparation and is formed by mixing resin, sodium salt, sodium perborate, sodium chloride, decomposition enzyme, polyvinyl alcohol, ethanol and water, and the mixing proportion of the components is as follows: 6-10% of resin, 0.2-0.4% of sodium salt, 0.3-0.5% of sodium perborate, 0.3-0.5% of sodium chloride, 0.4-0.6% of lyase, about 5% of ethanol and the balance of water.
Preferably, the mixed particle essence comprises three or more fragrances, the mixed particle essence is prepared into particles by taking plant essence as a raw material, and is coated with coatings, and the plant essences of different types are coated with coatings of different thicknesses and have different dissolution levels.
Preferably, the ultraviolet absorbent is a mixture of an ultraviolet absorbent UV-P and an ultraviolet absorbent UV-O.
Preferably, the antioxidant is one or more of Tea Polyphenol (TP), tocopherol, flavonoid and butyl hydroxy anisole.
A preparation method of novel washing powder comprises the following steps: weighing sulfonated polystyrene, sodium aluminosilicate, sodium disilicate, fatty alcohol-polyoxyethylene ether and sodium dodecyl benzene sulfonate according to a proportion, combining all the materials together, pouring the mixture into a slurry stirrer, adding water, stirring the mixture for 40 to 60 minutes under the state of the rotation speed of 800 plus materials being 1000 revolutions per minute, then adding a nonionic surfactant, a fiber antiscaling agent, protease, lipase, sodium citrate, puffing powder, an ultraviolet absorbent and an antioxidant, accelerating the mixture to 1000 plus materials being 1200 revolutions per minute, stirring the mixture for 90 minutes to prepare washing powder slurry, then stirring the washing powder slurry in a temperature-controlled sealed stirrer, controlling the temperature of the temperature-controlled stirrer to be 50 to 80 ℃, stirring the washing powder slurry for 60 to 120 minutes, filtering the washing powder slurry by using a 10-mesh screen to remove solid substances with overlarge particle size, and then inputting the slurry into a high-pressure temperature-controlled sprayer, spray drying to obtain hollow granules, cooling, transferring into soft agitator, adding mixed granule essence, stirring for 60-120 min to obtain the final product.
Compared with the prior art, the invention has the beneficial effects that:
1. the laundry clothes prepared by the invention have good cleaning effect, can reach or even exceed the common standard, and the clothes cleaned by the laundry powder have obvious fragrance, the fragrance has multiple levels, can be slowly emitted and can be kept lasting, so that the laundry clothes are popular with consumers and the market competitiveness is improved;
2. the washing powder disclosed by the invention is detected by direct sunlight for 100 hours, has an oxidation rate lower than 2%, has good oxidation resistance, and can meet the requirement of long-term use in families.
Detailed Description
The technical solutions in the embodiments of the present invention are clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention provides a technical scheme that: the technical solution of the present patent will be described in further detail with reference to the following embodiments.
The novel washing powder comprises the following components in percentage by weight: 10-15% of sulfonated polystyrene, 5-12% of sodium aluminosilicate, 5-10% of sodium disilicate, 1-4% of fatty alcohol-polyoxyethylene ether, 3-5% of sodium dodecyl benzene sulfonate, 12-16% of nonionic surfactant, 5-7% of fiber antiscale, 1-3% of protease, 1-4% of lipase, 4-6% of sodium citrate, 7-9% of puffed powder, 6-15% of mixed particle essence, 1-3% of ultraviolet absorbent, 0.5-2% of antioxidant and the balance of water.
A preparation method of novel washing powder comprises the following steps: weighing sulfonated polystyrene, sodium aluminosilicate, sodium disilicate, fatty alcohol-polyoxyethylene ether and sodium dodecyl benzene sulfonate according to a proportion, combining all the materials together, pouring the mixture into a slurry stirrer, adding water, stirring the mixture for 40 to 60 minutes under the state of the rotation speed of 800 plus materials being 1000 revolutions per minute, then adding a nonionic surfactant, a fiber antiscaling agent, protease, lipase, sodium citrate, puffing powder, an ultraviolet absorbent and an antioxidant, accelerating the mixture to 1000 plus materials being 1200 revolutions per minute, stirring the mixture for 90 minutes to prepare washing powder slurry, then stirring the washing powder slurry in a temperature-controlled sealed stirrer, controlling the temperature of the temperature-controlled stirrer to be 50 to 80 ℃, stirring the washing powder slurry for 60 to 120 minutes, filtering the washing powder slurry by using a 10-mesh screen to remove solid substances with overlarge particle size, and then inputting the slurry into a high-pressure temperature-controlled sprayer, spray drying to obtain hollow granules, cooling, transferring into soft agitator, adding mixed granule essence, stirring for 60-120 min to obtain the final product.
Detailed description of the preferred embodiment 1
The novel washing powder comprises the following components in percentage by weight: 12% of sulfonated polystyrene, 6% of sodium aluminosilicate, 8% of sodium disilicate, 3% of fatty alcohol-polyoxyethylene ether, 4% of sodium dodecyl benzene sulfonate, 15% of nonionic surfactant, 7% of fiber antiscaling agent, 2% of protease, 2% of lipase, 4% of sodium citrate, 9% of puffing powder, 6% of mixed particle essence, 3% of ultraviolet absorbent, 2% of antioxidant and the balance of water.
A preparation method of novel washing powder comprises the following steps: weighing sulfonated polystyrene, sodium aluminosilicate, sodium disilicate, fatty alcohol-polyoxyethylene ether and sodium dodecyl benzene sulfonate according to a proportion, combining all the materials together, pouring the mixture into a slurry stirrer, adding water, stirring the mixture for 60 minutes at the rotation speed of 800 revolutions per minute, then adding a nonionic surfactant, a fiber antiscale, a protease, a lipase, sodium citrate, puffed powder, an ultraviolet absorbent and an antioxidant, accelerating the mixture to 1200 revolutions per minute, stirring the mixture for 90 minutes to prepare washing powder slurry, then transferring the washing powder slurry into a temperature-controlled sealed stirrer, stirring the temperature of the temperature-controlled stirrer at 60 ℃ for 100 minutes, filtering the mixture by a 10-mesh screen to remove solid substances with overlarge particle size, then inputting the slurry into a high-pressure temperature-controlled sprayer, spray-drying the slurry to form hollow particles, cooling the hollow particles, and then conveying the hollow particles into a soft stirrer, adding the mixed granular essence, stirring with soft body for 60 min to obtain the washing powder.
Specific example 2
The novel washing powder comprises the following components in percentage by weight: 15% of sulfonated polystyrene, 11% of sodium aluminosilicate, 8% of sodium disilicate, 3% of fatty alcohol-polyoxyethylene ether, 3% of sodium dodecyl benzene sulfonate, 15% of nonionic surfactant, 6% of fiber antiscaling agent, 3% of protease, 4% of lipase, 5% of sodium citrate, 7% of puffing powder, 15% of mixed granular essence, 2% of ultraviolet absorbent, 0.5% of antioxidant and the balance of water.
A preparation method of novel washing powder comprises the following steps: weighing sulfonated polystyrene, sodium aluminosilicate, sodium disilicate, fatty alcohol-polyoxyethylene ether and sodium dodecyl benzene sulfonate according to a proportion, combining all the materials together, pouring the mixture into a slurry stirrer, adding water, stirring the mixture for 50 minutes at the rotation speed of 1000 revolutions per minute, then adding a nonionic surfactant, a fiber antiscale, a protease, a lipase, sodium citrate, puffed powder, an ultraviolet absorbent and an antioxidant, accelerating the mixture to 1100 revolutions per minute, stirring the mixture for 90 minutes to prepare washing powder slurry, then transferring the washing powder slurry into a temperature-controlled sealed stirrer, stirring the temperature of the temperature-controlled stirrer at 80 ℃ for 120 minutes, filtering the mixture by a 10-mesh screen to remove solid substances with overlarge particle size, then inputting the slurry into a high-pressure temperature-controlled sprayer, spray-drying the slurry to form hollow particles, cooling the hollow particles, and then conveying the hollow particles into a soft stirrer, adding the mixed granular essence, stirring with soft body for 80 min to obtain the washing powder.
Specific example 3
The novel washing powder comprises the following components in percentage by weight: 13% of sulfonated polystyrene, 11% of sodium aluminosilicate, 8% of sodium disilicate, 4% of fatty alcohol-polyoxyethylene ether, 3% of sodium dodecyl benzene sulfonate, 15% of nonionic surfactant, 6% of fiber antiscaling agent, 2% of protease, 4% of lipase, 6% of sodium citrate, 9% of puffing powder, 10% of mixed particle essence, 3% of ultraviolet absorbent, 1% of antioxidant and the balance of water.
A preparation method of novel washing powder comprises the following steps: weighing sulfonated polystyrene, sodium aluminosilicate, sodium disilicate, fatty alcohol-polyoxyethylene ether and sodium dodecyl benzene sulfonate according to a proportion, combining all the materials together, pouring the mixture into a slurry stirrer, adding water, stirring the mixture for 60 minutes at the rotation speed of 900 revolutions per minute, then adding a nonionic surfactant, a fiber antiscale, a protease, a lipase, sodium citrate, puffed powder, an ultraviolet absorbent and an antioxidant, accelerating the mixture to 1000 revolutions per minute, stirring the mixture for 90 minutes to prepare washing powder slurry, then transferring the washing powder slurry into a temperature-controlled sealed stirrer, stirring the temperature of the temperature-controlled stirrer at 70 ℃ for 120 minutes, filtering the mixture by a 10-mesh screen to remove solid substances with overlarge particle size, then inputting the slurry into a high-pressure temperature-controlled sprayer, spray-drying the slurry to form hollow particles, cooling the hollow particles, and then conveying the hollow particles into a soft stirrer, adding the mixed granular essence, stirring with soft body for 80 min to obtain the washing powder.
The washing powder prepared by the three embodiments has good cleaning effect and can completely reach or exceed the standard after performance detection, and meanwhile, the oxidation rate of the washing powder prepared by the three embodiments is lower than 2 percent after direct sunlight detection for 100 hours, so that the washing powder has good oxidation resistance and can meet the requirement of long-time use in families; in addition, clothes cleaned by the washing powder prepared by the method have obvious fragrance, and the fragrance has multiple layers, can be slowly emitted and can be kept for a long time.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (6)
1. A novel washing powder is characterized in that: the washing powder comprises the following components in percentage by weight: 10-15% of sulfonated polystyrene, 5-12% of sodium aluminosilicate, 5-10% of sodium disilicate, 1-4% of fatty alcohol-polyoxyethylene ether, 3-5% of sodium dodecyl benzene sulfonate, 12-16% of nonionic surfactant, 5-7% of fiber antiscale, 1-3% of protease, 1-4% of lipase, 4-6% of sodium citrate, 7-9% of puffed powder, 6-15% of mixed particle essence, 1-3% of ultraviolet absorbent, 0.5-2% of antioxidant and the balance of water.
2. A novel laundry powder according to claim 1, characterised in that: the fiber antiscaling agent is a mixed preparation and is formed by mixing resin, sodium salt, sodium perborate, sodium chloride, decomposition enzyme, polyvinyl alcohol, ethanol and water, and the mixing proportion of the components is as follows: 6-10% of resin, 0.2-0.4% of sodium salt, 0.3-0.5% of sodium perborate, 0.3-0.5% of sodium chloride, 0.4-0.6% of lyase, about 5% of ethanol and the balance of water.
3. A novel laundry powder according to claim 2, characterised in that: the mixed granular essence comprises three or more fragrances, the mixed granular essence is prepared into granules by using plant essence as a raw material, and is coated with coatings, and the plant essences of different types are coated with coatings of different thicknesses and have different dissolution levels.
4. A novel laundry powder according to claim 3, characterised in that: the ultraviolet absorbent is a mixture of an ultraviolet absorbent UV-P and an ultraviolet absorbent UV-O.
5. A novel laundry powder according to claim 4, characterised in that: the antioxidant is one or more of Tea Polyphenol (TP), tocopherol, flavonoid and butyl hydroxy anisol.
6. A method for preparing a novel laundry powder according to any of claims 1 to 5, characterized in that: the preparation method comprises the following steps: weighing sulfonated polystyrene, sodium aluminosilicate, sodium disilicate, fatty alcohol-polyoxyethylene ether and sodium dodecyl benzene sulfonate according to a proportion, combining all the materials together, pouring the mixture into a slurry stirrer, adding water, stirring the mixture for 40 to 60 minutes under the state of the rotation speed of 800 plus materials being 1000 revolutions per minute, then adding a nonionic surfactant, a fiber antiscaling agent, protease, lipase, sodium citrate, puffing powder, an ultraviolet absorbent and an antioxidant, accelerating the mixture to 1000 plus materials being 1200 revolutions per minute, stirring the mixture for 90 minutes to prepare washing powder slurry, then stirring the washing powder slurry in a temperature-controlled sealed stirrer, controlling the temperature of the temperature-controlled stirrer to be 50 to 80 ℃, stirring the washing powder slurry for 60 to 120 minutes, filtering the washing powder slurry by using a 10-mesh screen to remove solid substances with overlarge particle size, and then inputting the slurry into a high-pressure temperature-controlled sprayer, spray drying to obtain hollow granules, cooling, transferring into soft agitator, adding mixed granule essence, stirring for 60-120 min to obtain the final product.
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