CN114057272A - Ceramsite raw material for weak-base small-molecular-group spin-wave low-deuterium active water and preparation method thereof - Google Patents
Ceramsite raw material for weak-base small-molecular-group spin-wave low-deuterium active water and preparation method thereof Download PDFInfo
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- CN114057272A CN114057272A CN202111371444.2A CN202111371444A CN114057272A CN 114057272 A CN114057272 A CN 114057272A CN 202111371444 A CN202111371444 A CN 202111371444A CN 114057272 A CN114057272 A CN 114057272A
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- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
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Abstract
The invention independently develops a ceramic raw material containing various traditional Chinese medicine components and trace elements, extracts the ceramic raw material into round particles, and generates a hard ceramsite raw material through high-temperature roasting to prepare weak-base small-molecular-group spin-wave low-deuterium active water, belonging to the technical field of water quality improvement. The invention relates to a ceramsite raw material with weak base, small molecular group and low deuterium activity for water, which comprises the following components in percentage by weight: 30-50% of hexacyclic stone, 10-20% of medical stone, 10-20% of muyu stone, 10-15% of tourmaline and 20-30% of kaolin. The ceramsite material for the weak-alkali small molecular group spin wave low-deuterium active water provided by the invention has the advantages that under the action of the hexacyclic stone, the medical stone, the muyu stone and the tourmaline, the internal micropore structure is increased, the adsorption, mineralization and purification functions in water are improved, various trace beneficial elements are released into the water, the content of deuterium in the water is reduced, and the taste of the weak-alkali small molecular group spin wave low-deuterium active water is soft and sweet.
Description
Technical Field
The invention relates to the technical field of water quality improvement, in particular to a ceramsite raw material for weak-base small-molecular-group spin-wave low-deuterium active water and a preparation method thereof.
Background
With the improvement of living standard of people, the requirement of people on drinking water is higher and higher. The weak base small molecular group spin wave low deuterium active water is easy to be absorbed by human cells.
However, the existing small molecular group water is usually treated by adopting tap water to carry out a pulse electric field or a compound fluctuation excitation technology, so that the energy consumption is high, and beneficial trace elements in water cannot be increased when the water body is treated.
Disclosure of Invention
In view of the above, the present invention aims to provide a ceramsite raw material with weak base and small molecular group, spin wave and low deuterium for active water and a preparation method thereof. The ceramsite raw material for the weak-base small-molecular-group spin-wave low-deuterium active water provided by the invention can release various trace beneficial elements into water, so that the weak-base small-molecular-group spin-wave low-deuterium active water has sweet taste.
In order to achieve the above object, the present invention provides the following technical solutions:
the invention provides a ceramsite raw material for weak-base small molecular group spin wave low-deuterium active water, which comprises the following components in percentage by weight: 30-50% of hexacyclic stone, 10-20% of medical stone, 10-20% of muyu stone, 10-15% of tourmaline and 20-30% of kaolin.
The invention also provides a preparation method of the ceramsite raw material for the weak-base small molecular group spin wave low-deuterium active water, which comprises the following steps:
firstly, selecting high-quality hexacyclic ring stone, medical stone, muyu stone and tourmaline, extracting stone containing traditional Chinese medicine components and trace elements according to elements required by a human body and proportion, crushing, mixing, preparing into 600-plus 2000-mesh fine powder by a nano process, adding kaolin and water, putting into a ball rolling machine, preparing round particles of 3-10mm with different specifications according to requirements after 3 hours, drying in the sun, naturally drying, placing in a kiln for roasting, preheating at low temperature, according to the experience and the digital synthesis of the kiln thermometer, the change of the heating degree gradually is observed from the observation hole, after the trace elements are not damaged and the trace elements are raised to high temperature, the active particles containing the trace elements and the traditional Chinese medicine components are prepared by roasting for 48 to 72 hours at the high temperature of 700 and 1200 ℃, then slowly cooling, discharging, and bagging to prepare a high-quality ceramsite raw material of the weak-base small-molecular-group spin-wave deuterated active water; the process from stone selection to active particle preparation containing traditional Chinese medicine components and trace elements required by human body takes about seven days in total.
Preferably, the diameter of the round particles is 3-10 mm.
Preferably, the calcination temperature is 700-1200 ℃ and the calcination time is 48-72 hours.
The invention also provides a preparation method of the weak base small molecular group spin wave low deuterium active water, which comprises the steps of mixing the weak base small molecular group spin wave low deuterium active water with a ceramsite raw material and purified water, and decocting to obtain the weak base small molecular group spin wave low deuterium active water.
Preferably, the mixing weight ratio of the ceramsite raw material for the weak-base small molecular group spin wave low-deuterium active water to the purified water is 1: 3.
Preferably, the temperature of the decoction is 100 ℃, and the time is 3-5min after boiling.
The invention provides a ceramsite raw material for weak-base small molecular group spin wave low-deuterium active water, which comprises the following components in percentage by weight: 30-50% of hexacyclic stone, 10-20% of medical stone, 10-20% of muyu stone, 10-15% of tourmaline and 20-30% of kaolin. The ceramsite raw material for the weak base small molecular group spin wave low-deuterium active water can be used for preparing the weak base small molecular group spin wave low-deuterium active water.
Detailed Description
The invention provides a ceramsite raw material for weak-base small molecular group spin wave low-deuterium active water, which comprises the following components in percentage by weight: 30-50% of hexacyclic stone, 10-20% of medical stone, 10-20% of muyu stone, 10-15% of tourmaline and 20-30% of kaolin.
The raw material of the ceramsite for the weak-base small-molecular-group spin-wave low-deuterium active water comprises, by weight, 30-50% of hexacyclic stone, preferably 35-45%, and more preferably 38-42%. In the present invention, the hexacyclic stone is preferably a natural hexacyclic stone mineral which is composed of the following basic components: CaO: 30-50%; MgO: 15-40%; SiO 22：10～40％；Al2O3：3～9％；K2O：1～5％； Fe2O3：2～20％；TiO2：O.I～6％；P2O5：0.1～1.0％；CuO：O.1-1.05； MnO：0.1～1.0％；H2O：0.1～1.0％。
In the invention, the hexacyclic stone is a main raw material and can provide various trace elements required by human body.
The hexacyclic ring stone can be applied to the purification of various drinking water, the hexacyclic ring stone after being treated is placed in the drinking water, the anion produced by the hexacyclic ring stone can kill the harmful bacteria in the water body, achieve the purpose of sterilization, bacteriostasis and water purification, and change the drinking water into alkalescent ion water (the pH value is 7.4-8), the water molecular group becomes small, more suitable for the internal environment of human body, the human body absorption of being convenient for.
The raw material of the ceramsite for the weak-base small molecular group spin wave low-deuterium active water comprises 10-20 wt% of medical stone, preferably 12-18 wt%, and more preferably 15 wt%. In the present invention, the medical stone is preferably a natural medical stone mineral whose basic components are cobalt (Co), copper (Cu), zinc (Zn), molybdenum (Mo), chromium (Cr), vanadium (V), selenium (Se), iron (Fe), manganese (Mn), iodine (I), fluorine (F), silicon (Si), nickel (Ni), tin (Sn), lithium (Li), germanium (Ge), rubidium (Rb), strontium (Sr), boron (B), bromine (Br), arsenic (As), cerium (Ce, sh), praseodymium (Pr, p ǔ), neodymium (Nd, n Lu), promethium (Pr, p ǒ), samarium (Sm, sh ā n), europium (Eu, y ǒ u), gadolinium (Gd, g a), terbium (Tb, t, e), dysprosium (Dy, di), holmium (Ho, hu ǒ), erbium (Er, ě r), thulium (Tm, di, ytterbium), ytterbium (Yb, lutetium, Lu, l ǔ), yttrium (Y, Y ǐ) and scandium (Sc, k afng).
The raw material of the ceramsite for the weak-base small molecular group spin wave low-deuterium active water comprises 10-20 wt% of Muyu stone, preferably 12-18 wt%, and more preferably 14-16 wt%. In the present invention, the wooden fish stone is preferably a natural wooden fish stone mineral. In the invention, the natural Muyu stone mineral composition is limonite and Fe2O3The content of the lead-free acid is from 20% to 78%, other impurities are phosphate, a small amount of metasilicate and trace elements such as strontium (Sr), molybdenum (Mo), lithium (Li), zinc (Zn), selenium (Se) and the like.
The raw material of the ceramsite for the weak-base small molecular group spin wave low-deuterium active water provided by the invention comprises 20-30% by weight of tourmaline, and preferably 23-27%. In the present invention, the tourmaline is a multi-element mineral, and the main chemical component is SiO2 TiO2 CaO K2O LiO Al2O3 B2O3 MgO Na 2O Fe2O3 FeO MnO P2O5The main components of tourmaline include more than 10 trace elements such as magnesium, aluminum, iron and boron which are beneficial to human body. Because it is a structural crystal, it can generate electric ions for a long time and release negative oxygen ions in the air, and the emission quantity is 800-3. The water-soluble organic fertilizer also has the function of radiating far infrared rays, is antibacterial and bactericidal, has the characteristics of large specific surface area and strong adsorption capacity because the internal pore diameter channel keeps the original pore frame structure and molecular sieve function of mineral materials, and has super-strong adsorption capacity on residual heavy metals, organic matters, impurities and the like in drinking water. Has ion conversion function, and can convert large water molecular group and positive potential of drinking water into small molecular group and negative potential. Meanwhile, the peculiar smell of the drinking water and the residual chlorine can be removed, and the dissolved oxygen can be increased. On one hand, the mineral substances in the drinking water are reserved, and on the other hand, the mineral substances have the function of dissolving out trace elements and mineral substances beneficial to human health.
The raw material of the ceramsite for the weak-base small molecular group spin wave low-deuterium active water comprises 10-15 wt% of kaolin, and preferably 12-14 wt%. In the present invention, the kaolin, which is the main component of clay minerals, is rich in silicon, zinc, magnesium, aluminum and other minerals, and has a simple chemical molecule: AL4 (Si4O10)OH6Besides alumina, the silicon dioxide is also contained, and is a binding agent which is harmless to human bodies.
The invention also provides a preparation method of the ceramsite raw material for the weak base small molecular group spin wave deuterium-depleted active water, which comprises the following steps:
extracting and crushing the hexacyclic ring stone, the medical stone, the muyu stone and the tourmaline powder to obtain mixed powder;
adding kaolin into the mixed powder to prepare round particles;
and calcining the round particles to obtain the ceramsite material for the weak-base low-deuterium active water.
1. The invention extracts and crushes the six-ring stone, the medical stone, the muyu stone and the tourmaline powder to obtain the mixed powder. The invention preferably extracts the hexacyclic ring stone, medical stone, muyu stone and tourmaline mineral substance containing medicinal parts, the extraction method comprises the steps of firstly selecting high-quality hexacyclic ring stone, medical stone, muyu stone and tourmaline, extracting stone containing Chinese medicinal components and trace elements according to elements required by human bodies and proportion, crushing, mixing, preparing 600-plus 2000-mesh fine powder through a nano process, adding kaolin and water into a ball rolling machine, preparing 3-10mm round particles with different specifications according to requirements after 3 hours, placing the particles into a kiln after airing and natural drying, preheating at low temperature, comprehensively according to experience and kiln thermometer figure, observing the change of fire climate which is gradually increased from an observation hole, raising the temperature to high temperature after 48-72 hours and 700-plus 1200-degree high-temperature roasting, active particles containing trace elements and traditional Chinese medicine components are prepared, and then the active particles are slowly cooled, taken out of a furnace and packaged to prepare a high-quality ceramsite raw material of weak-base small-molecular-group spin-wave deuterated active water. The process from stone selection to active particle preparation containing traditional Chinese medicine components and trace elements required by human body takes about seven days in total.
In the invention, the particle size of the mixed powder is preferably 600-1000 meshes.
After the mixed powder is obtained, the kaolin is added into the mixed powder to prepare the round particles.
In the invention, the particle size of the round particles is preferably 3-10mm, the specific specification is preferably 3-4 mm, 4-5 mm, 5-6 mm, 6-7 mm, 7-8 mm, 8-9 mm and 9-10 mm to obtain the round particles, and then the round particles are calcined to obtain the ceramsite raw material for the weak-base small molecular group spin wave low-deuterium active water.
The invention preferably dries the round particles and then calcines the round particles; in the present invention, the calcination temperature is preferably 700 ℃ to 1200 ℃ and the time is preferably 48 to 72 hours. The calcination is preferably carried out in a high-frequency furnace. The calcination reaction is a chemical reaction with Δ H > 0 and Δ S > 0, and is calculated to be a spontaneous and vigorous chemical reaction of round particles under 102.32kPa and 1183K (i.e., 910 ℃), which requires a high temperature condition for "spontaneous" reaction, and the reaction proceeds as long as the temperature is maintained. The reaction is spontaneous depending on the temperature when Δ H < 0, Δ S < 0 or Δ H > 0, Δ S > 0, and the enthalpy change is dominant at low temperature and the entropy change is dominant at high temperature, and the reaction is in equilibrium when Δ G ═ 0.
The invention also provides a preparation method of the weak base small molecular group spin wave low deuterium active water, which comprises the steps of mixing the weak base small molecular group spin wave low deuterium active water with a ceramsite raw material and purified water, and decocting to obtain the weak base small molecular group spin wave low deuterium active water.
In the invention, the mixing weight ratio of the ceramsite raw material for the weak-base small molecular group spin wave low-deuterium active water to the purified water is preferably 1: 3, and the mixing is preferably carried out in a special container; the temperature of the decoction is preferably 100 deg.C, and the time is preferably 3min after boiling.
The weak base small molecular group spin wave low-deuterium active water is deuterated water, and the actually measured pH value is 9.3; the pH value of the standard weak alkaline water is 8.1-10; actually measuring the half-peak width of 92.92-95.64 Hz and NMR; deuterated water, wherein the standard NMR is 10-150; PPM; deuterium oxide (D) as deuterium substitute water2O, heavy water) was 0.05 wt.% 3- (trimethylsilyl) propionic acid-2, 2, 3, 3-D4Deuterated water of acid sodium salt. It is a safe and inexpensive source of deuterium (D) for the D/H exchange reaction. Has determined hydrogen (H) and D2Equilibrium constant of exchange of O molecules for deuterium. At D2The gelatin gel prepared in O has a higher hardness than the gel prepared in water. The influence of temperature on the crystalline state and liquid state heat capacity of the deuterium is researched by adopting a calorimetry method, and the melting point, melting point enthalpy and melting point entropy of the deuterium are measured.
The present invention provides a weak base small molecular group spin wave low deuterium active water ceramsite material and its preparation method, which are described in detail below with reference to the examples, but they should not be construed as limiting the scope of the present invention.
Example 1
A preparation method of weak base small molecular group spin wave low deuterium active water comprises the following operation steps:
weighing 35-45% of hexacyclic stone, 10-20% of medical stone and 10-20% of muyu stone: 10-15% of tourmaline, and crushing and extracting to obtain 350-1000 mesh mixed powder;
adding 15-25% of kaolin into the mixed powder, drying, preparing into round particles with different specifications of 3-10mm according to requirements after 3 hours, drying in the sun, naturally drying, then placing into a kiln for roasting, preheating at low temperature, digitally integrating according to experience and a kiln thermometer, observing the change of the temperature of the ceramsite raw material gradually rising from an observation hole, and starting to promote to high temperature when trace elements are kept not damaged; roasting in a high-frequency heating furnace at 700-;
and (3) placing the ceramsite raw material for the weak-base small-molecular-group spin-wave low-deuterium active water into a special container, adding 3 times of clean water, decocting for 3 minutes at 100 ℃, then slowly cooling, discharging from the furnace, and bagging to prepare the high-quality ceramsite raw material for the weak-base small-molecular-group spin-wave low-deuterium active water.
And (3) measuring the obtained weak base small molecular group spin wave low deuterium active water:
the pH was 9.3; the pH value of the standard weak alkaline water is 7.4-9.5; actually measuring the half-peak width of 92.92-95.64 Hz and NMR; deuterated water, wherein the standard NMR is 10-150 PPM; deuterated Water-deuterium oxide (D)2O, heavy water) was 0.05 wt.% 3- (trimethylsilyl) propionic acid-2, 2, 3, 3-D4Deuterated water of acid sodium salt.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, various modifications and decorations can be made without departing from the principle of the present invention, and these modifications and decorations should also be regarded as the protection scope of the present invention.
Claims (5)
1. The ceramsite raw material for preparing the weak-base small-molecular-group spin-wave low-deuterium active water is characterized by comprising the following components in percentage by weight: 30-50% of hexacyclic stone, 10-20% of medical stone, 10-20% of muyu stone, 10-15% of tourmaline and 20-30% of kaolin; the mineral-rich trace elements required by human bodies, including Co, Cu, Zn, Mo, Cr, V, Se, Fe, Mn, I, F, Si, Ni, Sn, Li, Ge, Rb, Sr, B, Br, As, Al, Ca, Mg, Ti and P, are integrated into the ceramsite raw material.
2. The preparation method of the ceramsite raw material with weak base and small molecular group, spin wave and low deuterium for active water as claimed in claim 1, is characterized by comprising the following steps: firstly, selecting high-quality hexacyclic ring stone, medical stone, muyu stone and tourmaline, extracting stone containing traditional Chinese medicine components and trace elements according to elements required by a human body and proportion, crushing, mixing, preparing into 600-plus 2000-mesh fine powder by a nano process, adding kaolin and water, putting into a ball rolling machine, preparing round particles of 3-10mm with different specifications according to requirements after 3 hours, drying in the sun, naturally drying, placing in a kiln for roasting, preheating at low temperature, according to the experience and the digital synthesis of a kiln thermometer, the change of the heating degree of the ceramsite raw material gradually rises is observed from an observation hole, after the trace elements are not damaged and the trace elements are raised to high temperature, the active particles containing the trace elements and the traditional Chinese medicine components are prepared by roasting for 48 to 72 hours at the high temperature of 700 and 1200 ℃, then slowly cooling, discharging, and bagging to prepare a high-quality ceramsite raw material of the weak-base small-molecular-group spin-wave deuterated active water; the process from stone selection to active particle preparation containing traditional Chinese medicine components and trace elements required by human body takes about seven days in total.
3. A preparation method of weak base small molecular group spin wave low deuterium active water is characterized in that the weak base small molecular group spin wave low deuterium active water ceramsite material of claim 1 or the weak base small molecular group spin wave low deuterium active water ceramsite material prepared by the preparation method of claim 2 is mixed with purified water and decocted to obtain the weak base small molecular group spin wave low deuterium active water.
4. The preparation method according to claim 3, wherein the mixing weight ratio of the ceramsite raw material with the weak base small molecular group, spin wave and low deuterium active water to the purified water is 1: 3.
5. The method of claim 3, wherein the frying is carried out at 100 ℃ for 3min after boiling.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN117658612A (en) * | 2023-12-05 | 2024-03-08 | 宜兴市海王陶瓷研究所 | Super-induction functional material and preparation method and application thereof |
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