CN114028251A - Artificial melanin washing and dyeing three-in-one lotion and preparation method thereof - Google Patents
Artificial melanin washing and dyeing three-in-one lotion and preparation method thereof Download PDFInfo
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- CN114028251A CN114028251A CN202111539456.1A CN202111539456A CN114028251A CN 114028251 A CN114028251 A CN 114028251A CN 202111539456 A CN202111539456 A CN 202111539456A CN 114028251 A CN114028251 A CN 114028251A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
- A61K8/492—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid having condensed rings, e.g. indol
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/10—Preparations for permanently dyeing the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention discloses an artificial melanin washing and dyeing three-in-one lotion and a preparation method thereof, wherein the three-in-one lotion comprises the following components: 5, 6-dihydroxyindole: 0.5 to 3 percent; stearic acid: 1% -4%; coconut oil acid: 1% -4%; tetradecyldimethylamine oxide: 0.2 to 2 percent; hexadecyltrimethylammonium chloride: 0.1 to 1 percent; coconut oil fatty acid diethanolamide: 0.2 to 2 percent; cysteine: 0.1% -2%; ascorbic acid ethyl ether: 0.1 to 0.5 percent; glycerol: 1% -4%; guar hydroxypropyltrimethylammonium chloride: 0.05 percent to 0.2 percent; cyclopentasiloxane: 0.5 to 2 percent; polydimethylsiloxane: 0.5 to 2 percent; quaternary ammonium salt-15: 0.05 percent to 0.1 percent; zinc PCA: 0.05 percent to 0.1 percent; proper amount of sodium bicarbonate; the balance of water, the mass percent of each component is 100 percent. The three-in-one lotion has the functions of washing, protecting and dyeing, and also has excellent antistatic and sunscreen effects.
Description
Technical Field
The invention belongs to the field of daily chemicals, and particularly relates to an artificial melanin washing and dyeing three-in-one lotion and a preparation method thereof.
Background
Today, with an increasing pace, people are increasingly pursuing functional integration, and hope that one product can have multiple functions while ensuring the effect. The two-in-one shampoo has the dual functions of cleaning and conditioning in the process of one-step hair washing, so the two-in-one shampoo is very popular with consumers. For hair coloring, it usually takes a long time. If the hair washing, protecting and dyeing are integrated, the hair dyeing is realized in the daily hair washing and protecting process, and the time of people can be greatly saved. However, the hair dyes commonly used in the market at present generally have potential toxicity, most of the hair dyes can be realized by matching two agents, and the hair dyes are not suitable for daily washing, protecting and dyeing integration.
At present, hair dye containing 5, 6-dihydroxyindole melanin is gradually exposed from the hair to the hair, and researches show that tyrosine in a human body is catalyzed and oxidized to form an active intermediate 5, 6-dihydroxyindole and then further oxidized to form melanin, and the active intermediate is utilized to biomimetic hair dyeing in vitro, so that the hair dye is green and safe. Thus, the application of 5, 6-dihydroxyindole melanin to daily washing and dyeing integration is considered.
Disclosure of Invention
The invention aims to provide an artificial melanin washing and dyeing three-in-one lotion and a preparation method thereof.
The technical scheme of the invention is as follows:
an artificial melanin washing and dyeing three-in-one lotion comprises the following components in percentage by mass:
5, 6-dihydroxyindole: 0.5 to 3 percent; stearic acid: 1% -4%; coconut oil acid: 1% -4%; tetradecyldimethylamine oxide: 0.2 to 2 percent; hexadecyltrimethylammonium chloride: 0.1 to 1 percent; coconut oil fatty acid diethanolamide: 0.2 to 2 percent; cysteine: 0.1% -2%; ascorbic acid ethyl ether: 0.1 to 0.5 percent; glycerol: 1% -4%; guar hydroxypropyltrimethylammonium chloride: 0.05 percent to 0.2 percent; cyclopentasiloxane: 0.5 to 2 percent; polydimethylsiloxane: 0.5 to 2 percent; quaternary ammonium salt-15: 0.05 percent to 0.1 percent; zinc PCA (zinc pyrrolidone carboxylate): 0.05 percent to 0.1 percent; a proper amount of sodium bicarbonate is used for adjusting the pH value to 6-7; the balance of water.
Preferably, the artificial melanin washing and dyeing three-in-one lotion comprises the following components in percentage by mass:
5, 6-dihydroxyindole: 2% -3%; stearic acid: 1% -4%; coconut oil acid: 1% -4%; tetradecyldimethylamine oxide: 0.2 to 2 percent; hexadecyltrimethylammonium chloride: 0.1 to 1 percent; coconut oil fatty acid diethanolamide: 0.2 to 2 percent; cysteine: 0.1% -2%; ascorbic acid ethyl ether: 0.1 to 0.5 percent; glycerol: 1% -4%; guar hydroxypropyltrimethylammonium chloride: 0.05 percent to 0.2 percent; cyclopentasiloxane: 0.5 to 2 percent; polydimethylsiloxane: 0.5 to 2 percent; quaternary ammonium salt-15: 0.05 percent to 0.1 percent; zinc PCA: 0.05 percent to 0.1 percent; a proper amount of sodium bicarbonate is used for adjusting the pH value to 6-7; the balance of water.
Preferably, the artificial melanin washing and dyeing three-in-one lotion comprises the following components in percentage by mass:
5, 6-dihydroxyindole: 3 percent; stearic acid: 1% -4%; coconut oil acid: 1% -4%; tetradecyldimethylamine oxide: 0.2 to 2 percent; hexadecyltrimethylammonium chloride: 0.1 to 1 percent; coconut oil fatty acid diethanolamide: 0.2 to 2 percent; cysteine: 0.1% -2%; ascorbic acid ethyl ether: 0.1 to 0.5 percent; glycerol: 1% -4%; guar hydroxypropyltrimethylammonium chloride: 0.05 percent to 0.2 percent; cyclopentasiloxane: 0.5 to 2 percent; polydimethylsiloxane: 0.5 to 2 percent; quaternary ammonium salt-15: 0.05 percent to 0.1 percent; zinc PCA: 0.05 percent to 0.1 percent; a proper amount of sodium bicarbonate is used for adjusting the pH value to 6-7; the balance of water.
In the three-in-one washing agent for washing and dyeing, 5, 6-dihydroxyindole is a coloring agent, stearic acid and coconut oil acid are solubilizing agents, tetradecyl dimethyl amine oxide is a foaming agent, hexadecyl trimethyl ammonium chloride and coconut oil fatty acid diethanolamide are emulsifying agents, cysteine and ascorbic acid ethyl ether are reducing agents, glycerin is a humectant, guar gum hydroxypropyl trimethyl ammonium chloride is a thickening agent, cyclopentadimethyl siloxane, polydimethylsiloxane and quaternary ammonium salt-15 are hair conditioners, and sodium bicarbonate is a pH value regulator and is used for regulating the washing agent to be weakly acidic, namely regulating the pH value to be 6-7. The three-in-one washing, protecting and dyeing lotion mainly utilizes 5, 6-dihydroxyindole and PCA zinc to jointly play the effects of dyeing hair, resisting static electricity and preventing sun, and other components are conventional components in the washing and protecting lotion, and the dosage of the other components is also conventional dosage, and the conventional components do not obviously contribute to black dyeing, resisting static electricity, preventing sun and the like.
The invention utilizes 5, 6-dihydroxyindole as a coloring agent, the 5, 6-dihydroxyindole can be gradually oxidized in the air without using additional stimulation, and the 5, 6-dihydroxyindole is utilized to dye hair in vitro, thereby being green and safe to human bodies. The 5, 6-dihydroxyindole also has metal chelating ability, which can form a dense conductive network with metal, the zinc PCA of the present invention is used to provide a source of metal ions, and the 5, 6-dihydroxyindole forms a melanin-metal conductive network with the zinc metal in the zinc PCA, which can reduce or even eliminate hair static. In addition, 5, 6-dihydroxyindole also has excellent ultraviolet absorption ability, so that drying up or damage to hair and scalp by ultraviolet rays can be reduced or even avoided.
The preparation method of the artificial melanin washing and dyeing three-in-one lotion comprises the following steps:
(1) mixing stearic acid, coconut oil acid and cyclopentadidimethyl siloxane, and heating to 70-90 ℃ to obtain an oil phase;
(2) mixing tetradecyl dimethyl amine oxide, hexadecyl trimethyl ammonium chloride, coconut oil fatty acid diethanolamide, cysteine, ascorbic acid ethyl ether, glycerol, guar gum hydroxypropyl trimethyl ammonium chloride, quaternary ammonium salt-15, PCA zinc and water, and heating to 70-90 ℃ to obtain a water phase;
(3) adding the water phase into the oil phase, stirring for 2-8 min, homogenizing and cooling to room temperature;
(4) adding a proper amount of sodium bicarbonate to adjust the pH value to 6-7;
(5) adding polydimethylsiloxane for homogenizing, adding 5, 6-dihydroxyindole, and mixing to obtain three-in-one lotion.
Compared with the prior art, the invention has the following characteristics and beneficial effects:
(1) 5, 6-dihydroxyindole is used as a coloring agent, and the 5, 6-dihydroxyindole is gradually oxidized and blackened in the air, so that the hair dyeing purpose can be achieved without using additional stimulation, and the hair dyeing method is safer and more environment-friendly.
(2) 5, 6-dihydroxyindole pigment micromolecules are blended in the washing and protecting process each time, the pigment is gradually accumulated and oxidized and blackened in the air, so that the hair dyeing is realized, the hair dyeing can be realized in the washing and protecting process, and the time and the labor are saved.
(3) The 5, 6-dihydroxyindole can form a melanin-metal conductive network with metal zinc in the zinc PCA, and the conductive network can reduce or even eliminate hair static electricity, so that the hair is more flexible.
(4)5, 6-dihydroxyindole also has excellent ultraviolet absorption ability, so that drying up or damage to hair and scalp by ultraviolet rays can be reduced or even avoided.
Detailed Description
The technical solution and the technical effect of the present invention will be further explained with reference to the following embodiments. The examples are only for illustrative purposes and are not intended to limit the scope of the present invention. The technical solution of the present invention is further described below with reference to specific examples.
In the following examples and comparative examples, the raw materials used were all purchased directly from the market, wherein 5, 6-dihydroxyindole was a product of Sichuan melanine Polymer materials Co., Ltd., purity was 97%; the other raw materials are all common products in the market.
Example 1
The lotion of this example had the following composition: 5, 6-dihydroxyindole: 0.5%, stearic acid: 2%, coconut oil acid: 2%, tetradecyldimethylamine oxide: 1.8%, cetyltrimethylammonium chloride: 0.4%, coconut oil fatty acid diethanolamide: 1.5%, cysteine: 1%, ascorbic acid ethyl ether: 0.4%, glycerin: 2%, guar hydroxypropyl trimonium chloride: 0.05%, cyclopenta dimethyl siloxane: 1%, polydimethylsiloxane: 1%, quaternary ammonium salt-15: 0.05%, zinc PCA: 0.05 percent of the detergent, a proper amount of sodium bicarbonate, the sodium bicarbonate is used for adjusting the pH value of the detergent to 6.5, and the balance of water is 100 percent.
Example 2
The lotion of this example had the following composition: 5, 6-dihydroxyindole: 2%, stearic acid: 2%, coconut oil acid: 2%, tetradecyldimethylamine oxide: 1.8%, cetyltrimethylammonium chloride: 0.4%, coconut oil fatty acid diethanolamide: 1.5%, cysteine: 1%, ascorbic acid ethyl ether: 0.4%, glycerin: 2%, guar hydroxypropyl trimonium chloride: 0.05%, cyclopenta dimethyl siloxane: 1%, polydimethylsiloxane: 1%, quaternary ammonium salt-15: 0.05%, zinc PCA: 0.05 percent of the detergent, a proper amount of sodium bicarbonate, the sodium bicarbonate is used for adjusting the pH value of the detergent to 6.5, and the balance of water is 100 percent.
Example 3
The lotion of this example had the following composition: 5, 6-dihydroxyindole: 3%, stearic acid: 2%, coconut oil acid: 2%, tetradecyldimethylamine oxide: 1.8%, cetyltrimethylammonium chloride: 0.4%, coconut oil fatty acid diethanolamide: 1.5%, cysteine: 1%, ascorbic acid ethyl ether: 0.4%, glycerin: 2%, guar hydroxypropyl trimonium chloride: 0.05%, cyclopenta dimethyl siloxane: 1%, polydimethylsiloxane: 1%, quaternary ammonium salt-15: 0.05%, zinc PCA: 0.05 percent of the detergent, a proper amount of sodium bicarbonate, the sodium bicarbonate is used for adjusting the pH value of the detergent to 6.5, and the balance of water is 100 percent.
Example 4
The lotion of this example had the following composition: 5, 6-dihydroxyindole: 3%, stearic acid: 2%, coconut oil acid: 2%, tetradecyldimethylamine oxide: 1.8%, cetyltrimethylammonium chloride: 0.4%, coconut oil fatty acid diethanolamide: 1.5%, cysteine: 1%, ascorbic acid ethyl ether: 0.4%, glycerin: 2%, guar hydroxypropyl trimonium chloride: 0.05%, cyclopenta dimethyl siloxane: 1%, polydimethylsiloxane: 1%, quaternary ammonium salt-15: 0.05%, zinc PCA: 0.1 percent of sodium bicarbonate, a proper amount of sodium bicarbonate, the balance of water and the balance of water, wherein the sodium bicarbonate is used for adjusting the pH value of the lotion to 6.5, and the mass percent of all the components is 100 percent.
Comparative example 1
The comparative example lotion had the following components: stearic acid: 2%, coconut oil acid: 2%, tetradecyldimethylamine oxide: 1.8%, cetyltrimethylammonium chloride: 0.4%, coconut oil fatty acid diethanolamide: 1.5%, cysteine: 1%, ascorbic acid ethyl ether: 0.4%, glycerin: 2%, guar hydroxypropyl trimonium chloride: 0.05%, cyclopenta dimethyl siloxane: 1%, polydimethylsiloxane: 1%, quaternary ammonium salt-15: 0.05%, zinc PCA: 0.05 percent of the detergent, a proper amount of sodium bicarbonate, the sodium bicarbonate is used for adjusting the pH value of the detergent to 6.5, and the balance of water is 100 percent.
Comparative example 2
The comparative example lotion had the following components: 5, 6-dihydroxyindole: 3%, stearic acid: 2%, coconut oil acid: 2%, tetradecyldimethylamine oxide: 1.8%, cetyltrimethylammonium chloride: 0.4%, coconut oil fatty acid diethanolamide: 1.5%, cysteine: 1%, ascorbic acid ethyl ether: 0.4%, glycerin: 2%, guar hydroxypropyl trimonium chloride: 0.05%, cyclopenta dimethyl siloxane: 1%, polydimethylsiloxane: 1%, quaternary ammonium salt-15: 0.05%, zinc PCA: 0.25 percent of the total weight of the components, a proper amount of sodium bicarbonate, the balance of water and the balance of water, wherein the sodium bicarbonate is used for adjusting the pH value of the lotion to 6.5.
The components of the lotions of examples 1 to 4 and comparative examples 1 to 2 are shown in Table 1. The hair dyeing effect of the lotions of examples 1 to 4 and comparative examples 1 to 2 was evaluated by the following method: applying three-in-one lotion once per day to white hair with L value of 66.2 and chromaticity of 10, and rubbing the white hair with the three-in-one lotion for 10 min; then washed by clean water and dried. The degree of hair blackness was evaluated daily. The evaluation method of the hair dyeing blackness comprises the following steps: and testing the blackness value for 3 times by using a color difference meter and taking an average value. And meanwhile, the chromaticity is obtained by referring to a chromaticity board. The blackness value L of normal black hair is 16-18, the chroma range is 2-3, and the smaller the L value or chroma is, the blacker the hair color is.
TABLE 1 Components of three-in-one lotions of examples 1 to 3 and comparative examples 1 to 2
The hair-dyeing blackness contrast using the lotions of examples 1 to 4 and comparative examples 1 to 2 is shown in Table 2. As can be seen from Table 2, the lotions of examples 1 to 4 all have the ability to blacken hair, and the blackening rate increases with the increase in the concentration of 5.6-dihydroxyindole, indicating that 5, 6-dihydroxyindole can gradually accumulate in hair care and can be oxidatively polymerized in air to blacken hair. The lotion of comparative example 1 did not contain 5, 6-dihydroxyindole and did not have the ability to darken hair. The lotion of comparative example 2 contains 5, 6-dihydroxyindole, but the metal content is too high, which has an effect on the degree of blackness.
TABLE 2 Hair dye blackness contrast
And evaluating the antistatic property of the hair after the sixth day by the following method: combing the hair after black dyeing for 50 times by using a plastic comb, measuring the surface electrostatic voltage of the hair by using a surface direct current voltmeter, and averaging the measurements for three times; while the softness of the hair was evaluated by touch. The surface electrostatic voltage of normal hair is about 4.9kV to 5.3 kV. The antistatic properties of hair using the lotions of examples 1 to 4 and comparative examples 1 to 2 are shown in Table 3. As can be seen from Table 3, the lotions of examples 1 to 4 all have good antistatic property, wherein the lotions of examples 2 to 4 with higher content of 5, 6-dihydroxyindole have better antistatic property and more smooth hair.
TABLE 3 Hair antistatic comparison
Example 1 | Example 2 | Example 3 | Example 4 | Comparative example 1 | Comparative example 2 | |
Degree of compliance | Drying fork | Is relatively compliant | Is relatively compliant | Is relatively compliant | Drying fork | Drying fork |
Surface static voltage | 2.12kV | 0.24kV | 0.13kV | 0.12kV | 5.10kV | 4.12kV |
And (3) carrying out ultraviolet resistance evaluation on the hair after the sixth day by the following method: the blackened hair was irradiated under an ultraviolet lamp for 2 hours, and the degree of breakage of the hair was evaluated. A comparison of the degree of hair breakage using the lotions of examples 1-4 and comparative examples 1-2 is shown in Table 4. As can be seen from Table 4, the hair using the lotions of examples 1 to 4 was slightly broken, indicating that all of them had a certain UV resistance, and that melanin formed by polymerization of 5, 6-dihydroxyindole had a good UV absorption ability and could protect the proteins in the hair from denaturation.
TABLE 4 Hair breakage comparison
Example 1 | Example 2 | Example 3 | Example 4 | Comparative example 1 | Comparative example 2 | |
Degree of fracture | Slight breakage | Slight breakage | Slight breakage | Slight breakage | Most of the fracture | Most of the fracture |
The foregoing are merely exemplary embodiments of the present invention, which enable those skilled in the art to understand or practice the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.
Claims (4)
1. An artificial melanin washing and dyeing three-in-one lotion is characterized in that:
the composite material comprises the following components in percentage by mass:
5, 6-dihydroxyindole: 0.5 to 3 percent; stearic acid: 1% -4%; coconut oil acid: 1% -4%; tetradecyldimethylamine oxide: 0.2 to 2 percent; hexadecyltrimethylammonium chloride: 0.1 to 1 percent; coconut oil fatty acid diethanolamide: 0.2 to 2 percent; cysteine: 0.1% -2%; ascorbic acid ethyl ether: 0.1 to 0.5 percent; glycerol: 1% -4%; guar hydroxypropyltrimethylammonium chloride: 0.05 percent to 0.2 percent; cyclopentasiloxane: 0.5 to 2 percent; polydimethylsiloxane: 0.5 to 2 percent; quaternary ammonium salt-15: 0.05 percent to 0.1 percent; zinc PCA: 0.05 percent to 0.1 percent; a proper amount of sodium bicarbonate is used for adjusting the pH value to 6-7; the balance of water.
2. The artificial melanin washing and dyeing three-in-one lotion as claimed in claim 1, which is characterized in that:
the composite material comprises the following components in percentage by mass:
5, 6-dihydroxyindole: 2% -3%; stearic acid: 1% -4%; coconut oil acid: 1% -4%; tetradecyldimethylamine oxide: 0.2 to 2 percent; hexadecyltrimethylammonium chloride: 0.1 to 1 percent; coconut oil fatty acid diethanolamide: 0.2 to 2 percent; cysteine: 0.1% -2%; ascorbic acid ethyl ether: 0.1 to 0.5 percent; glycerol: 1% -4%; guar hydroxypropyltrimethylammonium chloride: 0.05 percent to 0.2 percent; cyclopentasiloxane: 0.5 to 2 percent; polydimethylsiloxane: 0.5 to 2 percent; quaternary ammonium salt-15: 0.05 percent to 0.1 percent; zinc PCA: 0.05 percent to 0.1 percent; a proper amount of sodium bicarbonate is used for adjusting the pH value to 6-7; the balance of water.
3. The artificial melanin washing and dyeing three-in-one lotion as claimed in claim 1, which is characterized in that:
the composite material comprises the following components in percentage by mass:
5, 6-dihydroxyindole: 3 percent; stearic acid: 1% -4%; coconut oil acid: 1% -4%; tetradecyldimethylamine oxide: 0.2 to 2 percent; hexadecyltrimethylammonium chloride: 0.1 to 1 percent; coconut oil fatty acid diethanolamide: 0.2 to 2 percent; cysteine: 0.1% -2%; ascorbic acid ethyl ether: 0.1 to 0.5 percent; glycerol: 1% -4%; guar hydroxypropyltrimethylammonium chloride: 0.05 percent to 0.2 percent; cyclopentasiloxane: 0.5 to 2 percent; polydimethylsiloxane: 0.5 to 2 percent; quaternary ammonium salt-15: 0.05 percent to 0.1 percent; zinc PCA: 0.05 percent to 0.1 percent; a proper amount of sodium bicarbonate is used for adjusting the pH value to 6-7; the balance of water.
4. The preparation method of the artificial melanin washing and dyeing three-in-one lotion as claimed in any one of claims 1 to 3, which is characterized by comprising the following steps:
(1) mixing stearic acid, coconut oil acid and cyclopentadidimethyl siloxane, and heating to 70-90 ℃ to obtain an oil phase;
(2) mixing tetradecyl dimethyl amine oxide, hexadecyl trimethyl ammonium chloride, coconut oil fatty acid diethanolamide, cysteine, ascorbic acid ethyl ether, glycerol, guar gum hydroxypropyl trimethyl ammonium chloride, quaternary ammonium salt-15, PCA zinc and water, and heating to 70-90 ℃ to obtain a water phase;
(3) adding the water phase into the oil phase, stirring, homogenizing and cooling to room temperature;
(4) adding a proper amount of sodium bicarbonate to adjust the pH value to 6-7;
(5) adding polydimethylsiloxane for homogenizing, adding 5, 6-dihydroxyindole, and mixing to obtain three-in-one lotion.
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CN115006320A (en) * | 2022-05-11 | 2022-09-06 | 长沙千草颂电子商务有限公司 | Natural plant hair care agent without aniline and phenol for blackening and dyeing hair and preparation method thereof |
Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA2239191A1 (en) * | 1995-12-06 | 1997-06-12 | Bristol-Myers Squibb Company | Synthesis of quaternary melanin compounds and their use as hair dyes or for skin treatment |
EP2119429A1 (en) * | 2008-05-14 | 2009-11-18 | L'Oréal | Cosmetic composition containing a dibenzoylmethane derivative and a pyrrolidinone derivative; method for photostabilising the dibenzoylmethane derivative |
EP2191869A1 (en) * | 2008-12-01 | 2010-06-02 | L'oreal | Method for artificially colouring the skin using a mixture of carotenoid and of lipophilic green dye; novel mixture of lipophilic dyes; composition |
CN102223924A (en) * | 2008-11-25 | 2011-10-19 | 莱雅公司 | Photoprotective composition containing an unmodified gelling starch and polyamide particles |
CN104804301A (en) * | 2015-04-02 | 2015-07-29 | 安徽省康利亚实业有限公司 | Low-water-adsorbing cable material for high-speed railway motor train unit and preparation method of low-water-adsorbing cable material |
JP2018070503A (en) * | 2016-10-28 | 2018-05-10 | リアル化学株式会社 | Nonaqueous hair dye |
CN109528511A (en) * | 2019-01-17 | 2019-03-29 | 四川大学 | A kind of compound hair dye of artificial melanin and its application method |
CN110859766A (en) * | 2019-10-14 | 2020-03-06 | 澳宝化妆品(惠州)有限公司 | Scalp multi-directional nursing composition and application thereof |
CN111356438A (en) * | 2017-11-20 | 2020-06-30 | 花王株式会社 | Hair cosmetic |
CN113491654A (en) * | 2020-04-07 | 2021-10-12 | 美特瑞生物科技(上海)有限公司 | Formula of whitening skin care product |
-
2021
- 2021-12-16 CN CN202111539456.1A patent/CN114028251B/en active Active
Patent Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA2239191A1 (en) * | 1995-12-06 | 1997-06-12 | Bristol-Myers Squibb Company | Synthesis of quaternary melanin compounds and their use as hair dyes or for skin treatment |
EP2119429A1 (en) * | 2008-05-14 | 2009-11-18 | L'Oréal | Cosmetic composition containing a dibenzoylmethane derivative and a pyrrolidinone derivative; method for photostabilising the dibenzoylmethane derivative |
CN102223924A (en) * | 2008-11-25 | 2011-10-19 | 莱雅公司 | Photoprotective composition containing an unmodified gelling starch and polyamide particles |
EP2191869A1 (en) * | 2008-12-01 | 2010-06-02 | L'oreal | Method for artificially colouring the skin using a mixture of carotenoid and of lipophilic green dye; novel mixture of lipophilic dyes; composition |
CN104804301A (en) * | 2015-04-02 | 2015-07-29 | 安徽省康利亚实业有限公司 | Low-water-adsorbing cable material for high-speed railway motor train unit and preparation method of low-water-adsorbing cable material |
JP2018070503A (en) * | 2016-10-28 | 2018-05-10 | リアル化学株式会社 | Nonaqueous hair dye |
CN111356438A (en) * | 2017-11-20 | 2020-06-30 | 花王株式会社 | Hair cosmetic |
CN109528511A (en) * | 2019-01-17 | 2019-03-29 | 四川大学 | A kind of compound hair dye of artificial melanin and its application method |
CN110859766A (en) * | 2019-10-14 | 2020-03-06 | 澳宝化妆品(惠州)有限公司 | Scalp multi-directional nursing composition and application thereof |
CN113491654A (en) * | 2020-04-07 | 2021-10-12 | 美特瑞生物科技(上海)有限公司 | Formula of whitening skin care product |
Non-Patent Citations (2)
Title |
---|
DING: "Insights into the Aggregation/Deposition and Structure of a Polydopamine Film", vol. 30, no. 41 * |
吴宇婷等: "哺乳动物毛色形成机制与影响因素", vol. 30, no. 06 * |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115006320A (en) * | 2022-05-11 | 2022-09-06 | 长沙千草颂电子商务有限公司 | Natural plant hair care agent without aniline and phenol for blackening and dyeing hair and preparation method thereof |
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