CN114016081A - Self-flow type sewage-cleaning flow dividing device for manganese sulfate deep purification liquid - Google Patents
Self-flow type sewage-cleaning flow dividing device for manganese sulfate deep purification liquid Download PDFInfo
- Publication number
- CN114016081A CN114016081A CN202111314774.8A CN202111314774A CN114016081A CN 114016081 A CN114016081 A CN 114016081A CN 202111314774 A CN202111314774 A CN 202111314774A CN 114016081 A CN114016081 A CN 114016081A
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- China
- Prior art keywords
- flotation pontoon
- registration arm
- fixed
- manganese sulfate
- infusion hose
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 45
- 229940099596 manganese sulfate Drugs 0.000 title claims abstract description 16
- 235000007079 manganese sulphate Nutrition 0.000 title claims abstract description 16
- 239000011702 manganese sulphate Substances 0.000 title claims abstract description 16
- SQQMAOCOWKFBNP-UHFFFAOYSA-L manganese(II) sulfate Chemical compound [Mn+2].[O-]S([O-])(=O)=O SQQMAOCOWKFBNP-UHFFFAOYSA-L 0.000 title claims abstract description 16
- 238000004140 cleaning Methods 0.000 title claims abstract description 10
- 238000000746 purification Methods 0.000 title claims description 10
- 238000005188 flotation Methods 0.000 claims abstract description 33
- 238000001802 infusion Methods 0.000 claims abstract description 20
- 230000005484 gravity Effects 0.000 claims abstract description 5
- 230000002000 scavenging effect Effects 0.000 claims abstract description 3
- 238000005202 decontamination Methods 0.000 claims description 5
- 230000003588 decontaminative effect Effects 0.000 claims description 5
- 210000005056 cell body Anatomy 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 239000000243 solution Substances 0.000 description 11
- 239000000084 colloidal system Substances 0.000 description 4
- 238000007599 discharging Methods 0.000 description 4
- 238000004062 sedimentation Methods 0.000 description 3
- 238000005868 electrolysis reaction Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000010079 rubber tapping Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 229910003641 H2SiO3 Inorganic materials 0.000 description 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
- 229910052681 coesite Inorganic materials 0.000 description 1
- 229910052906 cristobalite Inorganic materials 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000008151 electrolyte solution Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 229910052682 stishovite Inorganic materials 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 229910052905 tridymite Inorganic materials 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C1/00—Electrolytic production, recovery or refining of metals by electrolysis of solutions
- C25C1/06—Electrolytic production, recovery or refining of metals by electrolysis of solutions or iron group metals, refractory metals or manganese
- C25C1/10—Electrolytic production, recovery or refining of metals by electrolysis of solutions or iron group metals, refractory metals or manganese of chromium or manganese
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B15/00—Operating or servicing cells
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C7/00—Constructional parts, or assemblies thereof, of cells; Servicing or operating of cells
- C25C7/06—Operating or servicing
Abstract
The utility model provides a manganese sulfate degree of depth scavenging solution gravity flow diverging device that decontaminates, be equipped with the flotation pontoon inner tube in the middle of the flotation pontoon, the registration arm passes this flotation pontoon inner tube, the flotation pontoon reciprocates along the registration arm along the change of liquid level, the registration arm is fixed on the registration arm support, the stopper is established at the registration arm lower extreme, the liquid level weight passes through the pulley system on the flotation pontoon, there is the spring in the infusion hose, the upper end system of spring is along the lower of flotation pontoon, the lower extreme and the reelpipe ware of spring are connected, the opposite side system on edge has balanced hanging flower basket under the flotation pontoon, the upper end of infusion hose is passed through the fixed pin and is connected with the flotation pontoon, infusion hose lower extreme links to each other with fixed transfer line, the mid portion relatively fixed of infusion hose is in the reelpipe ware, the bleeder valve is connected with fixed transfer line. The invention can reduce the resistance of the solution, reduce the power consumption, prolong the tank cleaning period to 15-18 days and is beneficial to the quantitative management of production.
Description
Technical Field
The invention relates to the technical field of hydrometallurgical equipment. In particular to a self-flow type decontamination flow divider for manganese sulfate deep purification liquid.
Background
In the prior production of electrolytic manganese and manganese sulfate thereof, the deep purification sedimentation tank is basically provided with a liquid discharge pipe with the height of 600-800 mm at the bottom, and the opening of the deep purification sedimentation tank is generally upwardAlthough the solution settled for 24 hours is measured, the solution is still separated into a dirty layer, a mixed flow layer and a clear liquid layer, so that when the solution is discharged, the gravity from top to bottom and the horizontal shearing force of the outward flow of the mixed flow layer exist, a spiral circumferential force is generated as a result of the action of the two forces, the solution is stirred invisibly, and the true clear liquid is difficult to achieve in practice. So the effect of sedimentation is not ideal, especially SiO2Generation of H2SiO3Colloid and Mg produced Mg (OH)2Also is colloid, and after the colloid is formed, the particles are also very fine. Due to the existence of colloid and the absence of equipment, the resistance is increased when qualified liquid is used for electrolysis, and the tank cleaning period is shortened to 8-10 days.
Disclosure of Invention
The invention aims to provide a self-flow type sewage-cleaning flow-dividing device for manganese sulfate deep-purified liquid. The method can reduce the resistance of the electrolytic solution, reduce the power consumption, prolong the tank cleaning period to 15-18 days, and is beneficial to the quantitative management of production.
The invention achieves the above purpose by the following technical scheme: the utility model provides a manganese sulfate degree of depth scavenging solution gravity flow diverging device that decontaminates, constitutes the component and includes cell body, fixed transfer line, bleeder valve, liquid level weight, infusion hose, balanced hanging flower basket, fixed pin, flotation pontoon inner tube, registration arm frame, pulley, stopper, reelpipe ware and blowoff valve, and the concrete structure and the joint relation of component are:
be equipped with the flotation pontoon inner tube in the middle of the flotation pontoon, the registration arm passes this flotation pontoon inner tube, the flotation pontoon reciprocates along the registration arm along the change of liquid level, the registration arm is fixed on the registration arm support, the stopper is established at the registration arm lower extreme, the liquid level weight passes through the pulley system on the flotation pontoon, there is the spring in the infusion hose, the upper end system of spring is along the lower of flotation pontoon, the lower extreme and the reelpipe ware of spring are connected, the opposite side system on edge has balanced hanging flower basket under the flotation pontoon, the upper end of infusion hose is passed through the fixed pin and is connected with the flotation pontoon, infusion hose lower extreme links to each other with fixed transfer line, the mid portion relatively fixed of infusion hose is in the reelpipe ware, the bleeder valve is connected with fixed transfer line, the bottom at the cell body is installed to the blowoff valve.
The scale plate is arranged outside the tank body, and the height of the liquid level in the tank body can be accurately seen through the up-and-down movement of the scale plate and the liquid level heavy hammer which are arranged outside the tank body along with the buoy.
The pipe coiling device consists of a fixed frame and a guide pulley.
For Mn-40 g/l (NH)4)2SO4100-120 g/l of manganese sulfate liquid, the distance between the tapping valve and the groove is 350-450 mm, and the distance between the stopper and the groove is 850-950 mm.
The invention has the outstanding advantages that:
1. the liquid discharge pipe can freely spiral in the pipe coiling device after passing through the pipe coiling device with a pulley guide design, and the pipe coiling device can be operated up and down very conveniently.
2. The resistance of the solution can be reduced, the power consumption is reduced, the tank cleaning period is prolonged to 15-18 days, and the quantitative management of production is facilitated.
3. Is more intuitive and can accurately measure.
Drawings
FIG. 1 is a schematic structural diagram of a self-flow type decontamination and diversion device for deep purified manganese sulfate liquid.
Labeled as: the device comprises a tank body 1, a fixed infusion tube 2, a liquid discharging valve 3, a liquid level heavy hammer 4, an infusion hose 5, a balance hanging basket 6, a fixed pin 7, a buoy 8, a buoy inner tube 9, a positioning tube 10, a positioning tube frame 11, a pulley 12, a limiter 13, a tube coiling device 14, a drain valve 15 and a guide pulley 16.
Detailed Description
The technical solution of the present invention is further illustrated by the accompanying drawings and examples.
As shown in fig. 1, the manganese sulfate deep purification liquid self-flow type decontamination and diversion device of the present invention comprises a groove body 1, a fixed infusion tube 2, a liquid discharge valve 3, a liquid level weight 4, an infusion hose 5, a balance hanging basket 6, a fixed pin 7, a float 8, a float inner tube 9, a positioning tube 10, a positioning tube frame 11, a pulley 12, a stopper 13, a tube coiling device 14, a blowdown valve 15 and a guide pulley 16, and the specific structure and connection relationship of the components are as follows:
be equipped with flotation pontoon inner tube 9 in the middle of the flotation pontoon 8, this flotation pontoon inner tube 9 is passed to registration arm 10, flotation pontoon 8 reciprocates along registration arm 10 along the change of liquid level, registration arm 10 is fixed on location pipe support 11, stopper 13 is established at registration arm 10 lower extreme, liquid level weight 4 is on flotation pontoon 8 through pulley 12, there is spring 17 in the infusion hose 5, spring 17's upper end is along the lower edge of flotation pontoon, spring 17's lower extreme and reelpipe ware 14 are connected, another side on edge is had balanced hanging flower basket 6 under flotation pontoon 8, so that the weight balance after infusion hose 5 income water, be unlikely to the card and die at registration arm 10 and the space of registration arm 8. The upper end of the transfusion hose 5 is connected with a buoy 8 through a fixing pin 7, the lower end of the transfusion hose 5 is connected with the fixed transfusion tube 2, the middle part of the transfusion hose 5 is relatively fixed in a tube coiling device 14, and the liquid discharging valve 3 is connected with the fixed transfusion tube 2. The lower end of the tank body 1 is provided with a blowoff valve 15.
The distance between the tapping valve 3 and the bottom of the tank is 350-450 mm, and the distance between the limiter 13 and the bottom of the tank is 850-950 mm.
The scale plate is arranged outside the tank body, so that the liquid level can be accurately measured, and the level of the liquid level in the tank can be accurately seen through the scale plate arranged outside the tank body and the liquid level heavy hammer moving up and down along with the buoy.
The pipe coiling device 14 is composed of a positioning pipe frame 11 and a guide pulley 16.
The installation and operation steps of the self-flowing type clear and turbid liquid flow dividing device after the deep purification of the manganese sulfate are as follows:
1. the main components of the transfusion hose 5, the positioning pipe 10, the limiter 13, the pipe winder 14 and the like are arranged in the groove in advance, when the solution is filled in the elevated groove, the floating barrel 8 and the balance hanging basket 6 are arranged, meanwhile, the transfusion hose 5 is filled with water, and the weight is added in the hanging basket 6 to ensure that the transfusion hose 5 can float up and down freely in the middle of the floating pipe 8.
2. The liquid level weight 4 is tied on the buoy 8 through the pulley 12, and then the device can be used.
The device is 25m in a pilot plant3When the liquid after deep purification is stood for 24 hours in the tank and the supernatant is extracted and filtered for electrolysis, the tank can be operated for 15 to 18 days without cleaning the tank.
The working principle and the process are as follows:
after the device is adjusted, as long as the liquid discharging valve 3 is opened, the solution flows out statically and slowly from top to bottom, at least more than 90% of the solution is clear, only a small amount of turbid matters possibly flow out when the lowest liquid discharging level is approached, and the solution can be stored separately and returned to the next round of liquid flow and then kept still.
Claims (5)
1. The utility model provides a manganese sulfate degree of depth scavenging solution gravity flow diverging device that decontaminates, its characterized in that constitutes the component and includes cell body, fixed transfer line, bleeder valve, liquid level weight, infusion hose, balanced hanging flower basket, fixed pin, flotation pontoon inner tube, registration arm, location pipe support, pulley, stopper, reelpipe ware and blowoff valve, and the concrete structure and the relation of connection of component are:
be equipped with the flotation pontoon inner tube in the middle of the flotation pontoon, the registration arm passes this flotation pontoon inner tube, the flotation pontoon reciprocates along the registration arm along the change of liquid level, the registration arm is fixed on the registration arm support, the stopper is established at the registration arm lower extreme, the liquid level weight passes through the pulley system on the flotation pontoon, there is the spring in the infusion hose, the upper end system of spring is along the lower of flotation pontoon, the lower extreme and the reelpipe ware of spring are connected, the opposite side system on edge has balanced hanging flower basket under the flotation pontoon, the upper end of infusion hose is passed through the fixed pin and is connected with the flotation pontoon, infusion hose lower extreme links to each other with fixed transfer line, the mid portion relatively fixed of infusion hose is in the reelpipe ware, the bleeder valve is connected with fixed transfer line, the bottom at the cell body is installed to the blowoff valve.
2. The self-flowing self-cleaning flow-dividing device for the manganese sulfate deep-purified liquid as claimed in claim 1, wherein the distance between the liquid discharge valve and the bottom of the tank is 350-450 mm.
3. The self-flowing type sewage-cleaning and shunting device for the manganese sulfate deep-purified liquid as claimed in claim 1, wherein the distance between the limiting stopper and the bottom of the groove is 850-950 mm.
4. The manganese sulfate deep purification liquid self-flowing type decontamination shunting device as claimed in claim 1, wherein a scale plate is arranged outside the tank body, and the level of the liquid level in the tank can be accurately seen through the scale plate and the liquid level heavy hammer which are arranged outside the tank body and move up and down along with the buoy.
5. The manganese sulfate deep purification liquid gravity flow type decontamination shunting device according to claim 1, wherein the pipe coiling device is composed of a fixed frame and a guide pulley.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111314774.8A CN114016081A (en) | 2021-11-08 | 2021-11-08 | Self-flow type sewage-cleaning flow dividing device for manganese sulfate deep purification liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111314774.8A CN114016081A (en) | 2021-11-08 | 2021-11-08 | Self-flow type sewage-cleaning flow dividing device for manganese sulfate deep purification liquid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN114016081A true CN114016081A (en) | 2022-02-08 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202111314774.8A Pending CN114016081A (en) | 2021-11-08 | 2021-11-08 | Self-flow type sewage-cleaning flow dividing device for manganese sulfate deep purification liquid |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN114016081A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2532064Y (en) * | 2002-03-05 | 2003-01-22 | 向辉 | Automatic on/off medicine filling machine without electricity |
| CN202246359U (en) * | 2011-09-16 | 2012-05-30 | 河南城建学院 | Gravity settlement sludge thickening tower |
| CN203075709U (en) * | 2012-10-24 | 2013-07-24 | 中国石油化工股份有限公司 | Settling tank for automatic solid-liquid separation |
| CN105002523A (en) * | 2015-08-27 | 2015-10-28 | 吉首大学 | Manganese electrolysis liquid supplementing system |
| CN211056796U (en) * | 2019-10-29 | 2020-07-21 | 河北海天环保工程设备股份有限公司 | Self-floating decanter |
-
2021
- 2021-11-08 CN CN202111314774.8A patent/CN114016081A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2532064Y (en) * | 2002-03-05 | 2003-01-22 | 向辉 | Automatic on/off medicine filling machine without electricity |
| CN202246359U (en) * | 2011-09-16 | 2012-05-30 | 河南城建学院 | Gravity settlement sludge thickening tower |
| CN203075709U (en) * | 2012-10-24 | 2013-07-24 | 中国石油化工股份有限公司 | Settling tank for automatic solid-liquid separation |
| CN105002523A (en) * | 2015-08-27 | 2015-10-28 | 吉首大学 | Manganese electrolysis liquid supplementing system |
| CN211056796U (en) * | 2019-10-29 | 2020-07-21 | 河北海天环保工程设备股份有限公司 | Self-floating decanter |
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