CN113977788A - Multimedia crystal ball ornament and preparation method thereof - Google Patents
Multimedia crystal ball ornament and preparation method thereof Download PDFInfo
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- CN113977788A CN113977788A CN202111514733.3A CN202111514733A CN113977788A CN 113977788 A CN113977788 A CN 113977788A CN 202111514733 A CN202111514733 A CN 202111514733A CN 113977788 A CN113977788 A CN 113977788A
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- crystal ball
- crystal
- multimedia
- polishing
- ball
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28D—WORKING STONE OR STONE-LIKE MATERIALS
- B28D5/00—Fine working of gems, jewels, crystals, e.g. of semiconductor material; apparatus or devices therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24B—MACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
- B24B1/00—Processes of grinding or polishing; Use of auxiliary equipment in connection with such processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B44—DECORATIVE ARTS
- B44C—PRODUCING DECORATIVE EFFECTS; MOSAICS; TARSIA WORK; PAPERHANGING
- B44C5/00—Processes for producing special ornamental bodies
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
Abstract
The invention provides a multimedia crystal ball ornament and a preparation method thereof, and relates to the technical field of crystal balls. The multimedia crystal ball ornament comprises a crystal ball and a crystal ball base, wherein the crystal ball is made of a natural crystal column, the crystal ball base is made of resin, and the crystal ball base are connected through grafting glue. Through soaking with wetting agent solution before the crystal ball is polished, make the surface of crystal ball fully moistened by water, then add certain polishing solution at the in-process of polishing and polish, make the impurity of crystal ball diminish and realize acid-base balance, the material stability of crystal ball strengthens when polishing, avoid it to appear the crackle at the in-process of polishing, then diacetone acrylamide and vinyl monomer copolymerization in the polishing solution, can improve the compactness on crystal ball surface greatly, thereby improve the hardness of crystal ball, make it have good early polishing nature and anti-stackability.
Description
Technical Field
The invention relates to the technical field of crystal balls, in particular to a multimedia crystal ball ornament and a preparation method thereof.
Background
The crystal ball is a transparent spherical object processed by a natural crystal column, the crystal is a crystal of silicon dioxide, and has higher hardness and cool touch compared with glass and transparent plastic, and only the crystal can transmit light under a polarization test.
The grinding of the crystal ball comprises two types of manual grinding and machine grinding, wherein the generation of one ball consumes 4-6 times more materials than the weight of the ball, and the ball is very risky when being ground into a circle, is easy to crack and is abandoned, and meanwhile, the natural crystal column also has the problems of long time and low working efficiency when being ground into a formed crystal ball manually.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides a multimedia crystal ball ornament and a preparation method thereof, and solves the problems that the crystal ball is low in polishing efficiency and is easy to crack in the polishing process.
(II) technical scheme
In order to achieve the purpose, the invention is realized by the following technical scheme: a preparation method of a multimedia crystal ball ornament comprises the following steps:
s1 preparation of crystal ball raw material
Selecting a natural crystal column with certain quality, placing the natural crystal column in clear water, cleaning and removing impurities, selecting a crystal ball base with a size matched with that of a crystal ball, placing the crystal ball base in the clear water, and cleaning and removing impurities;
s2 crystal ball blank making
Cutting the cleaned and impurity-removed natural crystal column in the step S1 by a cutting machine to obtain a crystal ball blank with a certain size, and then soaking the crystal ball blank in a wetting agent solution for 1-1.5 hours;
s3, crystal ball polishing and grinding
Placing the crystal ball blank soaked in the polishing solution in the step S2 in a stirring barrel, adding water during vibration for 5-6 hours, then placing the crystal ball blank in a ball mill for fine polishing, and simultaneously adding a certain amount of polishing solution for 2-3 hours;
s4 crystal ball ornament assembly
And (3) placing the finished product of the crystal ball polished and polished in the step S3 in clean water for cleaning again, drying by an air heater, performing vacuum coating on the finished product of the crystal ball, adopting a sputtering coating process to form a film with the thickness of 90-110nm, and finally connecting the crystal ball with the crystal ball base in the step S1 through a grafting adhesive to obtain the finished multimedia crystal ball ornament.
Preferably, the polishing solution is prepared from the following raw materials in parts by weight: 50-80 parts of water, 5-8 parts of iron powder, 3-5 parts of aluminum oxide, 0.5-0.8 part of dispersing agent, 0.2-0.3 part of wetting agent, 0.1-0.5 part of emulsifier, 2-3 parts of adipic dihydrazide, 0.1-0.2 part of initiator, 0.05-0.15 part of oxidant, 0.3-0.8 part of zinc oxide, 0.1-0.15 part of reducing agent and 1-3 parts of diacetone acrylamide.
Preferably, the dispersant is one or more of triethylhexyl phosphoric acid, sodium dodecyl sulfate, methyl amyl alcohol, polyacrylamide and fatty acid polyethylene glycol ester, and the emulsifier is one or more of fatty acid soap, alkyl sulfate, N-dodecyl dimethylamine and other amine derivatives, polyoxypropylene ether, ethylene oxide and propylene oxide block copolymer.
Preferably, the initiator is one or a mixture of sodium persulfate, ammonium persulfate and potassium persulfate, the oxidant is one or a mixture of sodium percarbonate, sodium perborate and potassium perborate, and the reducing agent is sodium sulfite.
Preferably, the wetting agent is one of an anionic surfactant and a nonionic surfactant or a mixture of the two.
Preferably, in the step S3, the driving device of the stirring barrel is a stirring motor, and a certain weight of 300- & lt340- & gt-mesh carborundum and quartz abrasive is put into the stirring barrel.
Preferably, a multi-media crystal ball goods of furniture for display rather than for use, including crystal ball and crystal ball base, the material of crystal ball is natural crystal post, the material of crystal ball base is the resin, link to each other through graft glue between crystal ball and the crystal ball base
(III) advantageous effects
The invention provides a multimedia crystal ball ornament and a preparation method thereof. The method has the following beneficial effects:
1. according to the invention, the surface of the crystal ball is fully wetted by water by soaking the crystal ball with a wetting agent solution before polishing, then a certain polishing solution is added in the polishing process for polishing, so that the impurities of the crystal ball are reduced and acid-base balance is realized, the stability of the crystal ball is enhanced during polishing, cracks are avoided in the polishing process, then diacetone acrylamide and vinyl monomer in the polishing solution are copolymerized, a polymer with an active group ketocarbonyl can be formed, the polymer with the active group ketocarbonyl can react with adipic acid dihydrazide dissociated in the polishing solution, self-crosslinking is realized, the compactness of the surface of the crystal ball can be greatly improved, and the hardness of the crystal ball is improved, so that the crystal ball has good early polishing property and anti-stacking property.
2. According to the invention, the crystal ball blank is placed in the stirring barrel for preliminary polishing, and then is placed in the ball mill for fine polishing after polishing, and a certain amount of polishing liquid is added in the polishing process, so that the surface of the crystal ball can be fully wetted, the polishing is convenient, and the efficiency of manufacturing the crystal ball is greatly improved.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows:
the embodiment of the invention provides a preparation method of a multimedia crystal ball ornament, which comprises the following steps:
s1 preparation of crystal ball raw material
Selecting a natural crystal column with certain quality, placing the natural crystal column in clear water, cleaning and removing impurities, selecting a crystal ball base with a size matched with that of a crystal ball, placing the crystal ball base in the clear water, and cleaning and removing impurities;
s2 crystal ball blank making
Cutting the cleaned and impurity-removed natural crystal column in the step S1 by a cutting machine to obtain a crystal ball blank with a certain size, and then soaking the crystal ball blank in a wetting agent solution for 1-1.5 hours;
s3, crystal ball polishing and grinding
Placing the crystal ball blank soaked in the polishing solution in the step S2 in a stirring barrel, adding water during vibration for 5-6 hours, then placing the crystal ball blank in a ball mill for fine polishing, and simultaneously adding a certain amount of polishing solution for 2-3 hours;
s4 crystal ball ornament assembly
And (3) placing the finished product of the polished and polished crystal ball in the step S3 in clear water for cleaning again, drying by an air heater, performing vacuum coating on the finished product of the crystal ball, adopting a sputtering coating process, wherein the film thickness is 90-110nm, so that the crystal ball has a gradual change or monochrome mirror surface effect, has the performances of salt spray resistance, high and low temperature resistance, good paint film adhesion and the like, and prolongs the service life of the crystal ball, and finally connecting the crystal ball with the crystal ball base in the step S1 through a grafting adhesive to obtain the finished product of the multimedia crystal ball ornament.
The polishing solution is prepared from the following raw materials in parts by weight: 50-80 parts of water, 5-8 parts of iron powder, 3-5 parts of aluminum oxide, 0.5-0.8 part of dispersing agent, 0.2-0.3 part of wetting agent, 0.1-0.5 part of emulsifier, 2-3 parts of adipic acid dihydrazide, 0.1-0.2 part of initiator, 0.05-0.15 part of oxidant, 0.3-0.8 part of zinc oxide, 0.1-0, 15 parts of reducing agent and 1-3 parts of diacetone acrylamide, wherein the diacetone acrylamide is a special functional monomer, contains vinyl and ketocarbonyl in a molecule, can be copolymerized with other vinyl monomers to form a polymer with active group ketocarbonyl, and the ketocarbonyl can react with the adipic acid dihydrazide to generate hydrazone and water at normal temperature and can carry out reversible reaction, the polymer with the active group ketocarbonyl can react with the adipic acid dihydrazide free in the polishing solution, the self-crosslinking is realized, and the compactness of the surface of the crystal ball can be greatly improved, so that the hardness of the crystal ball is improved, and the crystal ball has good early polishing property and stacking resistance.
The dispersing agent is one or a mixture of more of triethylhexyl phosphoric acid, sodium dodecyl sulfate, methyl amyl alcohol, polyacrylamide and fatty acid polyglycol ester, the components in the polishing solution can be prevented from precipitating through the dispersing agent, the components in the polishing solution can be ensured to be uniformly contacted with the crystal ball, the emulsifying agent is one or a mixture of more of fatty acid soap, alkyl sulfate, N-dodecyl dimethylamine and other amine derivatives, polyoxypropylene ether, ethylene oxide and propylene oxide block copolymers, and immiscible liquid in the polishing solution can be effectively subjected to phase dissolution through the emulsifying agent.
The initiator is one or a mixture of more of sodium persulfate, ammonium persulfate and potassium persulfate, the oxidation reaction and the reduction reaction in the polishing solution can be accelerated through the initiator, the processing and manufacturing time of the crystal ball is reduced, the oxidant is one or a mixture of more of sodium percarbonate, sodium perborate and potassium perborate, the reducing agent is sodium sulfite, impurities of the crystal ball can be reduced through the oxidant and the reducing agent, acid-base balance is realized, the substance stability of the crystal ball is enhanced during polishing, and cracks are avoided during polishing.
The wetting agent is one or a mixture of anionic surfactant and nonionic surfactant, and is used for wetting the solid material by reducing the surface tension of crystal spheres so that water can spread on the surface of the solid material or penetrate into the surface of the solid material.
In the step S3, the driving device of the stirring barrel is a stirring motor, a certain weight of 300-plus 340-mesh carborundum and quartz abrasive are put into the stirring barrel, and the certain weight of 300-plus 340-mesh carborundum and quartz abrasive are put into the stirring barrel, and then the crystal ball is placed inside the stirring barrel for stirring, so that the outer corner of the crystal ball can be ground flat, and subsequent fine grinding is facilitated.
The utility model provides a multi-media crystal ball goods of furniture for display rather than for use, includes crystal ball and crystal ball base, and the material of crystal ball is natural crystal post, and the material of crystal ball base is the resin, links to each other through graft glue between crystal ball and the crystal ball base
Example two:
the embodiment of the invention provides a preparation method of a multimedia crystal ball ornament, which comprises the following steps:
s1 preparation of crystal ball raw material
Selecting a natural crystal column with certain quality, placing the natural crystal column in clear water, cleaning and removing impurities, selecting a crystal ball base with a size matched with that of a crystal ball, placing the crystal ball base in the clear water, and cleaning and removing impurities;
s2 crystal ball blank making
Cutting the cleaned and impurity-removed natural crystal column in the step S1 by a cutting machine to obtain a crystal ball blank with a certain size, and then soaking the crystal ball blank in a wetting agent solution for 1-1.5 hours;
s3, crystal ball polishing and grinding
Placing the crystal ball blank soaked in the polishing solution in the step S2 in a stirring barrel, adding water during vibration for 5-6 hours, then placing the crystal ball blank in a ball mill for fine polishing, and simultaneously adding a certain amount of polishing solution for 2-3 hours;
s4 crystal ball ornament assembly
And (3) placing the finished product of the polished and polished crystal ball in the step S3 in clear water for cleaning again, drying by an air heater, performing vacuum coating on the finished product of the crystal ball, adopting a sputtering coating process, wherein the film thickness is 90-110nm, so that the crystal ball has a gradual change or monochrome mirror surface effect, has the performances of salt spray resistance, high and low temperature resistance, good paint film adhesion and the like, and prolongs the service life of the crystal ball, and finally connecting the crystal ball with the crystal ball base in the step S1 through a grafting adhesive to obtain the finished product of the multimedia crystal ball ornament.
The polishing solution is prepared from the following raw materials in parts by weight: 60-80 parts of water, 4-8 parts of iron powder, 3-5 parts of aluminum oxide, 0.6-0.8 part of dispersing agent, 0.15-0.3 part of wetting agent, 0.3-0.5 part of emulsifier, 3-5 parts of adipic acid dihydrazide, 0.1-0.2 part of initiator, 0.05-0.15 part of oxidant, 0.3-0.8 part of zinc oxide, 0.1-0, 15 parts of reducing agent and 2-3 parts of diacetone acrylamide, wherein the diacetone acrylamide is a special functional monomer, contains vinyl and ketocarbonyl in a molecule, can be copolymerized with other vinyl monomers to form a polymer with active group ketocarbonyl, and the ketocarbonyl can react with the adipic acid dihydrazide to generate hydrazone and water at normal temperature and can carry out reversible reaction, the polymer with the active group ketocarbonyl can react with the adipic acid dihydrazide free in the polishing solution, the self-crosslinking is realized, and the compactness of the surface of the crystal ball can be greatly improved, so that the hardness of the crystal ball is improved, and the crystal ball has good early polishing property and stacking resistance.
The dispersing agent is one or a mixture of more of triethyl hexyl phosphoric acid, polyacrylamide and fatty acid polyglycol ester, the components in the polishing solution can be prevented from precipitating through the dispersing agent, the components in the polishing solution can be ensured to be uniformly contacted with crystal balls, the emulsifying agent is one or a mixture of more of fatty acid soap, alkyl sulfate, N-dodecyl dimethylamine and other amine derivatives, polyoxypropylene ether, ethylene oxide and propylene oxide block copolymers, and immiscible liquid in the polishing solution can be effectively dissolved through the emulsifying agent.
The initiator is one or a mixture of more of sodium persulfate, ammonium persulfate and potassium persulfate, the oxidation reaction and the reduction reaction in the polishing solution can be accelerated through the initiator, the processing and manufacturing time of the crystal ball is reduced, the oxidant is one or a mixture of more of sodium percarbonate, sodium perborate and potassium perborate, the reducing agent is sodium sulfite, impurities of the crystal ball can be reduced through the oxidant and the reducing agent, acid-base balance is realized, the stability of the crystal ball is enhanced during polishing, and cracks are avoided during polishing.
The wetting agent is one or a mixture of anionic surfactant and nonionic surfactant, and is used for wetting the solid material by reducing the surface tension of crystal spheres so that water can spread on the surface of the solid material or penetrate into the surface of the solid material.
In the step S3, a driving device of the stirring barrel is a stirring motor, a certain weight of 300-mesh 400-mesh carborundum and quartz grinding materials are put into the stirring barrel, the certain weight of 300-mesh 400-mesh carborundum and quartz grinding materials are put into the stirring barrel, then the crystal ball is placed in the stirring barrel to be stirred, the outer corner angle of the crystal ball can be ground flat, and subsequent fine grinding is facilitated.
The utility model provides a multi-media crystal ball goods of furniture for display rather than for use, includes crystal ball and crystal ball base, the material of crystal ball is natural crystal post, the material of crystal ball base is the resin, link to each other through graft glue between crystal ball and the crystal ball base
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (7)
1. A preparation method of a multimedia crystal ball ornament is characterized by comprising the following steps: the method comprises the following steps:
s1 preparation of crystal ball raw material
Selecting a natural crystal column with certain quality, placing the natural crystal column in clear water, cleaning and removing impurities, selecting a crystal ball base with a size matched with that of a crystal ball, placing the crystal ball base in the clear water, and cleaning and removing impurities;
s2 crystal ball blank making
Cutting the cleaned and impurity-removed natural crystal column in the step S1 by a cutting machine to obtain a crystal ball blank with a certain size, and then soaking the crystal ball blank in a wetting agent solution for 1-1.5 hours;
s3, crystal ball polishing and grinding
Placing the crystal ball blank soaked in the polishing solution in the step S2 in a stirring barrel, adding water during vibration for 5-6 hours, then placing the crystal ball blank in a ball mill for fine polishing, and simultaneously adding a certain amount of polishing solution for 2-3 hours;
s4 crystal ball ornament assembly
And (3) placing the finished product of the crystal ball polished and polished in the step S3 in clean water for cleaning again, drying by an air heater, performing vacuum coating on the finished product of the crystal ball, adopting a sputtering coating process to form a film with the thickness of 90-110nm, and finally connecting the crystal ball with the crystal ball base in the step S1 through a grafting adhesive to obtain the finished multimedia crystal ball ornament.
2. The method as claimed in claim 1, wherein the step of manufacturing the multimedia crystal ball ornament comprises: the polishing solution is prepared from the following raw materials in parts by weight: 50-80 parts of water, 5-8 parts of iron powder, 3-5 parts of aluminum oxide, 0.5-0.8 part of dispersing agent, 0.2-0.3 part of wetting agent, 0.1-0.5 part of emulsifier, 2-3 parts of adipic dihydrazide, 0.1-0.2 part of initiator, 0.05-0.15 part of oxidant, 0.3-0.8 part of zinc oxide, 0.1-0.15 part of reducing agent and 1-3 parts of diacetone acrylamide.
3. The method as claimed in claim 2, wherein the step of manufacturing the multimedia crystal ball ornament comprises the steps of: the dispersing agent is one or a mixture of more of triethyl hexyl phosphoric acid, sodium dodecyl sulfate, methyl amyl alcohol, polyacrylamide and fatty acid polyglycol ester, and the emulsifying agent is one or a mixture of more of fatty acid soap, alkyl sulfate, N-dodecyl dimethylamine and other amine derivatives, polyoxypropylene ether, ethylene oxide and propylene oxide block copolymer.
4. The method as claimed in claim 2, wherein the step of manufacturing the multimedia crystal ball ornament comprises: the initiator is one or a mixture of more of sodium persulfate, ammonium persulfate and potassium persulfate, the oxidant is one or a mixture of more of sodium percarbonate, sodium perborate and potassium perborate, and the reducing agent is sodium sulfite.
5. The method as claimed in claim 2, wherein the step of manufacturing the multimedia crystal ball ornament comprises the steps of: the wetting agent is one or a mixture of two of an anionic surfactant and a nonionic surfactant.
6. The method as claimed in claim 1, wherein the step of manufacturing the multimedia crystal ball ornament comprises: in the step S3, the driving device of the stirring barrel is a stirring motor, and a certain weight of 300-.
7. A multimedia crystal ball decoration made according to the method of claims 1-6, comprising a crystal ball and a crystal ball base, wherein: the material of crystal ball is natural crystal post, the material of crystal ball base is resin, link to each other through the grafting glue between crystal ball and the crystal ball base.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202111514733.3A CN113977788A (en) | 2021-12-13 | 2021-12-13 | Multimedia crystal ball ornament and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202111514733.3A CN113977788A (en) | 2021-12-13 | 2021-12-13 | Multimedia crystal ball ornament and preparation method thereof |
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| CN202111514733.3A Pending CN113977788A (en) | 2021-12-13 | 2021-12-13 | Multimedia crystal ball ornament and preparation method thereof |
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