CN113967236A - Freeze-dried sealwort and process - Google Patents
Freeze-dried sealwort and process Download PDFInfo
- Publication number
- CN113967236A CN113967236A CN202111181381.4A CN202111181381A CN113967236A CN 113967236 A CN113967236 A CN 113967236A CN 202111181381 A CN202111181381 A CN 202111181381A CN 113967236 A CN113967236 A CN 113967236A
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- China
- Prior art keywords
- freeze
- rhizoma polygonati
- freezing
- drying
- polygonatum
- Prior art date
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Links
- 238000000034 method Methods 0.000 title claims abstract description 18
- 230000008569 process Effects 0.000 title claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 19
- 238000007710 freezing Methods 0.000 claims abstract description 16
- 230000008014 freezing Effects 0.000 claims abstract description 16
- 238000004108 freeze drying Methods 0.000 claims abstract description 15
- 238000005516 engineering process Methods 0.000 claims abstract description 13
- 238000005520 cutting process Methods 0.000 claims abstract description 9
- 238000007789 sealing Methods 0.000 claims abstract description 8
- 238000005406 washing Methods 0.000 claims abstract description 5
- 239000013543 active substance Substances 0.000 claims abstract description 3
- 230000000877 morphologic effect Effects 0.000 claims abstract description 3
- 230000009467 reduction Effects 0.000 claims abstract description 3
- 238000004806 packaging method and process Methods 0.000 claims description 10
- 241000037831 Polygonatum sibiricum Species 0.000 claims description 9
- 241000756042 Polygonatum Species 0.000 claims description 5
- 230000007306 turnover Effects 0.000 claims description 5
- 241000037826 Polygonatum kingianum Species 0.000 claims description 4
- 239000004743 Polypropylene Substances 0.000 claims description 4
- 238000004140 cleaning Methods 0.000 claims description 4
- OSVXSBDYLRYLIG-UHFFFAOYSA-N dioxidochlorine(.) Chemical compound O=Cl=O OSVXSBDYLRYLIG-UHFFFAOYSA-N 0.000 claims description 4
- 229920001903 high density polyethylene Polymers 0.000 claims description 4
- 239000004700 high-density polyethylene Substances 0.000 claims description 4
- 241000196324 Embryophyta Species 0.000 claims description 3
- 230000003247 decreasing effect Effects 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 239000012785 packaging film Substances 0.000 claims description 3
- 229920006280 packaging film Polymers 0.000 claims description 3
- -1 polypropylene Polymers 0.000 claims description 3
- 238000005086 pumping Methods 0.000 claims description 3
- 239000002689 soil Substances 0.000 claims description 3
- 238000009777 vacuum freeze-drying Methods 0.000 claims description 3
- 239000004155 Chlorine dioxide Substances 0.000 claims description 2
- 241001468611 Polygonatum cyrtonema Species 0.000 claims description 2
- 239000000654 additive Substances 0.000 claims description 2
- 230000000996 additive effect Effects 0.000 claims description 2
- 230000008859 change Effects 0.000 claims description 2
- 235000019398 chlorine dioxide Nutrition 0.000 claims description 2
- 239000002131 composite material Substances 0.000 claims description 2
- 238000007599 discharging Methods 0.000 claims description 2
- 235000013305 food Nutrition 0.000 claims description 2
- 230000014759 maintenance of location Effects 0.000 claims description 2
- 244000005700 microbiome Species 0.000 claims description 2
- 239000004033 plastic Substances 0.000 claims description 2
- 229920003023 plastic Polymers 0.000 claims description 2
- 229920001155 polypropylene Polymers 0.000 claims description 2
- 238000009210 therapy by ultrasound Methods 0.000 claims description 2
- 238000009461 vacuum packaging Methods 0.000 claims description 2
- 239000012535 impurity Substances 0.000 claims 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 1
- 238000009412 basement excavation Methods 0.000 claims 1
- 239000000460 chlorine Substances 0.000 claims 1
- 229910052801 chlorine Inorganic materials 0.000 claims 1
- 239000012528 membrane Substances 0.000 claims 1
- 230000000149 penetrating effect Effects 0.000 claims 1
- 238000012856 packing Methods 0.000 abstract 2
- 230000003712 anti-aging effect Effects 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 206010002660 Anoxia Diseases 0.000 description 1
- 241000976983 Anoxia Species 0.000 description 1
- 241000208340 Araliaceae Species 0.000 description 1
- 206010021143 Hypoxia Diseases 0.000 description 1
- 241000234280 Liliaceae Species 0.000 description 1
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 244000293846 Polygonatum multiflorum Species 0.000 description 1
- 235000004506 Polygonatum multiflorum Nutrition 0.000 description 1
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 235000001014 amino acid Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000007953 anoxia Effects 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 235000013325 dietary fiber Nutrition 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002212 flavone derivatives Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 235000008434 ginseng Nutrition 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 235000003642 hunger Nutrition 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 150000004053 quinones Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 210000000952 spleen Anatomy 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
- A61K36/8969—Polygonatum (Solomon's seal)
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B5/00—Drying solid materials or objects by processes not involving the application of heat
- F26B5/04—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
- F26B5/06—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum the process involving freezing
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/13—Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
Landscapes
- Health & Medical Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Microbiology (AREA)
- Epidemiology (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Medical Informatics (AREA)
- Medicinal Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Mycology (AREA)
- Pharmacology & Pharmacy (AREA)
- Alternative & Traditional Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Molecular Biology (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Packages (AREA)
Abstract
A freeze-dried sealwort is prepared from 4-year-old or more rhizomes (including fibrous root) of sealwort through digging, sorting, washing, packing, freezing, cutting, freezing, freeze drying, taking out, packing and sealing. The invention combines and innovations a frozen rhizoma polygonati cutting and finishing technology, a rhizoma polygonati freeze drying and dehydrating technology and an oxygen-free environment low-heat processing technology. The freeze-dried sealwort prepared by the process has the characteristics of original morphological structure basic characteristics and natural color, more active substances of the sealwort, great reduction of water and the like.
Description
Technical Field
The invention relates to a medicinal and edible lyophilized product of rhizoma polygonati and a processing technology thereof.
Background
Rhizoma Polygonati is dried rhizome of Polygonatum kingianum (Polygonatum kingianum L. et Hemsl.) or Polygonatum sibiricum Red (Polygonatum cyrtonema Hua.) belonging to Liliaceae and belonging to fairy maiden, rhizoma Zingiberis recens, radix Ginseng, etc.; it integrates medicinal, edible, ornamental and cosmetic functions, is one of 87 edible medicinal materials published by the ministry of health, has the functions of tonifying spleen, moistening lung, promoting the production of body fluid, tonifying kidney, resisting anoxia, fatigue and aging, can enhance immunity and metabolism, is a traditional Chinese medicine product for tonifying middle-jiao and replenishing qi, and has the functions of' losing weight and prolonging life without hunger after long-time taking; the book Ben Cao gang mu states that the essence of Dekun soil is the main herb for nourishing the middle energizer, and has the anti-aging and anti-aging effects when used alone, and the traditional anti-aging products such as Huang Jing cake, Huang Jing Gao and Huang Jing Wan in ancient prescription are not enumerated. The polygonatum plants in China are rich in germplasm resources and huge in storage amount, the polygonatum kingianum is mainly produced in provinces such as Guizhou, Guangxi and Yunnan, the polygonatum is mainly produced in provinces such as Hebei, inner Mongolia and Shaanxi, and the polygonatum multiflorum is mainly produced in provinces such as Guizhou, Hunan, Yunnan, Anhui and Zhejiang. Provides freeze-dried rhizoma polygonati with better and more complete preservation of bioactive substances of rhizoma polygonati for creating and developing the fitness and health-care market, and plays an important role in meeting the increasing health diet requirements of people.
Disclosure of Invention
The invention aims to provide freeze-dried rhizoma polygonati and a process thereof, which are rhizome total-nutrition health-care substances such as rhizoma polygonati source polysaccharide, flavone, quinone compounds, steroid saponin compounds, dietary fiber, trace elements, amino acid, mineral substances and the like by combining the modern low-temperature processing technology with the increasing practical requirements of rhizoma polygonati.
The object of the invention is achieved in the following manner:
the freeze-dried polygonatum sibiricum is prepared by adopting rhizome raw materials of polygonatum sibiricum plants through digging, sorting, cleaning, subpackaging, freezing, cutting, freezing, freeze-drying, taking out from a warehouse, packaging and sealing.
Digging with a digging device
Digging and selecting rhizome of Polygonatum sibiricum Rehd plant which can grow for 4 years or more, wherein the obtained rhizome (including fibrous root) is hereinafter referred to as Polygonatum sibiricum Rehd.
Sorting
Removing other or plant bodies or gravels in rhizoma Polygonati, and removing rhizoma Polygonati with mildew and rot, surface area above 5%.
Cleaning of
Washing off soil and microorganisms adhered to the surface of the sorted rhizoma polygonati with clear water or flowing clear water, or but not limited to, carrying out ultrasonic treatment on the rhizoma polygonati with clear water for 45-180 s, taking out the rhizoma polygonati and washing the rhizoma polygonati with clear water or flowing clear water until the water is clear.
Dispensing
The cleaned rhizoma polygonati is put into a clean turnover box which is cleaned by water containing 20mg-40mg/L of chlorine dioxide, has the length, width, height, inner dimension not more than 45.0 multiplied by 28.0 multiplied by 25.0cm, has no burrs on the inner wall and is made of HDPE (low-pressure high-density polyethylene) or PP (polypropylene).
Freezing of
Freezing the cleaned rhizoma Polygonati in a clean turnover box to below-20 deg.C within 12-24 h.
Slitting
Cutting the frozen rhizoma Polygonati with a size of more than 10cm or in a staggered form into pieces with a size of no more than 10cm according to the rhizome structure in a clean environment at 0-10 deg.C, wherein the processed rhizoma Polygonati is collectively called rhizoma Polygonati blocks or blocks for short.
Freezing and storing
Storing rhizoma Polygonati blocks at a temperature below-20 deg.C to-40 deg.C for at least 12h-24 h.
Freeze-drying
Placing the frozen blocks in a freeze-drying bin, and finishing by adopting five-section vacuum freeze-drying process of but not limited to-20 ℃/2-6h, -10 ℃/4-8h, -5 ℃/6-12h, 4 ℃/8-12h and 18 ℃ to 80 ℃/4-10h after 24-48 h; the number of segments and the temperature and time for each segment can be increased or decreased as appropriate according to, but not limited to, the freeze-drying condition or the change of the blocks.
Discharging from warehouse
After the freeze-drying is finished, breaking vacuum by clean, sterile and dry air, and taking out the freeze-dried blocks in a clean and sanitary operation room.
Packaging seal
Under clean conditions, adopting a vacuum packaging film bag or an aluminum-plastic composite film bag to carry out air-pumping packaging and sealing on the freeze-dried cut blocks; or a hard packaging sealable container with a certain pressure-proof or fixed structure is used for replacing the film bag and the film bag is sealed by filling nitrogen instead of pumping.
Examination of
The sanitation, physicochemical property and the use of the additive accord with the national standard of food safety, namely GB 16325-.
The freeze-dried polygonatum sibiricum processing technology has the following characteristics: the freezing and cutting finishing technology of rhizoma polygonati, the freeze drying dehydration technology of rhizoma polygonati and the low-heat processing technology in an oxygen-free environment are combined and innovated; the freeze-dried sealwort prepared by the freeze-dried sealwort process has the characteristics of morphological structure characteristics, natural color, full retention of active substances of the sealwort, great reduction of water and the like.
Claims (10)
1. A freeze-dried sealwort and a process are characterized in that: is prepared from fresh rhizome of Polygonatum cyrtonema or Polygonatum kingianum by digging, sorting, cleaning, subpackaging, freezing, cutting, freezing, freeze-drying, taking out of warehouse, packaging and sealing, and the method comprises the following steps:
1) excavating: digging and selecting rhizome of Polygonatum sibiricum plant growing for proper years, wherein the obtained rhizome (including fibrous root) is abbreviated as Polygonatum sibiricum;
2) sorting: removing impurities, and removing rhizoma Polygonati with mildew and rot and surface area above 5%;
3) cleaning: washing off soil and microorganisms adhered to the surfaces of the sorted sealwort by clear water or flowing clear water;
4) subpackaging: putting the cleaned rhizoma polygonati into a clean turnover box;
5) freezing: freezing the washed and boxed sealwort;
6) slitting: cutting frozen rhizoma Polygonati of more than 10cm or in staggered form into pieces with maximum size of not more than 10cm according to its rhizome structure, wherein the processed rhizoma Polygonati is collectively called rhizoma Polygonati block or cut block;
7) freezing and storing: storing rhizoma Polygonati blocks at a temperature below-20 deg.C to-40 deg.C;
8) freeze-drying: putting the frozen blocks into a freeze-drying bin for vacuum freeze-drying, and finishing 24-48 h;
9) discharging: breaking vacuum by clean, sterile and dry air after freeze drying is finished, and taking out the freeze-dried blocks in a clean and sanitary operation room;
10) packaging and sealing: under clean conditions, adopting a vacuum packaging film bag or an aluminum-plastic composite film bag to carry out air-pumping packaging and sealing on the freeze-dried cut blocks; or a rigid packaging sealable container with a certain pressure-proof or fixed structure is used for replacing the membrane bag for air suction sealing;
11) and (4) checking: the sanitation, physicochemical property and the use of the additive accord with the national standard of food safety, namely GB 16325-.
2. The method according to claim 1, wherein the suitable number of years of growth in the excavation of 1) means that the rootstocks are grown for 4 years or more.
3. The method according to claim 1, wherein the step of removing impurities in the step 2) is removing or penetrating or entraining other plant materials or gravels in the Polygonatum sibiricum.
4. The method as claimed in claim 1, wherein the washing in 3) can be, but not limited to, ultrasonic treatment with clear water for 45-180 s, and then the product is taken out of the clear water or washed with flowing clear water until the water is clear.
5. The method of claim 1, wherein the clean turnover container in the sub-package of 4) is but not limited to HDPE (low pressure high density polyethylene) or PP (polypropylene) material, the length and width of the inner dimension is not more than 45.0 x 28.0 x 25.0cm, the inner wall is free of burrs, and the clean turnover container is soaked in water containing 20mg-40mg/L chlorine dioxide for 45s-180s, taken out and washed with water until no residual chlorine exists.
6. The method according to claim 1, wherein the freezing step of 5) is carried out by freezing the washed rhizoma Polygonati without dripping water to below-20 ℃ within 12-24 hours.
7. The method according to claim 1, wherein the slitting in 6) is performed in a clean environment at 0 ℃ to 10 ℃.
8. The method of claim 1, wherein the freezing time of 7) is at least 12h-24 h.
9. The method of claim 1, wherein the lyophilization of 8) is completed in 24-48 h by using five-stage vacuum freeze-drying process, but not limited to-20 ℃/2-6h, -10 ℃/4-8h, -5 ℃/6-12h, 4 ℃/8-12h and 18 ℃ to 80 ℃/4-10 h; the sections can be increased or decreased according to the change of the freeze-drying condition or the cutting block, and the control temperature and time of each section can be properly increased or decreased; the packaging film bag in the packaging sealing of 10) can be replaced by a hard packaging sealable container with a certain pressure-proof or fixed structure, and is sealed by air suction.
10. The processing technology of lyophilized rhizoma Polygonati as claimed in claim 1, 2, 3, 4, 5, 6, 7, 8 or 9 has the following characteristics: combining and innovating a frozen rhizoma polygonati cutting and finishing technology, a rhizoma polygonati freeze drying and dehydrating technology and an oxygen-free environment low-heat processing technology; the lyophilized polygonatum obtained by the lyophilized polygonatum process according to claim 1, 2, 3, 4, 5, 6, 7, 8 or 9 has morphological structural characteristics and natural color, and also has the characteristics of sufficient retention of polygonatum active substances and great reduction of water content.
Priority Applications (1)
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CN202111181381.4A CN113967236A (en) | 2021-10-11 | 2021-10-11 | Freeze-dried sealwort and process |
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CN202111181381.4A CN113967236A (en) | 2021-10-11 | 2021-10-11 | Freeze-dried sealwort and process |
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Family
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CN202111181381.4A Pending CN113967236A (en) | 2021-10-11 | 2021-10-11 | Freeze-dried sealwort and process |
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Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102389526A (en) * | 2011-11-15 | 2012-03-28 | 重庆市秀山红星中药材开发有限公司 | Vacuum freeze-drying method of rhizoma polygonatum |
CN103039872A (en) * | 2011-10-12 | 2013-04-17 | 西南科技大学 | Kiwifruit pulp freeze-dried slice and processes |
CN110574923A (en) * | 2019-08-06 | 2019-12-17 | 福贡县马吉乡鑫禾生态扶贫专业合作社 | Preparation method of polygonatum kingianum freeze-dried food |
-
2021
- 2021-10-11 CN CN202111181381.4A patent/CN113967236A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103039872A (en) * | 2011-10-12 | 2013-04-17 | 西南科技大学 | Kiwifruit pulp freeze-dried slice and processes |
CN102389526A (en) * | 2011-11-15 | 2012-03-28 | 重庆市秀山红星中药材开发有限公司 | Vacuum freeze-drying method of rhizoma polygonatum |
CN110574923A (en) * | 2019-08-06 | 2019-12-17 | 福贡县马吉乡鑫禾生态扶贫专业合作社 | Preparation method of polygonatum kingianum freeze-dried food |
Non-Patent Citations (1)
Title |
---|
苗明三,等: "中药鲜药加工方法探讨", 《时珍国医国药》 * |
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