CN113967236A - Freeze-dried sealwort and process - Google Patents

Freeze-dried sealwort and process Download PDF

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Publication number
CN113967236A
CN113967236A CN202111181381.4A CN202111181381A CN113967236A CN 113967236 A CN113967236 A CN 113967236A CN 202111181381 A CN202111181381 A CN 202111181381A CN 113967236 A CN113967236 A CN 113967236A
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CN
China
Prior art keywords
freeze
rhizoma polygonati
freezing
drying
polygonatum
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202111181381.4A
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Chinese (zh)
Inventor
陈彦
晏飞利
陈艾萌
刘丹
陈维
黄学兵
吕向阳
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sichuan Tianyi Baicao Biotechnology Co ltd
Southwest University of Science and Technology
Original Assignee
Sichuan Tianyi Baicao Biotechnology Co ltd
Southwest University of Science and Technology
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Publication date
Application filed by Sichuan Tianyi Baicao Biotechnology Co ltd, Southwest University of Science and Technology filed Critical Sichuan Tianyi Baicao Biotechnology Co ltd
Priority to CN202111181381.4A priority Critical patent/CN113967236A/en
Publication of CN113967236A publication Critical patent/CN113967236A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)
    • A61K36/896Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
    • A61K36/8969Polygonatum (Solomon's seal)
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00Drying solid materials or objects by processes not involving the application of heat
    • F26B5/04Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
    • F26B5/06Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum the process involving freezing
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • A61K2236/13Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • A61K2236/15Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • A61K2236/17Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Microbiology (AREA)
  • Epidemiology (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Medical Informatics (AREA)
  • Medicinal Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Mycology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Molecular Biology (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Packages (AREA)

Abstract

A freeze-dried sealwort is prepared from 4-year-old or more rhizomes (including fibrous root) of sealwort through digging, sorting, washing, packing, freezing, cutting, freezing, freeze drying, taking out, packing and sealing. The invention combines and innovations a frozen rhizoma polygonati cutting and finishing technology, a rhizoma polygonati freeze drying and dehydrating technology and an oxygen-free environment low-heat processing technology. The freeze-dried sealwort prepared by the process has the characteristics of original morphological structure basic characteristics and natural color, more active substances of the sealwort, great reduction of water and the like.

Description

Freeze-dried sealwort and process
Technical Field
The invention relates to a medicinal and edible lyophilized product of rhizoma polygonati and a processing technology thereof.
Background
Rhizoma Polygonati is dried rhizome of Polygonatum kingianum (Polygonatum kingianum L. et Hemsl.) or Polygonatum sibiricum Red (Polygonatum cyrtonema Hua.) belonging to Liliaceae and belonging to fairy maiden, rhizoma Zingiberis recens, radix Ginseng, etc.; it integrates medicinal, edible, ornamental and cosmetic functions, is one of 87 edible medicinal materials published by the ministry of health, has the functions of tonifying spleen, moistening lung, promoting the production of body fluid, tonifying kidney, resisting anoxia, fatigue and aging, can enhance immunity and metabolism, is a traditional Chinese medicine product for tonifying middle-jiao and replenishing qi, and has the functions of' losing weight and prolonging life without hunger after long-time taking; the book Ben Cao gang mu states that the essence of Dekun soil is the main herb for nourishing the middle energizer, and has the anti-aging and anti-aging effects when used alone, and the traditional anti-aging products such as Huang Jing cake, Huang Jing Gao and Huang Jing Wan in ancient prescription are not enumerated. The polygonatum plants in China are rich in germplasm resources and huge in storage amount, the polygonatum kingianum is mainly produced in provinces such as Guizhou, Guangxi and Yunnan, the polygonatum is mainly produced in provinces such as Hebei, inner Mongolia and Shaanxi, and the polygonatum multiflorum is mainly produced in provinces such as Guizhou, Hunan, Yunnan, Anhui and Zhejiang. Provides freeze-dried rhizoma polygonati with better and more complete preservation of bioactive substances of rhizoma polygonati for creating and developing the fitness and health-care market, and plays an important role in meeting the increasing health diet requirements of people.
Disclosure of Invention
The invention aims to provide freeze-dried rhizoma polygonati and a process thereof, which are rhizome total-nutrition health-care substances such as rhizoma polygonati source polysaccharide, flavone, quinone compounds, steroid saponin compounds, dietary fiber, trace elements, amino acid, mineral substances and the like by combining the modern low-temperature processing technology with the increasing practical requirements of rhizoma polygonati.
The object of the invention is achieved in the following manner:
the freeze-dried polygonatum sibiricum is prepared by adopting rhizome raw materials of polygonatum sibiricum plants through digging, sorting, cleaning, subpackaging, freezing, cutting, freezing, freeze-drying, taking out from a warehouse, packaging and sealing.
Digging with a digging device
Digging and selecting rhizome of Polygonatum sibiricum Rehd plant which can grow for 4 years or more, wherein the obtained rhizome (including fibrous root) is hereinafter referred to as Polygonatum sibiricum Rehd.
Sorting
Removing other or plant bodies or gravels in rhizoma Polygonati, and removing rhizoma Polygonati with mildew and rot, surface area above 5%.
Cleaning of
Washing off soil and microorganisms adhered to the surface of the sorted rhizoma polygonati with clear water or flowing clear water, or but not limited to, carrying out ultrasonic treatment on the rhizoma polygonati with clear water for 45-180 s, taking out the rhizoma polygonati and washing the rhizoma polygonati with clear water or flowing clear water until the water is clear.
Dispensing
The cleaned rhizoma polygonati is put into a clean turnover box which is cleaned by water containing 20mg-40mg/L of chlorine dioxide, has the length, width, height, inner dimension not more than 45.0 multiplied by 28.0 multiplied by 25.0cm, has no burrs on the inner wall and is made of HDPE (low-pressure high-density polyethylene) or PP (polypropylene).
Freezing of
Freezing the cleaned rhizoma Polygonati in a clean turnover box to below-20 deg.C within 12-24 h.
Slitting
Cutting the frozen rhizoma Polygonati with a size of more than 10cm or in a staggered form into pieces with a size of no more than 10cm according to the rhizome structure in a clean environment at 0-10 deg.C, wherein the processed rhizoma Polygonati is collectively called rhizoma Polygonati blocks or blocks for short.
Freezing and storing
Storing rhizoma Polygonati blocks at a temperature below-20 deg.C to-40 deg.C for at least 12h-24 h.
Freeze-drying
Placing the frozen blocks in a freeze-drying bin, and finishing by adopting five-section vacuum freeze-drying process of but not limited to-20 ℃/2-6h, -10 ℃/4-8h, -5 ℃/6-12h, 4 ℃/8-12h and 18 ℃ to 80 ℃/4-10h after 24-48 h; the number of segments and the temperature and time for each segment can be increased or decreased as appropriate according to, but not limited to, the freeze-drying condition or the change of the blocks.
Discharging from warehouse
After the freeze-drying is finished, breaking vacuum by clean, sterile and dry air, and taking out the freeze-dried blocks in a clean and sanitary operation room.
Packaging seal
Under clean conditions, adopting a vacuum packaging film bag or an aluminum-plastic composite film bag to carry out air-pumping packaging and sealing on the freeze-dried cut blocks; or a hard packaging sealable container with a certain pressure-proof or fixed structure is used for replacing the film bag and the film bag is sealed by filling nitrogen instead of pumping.
Examination of
The sanitation, physicochemical property and the use of the additive accord with the national standard of food safety, namely GB 16325-.
The freeze-dried polygonatum sibiricum processing technology has the following characteristics: the freezing and cutting finishing technology of rhizoma polygonati, the freeze drying dehydration technology of rhizoma polygonati and the low-heat processing technology in an oxygen-free environment are combined and innovated; the freeze-dried sealwort prepared by the freeze-dried sealwort process has the characteristics of morphological structure characteristics, natural color, full retention of active substances of the sealwort, great reduction of water and the like.

Claims (10)

1. A freeze-dried sealwort and a process are characterized in that: is prepared from fresh rhizome of Polygonatum cyrtonema or Polygonatum kingianum by digging, sorting, cleaning, subpackaging, freezing, cutting, freezing, freeze-drying, taking out of warehouse, packaging and sealing, and the method comprises the following steps:
1) excavating: digging and selecting rhizome of Polygonatum sibiricum plant growing for proper years, wherein the obtained rhizome (including fibrous root) is abbreviated as Polygonatum sibiricum;
2) sorting: removing impurities, and removing rhizoma Polygonati with mildew and rot and surface area above 5%;
3) cleaning: washing off soil and microorganisms adhered to the surfaces of the sorted sealwort by clear water or flowing clear water;
4) subpackaging: putting the cleaned rhizoma polygonati into a clean turnover box;
5) freezing: freezing the washed and boxed sealwort;
6) slitting: cutting frozen rhizoma Polygonati of more than 10cm or in staggered form into pieces with maximum size of not more than 10cm according to its rhizome structure, wherein the processed rhizoma Polygonati is collectively called rhizoma Polygonati block or cut block;
7) freezing and storing: storing rhizoma Polygonati blocks at a temperature below-20 deg.C to-40 deg.C;
8) freeze-drying: putting the frozen blocks into a freeze-drying bin for vacuum freeze-drying, and finishing 24-48 h;
9) discharging: breaking vacuum by clean, sterile and dry air after freeze drying is finished, and taking out the freeze-dried blocks in a clean and sanitary operation room;
10) packaging and sealing: under clean conditions, adopting a vacuum packaging film bag or an aluminum-plastic composite film bag to carry out air-pumping packaging and sealing on the freeze-dried cut blocks; or a rigid packaging sealable container with a certain pressure-proof or fixed structure is used for replacing the membrane bag for air suction sealing;
11) and (4) checking: the sanitation, physicochemical property and the use of the additive accord with the national standard of food safety, namely GB 16325-.
2. The method according to claim 1, wherein the suitable number of years of growth in the excavation of 1) means that the rootstocks are grown for 4 years or more.
3. The method according to claim 1, wherein the step of removing impurities in the step 2) is removing or penetrating or entraining other plant materials or gravels in the Polygonatum sibiricum.
4. The method as claimed in claim 1, wherein the washing in 3) can be, but not limited to, ultrasonic treatment with clear water for 45-180 s, and then the product is taken out of the clear water or washed with flowing clear water until the water is clear.
5. The method of claim 1, wherein the clean turnover container in the sub-package of 4) is but not limited to HDPE (low pressure high density polyethylene) or PP (polypropylene) material, the length and width of the inner dimension is not more than 45.0 x 28.0 x 25.0cm, the inner wall is free of burrs, and the clean turnover container is soaked in water containing 20mg-40mg/L chlorine dioxide for 45s-180s, taken out and washed with water until no residual chlorine exists.
6. The method according to claim 1, wherein the freezing step of 5) is carried out by freezing the washed rhizoma Polygonati without dripping water to below-20 ℃ within 12-24 hours.
7. The method according to claim 1, wherein the slitting in 6) is performed in a clean environment at 0 ℃ to 10 ℃.
8. The method of claim 1, wherein the freezing time of 7) is at least 12h-24 h.
9. The method of claim 1, wherein the lyophilization of 8) is completed in 24-48 h by using five-stage vacuum freeze-drying process, but not limited to-20 ℃/2-6h, -10 ℃/4-8h, -5 ℃/6-12h, 4 ℃/8-12h and 18 ℃ to 80 ℃/4-10 h; the sections can be increased or decreased according to the change of the freeze-drying condition or the cutting block, and the control temperature and time of each section can be properly increased or decreased; the packaging film bag in the packaging sealing of 10) can be replaced by a hard packaging sealable container with a certain pressure-proof or fixed structure, and is sealed by air suction.
10. The processing technology of lyophilized rhizoma Polygonati as claimed in claim 1, 2, 3, 4, 5, 6, 7, 8 or 9 has the following characteristics: combining and innovating a frozen rhizoma polygonati cutting and finishing technology, a rhizoma polygonati freeze drying and dehydrating technology and an oxygen-free environment low-heat processing technology; the lyophilized polygonatum obtained by the lyophilized polygonatum process according to claim 1, 2, 3, 4, 5, 6, 7, 8 or 9 has morphological structural characteristics and natural color, and also has the characteristics of sufficient retention of polygonatum active substances and great reduction of water content.
CN202111181381.4A 2021-10-11 2021-10-11 Freeze-dried sealwort and process Pending CN113967236A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202111181381.4A CN113967236A (en) 2021-10-11 2021-10-11 Freeze-dried sealwort and process

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Application Number Priority Date Filing Date Title
CN202111181381.4A CN113967236A (en) 2021-10-11 2021-10-11 Freeze-dried sealwort and process

Publications (1)

Publication Number Publication Date
CN113967236A true CN113967236A (en) 2022-01-25

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Application Number Title Priority Date Filing Date
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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102389526A (en) * 2011-11-15 2012-03-28 重庆市秀山红星中药材开发有限公司 Vacuum freeze-drying method of rhizoma polygonatum
CN103039872A (en) * 2011-10-12 2013-04-17 西南科技大学 Kiwifruit pulp freeze-dried slice and processes
CN110574923A (en) * 2019-08-06 2019-12-17 福贡县马吉乡鑫禾生态扶贫专业合作社 Preparation method of polygonatum kingianum freeze-dried food

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103039872A (en) * 2011-10-12 2013-04-17 西南科技大学 Kiwifruit pulp freeze-dried slice and processes
CN102389526A (en) * 2011-11-15 2012-03-28 重庆市秀山红星中药材开发有限公司 Vacuum freeze-drying method of rhizoma polygonatum
CN110574923A (en) * 2019-08-06 2019-12-17 福贡县马吉乡鑫禾生态扶贫专业合作社 Preparation method of polygonatum kingianum freeze-dried food

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
苗明三,等: "中药鲜药加工方法探讨", 《时珍国医国药》 *

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Application publication date: 20220125

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